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( maxÿ min)/2; the mean stress, m, is ( max+ min)/2; sided test samples were cut to dimensions of 200 mm
and t and c are the monotonic tensile and compressive long by 20 mm or 40 mm wide on a water-cooled cir-
strengths, respectively. From previous observations on cular saw with a diamond wheel. The 20 mm wide sam-
these carbon-®bre composites, it appeared that f may be ples were used for establishing the fatigue behaviour of
a function of the laminate tensile strength. The expo- the undamaged material, as in previous studies carried
nents u and v separately characterise the shapes of the out by this group, while the 40 mm wide samples were
right (predominantly tensile) and left (predominantly used for impact and post-impact fatigue tests. The cut
compressive) wings of a bell-shaped curve represented edges of the samples were lightly polished and, after
by eqn (1), and allow for dierent degrees of asymmetry abrasion of the end surfaces, end tabs of 1.5 mm thick
in the curve: f, u and v have all been found to be linear soft aluminium were glued on with Ciba Geigy Redux
functions of log Nf. The use of eqn (1) to analyse stress/ 403 epoxy-resin paste. The adhesive was cured in a dry
life data allows interpolation and a limited amount of oven at 40 C for 24 h. The central gauge sections of the
extrapolation for the prediction, from only a modest test samples were 100 mm long. Direct measurements of
data base if necessary, of median fatigue lives repre- the ®bre volume fraction gave a mean value of 0.53 (cf.
sentative of conditions (stress range and stress ratio, R, the value of 0.6 that would have been expected from the
de®ned as min/ max) for which experimental data may `notional' resin content of the prepreg). A similar value
not yet be available. Harris et al. show,5 for example, (0.54) was also obtained for the comparator material,
that conservative prediction of a failure envelope HTA/913, although only the notional value of 0.6 was
covering a wide range of R values could be made for a reported in our previous papers relating to this and
`new' CFRP material when the only data available for other carbon-®bre-reinforced plastics.
that material were the tensile and compression strengths
and a stress/life curve for R=+0.1 de®ned by only ®ve 2.2 Testing procedures
or six data points, provided some experience of other The measurements of monotonic tensile properties on
CFRP materials was available. the 20 mm wide samples were carried out in a universal
In this paper we discuss the interaction between the Instron model 1195 machine at a crosshead speed of
fatigue response of a composite and a prior state of 2 mm minÿ1. Compression tests on virgin samples and
damage caused by low-velocity impact, and we study post-impact compression tests were carried out in a
the applicability of the constant-life model for predict- 100 kN servohydraulic Instron model 1342 testing
ing the lives of damaged laminates. We again start with machine at a ®xed loading rate of 20 kN minÿ1, anti-
a `clean slate' by working with a material for which we buckling ®xtures of the kind described by Curtis9 being
have not previously reported fatigue results, another used to support the coupons during compression load-
CFRP composite of [(45,02)2]S lay-up, in the virgin ing so as to prevent macrobuckling. The monotonic
and damaged states. tensile tests on 40 mm wide samples were carried out
under load control in a 200 kN servohydraulic Mayes
test machine model DH 200, again at a rate of
2 MATERIALS AND TESTING PROCEDURES 20 kN minÿ1.
Fatigue tests were carried out in 100 kN servohy-
2.1 Experimental material draulic Instron series 1300 machines under load control.
The material used in this paper is the carbon-®bre Post-impact fatigue tests at a stress ratio, R, of +0.1
composite HTA/982A manufactured by ICI Fiberite. were carried out, also under load control, in the 200 kN
It consists of the high-strength, standard-modulus, Mayes machine, and antibuckling ®xtures were again
continuous Tenax HTA 12k carbon ®bre in Fiberite used for compression±compression or tension±com-
982A, a modi®ed epoxy resin with good hot±wet char- pression fatigue tests. All fatigue tests were run at fre-
acteristics and a cure temperature of 120 C, coded quencies between 2.5 and 8 Hz with constant-amplitude
Fiberite HyE 3982AH. This material, which was sup- sine-wave loading, under ambient laboratory condi-
plied by Fiberite (Europe) in zero-bleed prepreg form, is tions.
thus a representative of the older-established variety of Impact damage was introduced into the test samples
carbon-®bre composites, similar in many respects to the by means of a purpose-built, falling-weight test instru-
more familiar T300 composites, and it aords a direct ment with a 12.7 mm diameter hemispherical tup, based
comparison with the Ciba-Geigy HTA/913 material that on BS 2782 part 3 method 353A. The mass of the
we have studied previously. impacter was 0.248 kg for 1 J and 2 J impacts, the
The main 16-ply lay-up sequence of [(45,02)2]S was impact energy being varied by changing the drop height.
selected to represent a structure of importance to the Impact events at 3 J and 5 J were made from a constant
aerospace industry. All of the composites were laid up height of 1 m by changing the mass of the impacter.
by hand and hot-pressed, following the manufacturer's During the impact event the specimen was clamped
recommendations (90 min at 120 C and 630 kPa) as between two steel rings of internal diameter 30 mm and
300 mm by 450 mm plates. After curing, the hot-pressed the impact head was captured on rebound after impact
laminates had a nominal thickness of 2 mm. Straight- to prevent secondary strikes.
A constant-life model of fatigue behaviour for carbon-®bre composites 11
Fig. 2. Ultrasonic C-scans of [(45,02)2]S HTA/982A samples impacted at two dierent energy levels. Scan area is 40 mm40 mm.
slightly steeper and hence the fatigue resistance of the that although the intrinsic compression strength of the
older material is marginally poorer than that of the laminate has been materially diminished by the small
HTA/982A composite. amount of prior damage, the relative sensitivity to sub-
Comparable fatigue data for the HTA/982A material sequent fatigue is less at these two stress ratios than in
with prior damage from a 1 J low-velocity impact are the virgin material. By contrast, during cycling in the
shown in Fig. 4, together with the curves ®tted to the mainly tensile ÿ0.3 reÂgime, the /log Nf curve is slightly
data for the virgin material from Fig. 3. It appears that steeper than that for the undamaged material, suggest-
a 1 J impact has had no eect on the tensile fatigue ing increased sensitivity to fatigue.
behaviour at R=+0.1, presumably because the tensile One possible explanation for the marked reductions
strength is itself unaected by this level of damage. At in the slopes of the /log Nf curves for high-compression
R=ÿ1.5 and +10, on the other hand, the /log Nf R values may be found in the results of a series of
curves are markedly aected. It can be seen that the experiments to determine the residual strength after
slopes have been considerably reduced, roughly in the cycling of the damaged laminate. It is a common feature
same proportion as the compression strength itself has of the fatigue behaviour of ®bre composites that the
fallen, and the relatively straight lines through the fail- residual strength of the material falls as a consequence
ure points are now very ¯at, almost horizontal. At of cycling. Examples may be found in12,13, among many
R=ÿ0.3, however, which is a tension±compression others. It is this behaviour which forms the basis of the
mode in which the compression component of stress is familiar `wear-out' model of fatigue failure. By contrast,
low, the /log Nf curve has also shifted downward but the eect of the impact damage in the HTA/982A in
to a less marked extent than those for R=ÿ1.5 and impairing the load-bearing ability of the laminate
R=+10. The ¯atness of these last two curves suggests appears to be reduced when the damage laminate is
cycled in repeated compression, as illustrated in Fig. 5. is defended in5] and plotted as shown in Fig. 6. The
The 5% or so increase in the compression strength after distribution for the undamaged material is similar to
106 cycles is well-de®ned and could reasonably explain those of other CFRP laminates described in5, but the
why the /log Nf curve for R=+10 is very ¯at and why eect of the prior impact damage is to change the
many of the individual fatigue experiments become run- shapes of both tails of the distribution. As the inset in
outs. Fig. 6 shows, the central parts of the two distributions
overlap substantially, but there are both more longer-
life failures and more shorter-life failures when the
4 DISCUSSION material has prior damage, re¯ecting the very ¯at /
log Nf curves for tests at high-compression R values.
4.1 Pooling of fatigue data The Weibull parameters for these curves were obtained,
In earlier papers,2,5 following the lead of Whitney,14 we as described in5, by a Levenberg±Marquardt non-linear
used the method of normalising and pooling fatigue least-squares routine in the Microcal Origin software,
data as a step towards more reliable life prediction. This and the characteristics of the HTA/982A laminate in the
procedure makes use of the assumption that the fatigue damaged and undamaged state can be compared in
lives follow a type III asymptote (Weibull) distribution Table 2 with those of the other CFRP laminates that we
and that the shape parameter of the distribution for the have studied. The standard errors of these ®ts were all
pooled data is the same as that for a subset of data for of the order of 0.002. The values of the location para-
any replicate group of constant-stress fatigue tests. meter, , are all close to zero, as would be expected
Design allowables for smaller subsets can therefore be since the distributions are necessarily bounded at zero,
predicted with greater con®dence because the value of and the scale parameter values, , are all approximately
the shape parameter, , is ®xed by the characteristics of unity, as expected for a normalised distribution. The value
the larger population. Much of this earlier work is in of the shape parameter, , for the HTA/982A laminate
agreement that the value of for such a pooled dis- is again within the range of values previously obtained,
tribution will be of the order of unity, but suciently and the average value for all of our undamaged
greater than unity to ensure that the distribution has not
degenerated to an exponential function with no mini- Table 2. Distribution parameters for pooled fatigue lives for
mum life. several CFRP laminates
The analysis is carried out by normalising each repli- Laminate Number of values
cate data set with respect to the median life, m(Nf), at
T800/5245 164 0.09 1.24 1.25
the operative fatigue stress and then pooling all nor- T800/924 90 0.03 0.94 1.49
malised data, for all stresses and all R values. The IM7/977 93 0.05 1.23 1.41
pooled data are then ranked [we use the mean-rank HTA/913 88 0.10 1.17 1.71
method, which gives the plotting position as i/(N+1), HTA/982A (virgin) 113 0.20 1.11 1.10
where i is rank number and N is the number of obser- HTA/982A 63 0.17 1.30 0.74
(damaged)
vations in the sample: our choice of this ranking method
14 M. H. Beheshty, B. Harris
Fig. 7. Constant-life plots for HTA/982A [(45,02)2]S laminate in the undamaged condition. The curves are obtained by freely
®tting all three parameters.
laminates is 1.39, with a coecient of variation of about the data points by Microcal Origin software. Note that
17%. The consistency of this parameter, and its simi- the choice of lives for this purpose must depend on the
larity to the value obtained by Whitney14 in his analysis spread of data. In our previous papers we used only 104,
of a quite dierent CFRP, suggests that median- or 105 and 106 cycles, but better predictions can be
extreme-value life predictions based on such an average obtained, provided there is a suciently wide spread of
value could be made quite con®dently from relatively lives at dierent R values, if the shortest life chosen is
small fatigue data bases. somewhat nearer to the left-hand axis of the /log Nf
The prior damage, though, appears to have the eect curve than 104 cycles. A constant-life plot showing the
of placing this approach in jeopardy, since the ¯attening (m,a) data pairs for the four stress ratios studied at the
of the /log Nf curves for R=ÿ1.5 and +10, in raising four lives referred to above, together with the extreme
the left-hand tail of the distribution and lowering its data pairs representing the monotonic tensile and com-
right-hand tail, results in a much lower value of the pression strengths, is shown in Fig. 7. The curves were
Weibull shape parameter. The value of =0.74 shown ®tted through the data sets by means of the non-linear
in Table 2 indicates a distribution with no minimum life, least-squares routine referred to earlier, and the values
such as the exponential distribution, for which =1. of the parameters f, u and v returned by the program,
Clearly, the analytical techniques that we are using are together with the associated standard errors for the
insuciently sensitive, when the slope of the /log Nf ®t, are shown in Fig. 8. It can be seen that all three
curve is very ¯at, to distinguish between a peaked dis- parameters decrease with increasing life, u and f at
tribution and a smoothly falling distribution. We could approximately the same rates, while v is much less
improve the situation somewhat by ignoring the very strongly dependent on log Nf. The relationships repre-
long normalised lives for the damaged material. These sented in the ®gure are:
are up to ®ve times greater than the longest values in the
distributions of the undamaged materials, and they can f 192 ÿ 018 log Nf
be ignored since, for extreme-value or median-life pre- u 261 ÿ 012 log Nf
2
dictions, it is only necessary to ensure a good ®t to the v 242 ÿ 004 log Nf
left-hand tail of the distribution, as pointed out by
Castillo.15 But even censoring of the longer-life data is
unlikely to raise the value of beyond unity.
Table 3. Slopes of the lines u,v=A+B log Nf for ®ve [(45,02)2]S CFRP laminates
Material Exponent Slope B Exponent Slope B
T800/5245 u 0.327 v 0.365
T800/924 u 0.398 v 0.396
IM7/977 u 0.333 v 0.256
HTA/982A u 0.280 v 0.400
Mean of above four (cv) u 0.335 (15%) v 0.354 (19%)
In previous papers we have noted that an average value ted, and there are also small dierences between the
of f could be used as a ®xed parameter for further curve values of the two exponents for a particular laminate,
®tting to obtain new relationships for the life depen- re¯ecting the asymmetries of the constant-life curves,
dence of u and v without signi®cantly reducing the the results are more notable for their similarities than
goodness of ®t, and from the results for dierent lami- for their dierences. There is, in fact, a remarkable
nates it appeared that the value of f was in fact related degree of uniformity of behaviour between these four
to the laminate tensile strength*, t. If the constant-life materialsÐnote the relatively small coecients of var-
curves for 104, 105 and 106 cycles in Fig. 7 are treated in iation within the group of four, particularly gratifying
the same way, then the correlation is extended to since the fatigue response of the new HTA/982A lami-
include HTA/982A, as shown in Fig. 9. Although this nate has been characterised here only at four R values,
linear plot is given by the relationship: rather than the ®ve used for all of the other materials. It
is all the more obvious, then, that the behaviour of the
f 242t ÿ 206
3 HTA/913 laminate is dierent. But our previous con-
clusion must also now be changed, since the distin-
with a correlation coecient of 0.977, it seems likely guishing feature of the laminate must be the resin rather
that a more realistic function for prediction purposes than the ®bre, as we had previously concluded, since the
may be a parabolic relationship, passing through the homogeneous group now includes both intermediate-
origin, of the form: modulus and high-strength ®bres, but only modern
modi®ed resins.
f 054t26
4
4.3 Life prediction for the undamaged laminate
When the value of f is ®xed and the curves of the type The next stage of the constant-life analysis is to use the
shown in Fig. 7 are re®tted to ®nd new values of u and information contained in Fig. 8 [or the equivalent
v, these exponents are found to be increasing linear
functions of log Nf instead of the decreasing functions
shown in Fig. 8, and the slopes of these lines were
shown in5 to be linked in a qualitative manner to the
nature of the composite. For the four laminates dis-
cussed in that paper, the slopes of the lines of u versus
log Nf and v versus log Nf were all similar for the three
composites that were reinforced with the intermediate-
modulus T800 and IM7 ®bres, whereas they were
markedly higher for the composite with the high-
strength HTA ®bres. When the latest results for the
HTA/982A composite are considered in the same con-
text, there is an interesting new feature which is shown
in Table 3.
We note that although there are small dierences in
the values of u and v among the ®rst four materials lis-
Fig. 11. Constant-life plots for HTA/982A [(45,02)2]S laminate following prior damage by a 1 J impact. The curve for 106 cycles
has been arti®cially forced to remain close to the other two curves above R=0.1.
A constant-life model of fatigue behaviour for carbon-®bre composites 17
Fig. 12. Constant-life curves for HTA/982A [(45,02)2]S laminate in the virgin condition and after prior impact with a low-velocity
impact of 1 J. The two sets of curves lie in the same sequence as that indicated on the graph. The curve ®ts have been made by ®xing
an average value of f for the three lives indicted.
maxima in the constant-life curves are also shifted to the response of an undamaged laminate (the f, u and v
right. The values of the ®tting parameters, f, u and v for parameters), together with the results of measurements
the damaged composite are shown, together with those of the compression strength after impact (CAI), could
for the virgin material, in Fig. 13. The values of the not be used to predict the fatigue response of that
three parameters are much closer together in the damaged laminate without the need for further fatigue
damaged material, re¯ecting the changes in shape of the data. Attempts to ®t constant-life curves to the data
constant-life curves, and all three lines showing the life points for the damaged laminate shown in Fig. 11 by
dependence of the parameters fall close together within ®xing the value of the f parameter at 0.87, as indicated
a space more or less bounded by the lines for f and u for by the relationship in Fig. 9, is simply not feasible. This
the undamaged laminate. An unexpected aspect of these suggests that other relationships between material
results, however, is the fact that the f values for the properties and the constant-life model parameters
damaged laminate are much higher than those for the should be sought.
virgin material, and do not ®t the pattern of relationship
with the laminate tensile strength that has so far covered
the behaviour of all CFRP [(45,02)2]S laminates tested 5 CONCLUSIONS
to date in the course of this work. An important con-
sequence of this is that, although the constant-life model 1. In this paper we describe preliminary attempts to
appears to work just as well with damaged as with predict the fatigue life of an impact-damaged
undamaged material, a simple knowledge of the fatigue CFRP laminate by the use of a constant-life model
that has been developed over a number of years
for a wide range of virgin CFRP composites.
2. Measurement of post-impact mechanical proper-
ties has shown that impact damage in the range 1±
5 J had little eect on the residual tensile strength
although the compression strength was markedly
reduced.
3. The constant-life model was used successfully to
predict the fatigue response of undamaged HTA/
982A from only four experimental /log Nf curves.
4. The constant-life model also appears to provide a
valid descriptor of the fatigue response of the
laminate after it had sustained damage from a 1 J
low-velocity impact event. The left-hand (pre-
dominantly compression) quadrant of the con-
stant-life diagram is substantially modi®ed by the
impact damage, through its eect in reducing the
compression strength of the material, but the curve
Fig. 13. Variation of the constant-life ®tting parameters, f, u in the right-hand is much less unaected. It can be
and v, with life for HTA/982A [(45,02)2]S laminate in the
virgin condition and after damage by a 1 J low-velocity concluded that the constant-life model remains
impact. The values of f, u and v were obtained by free ®tting of valid and can be used for prediction of fatigue life
all three parameters. for impact-damaged materials.
18 M. H. Beheshty, B. Harris
5. The relationship between the constant-life para- A. A. Balkema, Rotterdam, The Netherlands, 1995,
meter, f, and the laminate tensile strength has pre- pp. 63±73.
viously been shown to provide a means of 4. Harris, B., Gathercole, N., Lee, J. A., Almond, D. P.,
Adam, T. and Reiter, H., Fatigue-life prediction for ®bre-
establishing an approximate set of /log Nf curves reinforced plastics. In Proc. Seventh European Conference
for a new material from a very limited fatigue data on Composites, ECCM7. Woodhead Publishing, Abing-
base. When the laminate has sustained damage ton, UK, 1996, pp. 69±74.
which aects the compression strength and not the 5. Harris, B., Gathercole, N., Lee, J. A., Reiter, H. and
tensile strength, however, this relationship is no Adam, T., Life prediction for constant-stress fatigue in
carbon-®bre composites. Phil. Trans. Roy. Soc. (London),
longer valid. 1997, A355, 1259±1294.
6. Adam, T., Dickson, R. F., Jones, C. J., Reiter, H. and
Harris, B., A power-law fatigue damage model for ®bre-
ACKNOWLEDGEMENTS reinforced plastic laminates. Proc. Inst. Mech. Engrs,
1986, 200, 155±166.
7. Fernando, G., Dickson, R. F., Adam, T., Reiter, H. and
M.H.B. would like to acknowledge the ®nancial support Harris, B., Fatigue behaviour of hybrid composites: I
of the Ministry of Culture and Higher Education of Iran Carbon/Kevlar hybrids. J. Mater. Sci., 1988, 23, 3732±
during his study at the University of Bath. This work 3743.
builds substantially on a series of research programmes 8. Adam, T., Fernando, G., Dickson, R. F., Reiter, H. and
on the fatigue behaviour of carbon-®bre composites Harris, B., Fatigue life prediction for hybrid composites.
Int. J. Fatigue, 1989, 11, 233±237.
carried out at Bath with funding from the DERA 9. Curtis, P. T. (Ed.), CRAG Test Methods for the Mea-
(Farnborough). surement of Engineering Properties of Fibre-Reinforced
Plastics Composites. Technical Report TR 88012, Pro-
curement Executive, Ministry of Defence, Farnborough,
UK, 1988.
10. Krenchel, H., Fibre Reinforcement. Akademisk Forlag,
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