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ASM Handbook, Volume 21: Composites Copyright © 2001 ASM International®

D.B. Miracle and S.L. Donaldson, editors, p383-387 All rights reserved.
DOI: 10.1361/asmhba0003397 www.asminternational.org

Rapid Prototyping
David L. Bourell and Joseph J. Beaman, Jr., The University of Texas at Austin
Donald Klosterman, University of Dayton
Ian Gibson, University of Hong Kong
Amit Bandyopadhyay, Washington State University

RAPID PROTOTYPING (RP)—also known to each other and to the build platform at all Powder Sintering. Selective laser sintering
as solid freeform fabrication, automated fabri- times during the build process. Overhanging part (SLS) uses powder as the raw material (Fig. 2).
cation, layered manufacturing, and so forth— features must therefore be connected using ad- Parts are built on a platform, which indexes
consists of a range of technologies that are ca- ditional support structures, which are fabricated downward as more powder is added at the top.
pable of taking computer-aided design (CAD) at the same time. A laser melts or sinters the powder particles ac-
models and converting them to a physical form
or part. This process is automatic, generally in-
dependent of the model geometry, and does not
require special tooling or fixtures. Complex,
three-dimensional (3-D) contours are quantized
in the form of stacks of two-dimensional, finite
thickness layers or cross sections. If these layers Mirror
are very thin, then the parts made will be suffi- system
ciently accurate to suit a range of applications. Laser
Nearly all RP parts can be characterized by a
stair-step effect that approximates the original Ultraviolet beam
cures liquid
shape, which is most obvious on shallow slopes
and curves. A most comprehensive classification Computer
of RP processes was proposed by J.P. Kruth (Ref
1), in which the focus is on the initial state of Model
the raw materials used, namely solid, liquid, and Base to support structure
powder-based manufacture. Other sources for
Elevator platform
more detailed information are included as Ref 2
to 6. Liquid photopolymer tank

Fig. 1 Stereolithography (SLA) rapid prototyping system. Courtesy of Milwaukee School of Engineering
Review of Processes

Photopolymer Systems. Stereolithography


(SLA) (Ref 7) is regarded as the first commercial
RP process and uses liquid-based photopolymer
resin as the raw material (Fig. 1). Polymerization
occurs at a specific frequency of light, supplied
by a laser source, which scans across the surface
of the photopolymer. The laser intensity is
matched to the absorption of the photopolymer
so that solidification is limited to a short depth,
representing the layer thickness. Parts are built
on an elevator platform, which increments down
from the surface as layers are added. Stereolith-
ography was first commercialized by 3D Sys-
tems and is registered to their machines. There
are, however, a number of variations from other
companies that also use photopolymer resins.
Parts made using SLA are surrounded by liquid
resin during the build so there is a need to ensure
that all layers, and parts of layers, are connected Fig. 2 Selective laser sintering (SLS) rapid prototyping system. Courtesy of DTM Corporation
384 / Engineering Mechanics, Analysis, and Design

cording to the cross section at a particular layer. Sheet Lamination. Laminated Object Manu- cates parts from photopolymer resins but in a
Each layer cools rapidly, and laser penetration is facturing (LOM) (Ref 11) uses solid sheets of different way than stereolithography (Fig. 5).
such that it thermally bonds to the layer below. material, which are sequentially bonded together Resin is spread onto a platform, which is then
The powder material must therefore be thermo- and cut to form the part (Fig. 4). The thickness exposed to ultraviolet light through a mask,
plastic in its behavior. The use of powders means of the sheet material, which is normally paper, which is printed from the layer data onto a glass
that part surfaces have a granular texture, and represents the layer thickness. After each layer plate. Uncured resin is vacuumed away, and the
there is also a tendency for parts to be porous. is bonded and cut, the part is separated from the space is filled with molten wax. The wax solid-
Loose powder surrounds the solid part, thus feed material by cutting it around the outline. ifies and the whole layer is machined, level to
eliminating the need for specific support struc- Further cuts or “cross hatches” are required to the required layer thickness. Parts are therefore
tures. Thermal processing also leads to very permit easy removal of the waste material after a combination of resin and wax and do not re-
good part strength. Selective laser sintering is the entire part is complete. Thus, LOM parts are quire supports. Wax is removed using a chemical
registered to machines manufactured by DTM surrounded by solid material and do not require bath or autoclave. Solid ground curing can be
Corporation (Ref 8), but similar machines are support structures during the building process. considered a hybrid system since it uses solid
also made by EOS GmbH in Germany (Ref 9). LOM was first commercialized by Helisys Inc., wax and liquid resin.
Hot Melt Extrusion. Fused deposition mod- which used the approach described previously to Three-Dimensional Printing (3DP). Devel-
eling (FDM) material comes in solid form as a cut and bond adhesive-backed paper that was de- oped and licensed by the Massachusetts Institute
filament. This is extruded through a heated noz- livered on a continuous roll. Another laminating of Technology (Ref 14), 3DP can be found in a
zle, which deposits a thin “road” of material machine, which uses single sheets of paper for number of commercial forms. Powder is spread
(Fig. 3). First, roads are extruded to form the each layer, photocopying technology to apply onto a build platform (Fig. 6). Liquid is then
outline of the part. These roads are then filled in the adhesive, and a blade to cut the part outlines, printed from an ink-jet print head. The liquid
to complete the layer. Since the material is op- is made by Kira in Japan (Ref 12). dries and binds the powder particles together to
timally softened and not fully liquefied when it Solid Ground Curing (SGC) (Ref 13), a pro- form the layer. 3DP is therefore another hybrid
exits the nozzle, FDM generally uses amorphous cess developed by Cubital in Israel, also fabri- process using powders and liquid. Like SLS, the
polymers. Fused deposition modeling must also
use support structures for overhanging features.
Supports are extruded through a second nozzle UV light source
and can therefore be held at a different tempera- • Spray resin
ture or made from a different material. This al-
lows the supports to come away from the part • Develop photomask
easily. A recent development is the use of a sol-
uble support material that can be removed with • Expose mask
a minimum of mechanical damage to the part.
Fused deposition modeling is currently com- • Vacuum uncured resin
mercialized by Stratasys Inc. (Ref 10).
• Spray wax

Filament
• Mill flat

Drive wheels
Fig. 5 The solid ground curing (SGC) process from Cubital. Courtesy of Penn State University

Liquifier
Direction
Tip

Vector motion

Fig. 3 The fused deposition modeling (FDM) hot melt


extrusion process. Courtesy of Penn State Uni-
versity

Spread powder Print layer


Laser optics gantry Drop piston
CO2 laser
Cross hatch
Cut-out window Repeat cycle
Heated roller

Part block Material


Waste material Platform feed roll
take-up roll
Intermediate stage Last layer printed Finished part
Fig. 4 Sheet lamination using the laminated object
manufacturing (LOM) process. Fig. 6 The basic three-dimensional printing (3DP) process. Courtesy of MIT
Rapid Prototyping / 385

use of different powders results in different ap- direct fabrication of polymer and metal compo- polymer-ceramic precursor resin of sufficient
plications. The most common machine is the nents during this time period. Currently, a wide tack, or a tackifier can be used in between pre-
Z402 from ZCorp, which uses multiple nozzle variety of RP processes exists for direct fabri- preg layers. One study demonstrated the use of
ink-jet print heads to print large areas in one cation of particulate and fiber-reinforced com- a novel preform comprised of a layer of SiC fi-
pass, making it possible to create parts quickly. posites. ber/furfural unidirectional prepreg adhered to the
Like SLS, parts exhibit a granular texture and Fiber-Reinforced Composites. Of all the RP top of a SiC ceramic tape (Ref 21). Regardless
are porous. Three-dimensional printing parts techniques, LOM is the only one well-suited for of the preform type, the green CMC must un-
generally require strengthening using a resin- direct manufacture of fiber-reinforced compos- dergo significant postprocessing involving high-
based infiltrant. ites. Because LOM is essentially a sheet-pro- pressure consolidation, high-temperature resin-
Drop-on-drop systems, like 3DP, FDM, and cessing method (Fig. 4), it is capable of handling to-ceramic conversion, and possibly infiltration
others, use nozzles to create parts. The Sanders common sheet preforms such as fabrics and pre- or reinfiltration with additional ceramic precur-
ModelMaker (Ref 15) (Fig. 7) and Thermojet pregs that are traditionally used in composite sor resin or liquid metal.
(registered to 3D Systems) processes deposit fabrication. Regardless of the material type, LOM and
material in a molten droplet form. This material Recent research efforts have established the other RP processes are limited to building with
then solidifies rapidly to allow further droplets viability of LOM for direct fabrication of con- flat, horizontal layers. While it is true that com-
to be applied. These processes generally use wax tinuous-fiber reinforced polymer-matrix com- plex, curved geometries can be created with this
as the raw material. Sanders machines use two posites (PMCs) and CMCs. With PMCs, a full process, they must be built up from thin, flat lay-
types of wax, one for support structures that can discussion of the various issues involved is given ers and then postmachined to get the final part.
be removed from the part material at low tem- elsewhere (Ref 18, 19). The general approach is Thus, flat-layer RP processes are incapable of
perature. Thermojet systems create supports to use the LOM machine to lay up and shape a addressing the larger geometrical issues in-
from the same material, resulting in compara- green (partially cured and consolidated) com- volved with fiber composite fabrication, namely
tively rough, down-facing surfaces. posite, followed by additional off-line consoli- fiber orientation and continuity. In response to
Metal Systems. All of the above commercial dation and cure using a heated vacuum bag or this need, the first curved-layer RP process was
systems concentrate on polymeric materials or autoclave. Glass fiber/epoxy composites made developed. The new process, referred to as
materials with low melting points. A number of with LOM using a commercially available pre- curved LOM, was motivated by the need for
processes have been adapted so that they can preg, Scotch Ply (3M), exhibited approximately rapid fabrication of fiber-reinforced structures
process metals, but few of them have reached 85% of the strength (tension, compression, flex- containing sloping, curved surfaces, especially
commercial status to date. It is not difficult to ure, and interlaminar shear) of an autoclave thin curved-shell components. It is crucial to
see how FDM, LOM, and SLS can be developed cured panel. Figure 8 is a photograph of some maintain fiber continuity along the curved sur-
into metal systems. Direct sintering of metal PMC parts. The standard CO2 laser of the LOM faces of these components.
powders is possible with the EOSint M machine, machine can be used without modification to cut Details of the curved layer process are found
although the metals are, admittedly, relatively glass fiber/epoxy prepregs. However, for higher elsewhere (Ref 22). It begins with production of
low melting point. The Laser Engineered Net performance fibers such as carbon or silicon car- a matched tool or mandrel for the intended part.
Shape (LENS) directed material-deposition pro- bide, an entirely different cutting mechanism is This tool can be generated by any of several
cess commercialized by Optomec, Inc. (Ref 16) required. To this end, researchers have demon- other RP processes, including the standard LOM
feeds metal powder into a head, which then melts strated high-quality cutting of continuous sili- process using LOM paper. The finished LOM
and deposits in a similar manner to FDM. con-carbide (SiC) fibers via photoablation using mandrel is mounted to the flat building platform
StratoConception (Ref 17) uses machining to a copper-vapor laser in a bench-top LOM pro- in the curved LOM machine. Size limitation is
create metal sheet laminates, which are bonded cess (Ref 20). approximately 30 by 30 by 5.5 cm (12 by 12 by
together like LOM. Obviously, high power, tem- For CMCs, the LOM machine is used again 3 in.). Sheets of the desired build material (e.g.,
perature, and atmosphere considerations make only to lay up and shape a green composite. Ce- composite prepreg) are loaded onto an external,
these direct methods difficult tasks to achieve. ramic-matrix composite prepregs must contain a rotatable feed table, picked up with a vacuum
chuck, and shuttled to the mandrel. A flexible
thermoforming mechanism laminates each new
layer to the curved mandrel with steady, uniform
vacuum pressure and heat. After the laminator
Direct Fabrication of retracts, a CO2 laser cuts each layer, accounting
Composite Structures for the sloped surface. The fiber orientation can
be varied from layer to layer by programming
Significant advances in the technology of the rotatable feed table. The process proceeds
rapid prototyping during the 1990s have pro- one layer at a time until the part is finished. If
duced a new capability for directly fabricating necessary, the laminator can be used to provide
advanced material prototypes and end-use com- additional post cure to the final part. Subse-
ponents. The list of advanced materials includes
particulate and fiber-reinforced polymer, ce-
ramic-matrix composites (CMCs), and metal-
matrix composites (MMCs). Adapting the vari-
ous RP processes for direct fabrication of
ceramic materials has received the most effort
because, compared to techniques for fabricating
metals and polymers, traditional techniques for
small-lot fabrication of complex-shaped ceramic
components are difficult, time consuming, labor
intensive, and expensive. Thus, RP technology
was expected to yield the earliest and greatest
payoff for direct fabrication of ceramic materi- Fig. 7 Drop-on-drop system (Sanders ModelMaker) Fig. 8 Parts made with glass fiber/epoxy prepreg using
print jets, showing the two jetting heads above laminated object manufacturing (LOM). The part
als. Great strides, however, were also made with sample parts. Courtesy of Sanders Prototype International on the right has been fully cured.
386 / Engineering Mechanics, Analysis, and Design

quently, the part is removed from the mandrel, tion. Composites with fine features having 40 to tions. During the mid- to late 1990s, extensive
and the excess material is manually stripped 50 vol% of SiC particles were successfully pro- research was focused in the development of di-
away (decubed). Suitable postprocesses are then cessed via this approach. The Mg/SiC composite rect RP systems for ceramics and ceramic com-
performed to obtain a fully consolidated, cured, microstructure showed little or no residual po- posites. The SLS is one of the commercially
and/or densified PMC or CMC. rosity for structures where the pore sizes were available processes where ceramic parts can be
The viability of using curved LOM for pro- uniform and smaller in size. One of the problems produced directly using polymer-coated ceramic
duction of PMC (Ref 23) and CMC (Ref 21, 22) in this two-stage approach is the selection of powders. The parts require postprocessing, such
structures has been established. Curved-layer metal-ceramic combination. For the pressureless as binder removal and sintering. In fused depo-
CMC components are shown in Fig. 9. Wide- infiltration process to be successful, the surface sition of ceramics (FDC) (Ref 28), ceramic par-
spread industrial use of LOM or curved LOM tension of the liquid infiltrant must be lower than ticle loaded thermoplastic filaments were used
for direct fabrication of PMCs had not occurred the surface energy of the solid matrix. Usually with commercial FDM systems to directly pro-
by the year 2001, most likely because of size the surface energies of the ceramics tend to be duce green ceramic components. In situ rein-
limitations and the availability of automated tape quite low, causing difficulties in selecting the forced Si3N4, alumina, and lead zirconium titan-
placement (ATP) machines (Ref 24) used in the matrix metal for preforms of different ceramic ate (PZT) are some of the ceramic materials that
aerospace industry (see the article “Automated compositions. have been produced using this process. Postpro-
Tape Laying” in this Volume). However, com- Metal-Ceramic Composites. Bandyopadhyay cessing such as binder removal and sintering is
pared to ATP, the cost and ease of use of LOM et al. (Ref 26, 27) reported the fabrication of in- necessary for the green FDC parts. Due to high
machine is favorable for production of small terpenetrating phase metal-ceramic composites volume fraction of thermoplastic binder content
(e.g., 60 by 30 by 15 cm, or 24 by 12 by 6 in.) using FDM. Interpenetrating phase composites of the green part, parts greater than 15 mm (0.6
articles. Thus, with regards to PMCs, LOM are those where both the metal and the ceramic in.) thick are difficult to binder remove. The 3DP
holds the most short-term potential for the con- phases are connected to itself in all three direc- process was utilized to fabricate different struc-
sumer-goods industry. Ceramic and CMC arti- tions. In this approach, controlled porosity ce- tural, electronic, and bioceramic monoliths and
cles are often not as large as PMC structures, and ramic preforms were fabricated using the indi- composites. For small parts, most of these direct-
thus the potential benefits of LOM for these ma- rect FDM. Polymeric molds of desired parts deposition techniques are capable of achieving
terials still remain for all applications. were fabricated using ICW wax with different 98% theoretical density, but cracking and
Particulate-Reinforced Metal- and Ce- tool path variations. Molds were infiltrated with warpage during full densification of complex-
ramic-Matrix Composites. Processing of mullite (Al6Si2O13) ceramic slurry or gel, and shaped, large-size parts are still serious concerns.
MMCs and CMCs presents unique opportunities dried. The structures were then subjected to a Attempts have also been made to directly pro-
for RP techniques due to the inherent nature of binder removal and sintering cycle. The poly- duce functional ceramics and composites using
high-cost, low-volume production needs of meric roads of the mold formed the pores in the other RP processes, and some of the efforts are
value-added products. Net-shape fabrication of controlled porosity mullite preform. By varying still continuing for numerous applications.
controlled microstructure parts has already been the tool path and the slice thickness of the mold,
demonstrated, utilizing some of the commercial size, shape and distribution of the pores in the
RP systems. Although extensive research and ceramic preform can be varied. Mullite preforms Freeform Tooling for
development work is still pending for tailoring were then infiltrated using an Al metal via pres- Composite Part Lay-Up
these approaches to mature commercial tech- sureless reactive metal infiltration to form mul-
niques for industrial-scale production, some of lite-Al or alumina-Al composites in which the While some inroads have been made in the
the initial results show significant promise and metal phase filled the designed pores of the pre- area of composite part production using freeform
are herein discussed. forms. Uniform and functionally gradient com- techniques, another strong area of application of
Magnesium/Silicon Carbide Composites. posites with 20 to 50 volume percent metal con- these technologies is in production of tooling for
Wohlert and Bourell (Ref 25) utilized the SLS tents were fabricated having various shapes and composite part lay-up. This has been alluded to
process to fabricate particulate Mg/SiC metal- sizes. By varying the metal and the ceramic earlier in this article with the treatment of curved
matrix composites (Fig. 10). In their approach, phases in the composites, the properties of the LOM. In the commercial sector, tools for injec-
polymer-coated commercial SiC powders were final part could be tailored for specific applica- tion and compression molding of composites
used to produce porous SiC ceramic preforms. tion. represent a significant process expense, and lim-
Preforms were binder removed and sintered, Ceramic-Matrix Composites. Ceramics are ited success has been achieved in the application
prior to metal infiltration. Porous SiC preforms hard and brittle, difficult to machine, and have of toolless manufacturing processes to tool pro-
were infiltrated with commercial die-casting low-volume production in numerous applica- duction. One example is SLS of epoxy-infiltrated
AZ91D magnesium alloy under controlled nitro-
gen environment via pressureless metal infiltra-

Fig. 9 Aircraft engine flame holders. The piece on the


left illustrates the poor surface finish obtained
with the flat-layer LOM process compared to the curved Fig. 10 Particulate composite parts produced by SLS processing of SiC preforms followed by liquid-metal infiltration
layer LOM process. of a magnesium alloy. Source: Ref 25
Rapid Prototyping / 387

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