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Original Article
Fengxian Li a,∗ , Peng Chen a , Jin Han a , Long Deng a , Jianhong Yi a,∗ ,
Yichun Liu a , Jürgen Eckert b,c
a School of Materials Science and Engineering, Kunming University of Science and Technology, Kunming 650093, China
b Erich Schmid Institute of Materials Science, Austrian Academy of Sciences, Jahnstraße 12, A-8700 Leoben, Austria
c Department of Matrials Science, Chair of Materials Physics, Montanuniversität Leoben, Jahnstraße 12, A-8700 Leoben, Austria
a r t i c l e i n f o a b s t r a c t
Article history: The intrinsic properties and the damage behavior of powder metallurgy (P/M) connecting
Received 5 September 2019 rod preform have significant effects on its metal flow behavior during flashless forging into
Accepted 19 November 2019 its final complex shape with substantial densification. The P/M material constitutive equa-
Available online 3 December 2019 tion were established using isothermal compression tests, and then used to study the metal
flow behavior of a P/M connecting rod preform during flashless forging based on finite ele-
Keywords: ment modelling (FEM). Moreover, the preform geometry was designed based on these metal
Connecting rod flow mechanisms. Experiments and flashless forging of P/M connecting rod preforms were
Numerical simulation performed in order to verify the accuracy of the simulations. The simulated results are
Optimization well consistent with the experimental results. Results showed that the shank is much more
Powder metallurgy prone to cracking due to the higher deformation rate and the faster cooling rate. The optimal
dimensions of the P/M preform were obtained. When the preform geometry are optimized,
the average density of the connecting rod increases homogeneously, and becomes superior
to that of the original shape. This work suggests that the geometry of the preform can be
designed efficiently based on our models. This work can help to derive a P/M connecting rod
preform optimization methodology, which can offer the possibility of improving the quality
of the connecting rods efficiently.
© 2019 The Authors. Published by Elsevier B.V. This is an open access article under the
CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
1. Introduction
2. Materials, experimental methods and Table 1 – Element numbers and nodes of different
calculation simulation models.
Preform Bottom die Cavity block Top die
2.1. Materials Elements 72,341 14521 64899 76682
Nodes 17645 61235 15468 17812
A Fe-3Cu-0.5C (wt.%) alloy with a relative density of 0.8 man-
ufactured by powder metallurgy route (P/M Fe-Cu-C) was
Table 2 – Physical property data of the preform and the
selected as the model material.
mould [25,26].
P/M Fe-Cu-C alloy
2.2. Experimental methods
Elastic modulus 155
The isothermal compression test can be used to study the flow Poisson’s ratio 0.28
Tensile strength (MPa) 460
stress of the P/M Fe-Cu-C alloy. First, samples with diameter
Heat capacities per unit mass (Jkg−1 K−1 ) Cp = 317.202 + 0.433 × T
of 8 mm and height of 12 mm were prepared, and then heated
by induction coils at a heating rate of 5 K/s and soaked for 10 s H13
by the thermocouple feedback control system. Then, samples
Elastic modulus (1011 Pa) 2.10 (293 K) 1.91 (293 K)1.75 (293 K)
were hot compressed using a Gleebe-3500 thermal simulator
Thermal conductivity (Wm−1 K−1 )36.6 (293 K) 32.1 (293 K)29.7 (293 K)
to a final strain of 0.7 at temperatures of 1333, 1363, 1393 and
Heat capacities (Jkg−1 K−1 ) 445.6 (293 K)553 (293 K) 641 (293 K)
1423 K and strain rates of 5, 11.5 and 19.2s−1 , respectively. The
true strain-stress curves were obtained automatically.
form were 72,341 and 17645, respectively. More details can
In the fleshless forging operations, the punch velocity was
be seen in Table 1. An adaptive remeshing parameters and
determined as 250 mms−1 , while the preheating tempera-
an updated Lagrange procedure were chosen for large elastic-
ture of the preform and the moulds were 1403 and 573 K,
plastic deformation. This procedure can also help to reduce
respectively. In order to verify the accuracy of the above estab-
the total calculating time. In this work, H13 was utilized for
lished models, two connecting rod preforms with the initial
the moulds. The physical property data of the preform and H13
geometry were flashless forged under the same processing
are listed in Table 2 [25,26]. According to the forging conditions,
parameters. One of the preforms was forged to its final shape,
the friction factor for the porous P/M preform was determined
another one was stopped after 0.038 s when the preform was
as 0.3 for the porous P/M preform [27].
partially deformed. Samples with dimension of 8 × 12 mm
Compared with other damage criteria, the Cockcroft-
were cut at different axial locations. The density of the sam-
Latham criterion, which can give accurate results in three
ples was measured using a buoyancy weighing machine. In
dimensional high stress state applications, was utilized [28]:
order to verify the validity of the models, a flashless forging
experiment under the same processing conditions was carried
max
out on the optimized preform. dε̄ = Cd , (1)
¯
2.3. Numerical calculation Where max is the principal stress and dε̄ is the effective strain
increment. The damage factor Cd can be utilized to describe
The initial size and geometry of the porous P/M preform are the crack probability of materials in the DEFORM-3D software.
presented in Figs. 2 (a) and (b): the thickness of the small end Once Cd reaches a critical value C0 , fracture occurs.
section (A), the large end section (B) and the connecting section The heat transfer among the tooling, the billet and the
or the shank (E) were 42.4 mm, 23.4 mm and 26.4 mm, respec- ambient environment is an important factor for the material
tively. The outer radius of the large end section (C) and the flow behavior of the preform. Since the flashless forging of a
length of the shank (D) were 27.4 and 74.6 mm, respectively, P/M preform is a thermo-mechanical process, the heat balance
and the degree of the chamfering (F) was 3◦ . equation can be described as: [29]
The thermo-mechanically coupled simulation of the flash-
less forging of the porous P/M connecting rod preform was ∂2 T ∂2 T ∂2 T ∂T
QI + A + 2 + 2 − C = 0, (2)
performed with the finite-element software, DEFORM-3D. The ∂x 2 ∂y ∂z ∂t
tooling models were defined as rigid material. For a detailed
description of the finite element theory, the readers are where QI is the heat generated due to plastic deformation or
referred to [24]. In this work, the initial preform density the heat conversed from plastic work Q1 ; A is the thermal
affected by the P/M process was fixed as a constant for simplic- conductivity.
ity. The corresponding analysis FEM models of the preform, The heat loss at internal preform during cooling is calcu-
tool, punch and cavity are established in Fig. 3(a). Isoperimetric lated as:
four-node elements were utilized to define the element mesh,
as shown in Fig. 3(b). Q1 = h1 (T − Ta ) + ω T 4 − Ta4 , (3)
The mesh density was changed according to the strain
distributions. Namely, the mesh density in a large deforma- where Ta is the environment temperature, and ω and are
tion zones was higher than that in other areas. For example, the emissivity constant and the Stefan-Boltzmann’s constant,
the element numbers and nodes of the connecting rod pre- respectively.
j m a t e r r e s t e c h n o l . 2 0 2 0;9(2):1200–1209 1203
Fig. 2 – Represent size (a) and geometry (b) of the original connecting rod preform.
Fig. 3 – Simulation models of punch, cavity, tool and preform (a) and the definition of their element mesh (b).
The heat lose at the preform/model interface model can be The activation
energy ofhot
deformation
Q can be deter-
evaluated as: ∂lnε̇ ∂ ln[sinh(˛)]
mined by Q = R ∂ln[sinh(˛)] ∂(1/T)
. The constant ˛
T ε̇
is independent of the deformation temperature and can be
Q2 = h2 (T − Ta ) , (4) determined as 0.011 based on experimental results (Fig. 4). The
universal gas constant R is 8.314 J/mol. The average slope value
Compared with the hot forming process, the convection of line ln ε̇l̃n[sinh(˛)] derives the value of n, which is 5.95.
coefficients h1 is determined as 28 Wm−2 K-1 and h2 is taken Since Q=RnK, Q is 188.56 kJ/mol. Therefore, the constitutive
as 4.8 × 104 Wm−2 K−1 in this work [30,31]. equation of P/M preform are obtained as following:
The heat Q3 generated due to the friction between the pre-
form and the model is given as: 5.95
ε̇ = 5 × 107 [sinh(0.011)] exp [−188560/(8.314T)] (7)
Fig. 4 – The flow stress of the porous P/M preform at different temperatures and various stain rates: (a) 5 s−1 ; (b) 11.5 s−1 ; (c)
19.2 s−1 .
Calculated c-end 0.998 1.000 0.995 0.992 0.991 0.995 0.994 0.952 0.946
Experimental e-end 0.986 0.991 0.988 0.989 0.986 0.963 0.973 0.957 0.955
Calculated c-0.038 0.854 0.894 0.884 0.893 0.884 0.885 0.884 0.846 0.861
Experimental e-0.038 0.834 0.861 0.862 0.853 0.892 0.873 0.881 0.825 0.834
with the calculated results. For example, the calculated value age distribution profiles after nearly 0.02 s of deformation and
of c-0.038 = 0.846 at P
18 (at the small end section) of the con- for the fully deformed state are displayed in the colour maps. It
necting rod deformed for 0.038 s corresponds well with the can be seen that after nearly 0.02 s of deformation, the damage
measured value of e-0.038 = 0.825. The deviations between the factor value Cd at the shank is large compared with that of the
experimental and simulated results are small. Obviously, the fully deformed connecting rod. This means that the shanks
simulated density variation of the connecting rod compared are prone to crack at 0.02 s, which may lead to a decrease
with that measured by experiments at zero, 0.38 and 0.48 s can of the relative density. However, the fracture does not occur
well verify the accuracy of the above established models. at the end. Both the experiment and the simulated results
However, it should be noted that during the forging pro- reveal that Cd does not reach its critical value of C0 = 0.45. This
cess, at about 0.02 s, the relative density at P 14 decreases means that the crack probability decreases when this zone is
initially and then increases again. This is different from the completely filled and c increases at the end of the deforma-
findings at P , 18 as shown in Fig.5 (b). This phenomenon can tion. The finding that cracks occur easily at the shank is also
be well explained by the damage distribution profiles of the underlined by the variations of the metal flow behavior of the
connecting rod during flashless forging. In Fig. 5 (b), the dam- partially deformed (at 0 s, 0.38 s and 0.48 s) and fully deformed
j m a t e r r e s t e c h n o l . 2 0 2 0;9(2):1200–1209 1205
Fig. 5 – Ccomparisons of the relative density distribution (a) and the damage distribution (b) of the connecting rod at
different locations and after different forming time.
(the end) porous P/M preform at various locations, as shown in will be unavoidable. Once the shank is completely filled, the
Fig. 5 (b). deformation processed into the other areas, i.e., points , C ,
D
E and F at the large end section and point B at the small end
3.3. Metal flow behavior section), as shown in Figs. 6 (c) and (f).
The metal flow behavior of the preform during the forging
Figs. 6 (a) and (d) show that the connecting rod preform gets process was determined by the load history supplied by the top
initially in contact with the punch from a vertical view and a die, as shown in Fig. 7. The density increases with increasing
side view, respectively. Some representative points, i.e., A ,
B load supplied by the tool. When the forging time increase from
,
C ,
D ,E ,
F and ,G were selected for further analysis. While A 0.020 to 0.054 s, the load values exerted by the top die increase
is a point on the surface of the connecting section,
B and G are from 52 to 733 K N. As the P/M preform contains internal pores,
points at the small end section and , C ,
D E and F are points the density increases effectively with increasing load. Then,
at the large end section, respectively. From a vertical view, as a higher forging force is needed with increasing metal flow
shown in Fig. 6 (b), as well as from a side view in Fig. 6 (e), it resistance. It can be noticed that the deformation and den-
can also be observed that point A at the shank gets in contact sification of the porous P/M materials occur simultaneously
with the mold initially. This can lead to a long time and a large during flashless forging.
deformation. It can be safely speculated that the heat loss will
be quite pronounced. Moreover, the shank is prone to cracking 3.4. Optimization of the preform geometry
due to the high deformation rate and fast cooling. If this zone is
not fully densified, due to the inappropriate design of the pre- The orthogonal design method was used to optimize the pre-
form geometry or unsuitable processing parameters, cracking form geometry. Through this method, it is possible to optimize
1206 j m a t e r r e s t e c h n o l . 2 0 2 0;9(2):1200–1209
Fig. 6 – Metal flow behavior of a P/M preform during flashless forging: (a) 0 s, (b) 0.38 s and (c) 0.48 s are from a vertical view,
while (d) 0 s, (e) 0.38 s, (f) 0.48 s and (g) the end are from a side view.
Table 4 – The uniform designs L25 (5)6 and the orthogonal table of the maximum relative density c . The sizes of the
preform, A, B, C, D, E and F are described in Fig. 3(a).
Factors A (mm) B (mm) C (mm) D (mm) E (mm) F (o )
Table 5 – Comparison of the c and e . cooling rates at different times and different positions are dif-
ferent. The cooling rate at the shank of the connecting rod,
P
1 P
4 P
10 P
14 P
17 P
18
such as at point (14), is lower than that near the large end
Calculated c 0.995 0.998 1.000 1.000 0.998 0.998
section (point ) and the small ends (point ).20 This was
Experimental e 0.993 0.994 0.996 0.997 0.996 0.997
determined by the balance between the heat generated due to
the plastic deformation and the heat loss due to conduction,
obtained: A = 44.4 mm, B = 26.4 mm, C = 29.4 mm, D = 70.6 mm, convection, and radiation. Figs. 10 (b) and (c) reveal that the
E = 24.4 mm, and F = 1.5◦ , as shown in Fig. 8. effective stress and the effective strain at the shank increase
Compared with the initial geometric size of the P/M pre- dramatically. It can be safely speculated that the deformation
form, Fig. 3 (b), the optimal values of D, E and F are small, rates at different locations do not change significantly. This
and the optimal A, B and C values are large. In order to verify means that the deformation of the porous P/M preform occurs
the validity of the optimized preform geometry, experiments homogeneously during the flashless forging process. Hence,
were dones under the same processing conditions. As shown altogether, this work presents a method and an analysis to
in Table 5, the values c at different positions of the preform are manipulate the size and geometry of the preform, thus ensur-
compared with the values e . It can be seen that c agrees well ing a uniform density distribution that helps to improve the
with e . For example, the value c = 1.000 at P (14) in the shank quality of connecting rods.
closely matches the experimentally measured value e = 0.997.
Moreover, when the preform geometry is optimized, the value
c at P (14) of the connecting rod is increased and the density 4. Conclusions
distribution of the connecting rod is uniform.
More details about the density variations of the connect- The properties and the damage behavior of P/M connecting rod
ing rod for both the optimized and original geometries can be preform has a significant influence on its metal flow behav-
seen in Fig. 9 (a). Undoubtedly, the value c of the connect- ior during flashless forging. The metal flow behavior of a P/M
ing rods at different locations increases significantly when connecting rod preform during flashless forging were stud-
the geometry is optimized. This result is reasonable since a ied based on isothermal compression tests and FEM. First, the
larger deformation generates larger metal flow stresses in P/M P/M material constitutive equation was established. Then, an
materials, and these stresses improve the densification of the appropriate criterion satisfied for complex stress state appli-
materials. Accordingly, the density increases strongly. It can cations was selected, the boundaries conditions among the
be noted that the value c at P (14) of the connecting rod forged preform, the ambient environment and cavities changed with
with optimized preform geometry increases with increasing time were considered, as well as the damage behavior of the
time, which is different from the results for the connecting rod porous P/M material during the flashness forging process. Sec-
forged from the original preform (i.e., the c decreases initially ond, the metal flow behavior of a porous P/M preform during
and then increases again). flashless forging was investigated using FEM. The simulated
Specifically, when the forging time increases from 0.018 to results are consistently well with the experimental results.
0.054 s, the value of c at P (14) of the connecting rods forged Results showed that the shank is much more prone to cracking
with optimized geometry design increase from 0.858 to 0.999, due to the higher deformation rate and the faster cooling rate.
while c that of the connecting rods forged using the original The optimal dimensions of the P/M preform obtained by using
preform geometrys increases from 0.749 to 0.995. This means an orthogonal design method were: A = 44.4 mm, B = 26.4 mm,
that the cracks developing in the connecting rod using the C = 29.4 mm, D = 70.6 mm, E = 24.4 mm, F = 1.5◦ . When the
original preform can be eliminated effectively through opti- preform geometry are optimized, the average density of the
1208 j m a t e r r e s t e c h n o l . 2 0 2 0;9(2):1200–1209
Fig. 9 – c distribution (a) and damage distribution (b) of the connecting rod flashless forged from optimized preform
geometry, as well as the hot forged connecting rod.
Fig. 10 – Variations of temperature (a), effective strain (b) and effective stress (c) with forging times.
connecting rod increases homogeneously, and becomes supe- and 51904133), the Science Foundation of the Yunnan Provin-
rior to that of the original shape. This work suggests that the cial Education Department (No. 2016CYH08) and the Science
geometry of the preform can be designed efficiently based on Foundation of the Yunnan Provincial Science and Technology
our models. This work can help to derive a P/M connecting rod Department (No. 2017HC033).
preform optimization methodology, which can offer the pos-
sibility of efficiently improving the quality of the connecting
rods.
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