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H2S & TOTAL SULPHUR SPECIFICATIONS 903 H2S & TOTAL SULPHUR

PERFORMANCE Inputs: 4 - Dry contact inputs - user programmable ANALYZER


4 - Wet inputs – for remote calibration etc.
Ranges: Up to 0-2000ppm with no dilution; user programmable
up to 0-100% with dilution PATENT PENDING
Two isolated 4-20ma analog inputs to allow
Low Range: 0-1ppm or less (Please consult factory) 903 to be communication hub for other
Linearity: ±1% of full scale devices that do not include that capability
Repeatability: ±1% of full scale > 1ppm Intrinsically Safe Keypad has 20 keys for
±2.5% of full scale <1ppm easy menu navigation
±2.5% of full scale>200ppm
±2% of full scale for total sulfur
Cycle Time: Depends on range and gas concentration; INSTRUMENT SPECIFICATIONS
Maximum cycle time user configurable; Ambient: 10-50°C (without enclosure)
20 second response to alarm
Power 10W @ 24VDC
Consumption:
FUNCTIONS Power Universal AC 90-240V and 10-36V DC
Streams : 4 Streams
Input range: input
Each stream includes: H2S analysis run, Electrical: All systems are CSA C/US or field certified
zero run,reference 1 run, reference Class 1,Div I, Group B,C,D (pending)
2 run, calibration run and optional total Class 1,Div II, Group B,C,D (pending)
sulphur run Electronics: Dual processor design using intelligent
Each stream can have separate calibration colorimetric sensor
coefficient and range of measurement Sensor is using 24 Bit AD converter to
Tape Life: Typical tape life given 3 minute cycle time is achieve greatest sensitivity and
5 weeks; can be extended to 15 weeks incorporates temperature sensor
Tape Analyzer measures exact amount of Real Time Clock for accurate event time
stamping
Measurement: tape used
512 Kbytes non-volatile memory for Data
Auto/Manual In AUTO mode analyzer runs in predefined
Logging and Audit Trail (Up to 10 months of
Mode Of sequence that is user programmable H2S concentration data logs)
Operation: In MANUAL mode user can force any Field upgradeable firmware
stream to run Tape Length sensor to accurately measure
tape movement and usage
COMMUNICATION/INTERFACE Dimensions:
Independent Low Tape sensor is optional
28” H x 16” W x 16” D
Dual Processor Ensures accuracy Weight: 903 Div II, 40 lbs
Design: 903 Div 1, 80 lbs
Outputs: 6 - isolated 4-20mA user scalable and
programmable (16 Bits of resolution) OPTIONS
6 - Relay contact SPDT (form C) 8 Amps
220VDC max. – user programmable • Dilution System
8 - Solenoid drivers –3A max. – User • High Pressure Sampling System
programmable • Solar Power
1 - USB or RS-232 Serial Port • Diagnostic - Low Pressure
1 - RS-232 Serial Port (Modem)
• Diagnostic - Low Hydrogen
1 - RS-485 Serial Port (Isolated)
• Enclosure / Cabinet
1 - High Speed LAN connection at 2.5M
Bits per second • Total Sulphur
Ethernet Option • Back Panel
ISO 9001: 2000
All serial ports are MODBUS compatible
10 - Visual indicators (LED) for quick status
Large graphics display for easy viewing
March - 2008

RAPID RESPONSE
WWW.GALVANIC.COM 0020422:800260 WWW.GALVANIC.COM
SUPERIOR ACCURACY
Galvanic Applied Sciences Inc. Houston, Texas, USA Toll Free
7000 Fisher Road S.E.
Calgary, Alberta T2H 0W3
13211K Windfern Rd
Houston, TX 77064
1-866-252-8470 REDUCED COST AND MAINTENANCE
Telephone: 403-252-8470 Telephone : 281-477-9002 (US & Canada only)
Fax: 403-255-6287 Fax: 281-477-9004 OVER-RANGE & MULTI-RANGE CAPABILITY
W W W. G A LVA N I C . C O M • E - M A I L : I N F O @ G A LVA N I C . C O M
903 H2S TAPE ANALYZER 903 COLORIMETRIC SENSOR
The Galvanic Applied
The 903 Sensor Block achieves cutting precise by making accurate measurements at the source of the
Sciences Leadership continues Galvanic's 903 H2S Tape Analyzer is designed to measure up to 4 streams of hydrogen
chemical reaction. All measurements, diagnostics, and calibrations are performed by an independent
sulphide ( H2S) and total sulphur in gaseous streams. The new 903 H2S Tape Analyzer has the
Galvanic is the leading supplier of microprocessor on the sensor block.
same rapid 20 second response time of the traditional lead acetate tape, while making
H2S / Total Sulphur analyzers in unprecedented advances in accuracy and linearity, and reduced operation cost. • Microprocessor controlled sensor • Digital signal processing for best
the world. Our foundation is built on compensates for drift, aging and accuracy and repeatability
These advances are based on a patent pending algorithm and advanced digital sensor tape variances • Automatic light emitter intensity
years of innovation, leadership and
technology developed by Galvanic. • Automatic zero set compensation
customer satisfaction.
The 903 H2S Tape Analyzer new capabilities include: • Automatic span set • 24 Bit ADC converter for
Experienced • Remote diagnostics measurement in situ
• 0-2000 ppm range without dilution - at least 50 times greater than traditional
Over 25 years of experience. tape analyzers;
• Linearity and repeatability of just ± 1% of full scale;
MULTI-STREAM MULTI-RANGE
Established • 5-15 week tape life - up to 2 times greater than that of traditional tape analyzers; and Galvanic‘s 903 has the ability to measure more than one stream of varying concentration. Traditionally
Galvanic is a reliable and trusted • Over-range and multi-range measurement two analyzers were required when the concentration of two streams were significantly different. The
name in H2S analysis. Operators can now measure the extent to which H2S exceeds pre-set alarm levels as well as patent pending 903 algorithm allows one analyzer to measure 2 - and up to 4 - streams that have
use the quick response H2S analyzer in new, higher ppm applications. concentrations differing by up to 2 orders of magnitude. For example, one analyzer could be used to
Customer Service measure H2S in the 0-10 ppm range and Total Sulphur in the 0 -500 ppm range.
In addition, the 903 H2S Tape Analyzer can read samples from different ranges. This multi-
Our experienced field support range capability replaces the need for separate analyzers calibrated each for separate streams.
team is always there to meet your CONFIGURABLE SOFTWARE
Other new features of the 903 H2S Tape Analyzer include built-in modbus communications /
requirements. The 903 comes with a Windows application which can be used to configure and
RTU capabilities, a greater number of outputs and inputs, sensor auto-calibration on each
analysis and dual redundant power supply. monitor its operation. All aspects of the 903 can be configured including alarms,
sequence of analysis operation, digital inputs, digital outputs, analog inputs, analog
The 903 H2S Tape Analyzer also comes with a total sulphur option. Using the multi-range outputs, communications, and logging. Monitoring is achieved using the Analysis
capability 1 unit can measure up to 4 separate H2S and total sulphur streams of varying window, with further break downs of alarms on the Alarm window, and IO using the
APPLICATIONS: concentrations. Status window. In addition it is possible to download logs of analysis results, and an audit
trail showing alarms and configuration changes.
• Natural Gas Processing
• Natural Gas Transmission COMMUNICATIONS
• Liquified Petroleum Gas
• Liquified Natural Gas 903 IS THE MOST ADVANCED TAPE With built-in MODBUS communications / RTU capabilities, The 903 is equipped with
• Petrochemical Feedstock RS - 485 & RS - 232 communication ports. The 903 supports Modicon and Enron
• Fuel Cell
ANALYZER ON THE MARKET OFFERING: MODBUS protocols. The 903 can also take analog signals from other analyzers and
output the data via MODBUS communications.
• Refining Rapid Alarm
• Emission Monitoring 20 seconds to alarm
TOTAL SULPHUR OPTIONS
Reduced Cost and Maintenance
Up to 2 times greater tape life than other analyzers The hydrogenation reaction furnace allows a standard Galvanic Applied Sciences H2S analyzer
Auto-calibration of digital colorimetric sensor tomeasure total sulphur concentration.
Tape measurement output
The sample is mixed with a hydrogen stream and heated to approximately 900°C. At this temperature
Greater Accuracy in the presence of hydrogen all sulphur compounds will be converted to H2S. Also, any hydrocarbon
Dynamic Range: 0-2000 ppm with no dilution; 0-100% with dilution heavier than methane will be cracked to form methane.
Linearity: ±1% of full scale
Repeatability: ±1% of full scale at > 1ppm Examples of the sulphur reaction are:
900°C 900°C
Enhanced Communications COS + 4H2 ➪ CH4 + H2O + H2S (CH3CH2)2S + 4H2 ➪ 4CH4 + H2S
Built-in RTU capabilities: MODBUS on RS-232, Carbonyl Sulphide Diethyl Sulphide
RS-485, USB, Ethernet & Arcnet Increased I/O 900°C 900°C
Analog: 6 outputs & 4 inputs (CH3)2S + 2H2 ➪ 2CH4 + H2S C4H10 + 3H2 ➪ 4CH4
Digital: 8 inputs, 6 relays & 8 solenoid drivers Dimethyl Sulphide Butane: Example of Cracking

Uninterrupted Operation
Dual redundant power supply
LEAD ACETATE TAPES
Up to 4 Streams Galvanic’s controlled plant environment ensures top quality in our lead acetate tapes.
Over-range and Multi-range Measurement Our automated process and constant quality checks ensure consistent product. All our
tapes are cleaned after treatment to minimize problems caused by paper dust. We can provide tape
lengths up to three hundred and fifty feet. Analyzers run cleaner and smoother with Galvanic’s tape.

• No interferences • Colourless reactants


• Sensitivity to ppb • Linear respon
903 H2S TAPE ANALYZER 903 COLORIMETRIC SENSOR
The Galvanic Applied
The 903 Sensor Block achieves precise results by making accurate measurements at the source of the
Sciences Leadership continues Galvanic's 903 H2S Tape Analyzer is designed to measure up to 4 streams of hydrogen
chemical reaction. All measurements, diagnostics, and calibrations are performed by an independent
sulphide ( H2S) and total sulphur in gaseous streams. The new 903 H2S Tape Analyzer has the
Galvanic is the leading supplier of microprocessor on the sensor block.
same rapid 20 second response time of the traditional lead acetate tape, while making
H2S / Total Sulphur analyzers in unprecedented advances in accuracy and linearity, and reduced operation cost. • Microprocessor controlled sensor • Digital signal processing for best
the world. Our foundation is built on compensates for drift, aging and accuracy and repeatability
These advances are based on a patent pending algorithm and advanced digital sensor tape variances • Automatic light emitter intensity
years of innovation, leadership and
technology developed by Galvanic. • Automatic zero set compensation
customer satisfaction.
The 903 H2S Tape Analyzer new capabilities include: • Automatic span set • 24 Bit ADC converter for
Experienced • Remote diagnostics measurement in situ
• 0-2000 ppm range without dilution - at least 50 times greater than traditional
Over 25 years of experience. tape analyzers;
• Linearity and repeatability of just ± 1% of full scale;
MULTI-STREAM MULTI-RANGE
Established • 5-15 week tape life - up to 2 times greater than that of traditional tape analyzers; and Galvanic‘s 903 has the ability to measure more than one stream of varying concentration. Traditionally
Galvanic is a reliable and trusted • Over-range and multi-range measurement two analyzers were required when the concentration of two streams were significantly different. The
name in H2S analysis. Operators can now measure the extent to which H2S exceeds pre-set alarm levels as well as patent pending 903 algorithm allows one analyzer to measure 2 - and up to 4 - streams that have
use the quick response H2S analyzer in new, higher ppm applications. concentrations differing by up to 2 orders of magnitude. For example, one analyzer could be used to
Customer Service measure H2S in the 0-10 ppm range and Total Sulphur in the 0 -500 ppm range.
In addition, the 903 H2S Tape Analyzer can read samples from different ranges. This multi-
Our experienced field support range capability replaces the need for separate analyzers calibrated each for separate streams.
team is always there to meet your CONFIGURABLE SOFTWARE
Other new features of the 903 H2S Tape Analyzer include built-in modbus communications /
requirements. The 903 comes with a Windows application which can be used to configure and
RTU capabilities, a greater number of outputs and inputs, sensor auto-calibration on each
analysis and dual redundant power supply. monitor its operation. All aspects of the 903 can be configured including alarms,
sequence of analysis operation, digital inputs, digital outputs, analog inputs, analog
The 903 H2S Tape Analyzer also comes with a total sulphur option. Using the multi-range outputs, communications, and logging. Monitoring is achieved using the Analysis
capability 1 unit can measure up to 4 separate H2S and total sulphur streams of varying window, with further break downs of alarms on the Alarm window, and IO using the
APPLICATIONS: concentrations. Status window. In addition it is possible to download logs of analysis results, and an event
log showing alarms and configuration changes.
• Natural Gas Processing
• Natural Gas Transmission COMMUNICATIONS
• Liquified Petroleum Gas
• Liquified Natural Gas 903 IS THE MOST ADVANCED TAPE With built-in MODBUS communications / RTU capabilities, The 903 is equipped with
• Petrochemical Feedstock RS - 485 & RS - 232 communication ports. The 903 supports Modicon and Enron
• Fuel Cell
ANALYZER ON THE MARKET OFFERING: MODBUS protocols. The 903 can also take analog signals from other analyzers and
output the data via MODBUS communications.
• Refining Rapid Alarm
• Emission Monitoring 20 seconds to alarm
TOTAL SULPHUR OPTIONS
Reduced Cost and Maintenance
Up to 2 times greater tape life than other analyzers The hydrogenation reaction furnace allows a standard Galvanic Applied Sciences H2S analyzer to
Auto-calibration of digital colorimetric sensor measure total sulphur concentration.
Tape measurement output
The sample is mixed with a hydrogen stream and heated to approximately 900°C. At this temperature
Greater Accuracy in the presence of hydrogen all sulphur compounds will be converted to H2S. Also, any hydrocarbon
Dynamic Range: 0-2000 ppm with no dilution; 0-100% with dilution heavier than methane will be cracked to form methane.
Linearity: ±1% of full scale
Repeatability: ±1% of full scale at > 1ppm Examples of the sulphur reaction are:
900°C 900°C
Enhanced Communications COS + 4H2 ➪ CH4 + H2O + H2S (CH3CH2)2S + 4H2 ➪ 4CH4 + H2S
Built-in RTU capabilities: MODBUS on RS-232, Carbonyl Sulphide Diethyl Sulphide
RS-485, USB, Ethernet & Arcnet Increased I/O 900°C 900°C
Analog: 6 outputs & 4 inputs (CH3)2S + 2H2 ➪ 2CH4 + H2S C4H10 + 3H2 ➪ 4CH4
Digital: 8 inputs, 6 relays & 8 solenoid drivers Dimethyl Sulphide Butane: Example of Cracking

Uninterrupted Operation
Dual redundant power supply
LEAD ACETATE TAPES
Up to 4 Streams Galvanic’s controlled plant environment ensures top quality in our lead acetate tapes.
Over-range and Multi-range Measurement Our automated process and constant quality checks ensure consistent product. All our
tapes are cleaned after treatment to minimize problems caused by paper dust. We can provide tape
lengths up to three hundred and fifty feet. Analyzers run cleaner and smoother with Galvanic’s tape.

• No interferences • Colourless reactants


• Sensitivity to ppb • Linear response
H2S & TOTAL SULPHUR SPECIFICATIONS 903 H2S & TOTAL SULPHUR
PERFORMANCE Inputs: 4 - Dry contact inputs - user programmable ANALYZER
4 - Wet inputs – for remote calibration etc.
Ranges: Up to 0-2000ppm with no dilution; user programmable
up to 0-100% with dilution PATENT PENDING
Two isolated 4-20ma analog inputs to allow
Low Range: 0-1ppm or less (Please consult factory) 903 to be communication hub for other
Linearity: ±1% of full scale devices that do not include that capability
Repeatability: ±1% of full scale > 1ppm Intrinsically Safe Keypad has 20 keys for
±2.5% of full scale <1ppm easy menu navigation
±2.5% of full scale>200ppm
±2% of full scale for total sulfur
Cycle Time: Depends on range and gas concentration; INSTRUMENT SPECIFICATIONS
Maximum cycle time user configurable; Ambient: 10-50°C (without enclosure)
20 second response to alarm
Power 10W @ 24VDC
Consumption:
FUNCTIONS Power Universal AC 90-240V and 10-36V DC
Streams : 4 Streams
Input range: input
Each stream includes: H2S analysis run, Electrical: All systems are CSA C/US or field certified
zero run,reference 1 run, reference Class 1,Div I, Group B,C,D (pending)
2 run, calibration run and total sulphur run Class 1,Div II, Group B,C,D (pending)
Each stream can have separate calibration Electronics: Dual processor design using intelligent
coefficient and range of measurement colorimetric sensor
Tape Life: Typical tape life given 3 minute cycle time is Sensor is using 24 Bit AD converter to
5 weeks; can be extended to 15 weeks achieve greatest sensitivity and
Tape Analyzer measures exact amount of incorporates temperature sensor
Measurement: tape used Real Time Clock for accurate event time
stamping
Auto/Manual In AUTO mode analyzer runs in predefined
512 Kbytes non-volatile memory for Data
Mode Of sequence that is user programmable
Logging and Audit Trail (Up to 10 months of
Operation: In MANUAL mode user can force any H2S concentration data logs)
stream to run Field upgradeable firmware
Tape Length sensor to accurately measure
COMMUNICATION/INTERFACE tape movement and usage
Independent Low Tape sensor is optional
Dual Processor Ensures accuracy Dimensions: 28” H x 16” W x 16” D
Design: Weight: 903 Div II, 40 lbs
Outputs: 6 - isolated 4-20mA user scalable and 903 Div 1, 80 lbs
programmable (16 Bits of resolution)
6 - Relay contact SPDT (form C) 8 Amps
220VDC max. – user programmable
OPTIONS
8 - Solenoid drivers –3A max. – User • Dilution System
programmable • High Pressure Sampling System
1 - USB or RS-232 Serial Port • Solar Power
1 - RS-232 Serial Port (Modem)
• Diagnostic - Low Pressure
1 - RS-485 Serial Port (Isolated)
• Diagnostic - Low Hydrogen
1 - High Speed LAN connection at 2.5M
Bits per second • Enclosure / Cabinet
Ethernet Option • Total Sulphur
All serial ports are MODBUS compatible • Back Panel
10 - Visual indicators (LED) for quick status ISO 9001: 2000
Large graphics display for easy viewing
March - 2008

RAPID RESPONSE
WWW.GALVANIC.COM 0020422:800260 WWW.GALVANIC.COM
SUPERIOR ACCURACY
Galvanic Applied Sciences Inc. Houston, Texas, USA Toll Free
7000 Fisher Road S.E.
Calgary, Alberta T2H 0W3
13211K Windfern Rd
Houston, TX 77064
1-866-252-8470 REDUCED COST AND MAINTENANCE
Telephone: 403-252-8470 Telephone : 281-477-9002 (US & Canada only)
Fax: 403-255-6287 Fax: 281-477-9004 OVER-RANGE & MULTI-RANGE CAPABILITY
W W W. G A LVA N I C . C O M • E - M A I L : I N F O @ G A LVA N I C . C O M
151909_Galvanic_BRO 3/30/04 10:37 AM Page 1

TYTRONICS®
SENTINEL
THE WATCHDOG OF CHEMICAL
ANALYSIS AND WATER MONITORING

WWW.GALVANIC.COM
151909_Galvanic_BRO 3/30/04 10:37 AM Page 2

ON-LINE ANALYSIS AND MONITORING


The Tytronics® Sentinel is the first on-line analyzer capable of both process chemical
analysis and the monitoring of potable water and wastewater. Offering an unmatched
performance to price ratio, the Tytronics® Sentinel provides measurement qualities and
accuracies simply not seen before. There is built-in reliability, thanks to a simple and
patented sample capture system and wide-bore tubing. This is an analyzer that can
handle difficult and dirty samples.

Whether you are currently analyzing or monitoring liquids, or looking to do so, the
Tytronics® Sentinel is your first choice in on-line analysis or monitoring.

EASE OF OPERATION
Simple menu-driven operation and a modular design make the Tytronics® Sentinel easy
to use and maintain. A person with little chemical background can use the analyzer with
minimal training. Simple step by step instructions are displayed to guide the operator
through the procedure to complete a calibration and to set the unit in the automatic
analysis mode.

THE BEST METHODOLOGY FOR THE APPLICATION


APPLICATIONS:
One of the keys to Tytronics® leadership in on-line analysis is the commitment to provide
the best possible methodology (colorimetry, ISE, colorimetric or potentiometric titrations)
• Acids for the application at hand. Thus, you can be assured that your measurements of acids,
• Alkalinity ammonia, bases, metals, nitrate, phosphate, etc., are done in the very best way.
• Aluminum All parameters in the Tytronics® Sentinel are user programmable. Multiple analysis
• Ammonia methods can be configured to tackle different concentration ranges. Multiple calibration
• Caustic & Carbonate setups can be used to define different low and high range calibration curves. A cleaning
cycle can be programmed to clean out or dissolve any buildup on the measurement
• Chlorine
sensor or reaction cell. Analysis, calibration and cleaning cycles can be executed at
• Chrome periodic (user-programmable) intervals to provide hands- free automation of the
• Color analyzer.
• Copper
• Fluoride
• Hardness UNIQUE BATCH SAMPLING CAPTURE TECHNIQUE
• Hardness in Brine
The Tytronics® patented sample capture technique is incorporated into the Tytronics®
• Iron Sentinel. This means of sample capture provides the simplest and most reliable method
• Manganese of capturing a reproducible volume of sample that is available. The sample inlet uses
• Nickel 1/4" tubing, thus minimizing blockages and allowing even high turbidity samples to be
readily handled.
• Nitrate
• Nitrite The sample inlet system uses an internal fast loop ensuring that a fresh and representative
• Peroxide sample is always available for analysis. Sample capture volume can range from 5 to 30
ml. This allows the Tytronics® Sentinel to be used for ppb as well as ppm levels of
• Phosphate measurement.
• Silver
• Sulfide Mixing is accomplished through the use of a magnetic Teflon™ coated stir bar. Two types
of measurement sensors, colorimetric and potentiometric, can be mounted in the reaction
• Zinc cell. Sensor Types:
...and many more... Colorimetric/Potentiometric

Peristaltic pumps are


used to introduce
calibrating and cleaning Sample In To Water To Water
solutions.

Reagents are introduced


through high precision
positive displacement
piston pumps which
require minimum
maintenance. Sample cleans the cell Flow is stopped and sample is Reagents are added directly
captured by siphon to the cell
151909_Galvanic_BRO 3/30/04 10:37 AM Page 3

TYTRONICS® SENTINEL: DESIGNED FOR OPTIMUM


PERFORMANCE
Colorimeter
The colorimetric system uses dual wavelength optical configuration and an autoblank feature
which compensate for background color and turbidity. Colorimetric sensors are used to make
absorbance measurements for direct colorimetric measurements (Beers Law). A submerged
colorimetric probe measures the absorbance of the solution after reaction of sample and
reagents. The probe is cleaned and rinsed between analyses, thus eliminating the problems
of optics fouling. The probe is made of Kynar™ and the reflector of Hastalloy C, which
provides excellent chemical resistance. The probe can be supplied in two different optical
pathlengths, 2 and 4 cm, determined by concentration

CALIBRATION: True multi-featured two point calibration technique allows trace analysis to be
routinely checked by simply using distilled water. Periodic checking of span standard can be
easily performed.

Titrator
Tytronics® Sentinel on-line colorimetric and potentiometric (pH and Redox) Titrations deliver
simple, reliable and highly cost-effective on-line analysis. Acids, Alkalinity, Caustic,
Carbonate, Cyanide, Hardness, Iron, Peroxide, Silver and many other analyses are common
applications across a wide variety of process industries. Tytronics’® Sentinel Titrators have the
capability of performing single or dual end-point titrations. The Titrator is equipped with three
detection methods (fixed, relative and derivative endpoint) to insure flexibility and accuracy.
Expanded diagnostic capabilities include programmable learn cycles to automatically detect
chemistry endpoints. Users may program several methods and the system allows for multiple
reagents to be added. Analyses are fully automatic in all cases. Users can easily change the
frequency of analysis and calibration, as well as most of the default values, to improve or
customize a setup; three different access levels provide system security. The Tytronics® Sentinel
also features a full auto-cleaning capability for reliability and reduced maintenance. In sum,
this results in an extremely reliable, flexible, and user-friendly general purpose Titrator.

CALIBRATION: Automatic calibration is user selectable and configurable with calibration


repeat and alarm limits.

ISE
Potentiometric sensors are used for ion selective measurements. The single known addition
(SKA) technique compensates for electrode drift on every analysis. Tytronics® Sentinel ISE
analyzer is fitted as standard with an RTD-100 temperature sensor which permits automatic
temperature compensation of the analysis. Direct Method is used for high concentration
analysis.

CALIBRATION: Automatic calibration is user-selectable and configurable with calibration repeat


and alarm limits. The calibration is performed using the SKA method on a calibration standard.

SAMPLING OF TYTRONICS® SENTINEL ANALYSIS METHODOLOGIES


Measure Technique Typical Range(s) Remarks
Acids Titration varies Potentiometric titration; various acids
Alkalinity Titration Varies Colorimetric titration for total alkalinity and potentiometric for P and M values.
Aluminum Colorimetric 0 to 100 ppb to 0 to 2 ppm Lower levels measured on potable water.
Ammonia Colorimetric 0 to 100 ppb to 0 to 25 ppm Uses the modified Berthelot method.
Ammonia ISE 0 to 2 ppm to 0 to 100 ppm Direct or using SKA method.
Caustic & Carbonate Titration varies Caustic scrubber
Chlorine Colorimetric 0 to 500 ppb to 0 to 3 ppm Free and/or total available chlorine may be measured.
Color Direct Spectrometry 0 to 10 to 0 to 500 Hazen Hazen or APHA color units.
Copper Colorimetric 0 to 500 ppb to 0 to 10 ppm Lower levels for potable water, higher levels usually on industrial waste streams.
Cyanide Colorimetric 0 to 200 ppb to 0 to 1 ppm Used on purified waste water streams.
Cyanide ISE 0.5 ppm and higher Waste water streams.
Fluoride ISE 0 to 2 ppm and higher Potable water using SKA technique.
Hardness Colorimetric 0 to 1 ppm to Hardness in water or brine
0 to 10 ppm
Hardness Titration 0 to 20 to 0 to 500 ppm Complexometric colorimetric titration.
Iron Colorimetric 0 to 100 ppb to 0 to 2 ppm Potable water.
Manganese Colorimetric 0 to 200 ppb Potable water.
Nitrate ISE 0 to 10 ppm to 0 to 100 ppm Direct or SKA method used.
Nitrate Direct UV Spectrometry 0 to 1000 ppm Consult factroy for suitability.
Nitrite Colorimetric 0 to 1 ppm Potable water derived from deep wells.
Phosphate Colorimetric 0 to 500 ppb to 0 to 3 ppm Used for corrosion prevention in potable, cooling tower and boiler water supplies.
Phosphate Colorimetric 0 to 10 ppm and higher Mainly used on waste water streams.
And many more...
151909_Galvanic_BRO 3/30/04 10:37 AM Page 4

TYTRONICS ®

Galvanic Applied Sciences USA manufactures the complete brand of Tytronics® on-line wet
chemical and gas analyzers. The Tytronics® products include the Sentinel On-line Analyzers.
These analyzers use "state of the art" technology to perform colorimetric, titrimetric, ISE,
and spectrophotometric analyses. These analyzers can be configured to perform many
EPA and ASTM wet chemical methods, as well as many Standard Methods. The Sentinel
analyzers use a modular design that can be configured to meet the specific requirements of
the customer's application.

The Sentinel Analyzers are capable of both process chemical analysis and the monitoring
of potable water and wastewater. This instrument can analyze up to six streams for the same
chemical parameter, at different concentration ranges. The Sentinel can measure the
chemical composition of liquid processes from A (aluminum) to Z (zinc).

FEATURES
MULTI-STREAMING: The instruments can be expanded to analyze up to 6 sample streams per
analyzer. The frequency and order of stream analysis is fully programmable. Each stream has a
separate alarm and analog output with multi-range capability. The ability to optimize the method
used for each sample stream further proves the superiority of the advanced capabilities of the
Tytronics® Sentinel.

SAMPLE STREAM: Flow rate of 50 to 900 ml/min; pressures from 0 to 50 psig; temperature
from 5˚ to 70˚ Celsius and 1/4” sample inlet connection.

OPERATING TEMP: 5˚ to 45˚ Celsius; vortex air cooler recommended above 45˚ Celsius

AUTO CLEANING: An automatic wash pump to do periodic (user-programmable) cleaning


cycles; a suitable wash solution is introduced using the wash P-Pump to clean out or dissolve any
buildup on the electrode or reaction cell.

ANALOG OUTPUTS: 1 output per stream; isolated 0/4 to 20 mA; fully range-programmable;
maximum load 1000 Ohms; result values are held until the reading is updated.

DIGITAL OUPTUTS: Dual-isolated RS-232C for printer and computer interface at user-
selected baud rates, with remote control capability.

DIGITAL INPUTS: 8 digital inputs with fully programmable functions allow interface to a PLC and/or
interface to voltage-free contact from sensors; expandable to 16 inputs with multiplexor board option.

RELAY CONTACTS: Programmable voltage-free contacts (minimum 8 relays configurable to


N.C. or N.O.), expandable to 14 relays with multiplexor board option; contact rated at 5A at
240VAC maximum with a non-inductive load.

ALARMS: Stream-specific High and Low set point alarms; loss of sample flow alarm; fail-safe
power failure alarm; general, hardware and stream-specific fault signals,; result-ready, test-in-
progress, calibration-in-progress and other alarm and interface functions (consult Manual); alarms
can be assigned in software to voltage-free contact relays; grouping of alarms to relays is fully
programmable.

DATA STORAGE: Non-volatile memory saves the last 120 analysis results and last 25
calibration results; data retention is approximately 5 years.
SENTINEL 03 - 04 Printed in Canada
POWER SUPPLY: Universal power supply 100 to 240 VAC, 50-60 Hz; consumption 200 watts
maximum.

ENCLOSURE TYPE: IP65, NEMA 4X, fiberglass wall-mounted industrial enclosure; modular design
of the fluidic and electronic sections results in easy maintenance and simple field retrofits or upgrades.

DIMENSIONS: (W x H x D) 24” x 25” x 13” or 61cm x 64cm x 33cm

WEIGHT: Approximately 80lb (36kg) fully equipped.

Galvanic Applied Sciences USA Inc. Galvanic Applied Sciences Inc. Calgary, Alberta Edmonton, Alberta
41 Wellman Street Bay 6, 6325-12 Street S.E. 1200, 715-5th Avenue S.W. Telephone: 780-430-0142
Lowell, MA. 01851 Calgary, Alberta T2H 2K1 Calgary, Alberta T2P 2X6 Fax: 780-430-0172
Telephone: 978-848-2701 Telephone: 403-252-8470 Telephone: 403-252-8470 Houston, Texas
Fax: 978-848-2713 Fax: 403-255-6287 Fax: 403-571-2684 Telephone: 281-477-9002
Fax: 281-477-9004
Toll Free 1-800-370-2345 (US only)

W W W. G A LVA N I C . C O M • E - M A I L : I N F O @ G A LVA N I C . C O M
Model BRM 941-LS
Liquid Sulphur Analyzer System  
Analyzer H2S and H2Sx in Liquid Sulphur
Residual H2S in Claus‐produced sulphur contains both H2S and H2Sx, which exist in   
equilibrium with elemental sulfur (S8).  
 
• Analyses can be conducted in 2 minutes                                                                     
     (wet chemical method requires several hours) 
• Analyses independent of operator skill  
 
The use of state ‐of‐ the‐ art Fourier transform  infrared spectrometers allows the 
resolution of the H2S and H2Sx   absorptions giving accurate (± 10% of the measure‐
ment value) determinations of total H2S in the 0‐350 ppmw range with quantification 
down to 2 ppmw.  
 

Key Component

FTIR Analyzer                                
Calibrated heated cell                  
Sulphur sampling device (hot pot)  
Proprietary software package  

Can be used for:


• Verification that run‐down pit liquid sulphur meets specification  
• Verification that degassing process is producing on spec product 
• Monitoring and control of degassing process                                               
(energy consumption management)  
• Providing documented Quality Assurance for marketing of liquid sulfur 
product  
• Allowing assessment of safety issues in the handling of the liquid sulphur  
• Monitoring of performance of catalytic convertors in Claus train.              
(high  H2S residual may indicate low catalyst activity.)  
• Determination of H2S content in front end furnace condenser stream  
Analysis time: 2 minutes
Accuracy: ± 10% of total residual H2S
Calibration : H2Sx = 150 ppmw
Limits: H2S = 200 ppmw
Total = 350 ppmw
Head office: 7000 Fisher Road S.E. Calgary, Alberta Canada T2H 0W3 Tel: 403.252.8470 Fax: 403.255.06287                                                             
Galvanic Applied Sciences USA  Inc. 41 Wellman Street, Lowell MA 01851 Tel: 978.848.2701 Fax:978.848.2713                                                       
Houston Office  13211K Windfern Road, Houston Texas, 77064 USA Tel: 281.477.9002 Fax: 281.477.9004  

info@galvanic.com  • www.galvanic.com  

WWW.GALVANIC.COM 
PLGC II
GAS CHROMATOGRAPH

GAS COMPOSITION INCLUDING


BTU/HEATING VALUE CALCULATION
SPECIFIC GRAVITY CALCULATION

WWW.GALVANIC.COM
PLGC II GAS CHROMATOGRAPH FOR
PIPELINE AND PROCESS APPLICATIONS
2 3
5 The PLGC II is a compact and low cost gas chromatograph equipped with a universal
1 thermal conductivity detector. The unit offers a wide range of applications where
4
hydrocarbon gas or fixed gas analysis is required, such as in BTU measurement for the
natural gas industry.

6 Remember when field chromatography was considered too complex or expensive for
many applications. The PLGC II removes these drawbacks. The Galvanic Applied
7 Sciences PLGC II analyzer is a low cost, low maintenance chromatograph. The PLGC II
8 can be used in many measurement applications where an isothermal TCD scheme is
suitable. The PLGC II is fully automated and designed to perform on-line, real time
6 analysis. The Windows® based configuration program allows the user to view most
recent or saved chromatograms as well as configure the analyzer.

The PLGC II calculates the following for up to 8 streams:

• Heating value • Compressibility


9
• Specific gravity • Specific heat ratios
10 • Wobbe index • Component concentrations

Features:

• 24 Volt DC operation • No instrument air required


• Division II electrical classification • Low helium consumption
1 The TCD measures the concentration of the standard (Div I optional) • Reliability
components of the sample gas based on
• Thermistor TCD detector • Low maintenance
changes in the thermal conductivity of the
components.

The Excitation Board provides power for


DETECTOR
2
the thermal conductivity detector. The Detector is a thermistor type TCD selected for high sensitivity at ambient
temperatures and short response time. It consists of a heated filament contained in a
3 The individual components are separated in stainless steel block. Gas flowing through the block loses heat to the block depending
the column by process of absorption and on the concentration and the thermal conductivity of the gas.
diffusion. Up to two columns are supported.
The detector is a temperature controlled enclosure to minimize the effect of ambient
4 The micro volume diaphram valve is temperature changes. To further reduce temperature and flow effects, a reference
actuated by carrier gas to perform the filament is used in a wheatstone bridge configuration.
sample injection.

5 Customer Connections for Helium carrier TCD Detection 8 Milliamp Constant Current
4

gas, Calibration gas and Sample gas. Analyzer Detector


ED

R
ED
R

Filament Support 525 T T


N
R

B
G

Solenoids electromechanically switch the


LU

6 A-A Mount
5 6

flow of gas to inject sample gas into the 2 3 Output to Pre-amp

system. 500 Ohm 500 Ohm


FILAMENT SUPPORT 525 1

7 The computations, setup and


communications for the PLGC II are
performed by the Motherboard. THE PLGC II LCD
8 The LCD display is capable of displaying Displays a choice of:
all information about the sample or status
of the PLGC II. • Heating valve/specific gravity • Temperature control
• Component values • Output alarms
9 Optional AC Power Adapter
• Chromatograms • Status
10 Optional Extended box to allow such
options as: AC Power and multiple
streams.
Sample

SAMPLE INJECTION VALVE Vent

1
10
The chromatograph is composed of 2
9
a 10-port micro volume diaphragm PLGC II Sample Handling Equipment 3
valve and generally 2 columns 8 Carrier
4
(some applications may only col 1
require one). The DV22 performs 7
6
5

the injection and the backflush. It is


specifically designed for heavy-duty
applications and is rated at Detector
col 2
1,000,000 injections before
requiring service. In two column Valve On
systems, column 1 passes all
components except C6+, trapping Sample
C6+ for a quick backflush out. Notes: Vent
Column 2 separates the remaining 1 - Sample loop volume =.025 cu cm 1
components. Total analysis time is 10 2

about 15 minutes and is run iso- 9


3
thermally at 40°C. The temperature 8 Carrier
4
of the chromatography enclosure is col 1
controlled to minimize retention 7
6
5

time shifts due to ambient


temperature changes.
col 2
Detector

PLGC II SOFTWARE Valve Off

The PLGC II software has been designed to receive, interpret, and plot data from the
PLGC II gas chromatograph. Peaks in the resulting chromatogram identify the
compounds by retention time and the concentration by the area of the peak. Various
parameters, including heating value, specific gravity, and compressibility factor, can be
displayed with the software. The Graphical User Interface (GUI) for the software is a
user friendly Windows® based system.

Computer Requirements:

Operating System:
DIMAC Gas Chromatogram
®
An IBM compatible PC with “Windows 98,
NT or ME” operating system will be required.

Memory:
The PC must have a minimum of 64 MB of
RAM and Windows®98.

Disk Drives:
The PLGC II configuration program is
provided on CD Rom, and requires at least
20MB on the disk drive. Extra space will be
required to save data.

Serial Port:
To run the PLGC II configuration program a
serial cable is required to connect the
personal computer to the PLGC II. Most
computers will have multiple COM ports to
select from. The COM port selected cannot
be shared with any other device.
SPECIFICATIONS

DIMENSIONS Range: Analog:


0-2000 ppm to 100% Four isolated 4-20 mA (user selectable)
for individual components
PLGC II - DIVISION II Serial:
(Optional Cabinet - 28”x28”x15) Components: Two RS-232,
16 maximum One RS-485 modbus

25” Streams: Data logging:


8 plus calibration 128 days hourly averages
12 months daily averages
Response: 1 year monthly averages
9” 15 minutes to C6+ (5 minutes optional), Last 64 calibrations
16” 2 minutes nominal for single components 2 user configurations
12” depending on background composition 1 factory configuration
Linearity: Input A/D:
25” 1% for individual components
Three channels 24 bit sigma delta
17”
Repeatability:
Real time clock:
0.5 BTU/1000 0.05%
Time and date stamp,
1 ms resolution
Temperature Ambient:
10 to 40° C
Sampling Rate:
60 HZ
Humidity:
0-95% non-condensing Chromatograph Valve:
Maximum eight
PLGC II - DIVISION I Electrical:
(Optional Cabinet - 30”x36”x15) 24 volts DC @ 50 watts Columns:
Class 1 Div 2 Grp B, C, D One to four 1/16” stainless steel
Temp code T3 (application dependent)
10”
27” Inputs: Dimensions:
6 dry contact 2-24 VAC 14” H X 12” W X 8” D

Outputs: Weight:
240 x 64 backlit LCD 35 pounds

33” Relays: Utilities:


Four user selectable for alarm or fault UHP helium @ 10 cc/min @ 60 PSI
(SPDT, 5 amps, 250 VAC)
Sample:
10 to100 PSI clean,
Dry gas @ 95 cc/min

MODIFIED SPECIFICATIONS FOR THE PLGC II EXPLOSION PROOF

Electrical: Weight:
120/240 VAC @ 50 watts 50 pounds
PLGC II 10 - 03 Printed in Canada

Class 1 Div 1 Grp C,D


Temp Code T3

Dimensions:
29” H X 13” W X 9” D

Cabinet may vary in size according to the number of streaming of values.

Galvanic Applied Sciences Inc. Calgary, Alberta Edmonton, Alberta Houston, Texas
Bay 6, 6325-12 Street S.E. 1200, 715-5th Avenue S.W. Telephone: 780-430-0142 Telephone: 281-477-9002
Calgary, Alberta T2H 2K1 Calgary, Alberta T2P 2X6 Fax: 780-430-0172 Fax: 281-477-9004
Telephone: 403-252-8470 Telephone: 403-252-8470
ISO 9001: 2000 Fax: 403-255-6287 Fax: 403-571-2684
Registered QMS
Toll Free 1-866-252-8470 (US & Canada only)

W W W. G A LVA N I C . C O M • E - M A I L : I N F O @ G A LVA N I C . C O M

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