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fOCT 22254-92

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fOCT
Diesel fuels. Cold fitter method 22254-92
for detemination of lowest filtering- temperature

OKCTY 0251

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fOCT 22254-12 C 2

4. CflllHOCTb ME.TOM

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(20 M6ap}.
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pa<P1rna, Bbl.lleneHHOro Ha pacTBOpa Ha cl>HJI&yp, e1:i1a1:i1sa10T npeKpaine·
HHe HJIH saMeAJieHHe npoTeKaHHff B TaKoA CTeneHn, qTo BpeMjl Hano.11 4
HeHHH IlHneTKH npeBblWaeT 60 c, HJlH TORJlHBO He CTeKaeT nonHOC'TblO
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5.1. YaH:T-cnHpHT, KHmlllJ.HH e npeAe,nax 60-80 °C.


5.2. AneToH.
5.3. <l>HJibTpoBaJibH3R 6yMara HeBOJIOKHHCTaR.
PacTeopuTeAu: 1-tet/Jpac c 50/170 no rocr 8505 UAU neTpOAellfiblll
at/Jup no TY 6-021244;
At{eron no I'OCT 2603;
<PUAbTpbt 6yMa~Hbte ~seAaR AeHTa,.

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(45±0,25) MM, Hapy:>KHblM ,llH8MeTpOM (48±0,25) MM ll BhlCOTOH
I 15 MM. 11cnOJib3YIOT B Ka11ecTBe BOASIHOH,6aHH.
6.3.
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cToAKoro MaTepHana, KOTopoe n0Mew.a10T Ha JI.HO Ko>Kyxa (n. 6.2) .n.ru1
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nO]J..OrHaHO K KO*YXY H ,llOJJ.>KHO HMeTb TOJllUHHy (6+~.3) MM.
6.4. ,ll,Be npoKJiaJJ.KH (3 H 6) TOJILU.HHOH 5 MM, H3 MaCJJOCTOJiKOfO
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C. S roCT 2225~92

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npo6KH (n. 6.6) B neHTpHpoeaHHOM nono:mennn. Konbuo Mo:>«eT oblTb
MOJJ.R<l>HU.HPOBaHO .D,JUInpHcnoco6JieHHff B OXJiaik..a.aromeA 6aae.
6.6. IlpotiKa (qepT. 5) H3 MacJiocTOHKoro MaTepnana, no.norHa1rnaa
K H3MepnrenbHOMy COCY/J.Y a no.lU{ep»mBalOil.(eMy KOJlbIJ.Y-. Ilpo6Ka
.ZI.OJUKRa HMeTb TPH OTBepCTlfff'.: JI.mt nHneTKH (n. 6.7) ~ TepMOMeTpa
(n. 6.8) II BblXO){a B aTMOCcpepy. EcJIH HCD01Ib3YIOT TepMOMeTp c 60 4

Jiee mapoKHMH npeJJ.eJlaMH TeMnepaTyp, eepxHJtst qacTb npo6KH MO;


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TeMnepaTyphl no TepMOMeTpy (6.8) JJ.O MHHyc 30 °C. I( aepxuei1 no·
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nonoJKeHHH Ha.no HCilOJib30B3Tb 3a>KHM H3 npy>KHHHOH rrpOBOJIOKIL
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Jiatynuoro Kopnyca c pe3b60BhlM OTBep~nteM, a KotopoM noMeme-
Ha <f>RJ1bTpau;1roHHaR CeTKa B onpaeKe. 0TBepCTHe ft.OJI.iKHO OblTb caa6·
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JI3TYffHOJf raHKff .llJIH coe,llRHeHlrn BepxHeA lJ3CTH KOpnyca <iJHJibTpa
c HH>KHeA qacTbJO nHneTKH .n.;u1 06ecne11emrn nnoTHoro coe.n.aHemrn.
npnMep npaBHJI&Horo coe.n.HHeHH11 rrpe.ncTaBJJeH Ha qept. 7;
<f>RnbTpau,HOHHOH ceTKH ,nuaMeTpoM 15 MM, H3rOTOBJieHHOH 113 npo-
BOJJOKH H3 6pOH3bl HJIH Hep:>KaBelOmeii CT3Jlli, c HOMHH3JlbHblM pa3-
MepoM OTaepcTHH 45 MKM. HoMHHaJibHhlH ,nuaMeTp rrpoao.110KH p.on-
>KeH 6blTb 32 MKM, a norpeIIIHOCTb paaMepoB OT.QeJihHhlX .flqeeK .nomK-
Ha 6b1Tb c.ne.ny10maH;
l(a>KJJ.ast Hqei{Ka He ll,OJliKHa npeBblW8Tb HOMHHaJibHOrO_ paaMepa
OOJlbWe cteM Ha 22 MKM.
Cpe.n.HHH pa3Mep HtJ:eAKH ue JJ.OJDKeH npeshlWaTb HOMHHaJJLHblH
pa3Mep Ha ±3,l MKM.
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~'laTyHHOH onpaBKH (ltepT. 8), B Koropon 3a>KaTa <f>unbtpau.Houuan
cenrn (n. 6.7.2) yKpenJUUOlll.HM KOJibUOM, BTHCHYTWM B ~eplKaBKy.
JlHaMeTp pa6ocieil t{8CTH ceTKH ,D;OJJ>KeH paBf.UITbCH ( 12-+-i· 1 ) l\1M;
fOCT Z2254-92 C. 4

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HYTh B OTBepcTHe Kopnyca (n.- 6.7.2) JlJUI JJ.O>KaTHJI onpaBK.H' CeTKH
(n. 6.7.2) 11epea npoKJiaJl.Ky (n •. 6.7.. 2) ... B HH)KHeii 'laCTH Jl.OmKHb1 ua-
XO.ltHTbCH qeTblpe xaaaBKH, o6ecneqHBBIOIUHe CTeKaHHe npo6bl B
cf>HJJbTpall,HOHHhlii annapaT.
6.8. TepMoMeTpbl c µpe.D.enaMH H3MepeH.HH OT MHHyc .30 .no nJIIOC
50 °C - Jl.JUI onpe.n.e.neHHff npe.n.en&HOH TeJ.meparyphl <l>HJJbTpyeMOCTH
)lO MHHYC 30 °C, OT MHHYC 80 .n.o nmoc 20°C - ~JUI onpe.neneHHSI
npe~eJibHOH TeMnepaTyphl cpHJJbTpyeMOCTff HH)f{e MHHyc 30 °c.
TepMOMeTP .D.Jut OXJla>K,D.arom.eii C5aHH c npe)l.eJJ3MH JJ3MepeHHH
TeMneparyp OT MHHYC 80 JJ.O DJIIOC 20 °C.
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6nnbHOM sepTHKaJihHOM nono:meHHH Ha Heo6xo.u.H~yio rny61rny. EaHH
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llpo6y TOnAUBa OT6upa10T no I'OCT 2517. ,ll.11.n. yaaAeH.Ufl. Mexa-
nu'leCKUX npuMecea u 800bl T0nAU80 </JUftt>TPYIOT 'lepea </JUJtbTP c6e-
.11.aR JLeHTa:» npu Te.MnepaType 11.e .MeHee tte.M na 15 °C Bbtut.e TeMnepa-
rypbt noMyrHeHUR.

8. nonroTOBKA ADOAPATYPbl

flepe,D. K3)KJtblM HCilblTaHaeM pa36HpaJOT <1>HnbTP (n~ 6.7.2) H npo-


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BalOT au.eTOHOM H cyUiaT ttHCTblM cyXHM 803.IJ.YXOM. IlpoBepsnoT ltllCTO-
ry H cyxoc-rh acex .n.eraneii H KO)Kyxa. TiposepsnoT, He noape)KJI.eHbl JlH
cpHJibTpanHOHHast ceTKa H coe.nHHemrn, np11 Heo6xo.AHMOCTH 3aMeH51~
!OT HX HOBhIMH. 3aTeM C06HpaIOT a11napaTypy, KaK yKa3aHO Ha qepT. I.
Dpoaep£IOT nJIOTHOCTb pe3h6osoii raiiKH (n. 6.7.2), HeT m1 yrc111-.:1t.

9. nPOBE)J.EHHE HCnblTAHH5i

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(n. 6.2).
c. 11 rocr 222s.f-s2

9.2. Ecnn npoKJJaJJ.KH (n. 6.4) He HaroTOeneHpt KaK o.nno ueJioe c


H30nllUHOHHblM KOJiblt.OM (n. 6.3), HX noMelll,alOT Ha pacCTOSIHHH OKO-
JJO J5 H 75 MM OT AH a H3MepHTeJibHOro cocy.n.a (n. 6.1).
9.3. H3MepHTeJibHblH cocy.zr. HanonmuoT HCnblTyeMbr:M ronJJHBOM JJ.o
MeTKH, COOTBeTCTBYIOill.eii 45 CM 3•
9.4. l1aMepHTeJibHblH cocy.n. 38Kpb1BalOT npo6KOH c H3XOJU111J.HMHCH
B Heu mmeTKOA c cf>HJibTpoM (rr. 6.7) H COOTBeTcheyroll.J,HM TCpMOMeT-
poM (n. 6.8). npH Q)l\HJI.aeMOJi npe.n.eJJbHOH TertmepaType cpHJJbTpye-
MOCTH HH)Ke MJtHyc 30 °C npHMeHSUOT TepMoMeTp c HH3illlfMH npe,a.ena-
MH TeMnepacyp. Bo BpeMSI HCnIJITaHHSI' TepMoMerrp HeJib3SI MeHSITb.
AnnapaTypy ycTanaenneaIOT raKHM olSpasOM, lJTOObI HH>KJUHI
ll8CTb q>HJlbTpa (n. 6.7.2) H8XO)l.HJI8Cb Ha .n.ae ~3MepnTeJibHOtO cocy-
.na; TepMOMeTp ycTaHaB.llHBaJOT napaJIJJeJihHO nuµeTKe H TaKHM o6pa-
30M, tJT06hl ero HH:>KHHii KOHeu. H8XOAHJICSI Ha ( 1,5±0,2) MM OT JJ.Ha
n3MepnTeJihHOro cocyJI.a. lliapHK TepMOMeTpa Hie JJ.O.rrlKeH conpHKa-
caThC51 HH co CTeHKOlI Jf3MepHTeJibHOfO cocy.n.a, H~ c cpfl.%TpOM.
9.5. Ko)Kyx noMeruaIOT BepTHKaJibHO Ha rJiy61rne (85±2) MM a
oxJiaR<)laIOuteii 6aHe, B KOTopoii nOJI.JI.ep:11rnaaJOT Tef\mcparypy MHHyc
(34+0,5) °C.
9.6. 113MepHTeJlbHhlH COCYJI. noMeUJ,alOT B KO}l<yx B CTa6HJJbHOM
BepTHK3JibHOM IlOJIO)KeHJrn.
9.7. flpH OTKpblTOM 3anopHOM Kpatte (n. 6.10) coe,DJfH51lOT nHner-
Ky c BaKyyMHOH ycraHOBKOH (nn. 6.11, 6.12) npn nOMOlllH rHOKHX
lllJiaHroe, npHcoe.n.1rneHHbrx K KpaHy (11epT. 1). BKJI10tta10r eaKyyM H
ycTaHas.nnaaioT B03Jl.YllIHblH noTOK TaK, '11T06hr O-o6pa3HbIH MaHOMetp
IlOK83b1BaJI nan.eHHe Jl.8BJiemrn 200 MM BO)l.SIHOr<!> CTOJI6a BO BpeM.H
Bcero HCilblT3HHH.
9.8. OnpeJl.eJiemre HallHHaroT cpa3y noCJie noMeu.r.eHHH HJMep.uTe.1b-
noro cocyJJ.a a KOLl<yx. Ecnn reMneparypa noMytaemrn npo6bl H3Becr-
Ha, JI.onycKaeTcsi HatIHHaTb onpe.n.eneHHe e MoMeHT, Kor.n.a npo6a ox-
JJaJK.n.eHa AO TeMneparypbl. KOTop·aH BblUie TeMnepaTyphI noMyTHeHHSl
ne MeHee 11eM Ha 5 °C. B nepBOM 3Tane ox.11a:>K,n.eHHH scerJJ,a HaJJ.o
npHMeHHTb 6a1no c TeMnepaTypoH MHHYoC (34±0,5) °C.
Kor)la TeMnepaTypa npoobl ,n;ocTHtHeT cooTBeTCTByromeii BeJJH4H~
Hbl, YCT8H3BJIHB310T 3anopHblH KpaH (n. 6.10), raK qT06bI qJH .TibTP 6blJ!
coe.a.HHeH c BaKyyMOM, Bhl3blBaH scacblBaHHe npo6bl Ton:rnea 11epe3
QJHJibTpaUHOHHYIO ceTKY B nnnerKy, O,ZJ;HOBpeMeHHO BKJllOllaIOT ceKyH-
.n.oMep. Kor.n.a TonJIHBO ,n..oii,n..eT JI.O MeTKH Ha mmerKe, ocrauaBJIHBaIOT
CeKYHAOMep H )'CT3HaBJJHB3lOT KpaH B H3tf3JlbHOM TI0.7J0)f{eHJm, qTQ6bI
npo6a Morna cTe% e H3MepHTeJihHbIA cocy.a..
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onpe.lleJJ-eHHe npeKpamaJOT H noBTOpRIOT co caeJKeii Maccol1 JJ,.rrn ncnbI-
ramrn, II ~l1HfH an c 60.JJee BhICOKOH TeMnepaTypbl.
9.9. Onepaumo (n. 9.8) noBTOpRIOT nocJie Ka>I<JI.Oro cH n.mett H.R
Te:\rnepaTypbI npo6bl Ha I °C )lO )lOCTIDKCHHH TeMneparypbl, npn KO-
rOCT 22254-92 C. 12

ropo.K Te?Jelrn~ q-epe3 <f>HnbTP npeKparuaercH, HJIK mmeTKa ne HanoJJ-


HReTC.H .n.o MeTKH B TeqeHHe 60 c.
• 3a1rncL1Ba10T TeMnepaTypy Haqana nocneJ(ueA <l>HJlbTpau.aa.
9.10. Ee.rm noc;re oXJra1KiteHH11 corJiaCHO n. 9.9 H 9.11 HJIH 9.12
npo.6a 3anonHS1eT nuneTKY .no MeTKH He .non&we 60 c, Ho He creKaeT
o6paTHO B H3MepHTenbHblH cocy.n noCJJe ycTaHOBJJ:eHH.H KpaHa (n. 6.10)
B nepaoHattaJibHOM ROJIO>KeHBH, TO Ha.a.o 33RHC8Tb TeMneparypy
Ha1.1aJia qrnnbTPaU.HH.
9.11. Ecnu npH TeMnepa-rype MHHyc 20 °C He npeKpamaeTcff reqe-
tme TOilJIHBa qepe3 cf>HnbTp, .n.aJibHeihnee OXJIUKJJ.eHHe ee)lyT B OXJJa}f{-
.a.aJOUleH 6aae c Ter.mepatypoA MHHYC (51±1) '°C HnH B COOTBeTCTBeH-
HO nepeKJIIOlleHHOM XOJIO.D.HJibHHKe H noeTOplllOT onepaumo (rr. 9.8)
noCJie Ka.>K}l.oro CHH>KeHHH TeMnepaTypbl Ha 1 °C.
H3Memrn 6aHIO, 6hlCTPO nepeHOCHT H3MepHTCJibHblH COCYJI. B HOBblH
KoiKyx, noMeUteHHhlH BO BTOpoii oxJia>K.na10meu 6aHe, HnH pery1rnpyS1
xonOJJ.llJlbHHK.
9.12. EcJIH npn reMneparype MHuyc 35 °C ue npeKpamaeTcH Teqe-
HHC TOnmma tfepe3 cj>HJlbTp, .aaJ1hJieih11ee ox.naM(lleHHC Be,ll.}T 8 Tpcnci1
6aHe c Ter-.rnepaTypoi{ MHHYC (67±2) °C IIJJH perynnpyH ).QJIO!l.HJlb-
HHK.
flepeHOCSIT KOMil.JleKT, KaK yKa3aHO B fl. 9.11.

JO. nPOTOKOn HCTiblTAHHSI

Pernctp11py10T TeMnepaTypy B Hatiane .noCJie.n,Hero <PHnbTpoaaunSl


c TOtIHOCTblO .ll.0 1 °C (nn. 9.9-9.10) K3K npe.ztenbHYIO TeMnepaTypy
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pe3yAbTQT08 asyx nocAeaosareAbHWX onpeoeAeHua, OKPY2AeHH.Oe ao
qeAOZO 'lUCAa.

11. TOii HOCTb METOJl.A

ToqaocTb MeTo~a nonyqeHa cTaTHCTHq~cKHM HCCJJe.n.osauHeM MeiK-


JtatJopaTOpHblJC pe3yJibT8TOB HCilblTaHHA H yKaaaHa B rm. l l.1-l J.2
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mm~ TIOJlYl.JeHHOe O.AHlfM H TeM JKe onepaTOPOM Ha O.AHOH H TO~i )KC
annapaType B o.zurnaKOBblX YCJIOBHHX Ha HAeHTH'lHOM HCCJle.n.yeMOM
MaTepHaJie npH npaBllJJbHOM BhlTIOJJHeHJm HCilblT3HHH, npeawuaeT
3Haqeum1, yKa3aHHhle Ha qepT 9, B o.n.HoM cnyrrne H3 11saauaT11
/J.ea pe3y./lbTQTQ onpeaeAeHUU, no.Ay'(eHHbte oaHUM UCllOAHUTeAeJrt
13 08HOU JZa6oparopuu, npU3HQ10TCJl aoCTOBepHblMU (npu aoeepUTeAb-
c. n rocT 22254-92

HOU eepoRTHOCTU95 %), eCAU pacxo"'aeHue Me31Coy HUMU He npe8bl-


UlQeT 1 °C.
11.2. B O C n p O H 3 BO A H M O CT b
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11eHHNMH pa)rnNMH oneparopaMH, pa60T8IOIIlHMH B pa3HhlX na6opa-
ropnsx ua nAeHTHtJHOM HCCJie,nyeMOM MaTepuaJie, npH npaBHJlbJIOM Blil-
OOJIHeHHH HCnblT3HRH. npeBblwaeT 3Ha11eHHH, npeACTaBJieHHble Ha
11epT. 9. B OJtHOM CJJyqae H3 JI.BaJt.u.aTH.
n p ff Me 1l a ff 11 C.
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no nporpaMMe, no- Koropoii npHMeH11J1HCb cnoco6Y KaK aaTOMa/THqecKHlt, TaK H PY'l-
noA.
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tTu 95 %), ecAu pacxo:HCoeHue Me:HCay HU.Mu ne npeebttuaer 2 °C.
norpemttocT& onpeJJ.eJreHHR npe.AcJrbHOii TCMnepa-
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npeiJP.RbHQR mPMnepamypa QJU/ltJmpy2MOC"1U

n p II MC II a H He. HH:>Ke P.~nHyc 35 °C norpeWHOCTb HC ycTaHoB.1t'H3.


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pwe nonollteHHR EsponeAcKoro cTaH)l.apTa EN-116 <CTaH)l'.apTHblH
MCTO)l. onpe)l'.eAeHHR npeAeJILHOA TeMnepaTJpLI cl>HnbTpyeMOCTH TO-
nAHB Ha XOJIO)l'.HOM cl>ilnLTJJe>
3. B3AMEH rocr 22254-76
4. CCLlnoq HblE HOPMATHBHO-TEXHUqECKHE JI.OKY· -
MEHTbl

6 rocr 1a1-G1
6 rocr·-400--80
7 rocr 2s11-ss
5 rocr .2003-79
5 rocr asos-ao
6 rocr 12162-11
6 rocr t8300-s1
6 .rocr 20287-91 11co 0016-11
6 rocr 9100-st uco 261-13
5 TY 6--0'2 J.244-88
6 TY 38.44710263-90
6 rocr 001 a-ss

PeAaKTOp P. C. <Pe8oposa
TexHH'leCKHA pe.n.aKTOp B. H. npycaJCOBa
KoppeKTOp B. C. l/epHa1i

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