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Construction and Building Materials 198 (2019) 786–795

Contents lists available at ScienceDirect

Construction and Building Materials


journal homepage: www.elsevier.com/locate/conbuildmat

Physical performance of industrial and EPS and cork experimental


thermal insulation renders
M. Glória Gomes ⇑, Inês Flores-Colen, Humberto Melo, António Soares
CERIS, Department of Civil Engineering, Architecture and Georesources, Instituto Superior Técnico, Universidade de Lisboa, Av Rovisco Pais, 1049-001 Lisbon, Portugal

h i g h l i g h t s

 Experimental campaign on industrial and experimental thermal renders.


 Formulations with EPS, cork, and several binders and admixtures.
 Physical properties at fresh and hardened states.
 Standard and non-standard specimens and brick-render models.

a r t i c l e i n f o a b s t r a c t

Article history: Nowadays, there is a concern in getting buildings with reduced environmental impact and improved
Received 24 October 2017 thermal and energy performance. The need to use new technologies to comply with the thermal require-
Received in revised form 17 November 2018 ments has been driven by the regulation for buildings. With this goal in mind, the use of thermal insu-
Accepted 19 November 2018
lation systems on facades has increased. In this context, renders with high thermal insulation
Available online 10 December 2018
performance have recently emerged on the market. This paper discusses the physical characteristics of
four industrial thermal renders, comparing with two experimental render mixtures in which sand is
Keywords:
replaced by aggregates with thermal insulating properties (EPS and cork) without any additions or
Thermal renders
Performance
admixtures. It is noticed a need to incorporate high ratios of aggregate with thermal characteristics to
Physical properties achieve thermal insulation renders, affecting other physical properties of the renders at both fresh (work-
Thermal conductivity ability, air content and bulk density) and hardened (water absorption under low pressure, capillary, dry
bulk density, open porosity and drying capacity) states.
Ó 2018 Elsevier Ltd. All rights reserved.

1. Introduction conductivity below 0.05 W/m.K [6]. Lightweight aggregates can


also be categorized according to their origin and transformation
The growing concerns with sustainability and more demanding process. Such categorization falls into inorganic (e.g. porous sedi-
energy and environmental requirements in European directives mentary rocks; expanded glass; and expanded clay), and organic
(2012/27/UE and 2010/30/UE [1,2]) promote energy efficiency (e.g. expanded polystyrene or cork) [7,8] materials. Also, the incor-
and nearly zero-energy buildings by the end of 2020. In order to poration of innovative high thermal insulating aggregates has been
meet such goals, and taking into account the importance of energy studied but its presence on the market is still at a low level [9,10].
issues, more thermal insulation systems in buildings’ envelope Expanded polystyrene (EPS) and cork are one of the most used
have been developed. A trend of thermal renders has recently been lightweight aggregates in industrial thermal renders formulation.
observed in the industry to meet the objectives regarding build- Cork is a cellular, natural and renewable material, featuring low
ings’ enhanced thermal performance [3,4] and standard require- thermal conductivity (0.035–0.07 W/m.K), slow combustion
ments [5]. (despite being an organic material), and good physical and
In order to improve renders’ thermal properties, innovative mechanical properties [11,12]. The cork good insulation properties
solutions have been developed incorporating lightweight insulat- are related to its internal microstructure with closed and hollow
ing materials, with density typically below 150 kg/m3 and thermal small cells, much smaller than common cell matter, filled with
air [13]. Previous research studies show that cork and render are
⇑ Corresponding author. reciprocally compatible and new renders’ formulations can be
E-mail addresses: maria.gloria.gomes@tecnico.ulisboa.pt (M.G. Gomes), ines. made by mixing cork in different quantity percentage [3,11,14].
flores.colen@tecnico.ulisboa.pt (I. Flores-Colen).

https://doi.org/10.1016/j.conbuildmat.2018.11.151
0950-0618/Ó 2018 Elsevier Ltd. All rights reserved.
M.G. Gomes et al. / Construction and Building Materials 198 (2019) 786–795 787

Karade et al. [14] studied the influence of cork granules size and rizes the standard physical properties of some industrial thermal
density (90–280 kg/m3) on the cement hydration and found that renders available on the manufacturers’ technical documentation.
large and medium granules size (2–3 mm; 1 mm) are more com- It is possible to observe in Table 1 that most of the thermal ren-
patible with cement than fine granules, allowing incorporations ders with cork and EPS aggregates in the European Market has T1
of up to 30% by mass of the binder. Panesar and Shindman [3] con- class (0.1 W/m.K [5]), presenting with 0.042 W/m.K as the lowest
cluded that higher percentages of cork (330–670 kg/m3) as sand value. This is in accordance with Barbero et al. [20] study that anal-
replacement had a beneficial impact on concrete thermal resis- ysed thirty one thermal renders, most reaching T1 class, with a
tance (46% of thermal resistance increase for 20% by volume cork minimum value of 0.055 W/m.K. The majority of the thermal ren-
incorporation) but not directly correlated with size distribution ders of Table 1 has hydraulic binders. The collected data also shows
of cork granules (0.5–14 mm) for 10% by volume cork that not all thermal renders have declared values of capillary water
incorporation. absorption, fire reaction, and to a lesser extent, of dry bulk density
Brás et al. [11] concluded that cork granules with bulk density and water vapour diffusion resistance. Nevertheless, it is possible
of 112.4 kg/m3 can decrease the thermal conductivity of conven- to conclude that most of thermal renders present low water vapour
tional cement render in 75% and the water capillary absorption diffusion resistance coefficient and dry bulk density (q of 130–
when sand is replaced by cork with percentage replacements by 500 kg/m3). The majority of the thermal renders fulfils the water
mass of up to 80%. Expanded Polystyrene (EPS) is a rigid and resis- vapour diffusion resistance standard requirements (m  15 [5]).
tant thermoplastic polymer, with closed cells, which is used in con- On the other hand, the information of the capillary water absorp-
struction work. Given that it is composed of 98% air and 2% plastic tion of these thermal renders is scarce but most are suitable to
with low thermal conductivity (0.033–0.057 W/m.K), it features be used on external elements (C  0.40 kg/m2.min0.5 [5]).
outstanding thermal insulation properties [11,12,15–17]. In the present study, industrial and experimental thermal ren-
Sayadi et al. [18] conclude that lower thermal conductivity was ders physical properties are studied on both specimens and
reached with high volumes of EPS aggregate (bulk density of brick-renders models, applying standardized and expedient testing
16.6 kg/m3) replacements (thermal conductivity is 2.5 times higher techniques. This study contributes to discuss several physical prop-
with 28% EPS than with 82% EPS volume replacement). Babu et al. erties (declared and non-declared on standards) and to enhance
[19] reached to the conclusion that higher size and volumes of EPS the physical performance knowledge of thermal renders with cork
aggregates (bulk density of 9–23.6 kg/m3) in concrete induce and EPS aggregates.
greater moisture migration and absorption phenomena. In that
study 2.36–6.3 mm EPS granules size and 20–50% of EPS replace- 2. Experimental work
ment in total volume were considered. Brás et al. [11] concluded
that EPS aggregates (bulk density of 16.7 kg/m3) can decrease the 2.1. Renders and specimens production
thermal conductivity of conventional cement render in 60% when
sand is replaced by EPS with percentage replacements by mass of The aim of the experimental programme was to make a com-
up to 80%. parative analysis of the physical characteristics of different renders
It is worth mentioning that according to EN 998-1 standard [5], with improved thermal performance. In order to achieve this
thermal renders should present thermal conductivity (k) less than objective, two experimental (FT(cork); GT(EPS)) and four industrial
0.1 and 0.2 (W/m.K), categorized respectively as T1 and T2. The thermal renders (AI(EPS); BI(EPS);CI(cork); DI(cork)) were produced
physical performance of these renders to be used in external ele- according to EN 196-1 standard [21]. A reference sand-based ren-
ments is also characterized by a capillary water absorption coeffi- der was also produced (ET) for comparison purposes. The selected
cient (C) lower or equal to 0.4 kg/(m2.min0.5) (W1 class), and by a renders compositions are summarized in Table 2. The 1:3 (cement:
water vapour diffusion resistance coefficient (m) lower or equal to sand) volumetric ratio was chosen for producing all experimental
15. renders for results comparison. In the course of the experimental
There are already several industrial thermal renders in the programme, to achieve lower values of thermal conductivity in
European Market, with cork and EPS aggregates. Table 1 summa- accordance with Brás et al. [11] and Sayadi et al. [18], cork and

Table 1
Examples of industrial cork and EPS based-thermal renders properties in the European Market.

Render (manufacturer) Binder Insulation aggregates q [kg/m3] CFR C [kg/m2.min0.5] l [–] k [W/m.K]
Diathonite evolution (Diasen) Hydraulic lime NHL 3,5 Cork; clay; diatomaceous earth 360 ± 20 A1 W2 4 0.045 (T1)
Diathonite acoustix (Diasen) Hydraulic binder Cork; clay; diatomaceous earth 470 ± 30 A1 W2 4 0.083 (T1)
Diathonite deumix (Diasen) Hydraulic lime NHL 5 Cork; clay; diatomaceous earth 450 ± 45 A1 W2 4 0.080 (T1)
ISODUR (Secil) Binder mix EPS 300 ± 50 B W2 <5 0.050 (T1)
RHP ECOCORK (Secil) Hydraulic binders Cork 900 ± 50 A2-S1, d0 W2 <15 T2
AISLON (Weber) Lime Lightweight and mineral fillers 150 ± 5 B s1 d0 <0,4 (W1) 5 0.042 (T1)
Fassa Bortolo KT 48 (Fassa Bartolo) Hydraulic binder EPS 500 0,4 (W1) 9 0.083 (T1)
Ardex Isolteco (Ardex) Hydraulic binder EPS 250 A2 s1 d0 W1 9 0.058 (T1)
THW Cork (Thermowall) Hydraulic binder Cork; silica based 825 ± 75 A1 W1 14 0.065 (T1)
CVR TERMOPOR (CVR) Hydraulic binder EPS 250 12 0.062 (T1)
Chiraema Asciugo Drywall (Chiraema) Hydraulic binder EPS 290 9 0.053 (T1)
ISOLCAP XX 500 (Edilteco) Hydraulic binder EPS 500 21 0.104 (T2)
ISOLTECO Light 110 (Edilteco) Hydraulic binder EPS 130 0.043 (T1)
Isolcap Speed 525 (Edilteco) Hydraulic binder EPS 21 0.095 (T1)
Isolcap Fein 300 (Edilteco) Hydraulic binder EPS 300 12 0.080 (T1)
Isolcap max 800 (Edilteco) Hydraulic binder EPS 815 0.176 (T2)
Edilteco protherm light (Edilteco) Hydraulic binder EPS 300 A1 9 0.079 (T1)

Caption: q – dry bulk density [kg/m ]; CFR – Class of fire reaction (A1 – non-combustible materials; A2 e B – combustible materials; s1 – smoke production class; d0 – no
3

flaming droplets; C - water absorption due to capillary [kg/m2.min0,5] (W0 – not specified; W1 – C  0,4 kg/m2.min0.5; W2 – C  0,2 kg/m2.min0.5); l – water vapour diffusion
resistance coefficient; k – thermal conductivity coefficient [W/m.K] (T1  0.1 W/m.K; T2  0.2 W/m.K).
788 M.G. Gomes et al. / Construction and Building Materials 198 (2019) 786–795

Table 2
Renders compositions in the experimental work.

Renders Binder [%] (by Dmax Other materials Water/ Water/dry Additions/Admixtures
volume) [mm] binder ratio constituents ratio
Industrial AI(EPS) Lime/cement 100% EPS 3 without incorporation Not specified 1.14 Re-dispersible polymer;
hydrophobic agent; expansive
agent; water-retaining agents
BI(EPS) Lime/cement/ 70–80% EPS 1.5–2 Sand (siliceous and calcareous) Not specified 0.7 Not specified
synthetic binder
CI(cork) Cement 70–80% cork 1.5–2 Sand (siliceous and calcareous) Not specified 0.33 Re-dispersible powder; air
introducing agent; hydrophobic
powder; shrinkage control
agent; water retaining agents
DI(cork) Natural hydraulic Cork 3 Diatomaceous earth and clay Not specified 0.55 Natural additions; fibres, air
lime entraining agent
Experimental ET Cement – – Sand (quartz, quartzite, feldspar) 0.8 – With no additions
FT(cork) Cement 80% cork 1–2 Sand (quartz, quartzite, feldspar) 0.7 – With no additions
GT(EPS) Cement 85% EPS 3.4–4 Sand (quartz, quartzite, feldspar) 0.5 – With no additions

EPS based-renders were produced: i) replacing sand with cork, by mortar (workability) was tested by means of flow table test
80% of the volume of aggregates, and a bulk density of 101 kg/m3 (Fig. 4a), according to standard EN 1015-3 [24], with the flow
(FT(cork)); and ii) replacing sand with EPS, by 85% of the volume of value as function of bulk density of fresh mortar, in accordance
aggregates, and a bulk density of 11 kg/m3 (GT(EPS)). with standard EN 1015-2 [22]. In turn, the bulk density of fresh
It should be noted that, in all of the experimental renders, Port- mortar test (Fig. 4b) was performed following the standard EN
land cement of the CEM II B/L type, 32.5 N class was used as the 1015-6 [25]. The air content of fresh mortar was evaluated by
binder; while the mixing water was added to ensure a good work- the pressure method (Fig. 4c), standard EN 105-7 [26]. All these
ability of the experimental renders, according to the EN 1015-2 tests were performed on 21 samples (three for each render
standard [22]. composition).
The production of dry industrial renders (Fig. 1a–c), supplied in For hardened state, the determination of open porosity (Fig. 5a)
bags, followed the manufacturers’ instructions in particular, was conducted in accordance with RILEM/PEM25 [27], and the dry
regarding the amounts of water that should be added to the pow- bulk density was made by geometric method following the stan-
der product (Table 2). dard EN 1015-10 [28], both in standard specimens
Thirteen moulds were produced in the experimental program for (40  40  160 mm3). To assess the water absorption due to capil-
each render type: nine standard specimens 40  40  160 (mm3) – lary it was used the procedure described in the standard EN 1015-
Fig. 2a; three with 80  70  25 (mm3) – Fig. 2b; and one with 18 [29], using standard specimens (40  40  160 mm3) without
300  300  50 (mm3) dimensions – Fig. 2c. Furthermore, 2 brick- waterproofing their lateral faces. This test (Fig. 5b) allows deter-
render models (Fig. 3a) were also prepared by pressing the render mining the rate of the capillary water absorption represented by
against the brick with a masonry trowel, in successive thin coats the water absorption coefficient. All these tests were also per-
until the intended thickness of 4 cm was achieved (Fig. 3b), and formed on 21 specimens (three for each render composition).
finally the render was levelled with a ruler to give a smooth finish. The measurement of water absorption under low pressure was
The storage and curing of the samples were performed accord- carried out with Karsten tubes according to RILEM 25-PEM [30].
ing to the EN 1015-11 standard [23]. Wet curing in polyethylene This methodology allows to evaluate the water permeability of
bags (7 days) was followed by dry curing (21 days) in a climatic renders from readings of water absorption (in cm3) made during
chamber under controlled conditions, corresponding to 65% ± 5% the first 5, 10, 25, 30 and 60 min. From this readings, it is possible
of relative humidity and a temperature of 20 °C ± 2 °C. to obtain water absorption as function of time and thereafter
determine the water absorption coefficient express in kg/
2.2. Testing procedures (m2 min0.5). For this study, it were used 2 Karsten tubes (Fig. 5c)
in each brick render model (2 models for each render’s composi-
The testing procedures included both fresh and hardened tion), in smooth areas and without cracking, totaling 28 Karsten
state techniques. The determination of consistence of fresh tube measurements.

Fig. 1. Production of industrial render: (a) render’s powder weighting; (b) powder and water mixing; (c) render at fresh state.
M.G. Gomes et al. / Construction and Building Materials 198 (2019) 786–795 789

Fig. 2. Moulds: (a) standard specimens; specimens for thermal conductivity measurements with (b) transient and (c) steady-state methods.

Fig. 3. Brick-render models: (a) moulds and (b) 4 cm render’s thickness on brick block.

Fig. 4. Fresh state testing: (a) workability; (b) bulk density; and (c) air content.

Fig. 5. Hardened state testing: (a) open porosity; (b) capillary water absorption; and (c) water absorption under low pressure – Karsten pipe.

The drying index was calculated as the relationship between RILEM Test n°. II.5 [32]. The test finished when the relationship
the drying integral curve (which relates the moisture content to between the mass variation and the initial dry mass was below
the test time, in hours), and the initial moisture content multiplied 2%. For the drying test, saturated specimens from the open porosity
by the test’s duration, in accordance with NORMAL 29/88 [31] and and apparent specific gravity tests were used, without waterproof-
790 M.G. Gomes et al. / Construction and Building Materials 198 (2019) 786–795

ing the lateral faces. These specimens (Fig. 6a) where dried in a 3. Results and discussion
controlled environmental chamber with relative humidity (RH) of
55 ± 5% and a temperature of 20 ± 2 °C. 3.1. Fresh state results discussion
The thermal conductivity was assessed by two different meth-
ods (transient and steady state) and equipments (ISOMET 2114 Table 3 shows fresh state results of the studied renders. It can
and Holometrix Rapid-k). The ISOMET 2114 (Fig. 6b) operates in be observed that, as expected, the highest value of bulk density
transient mode, according to ASTM D5930-09 [33], and the ther- at fresh state was reached by the sand-based reference render
mal conductivity measurement range of this equipment varies (ET) without lightweight aggregates. The cork-based renders pre-
between 0.04 W/m.K and 6.00 W/m.K. The equipment Holometrix sent higher values of bulk density than EPS-based renders, which
Rapid-k (Fig. 6c) follows the ASTM C518-91 [34] and ISO 8301 can be related with the difference of bulk density of these two
[35] standards. This instrument measures, by the heat flow types of aggregates (e.g. qcork = 101 kg/m3; qEPS = 11 kg/m3, deter-
method, the heat flux in steady state between two parallel plates mined for FT(cork) and GT(EPS) experimental renders according to
with different temperatures (in the present study 40 °C and 30 °C EN 1097-3 [37]). The adding mixing water (Table 2) in both exper-
were selected, respectively). The range of thermal conductivity val- imental and industrial renders production allowed an adequate
ues reported by Holometrix Rapid-k varies between 0.015 W/m.K consistence in fresh state (workability, Table 3), in compliance
and 0.43 W/m.K. with EN 1015-2 standard [22].
Three different types of specimens were tested with transient The experimental results also show that, in general, the rate of
method (ISOMET 2114): 21 specimens with 80  70  25 (mm3), air content in fresh state in industrial renders ranges between 5
type 1 – Fig. 7a; 7 specimens with 300  300  50 (mm3), type 2 and 7%, except for the AI(EPS) render, where this value is close to
– Fig. 7b; and 14 brick-render models with 4 cm render thickness 10%. It is worth referring that EPS was the only aggregate used in
(type 3 – Fig. 7c). The specimens type 2 with 300  300  50 AI(EPS) and the amount of water used in the mixture was greater
(mm3) were also used in steady state method (Holometrix Rapid- than that used in other industrial renders. The high value for air
k) measurements. Both methods were carried out at 14 and content in cement-based render CI(cork) (6.6%), despite the low
28 days of curing. Moreover, all the renders’ specimens, except amount of incorporated water, could be related with the absence
brick models, were also tested under the dry state conditions using of lime in the binder of this render, which can lead to higher air
an oven at a constant temperature of 60 °C. Additionally, the mois- contents at fresh state [38], and/or the presence of admixtures,
ture content volume by volume (volume of evaporable water such as air entraining-agents.
divided by volume of dry material) of 80  70  25 (mm3) speci- In experimental lightweight renders, the values of air content
mens was determined at 14, 28 days of curing and at saturated are also close to those found in industrial renders, ranging between
state, in accordance with ISO 12570 [36]. 5 and 6%, thus being slightly higher than those in the reference

Fig. 6. Hardened state testing: (a) drying index; thermal conductivity, (b) transient method and (c) heat flow steady state method.

Fig. 7. Types of specimens used on thermal conductivity measurements by transient method: (a) type 1: 80  70  25 (mm3); (b) type 2: 300  300  50 (mm3); and (c) type
3: brick-render models with 4 cm render thickness.
M.G. Gomes et al. / Construction and Building Materials 198 (2019) 786–795 791

Table 3
Fresh state results.

Renders Bulk density Workability Air content


3
Mean values [kg/m ] CV [%] Mean values [mm] CV [%] Mean values [%] CV [%]
AI(EPS) 411 0.49 141 0.58 9.6 3.40
BI(EPS) 563 0.89 132 1.09 5.2 3.14
CI(cork) 1016 1.58 152 0.82 6.6 3.71
DI(cork) 896 2.57 151 0.83 6.0 6.80
ET 2105 0.57 173 0.47 4.7 3.47
FT(cork) 1056 2.56 158 2.07 5.0 0.94
GT(EPS) 662 3.93 151 0.41 6.2 2.63

Caption: CV – variation coefficient.

render (with air content close to 5%). In these experimental ren- than the ones measured at fresh state. As already observed in fresh
ders, the incorporation of EPS lead to higher air content. state, renders with incorporation of granulated cork have bulk den-
To sum up, renders incorporating a high percentage of insulat- sity values higher than renders with incorporation of granulates
ing aggregates tend to contain greater amounts of air. This influ- EPS. The introduction of granulated cork and EPS caused a decrease
ence is even more noticed in experimental renders with EPS in the dry bulk density in the range of 55% and 65%, respectively,
incorporation, whereas in the industrial renders the influence of when compared to the reference render (ET).
other admixtures misleads the results of this property. Open porosity could only be ascertained in cork renders, due to
the reduced density of renders with EPS, which made the hydro-
3.2. Hardened state results discussion static weighting of samples unfeasible. The results for renders’
open porosity have shown that cork incorporation rates higher
Table 4 shows hardened state results of the studied renders at than 70% result in open porosity values between 38% and 47%,
28 days of curing. The thermal conductivity is also analysed in this while the value for open porosity in the cement-based reference
section (Table 5, Figs. 8 and 9), with transient and steady-state render is close to 26%.
method at different days of curing (14 and 28 days) and for both In experimental renders incorporating cork (FT(cork)) and EPS
saturated and dry states. (GT(EPS)) there were a reduction in the water absorption capillary
Dry bulk density in the hardened state of renders incorporating coefficient when compared with the reference render (ET). This
insulating aggregates presents values ranging between 237 and reduction is significantly higher (about 70%) in GT(EPS) which can
863 kg/m3 (Table 4). According to EN 998-1 [5], these renders be explained by the hydrophobic nature of the EPS aggregates.
can be classified as lightweight renders (dry bulk den- The same conclusion was drawn by Babu et al. [19]. Regarding
sity  1300 kg/m3). As a result of the water evaporation during cork-based render (FT(cork)) there was a slight decrease when com-
the curing process, dry bulk densities at hardened state are lower pared with the reference render. Bras et al. [11] have also observed

Table 4
Hardened state results at 28 days of curing.

Renders Dry bulk density Open porosity Water absorption Water absorption under low pressure – Karsten tube Drying test
coefficient due to
capillary action
Mean values [kg/m3] CV [%] Mean values [%] CV [%] Mean values [kg/ Mean values [cm3] CV [%] Ca [kg/(m2.min0.5)] Di [–]
(m2.min0.5)]
C R2
AI(EPS) 237 17 – – 1.01 0.962 6.65 16.03 1.51 0.23
BI(EPS) 432 17 – – 0.34 0.981 0.93 6.24 0.21 0.24
CI(cork) 863 13 46.4 2.37 0.14 0.994 0.43 23.53 0.11 0.44
DI(cork) 642 13 47.3 0.85 0.70 0.951 1.33 26.50 0.30 0.31
ET 1885 8 25.6 0.78 0.74 0.989 1.60 14.43 0.36 0.32
FT(cork) 855 21 37.5 0.27 0.67 0.995 0.38 40.73 0.09 0.28
GT(EPS) 683 20 – – 0.22 0.984 0.83 7.00 0.19 0.29

Caption: CV – variation coefficient; C – water absorption due to capillary [kg/m2.min0,5]; Ca – water absorption coefficient under low pressure [kg/m2.min0,5]; Di – drying
index [–].

Table 5
Thermal conductivity measurements with transient method (ʎTM) as function of moisture content (volume by volume) for specimens with 80  70  25 (mm3).

Renders Saturation stage 14 days of curing 28 days of curing Dry state


ʎTM [W/m.K] W [%] ʎTM [W/m.K] W [%] ʎTM [W/m.K] W [%] ʎTM [W/m.K]
AI(EPS) 0.33 45.15 0.07 0.65 0.06 0.09 0.06
BI(EPS) 0.29 38.14 0.11 3.61 0.10 2.55 0.09
CI(cork) 0.32 38.86 0.24 5.68 0.23 2.93 0.17
DI(cork) 0.26 38.75 0.16 3.07 0.14 2.17 0.12
ET 2.07 27.71 1.54 2.34 1.34 1.46 1.33
FT(cork) 0.69 38.96 0.30 4.36 0.27 3.07 0.23
GT(EPS) 0.30 26.09 0.29 3.99 0.23 3.31 0.22
792 M.G. Gomes et al. / Construction and Building Materials 198 (2019) 786–795

0.60 was not observed in lightweight experimental renders, which can


be justified by the high variability of Karsten tube test (e.g.
0.50 y = 1.057x + 0.022 CV = 41% in FT(cork)) and the sensitivity of these values to the ren-
R² = 0.935
der’s surface condition (such as, high roughness due to the aggre-
0.40 gate grade size) [39].
Table 4 also shows that there was a decrease in the drying index
SM [W/m.K]

14 days of curing of lightweight renders (FT(cork)) and (GT(EPS)) of about 10–13%, when
0.30
28 days of curing compared to the reference render. This is expected because these
0.20
Dry state renders have higher open porosity as a result of lightweight aggre-
gates incorporation in renders as a replacement for sand.
The renders which absorb more water tend to be the ones that
0.10
show better drying behaviour [40]. In this study the same tendency
was observed in AI(EPS) industrial render, while the CI(cork) render
0.00
0.00 0.10 0.20 0.30 0.40 0.50
showed the smallest water absorption coefficients due to both cap-
TM [W/m.K] illary and under low pressure, and the worst drying index. Despite
of the high open porosity (46%) of CI(cork), the presence of
Fig. 8. Thermal conductivity measurements with both transient (ʎTM) and steady hydrophobic compounds can justify this difference between hydric
state (ʎSM) methods for specimens with 300  300  50 (mm3). and drying behaviour [41].
It can also be referred that the drying index can be used to indi-
a tendency of decrease of capillary water absorption, in cases when rectly assess water vapour diffusion resistance coefficient (stan-
cork incorporation was made by 80%, and when particle size ran- dard characteristic in the EN 998-1 [5]) [41].
ged between 0.5 and 2 mm. Table 5 shows the thermal conductivity measurements with
By analysing the capillary water absorption of industrial transient method (ISOMET 2114) on specimens with
lightweight renders (Table 4), it can be concluded that render BI 80  70  25 (mm3) for the studied renders as function of moisture
2 0.5
(EPS) belongs to the W1 class (C  0.40 kg/m .min ) and the render content (volume by volume) and curing days.
CI(cork) to the W2 class (C  0.20 kg/m2.min0.5) in accordance with The thermal conductivity of industrial renders for dry state
EN 998-1 [5], whereas AI(EPS) and DI(cork) have shown which corresponds to the set of conditions IIa (23 °C of reference
non-expected higher values due to probable different mixing and temperature at dry state), in accordance to ISO/FDIS 10456 [42]
production procedures and distinguish formulations (e.g. lime; are in the range of 0.06–0.17 W/m.K, that fall into the category of
hydrophobic agents; air entraining agents). thermal renders (T1 or T2, according to the European standard
Despite the high porosity of CI(cork) render (about 46.4%), it has EN 998-1 [5]). When comparing experimental renders with the ref-
shown a low coefficient of capillary water absorption. The signifi- erence render (ET), the addition of thermal insulation materials has
cant difference found in water absorption, in renders with approx- resulted in a substantial reduction (about 80%) of the value of
imate open porosity CI(cork) and DI(cork) (of about 47%), can also be thermal conductivity (values close to 0.2 W/m.K, as opposed to
explained by particular differences of formulations, by the pres- 1.33 W/m.K for the reference render). Bras et al. [11] have also
ence of hydrophobic agents in render CI(cork), by the variations of concluded that renders’ thermal conductivity decreases with the
the binder, non-insulating aggregate, and by the percentage varia- introduction of the lightweight aggregates such as cork and EPS.
tion of aggregate incorporation (absent in the case of DI(cork)). This was also accompanied by a substantial decrease in appar-
Regarding the water absorption under low pressure (water ent bulk density. In fact, renders with higher percentages of incor-
absorption volume and coefficient), a 75% and 50% decrease can poration of insulation aggregates show lower values of apparent
be seen in the cork (FT(cork)) and EPS (GT(EPS)) based experimental bulk density (Table 4) and lower thermal conductivity (Table 5).
renders, when compared with the reference render (ET). By analys- It should be noted that the lowest values of bulk density and ther-
ing industrial renders, it can be concluded that there is a strict rela- mal conductivity were obtained in renders with EPS aggregates
tionship between water absorption under low pressure and incorporation.
capillary water absorption coefficients, with higher values of both Table 5 also shows that the increase of moisture content leads
coefficients in AI(EPS) and lower in CI(cork) renders. This relationship to higher thermal conductivity values. It is observed that render

0.40

0.35

0.30

0.25
[W/m.K]

0.20

0.15
TM

0.10

0.05

0.00
14 days 28 days 14 days 28 days 14 days 28 days 14 days 28 days 14 days 28 days 14 days 28 days
AI(EPS) BI(EPS) CI(cork) DI(cork) FT(cork) GT(EPS)
Indus tri al r enders Conventi onal r enders

Specimens type 1 Specimens type 2 Specimens type 3

Fig. 9. Thermal conductivity measurements with the transient method on different specimens at 14 and 28 days of curing: type 1: 80  70  25 (mm3); type 2:
300  300  50 (mm3); and type 3: brick + 4 cm render.
M.G. Gomes et al. / Construction and Building Materials 198 (2019) 786–795 793

Table 6
Matrix of correlations between properties of renders with improved thermal performance.

Air Water absorption under low Water absorption capillary Dry bulk Drying ʎTM, 28 days Open
content pressure [cm3] [kg/(m2.min0.5)] density [kg/m3] index [–] [W/m.K] porosity
[%] [%]
Air content [%] D Lin. Lin. Exp. Pow. Pow. Log.
Water absorption under low +++ D Lin. Exp. Pow. Pow. Lin.
pressure [cm3]
Water absorption capillary + ++ D Exp. Log. Exp. Lin.
[kg/(m2.min0.5)]
Dry bulk density [kg/m3] ++ +++ + D Exp. Pow. Exp.
Drying index [–] + ++ ++ D Pow. Log.
ʎTM, 28 days [W/m.K] + ++ + +++ + D Pow.
Open porosity [%] +++ + + + ++ D

Caption: Lin. – linear; Exp – exponential; Pow. – power; Log. – logarithmic; D – same test; = R2 < 0.2 (no relation);+ = (0.2 < R2 < 0.4) (a tendency); ++ = (0.4  R2 < 0.8)
(a relation); +++ = R2  0.8) (a good correlation).

AI(EPS) presents the lowest values of moisture content at 14 and loss of internal cohesion of the render. GT(EPS) showed the highest
28 days of curing, despite the highest water/pounder ratio thermal conductivity difference between specimen’s type 3 and
(Table 2), which can be explained by a faster drying of this render types 1 and 2, which can be justified by a non-uniform distribution
(low drying index, Table 4). In the experimental renders, the same of EPS particles within the render more which are more confined at
tendency, but more slightly, was observed. Moreover, the AI(EPS) the surface and induce higher roughness of the surface, affecting
render has the highest water absorption both due to capillary the measurement with the surface probe of the ISOMET equipment
and under low pressure (Table 4), which explain the highest mois- (transient method).
ture content at saturated state. On the other hand, since this render
has the lowest drying index (Table 4) that corresponds to a better
3.3. Correlations
drying, the variation of moisture content, and thus of thermal con-
ductivity, between saturated and dry states is high.
The obtained results have made it possible to establish correla-
The significant difference in thermal conductivity between ren-
tions between the different properties of the studied renders with
der FT(cork) and GT(EPS) at saturated stage can be attributed to a
improved thermal performance, which are shown in Table 6.
higher moisture content in render FT(cork) [43]. The thermal con-
Reasonable good correlations (R2 > 0.8) were identified between:
ductivity of EPS shows a less dependence of moisture content than
thermal conductivity and dry bulk density; water absorption under
cork [44,45]. Fig. 8 shows the thermal conductivity measurements
low pressure and dry bulk density; water absorption under low
on specimens with 300  300  50 (mm3) with both transient
pressure and air content; air content and open porosity. Panesar
(ISOMET 2114) and steady state (Holometrix Rapid-k) methods
and Shindman [3] have also noted that there was a direct relation-
for the studied thermal renders.
ship between thermal conductivity and density, when cork was
It can be observed that the results obtained with both methods
incorporated. Open porosity is also correlated with air content but
are very similar, with a linear regression line with a Pearson linear
shows lower relationships with the other analysed properties. How-
coefficient of 0.935 and with a slope of near 1. The thermal conduc-
ever, it is important to refer that the number of open porosity results
tivity results obtained with the steady-state method are slightly
were limited to only three lightweight renders.
higher than the ones measured with the transient method, due
Finally, other correlations involving water absorption under low
to the different testing conditions, in particular the highest mean
pressure and dry bulk density and air content could be related to
testing temperature 35 °C in the heat flow meter steady-state
the directly dependency of those properties with the internal voids
method against to 23 °C in transient method.
at both fresh and hardened states. Water absorption can be also
Fig. 9 shows the thermal conductivity coefficient measured
influenced by the incorporation of hydrophobic agents and the
with the transient method, for different types of specimens at 14
affinity of the pore walls to water [9] not studied in this paper.
and 28 days of curing (as referred, types 1 and 2 are specimens pro-
duced with moulds, and specimens type 3 includes de brick models
with the application of 4 cm coat thickness of render). 4. Conclusions
It is possible to observe that, in general, the thermal conductiv-
ity values for specimens’ type 2 are higher than the values on spec- This study compares the physical characteristics of four thermal
imens’ type 1. These differences are significant for 14 days of industrial and two experimental renders with enhanced thermal
curing when the specimens have higher moisture content. This performance with high percentages (up to 80% in aggregate vol-
can be explained by the higher moisture content of specimens type ume) of incorporation of EPS and granulated cork. A sand-based
2 when compared with specimens type 1, which might be associ- reference render was also used for comparison purposes. Four dif-
ated with the higher dimensions of specimens type 2 that difficult ferent specimens were produced: standard prismatic dimensions;
the drying process. In fact, the moisture content of specimen’s type 80  70  25 (mm3); 300  300  50 (mm3); and brick-render
1 and 2 were respectively of 0.6–6% and 2–14% at 14 days of curing, models with 4 cm of applied render.
and of 0.8–3% and 0.3–11% at 28 days of curing. Physical performance of thermal renders should be based not
Although the brick substrate suction can increase the compact- only on thermal conductivity but also on standard (e.g. water
ness of the applied render that would rise the thermal conductiv- absorption capillary coefficient) and non-standard physical proper-
ity, the thermal conductivity for the specimeńs type 3 presents, ties (e.g. air content, open porosity) at fresh and hardened states.
in general, the lowest values. Adherence tests conducted on spec- When analyzing the physical characteristics, significant
imens type 3, that are not within the scope of this paper, showed improvements in thermal performance were found with incorpora-
that these renders do not have good adherence (0.3 MPa), which tion of lightweight aggregates (EPS and cork). A decrease of about
can explain the decrease of thermal conductivity due to a probable 80% of the thermal conductivity was reached, in comparison to the
794 M.G. Gomes et al. / Construction and Building Materials 198 (2019) 786–795

reference render, with values in the range of 0.06–0.17 W/m.K, in tion for Science and Technology, Portugal) through the financial
industrial thermal renders, and close to 0.2 W/m.K, in experimen- support on the Project FCT PTDC/ECM/118262/2010 and PhD Grant
tal thermal renders. This has resulted in more porous renders SFRH/BD/97182/2013. The authors also would like to thank the
(open porosity values ranging between 38 and 47% in renders with manufacturers who provided the industrial renders for the exper-
cork when compared to 26% of the reference render), with a signif- imental campaign carried out.
icant decrease in dry bulk density values up to 87%. Also at fresh
state thermal renders showed lower bulk densities than the refer-
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