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Quality Certificate

VWR* CONDUCTIVITY CALIBRATION STANDARD


This document certifies that the below product meets the following criteria:

North American Catalog N°: 62344-938


Lot Number: CC10630
Description: VWR CONDUCTIVITY STANDRD 100ML
Expiration Date: May 4, 2013
Certified Value: 1,412 µS/cm U = ±3.6µS/ cm (k=2) at 25⁰C
Derived Values: 1412 micromho / cm, 708 ohm-cm, 941 PPM D.S.

Certification measurements are preformed under ISO Guide 34, A2LA accreditation no. 1750.02 and are
traceable to recognized national and international standards via an unbroken chain of comparisons.
Electrical conductance is the reciprocal of electrical impendance. The International Systems of Units (SI),
derived unit of conductance, is Siemens (S), also referred to as (mhos) the reciprocal of ohms. The certified
value is expressed in microsiemens per centimeter (µS/cm).

MEASUREMENT: Ten (10) 100 ml samples were measured from this lot. The conductivity of each sample
was derived from a measurement of the impendance of the solution using a conductivity meter and
calibrated cell. The cell and sample were temperature controlled by submersion in a water bath at
25ºC±0.015ºC.

UNCERTAINTY: The certified value is given as the average of the measured samples. The reported
expanded uncertainty (U) is determined from the uncertainty of the measurement variation from sample to
sample, change due to shelf life, and from the uncertainty of the measurement process. The value of
uncertainty is multiplied by k=2, which for a normal distribution corresponds to a coverage probability of
approximately 95%. Uncertainty is calculated in accordance with the ISO “Guide to the Expression of
Uncertainty in Measurement” (GUM).

METHOD: The certified reference material is prepared and analyzed by the manufacturer.The certified
reference material consists of a mixture of a dilute solution of less than 0.1% (by mass) potassium chloride
(KCL), of less than 1% (by mass) propanol, and of less than 99.5% (by mass) deionized water in
equilibrium with atmospheric carbon dioxide. Mixing was performed by circulation utilizing a propriety
method.

Traceability: Standards and Equipment Used

Decription Serial Number Due Date Traceable Reference

Conductivity Standard 1000.0 uS 11090801PTJ, #4 9/09/12 C RM 1111

Conductivity probe (4W)/Meter 876-11-003 10/09/12 TC25-4284301

Digital Thermometer 111879346 3/28/13 4000-4265850

Temperature Calibration bath TC- 191 A42238

Laboratory Enviromant conditions: 24.0 ºC 38%RH 1,013mb/hPa

VWR International LLC, Radnor Corporate Center, Building One, Suite 200, 100 Matsonford Road Radnor, PA 19087
VWR International bvba/sprl, Haasrode Research Park Zone 2020, Geldenaaksebaan 464, 3001 Leuven, Belgium
http://www.vwr.com
Quality Certificate

VWR* CONDUCTIVITY CALIBRATION STANDARD

TM
PACKAGING: This material is available in both a 460 ml bottle and a 100 ml One-Shot .

INTENDED USE: The certified reference material is intended for the calibration of conductivity cell
constants, for conductivity measurement, for the validation of analytical methods, and for the preparation of
working reference standards

INSTRUCTIONS FOR USE: The certified reference material should be open for the minimum time.Rinse
the cell in a small amount of the certified reference material and discard. The recommended sample size
for measurement is 100 ml. Discard the standard after use and under the following circumstances: if the
expiration date is past due, four months after opening,or if any color, turbidity, or visible microbiological
growth become evident. Standards which have been opened are not protected from growth. Do not
returned used solution to this standard closed. Keep the standard stored at a stable temperature. Select
standard as near as possible to that of the unknown solution to be measured. Do not standardize at 10,000
uS and then measure unknown at 100 uS. Reference any accompanying instructions with this product.

Temperature has a significant effect on conductivity. For measurements at a temperature other than 25°C,
refer to the temperature correction table provided. The product should be used as near as possible to 25°C.

HOMOGENEITY:Ten (10) 100 ml samples were selected for analytical control. Results from different
samples showed no statistically significant differences, nor was there any correlation between values
TM TM
obtained and the bottling sequence. Bottle-to-bottle (One-Shot to One-Shot ) variations of the samples
measured are included as a part of the calculated measurement uncertainty stated on page 1 of this
certificate. A minimum sample size of 100 ml should be used to maintain the certified value and the
associated statement of uncertainty. This standard as formulated is considered infinitely soluble

STABILITY, SHELF LIFE: The expiration date stated on page 1 indicates the period of time which the
certified reference material in a properly packaged, unopened, unused, and stored under environmentally
controlled and monitored conditions remains within the specified uncertainty range.

EXPIRATION DATE: The date after which a certified reference material should be discarded.

STORAGE: Store below 40°C and above 0°C.

SHIPPING: Ship below 50°C and above 0°C.

MSDS INFORMATION: Please refer to the Material Safety Data sheet for information regarding this
certified reference material .

VWR International LLC, Radnor Corporate Center, Building One, Suite 200, 100 Matsonford Road Radnor, PA 19087
VWR International bvba/sprl, Haasrode Research Park Zone 2020, Geldenaaksebaan 464, 3001 Leuven, Belgium
http://www.vwr.com
Quality Certificate

VWR* CONDUCTIVITY CALIBRATION STANDARD

QUALITY STANDARD DOCUMENTATION:

ISO/IEC Guide 34:2000 General Requirements for the Competence of reference Material Producers,
accredited A2LA Certificate Number 1750.02.

ISO Guide 31:2000 Reference Materials - Contents of Certificates and Labels.

ISO Guide 35:2006 Certification of Reference Materials - General and Statistical Principals.

ISO/IEC 17025:2005 General Requirements for the Competence of Testing and Calibration
Laboratories, accredited A2LA Certificate Number 1750.01.

ANSI/NCSL Z540-1:1994 Calibration Laboratories and Measuring and Test Equipment-General


Requirements.

ISO 9001:2008 Quality Management System Registration - DNV


Certificate Number CERT-01805-2006-AQ-HOU-ANAB
SUPPORTED METHODS: This certified reference material meets test requirements for Federal, State,
and local agencies, CAP, CLSI, ACS, and CLIA. Traceable® Certified Reference Material complies with
and is essential for use in these official methods: AOAC 973.40, EPA 120.1, Standard Method 2510
(APHA,AWWA,WEF),ISO 7888,DIN 38404, ASTMD 1125 USGS 1-1780, USP 645, OIML R56, IUPAC,
and for A2LA/NVLAP accreditations /ISO 9000 certifications. Material may be used to calibrate all
conductivity meters and to determine all conductivity cell constants.

Temperature Correction Information: 1.956 %


If your conductivity meter allows you to set a temperature coefficient (temperature correction) then the
underlined number shown above is the best approximation for this specific analysis for this specific
Traceable® Certified Reference Material. For more precise measurements use the chart. Use the chart
below only if you are making absolute measurements. That is, measurements without any automatic
temperature correction (temperature coefficient set to 0). The chart below displays derived values.
Using a thermometer, measure the temperature of this certified reference material. Shown on the chart is
temperature(in the far left column)in whole degrees. Shown across the top row is temperature in tenths of a
degree.Locate the measured temperature in whole numbers on the far left column, and then follow across
the row to the temperature in tenths of a degree. At the intersection is the certified reference material value
at that specific temperature. Standardize your meter using that value. Example: Measured temperature is
25.0°C.Find 25°C in the far left column, find the row 0.0°C. Where 25°C and 0.0°C intersect, read the value
in microsiemens/cm.

VWR International LLC, Radnor Corporate Center, Building One, Suite 200, 100 Matsonford Road Radnor, PA 19087
VWR International bvba/sprl, Haasrode Research Park Zone 2020, Geldenaaksebaan 464, 3001 Leuven, Belgium
http://www.vwr.com
Quality Certificate

VWR* CONDUCTIVITY CALIBRATION STANDARD


Temperature Correction Chart in microsiemens/cm

0.0°C 0.1°C 0.2°C 0.3°C 0.4°C 0.5°C 0.6°C 0.7°C 0.6°C 0.9°C
15°C 1139 1142 1144 1147 1150 1152 1155 1158 1160 1163
16°C 1166 1168 1171 1174 1176 1179 1182 1185 1187 1190
17°C 1193 1195 1198 1201 1204 1206 1209 1212 1214 1217
18°C 1220 1222 1225 1228 1231 1233 1236 1239 1241 1244
19°C 1247 1250 1252 1255 1258 1261 1263 1266 1269 1271
20°C 1274 1277 1280 1282 1285 1288 1291 1293 1296 1299
21°C 1302 1304 1307 1310 1313 1315 1318 1321 1324 1326
22°C 1329 1332 1335 1337 1340 1343 1346 1348 1351 1354
23°C 1357 1359 1362 1365 1368 1370 1373 1376 1379 1382
24°C 1384 1387 1390 1393 1395 1398 1401 1404 1407 1409
25°C 1412 1415 1418 1420 1423 1426 1429 1432 1343 1437
26°C 1440 1443 1446 1448 1451 1454 1457 1460 1460 1465
27°C 1468 1471 1474 1476 1479 1482 1485 1488 1490 1493
280C 1496 1499 1502 1504 1507 1510 1513 1516 1519 1521
290C 1524 1527 1530 1533 1536 1538 1541 1544 1547 1550
30°C 1552 1555 1558 1561 1564 1567 1570 1572 1575 1578
31°C 1581 1584 1587 1589 1592 1595 1598 1601 1604 1606
32°C 1609 1612 1615 1618 1621 1624 1626 1629 1632 1635
33°C 1638 1641 1644 1647 1649 1652 1655 1658 1661 1664
34°C 1667 1669 1672 1675 1678 1681 1684 1687 1690 1693
35°C 1695 1698 1701 1704 1707 1710 1713 1716 1718 1721

Signed:

Ken Crossley
Manager
Quality Assurance Date: May 4, 2012

VWR International LLC, Radnor Corporate Center, Building One, Suite 200, 100 Matsonford Road Radnor, PA 19087
VWR International bvba/sprl, Haasrode Research Park Zone 2020, Geldenaaksebaan 464, 3001 Leuven, Belgium
http://www.vwr.com

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