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Feasibility Study On Use of Washed-Reclaimed Asphalt As
Feasibility Study On Use of Washed-Reclaimed Asphalt As
Abstract: Dry-lean concrete (DLC) lies below the wearing course of the rigid pavement section to overcome the major reasons for its failure,
such as improper base support, seepage of underground water, and frost action. DLC is generally manufactured with a huge aggregate-to-
cement ratio, which lies below the wearing course of the rigid pavement section. In this study, reclaimed asphalt pavement (RAP), a waste
material, derived from the milling process of flexible pavement wearing course, has been used as a partial replacement of natural coarse
aggregates in DLC made from portland pozzolana cement (PPC). Initially, the feasibility of using washed reclaimed asphalt pavement
(WRAP) and comparing the results with dirty reclaimed asphalt pavement (DRAP) as a partial replacement of natural coarse aggregate
has been investigated. It was found that WRAP gave better results as compared to DRAP for satisfying DLC conditions. The reason is
demonstrated using SEM images showing variation in formation of CSH gel due to the presence of dust particles. Further, strength and
durability properties (acidic environment, water absorption, and alkalinity) were determined to check its durability of WRAP-incorporated
concrete (WRAPC). The percentage of WRAP and DRAP was varied from 0%–50% by weight of natural aggregate. Also, nondestructive
tests like ultrasonic pulse velocity (UPV) and rebound hammer test were performed to determine the quality and dynamic young’s modulus of
WRAPC. It was found that the optimal curing period and optimum WRAP addition were 21 days and 20% respectively. An equation has been
developed to determine the optimum moisture content (OMC) for varying percentage of moisture and RAP content. The equation was
validated with the results of researchers and a variation of only 3.3% was found. It was observed that 20% WRAP incorporated in
DLC gives optimal results in terms of strength and durability. DOI: 10.1061/(ASCE)MT.1943-5533.0003339. © 2020 American Society
of Civil Engineers.
Author keywords: Portland pozzolana cement (PPC); Dry-lean concrete (DLC); Optimum moisture content (OMC); Reclaimed asphalt
pavement (RAP); Washed reclaimed asphalt pavement (WRAP); Washed reclaimed asphalt pavement incorporated concrete (WRAPC).
Introduction Montepara and Tebaldi 2000). RAP is one such solid waste product
that can be utilized as aggregate in highway construction. RAP is a
Natural aggregates (NA) are getting exploited and due to their lim- by-product obtained during the milling process of distressed flexible
ited availability in today’s market, the use of waste materials that pavement (Arulrajah et al. 2014; Farina et al. 2017). About 80% of
have the potential of replacing natural aggregate is increasing rap- the total road networks in the world are comprised of asphalt pave-
idly (Olawale et al. 2014; Wagih et al. 2013). The increasing de- ment and India has the 2nd largest road network after the United
mand of aggregates around the world has compelled researchers to States. As per the Federal Highway Administration, in the United
find alternate solutions. On the other hand, in the past decade, States, 91 million metric tons of RAP aggregate gets accumulated
global production of solid waste from the demolition of construction because of resurfacing flexible pavement roads (Xiao et al. 2009).
(roads and buildings related structures) has reached its height and Unfortunately, these valuable aggregate gets landfilled, causing
its disposal has become a world-wide problem (Kabir et al. 2016; environment problems (Arulrajah et al. 2013).
1
Looking at the Indian scenario, the total road network is about
Assistant Professor, Thapar Institute of Engineering and Technology, 4.69 million km. Out of that, 2.53 million km of roads are of flex-
Patiala, Punjab 147004, India (corresponding author). ORCID: https://
ible pavement as per MORTH (2012). Cardoso et al. (2016) found
orcid.org/0000-0001-5845-840X. Email: manpreetsingh2@thapar.edu
2
M.Tech. Student, School of Civil Engineering, Lovely Professional that flexible pavements consist of 90% NA, and once this flexible
Univ., Phagwara, Punjab 144411, India. Email: anuz.dot.dot@gmail.com pavement ages and deteriorates these aggregates are thrown away
3
M.Tech. Student, School of Civil Engineering, Lovely Professional as solid waste. Considering the issues and availability of aggregate
Univ., Phagwara, Punjab 144411, India. Email: manishmaurya603@gmail in flexible pavement, these recycled aggregates can be used in vari-
.com ous forms of road construction like sidewalks, driveways, gutter,
4
Associate Professor, Birla Institute of Technology and Science, Pilani, etc. (Delwar et al. 1997). RAP aggregates generally contain huge
Rajasthan 333031, India. Email: anshu@pilani.bits-pilani.edu amounts of dust, agglomerate particles, and aged asphalt, which do
5
Research Scholar, Indian Institute of Technology Roorkee, Roorkee, not allow binder material to bind with them; hence, a mechanical
Uttarakhand 247667, India. Email: rishi.chhabra@gmail.com
Note. This manuscript was submitted on June 15, 2019; approved on
roughening process like abrasion and attrition, or chemical solvents
February 27, 2020; published online on July 2, 2020. Discussion period like turpentine, can be employed to remove these contaminants
open until December 2, 2020; separate discussions must be submitted (Al-Mufti and Fried 2017; Singh et al. 2017). Moreover, removal
for individual papers. This paper is part of the Journal of Materials in Civil of asphalt content in aggregate can be removed by using a bitumen
Engineering, © ASCE, ISSN 0899-1561. extractor; however, this requires a huge amount of energy and
capital cost. These agglomerated particles are the combination of SP-49 (BIS 2014), PPC can be used for the construction of
dust and aged asphalt formed from the oxidation process during DLC but does not specify the concrete mix proportion. However,
Downloaded from ascelibrary.org by University of Liverpool on 07/05/20. Copyright ASCE. For personal use only; all rights reserved.
stockpiling (De Lira et al. 2015). DLC should have a maximum aggregate-to-cement ratio of 12∶1
Many studies have been conducted on the incorporation of RAP and cement content should not be less than 140 kg=m3 . DLC pro-
aggregate in flexible pavement in partial form, and incorporating vides uniform and strong support, high resistance to deformation,
them in flexible pavement is currently a common practice due and reduction in depth of pavement slabs, making positive impact
to environmental and economic considerations. On-the-spot utiliza- in terms of economic consideration.
tion of RAP for concrete pavements would not only offset the trans- The initial investigation of addition of RAP on concrete roads
portation cost of the materials but would also immensely help in was done by Delwar et al. (1997). It was observed that the density
reducing carbon footprint. It also reduces the energy consumption of hardened concrete reduces during the addition of RAP in cement
and green house emission (Yan et al. 2016). One common practical concrete. The incorporation of RAP in cement concrete has
example is the Jalandhar-Chandigarh highway in India, where 10% increased its workability but has reduced the hardening properties.
of RAP is incorporated with NA in flexible pavement construction. This increase in workability is because of the asphalt present in the
Stabilization of base course plays a vital role and in recent years surface area of aggregates (Brand and Roesler 2014). Due to scar-
several material and methods have been adopted to stabilize the city of NA this study focuses on the use of RAP aggregate in DLC
base course in flexible pavement because it lies near to the wearing in partial form. However, the addition of RAP in DLC or in roller-
section (Wahhab et al. 2012; Montepara et al. 2012). This can be a compacted concrete was found to lose its mechanical and durability
reason for why the base course must possess higher resistance to properties (Debbarma et al. 2020; Settari et al. 2015; Singh et al.
load as compared to lower subsequent layers of pavement. Thus, 2018b). Keeping in mind the points of view of the previous liter-
stronger base is always a basic requirement for better stability. ature, an effort has been made to increase the utility of RAP
When RAP is used in surface course, texture plays an important aggregate and replacement of base/subbase course with DLC. A
role because it governs frictional resistance and safety of a driver study was carried out on RAP and inferred that if these aggregates
(Praticò and Vaiana 2015). Hence, RAP is encouraged to be used are properly selected, processed, and compacted, then they may
in base/subbase course material but RAP alone cannot meet the provide a property comparable to NA (Vieira and Pereira 2015).
desired strength; therefore, blending them with some stabilizing It was found that the nominal size and particle size distribution
agents like cement or lime improves the overall strength and of RAP and NA is not the same; this might affect the mechanical
durability properties (Puppala et al. 2011; Sireesh et al. 2016; Taha and durability property of concrete (Abed et al. 2018). Hence, an
et al. 1999). Moreover, RAP aggregate alone in base/subbase attempt was made to match the particle size distribution of RAP and
course undergoes permanent deformation under traffic loading NA in the present study as per the gradation chart given in IRC
(Thakur et al. 2012). This loss in strength is due to the presence SP-49 (BIS 2014). The presence of aged asphalt, dust, and agglom-
of dust and agglomerated particles present around the periphery erated particles would also affect the slump value and workability
of RAP aggregate (Huang et al. 2006). Moreover, the findings of of fresh concrete by absorbing water, so the RAP aggregate was
Huang et al. (2005, 2006) stated that at 100% coarse RAP replace- washed and dried to bridge the gaps found in the literature.
ment to NA the reduction in strength was up to 75%, for a binder The aggregate was dried at room temperature for 72 h before batch-
content of 396 kg=m3 . Also, a decrease in flexural strength and ing and the same water was used (after sedimenting) during the
splitting tensile strength was reported by Abraham and Ransinchung curing process to reduce environmental impacts. With this gap in
(2018) and Hossiney et al. (2010) for all curing ages. Moreover, mind, RAP was collected from the stockpile after being crushed
reduction in durability properties was reported by Abraham and and screened from the milling machine. Trial mixes were per-
Ransinchung (2018) and Singh et al. (2018b), where the addition formed with varying moisture content (5.0%, 5.5%, 6.0%, 6.5%,
of RAP at a higher percentage contributed to a reduction in and 7.0%) in order to obtain OMC. NA was partially replaced by
durability property. WRAP and DRAP up to 50% (0%, 10%, 20%, 30%, 40%, and
The strength in base/subbase course can also be achieved by 50%). The slump value was determined to obtain workability of
using DLC by using either PPC, ordinary portland cement (OPC), concrete for various percentages of WRAP and DRAP. Compres-
or portland slag cement (PSC) as per [IRC SP-49 (BIS 2014)], as sive strength, flexural strength, and splitting tensile strength tests
shown in Fig. 1. Moreover, it has been found that the use of PPC were performed in order to determine the mechanical property
poses higher strength compared to OPC. Also, the cement aggre- of aggregate. WRAP showed better mechanical results, and hence
gate ratio for PPC was significantly lower compared to OPC. How- acidic environment, water absorption, and alkalinity tests were per-
ever, the density of the DLC mix gets reduced on manufacture with formed on WRAPC in order to check the durability property of
PPC (Kumar 2016). concrete. So far, none of the past researchers have developed a re-
In today’s road construction practice, the construction of rigid lation to determine OMC, compressive, flexural, and splitting ten-
pavement structure requires a layer of DLC as base/subbase course sile strength with varying percentages of RAP aggregates, which
over which pavement quality concrete layers rest. As per IRC has been studied in this paper.
the particle size distribution between NA and RAP was made as per
The presence of dust particles in RAP aggregate due to stockpiling IRC SP-49 (BIS 2014), as shown in Fig. 3. Because the gradation of
is reported as the primary cause for reducing the overall RAP added RAP and NA was not similar, these aggregate nominal sizes were
concrete properties. Washing them before incorporating in a mix matched in reference to IRC SP-49 (BIS 2014). Table 2 presents the
can be a factor that may increase the fresh concrete property as well physical properties of aggregate and RAP. Potable water conform-
as the overall mix of concrete. Moreover, the nominal size and gra- ing to IS 456 (BIS 2000) was used for the preparation of trial mixes
dation is not the same, which influences the strength characteristics. and concrete mixes. The same water used for washing the aggre-
Matching the size distribution using Indian standard sieves nullifies gates was used for mixing and curing purposes (after sedimenting)
the effect. The experimental investigation is done in three parts. The to reduce environmental impact.
first part deals with the fresh properties of WRAPC and Dirty Trial mixes were made as per IRC SP-49 (BIS 2014) in order to
Reclaimed Asphalt Pavement Incorporated Concrete (DRAPC). determine the OMC. A nominal mix of 1∶3∶6 proportions was used
The second part deals with mechanical properties like compressive, during the study. The proportion of materials used during study is
flexural, and splitting tensile strength of WRAPC and DRAPC. On shown in Table 3. The quantity of coarse RAP was varied from 0%
the basis of compressive strength, the optimal curing period and to 50% with water content varying from 5% to 7% of the total mix
optimal RAP addition was determined. WRAPC in comparison comprising of cement, sand, and aggregates. Cubes of standard size
with DRAPC showed better mechanical properties, which satisfied (150 × 150 × 150 mm) were casted and demolded after 24 h. They
the DLC conditions given in IRC SP-49 (BIS 2014). Hence, the were weighed after demolding. Five samples each were made for
third part deals with the nondestructive test of concrete and durable each varying percentage of water as per IRC SP-49 (BIS 2014). The
properties like acidic environment, water absorption, and alkalinity relation between bulk density, dry density, and water content is de-
for WRAPC. Finally, an equation has been developed to determine termined by the Eq. (1) and the procedure is followed as done
the OMC for varying percentages of moisture and RAP content. by Singh (2001)
Also, a relation has been established to determine compressive
strength, flexural strength, and splitting tensile strength with vary- γb
γd ¼ ð1Þ
ing percentages of WRAP. 1þw
where γd = dry density; γb = bulk density; and w = moisture to calculate fresh property (workability and density), mechanical
content. property (compressive, flexural, and splitting tensile strength), non-
The difference between DRAP and WRAP is shown in Fig. 4. destructive property (ultrasonic pulse velocity and rebound hammer),
and durability property (acidic environment, water absorption, and
alkalinity of concrete for same proportion of mix). Five samples each
Experimental Program are casted for percentage of water determined during trial mix as
per IRC SP-49 (BIS 2014) for the compressive strength test. Further,
Trial mixes were made to determine the optimal moisture content. to test all the other properties, three samples each for 7- and 28-day
The optimal water content determined during trial mix is used curing were casted and tested according to the IS codes.
linear regression. The results were analyzed statistically by the aggregates is done by an uncontrolled milling technique using a
principle of least squares, and Eq. (5) was derived bulldozer, which causes huge dust particles to accumulate in cluster
form. Moreover, these dust particles get further added in layers dur-
y
log yd ¼ 1.413 þ 0.57 log ð5Þ ing stockpiling from the vicinity of the landfill area. The present
ð1 þ wÞ0.117 study indicates that with the use of WRAP aggregate the workabil-
ity increases to some extent, which increases the travel time of mix
The value of the correlation coefficient was 0.763. The standard to the sites.
error was 0.031 at the 95% confidence interval. The equation was
derived for varying water content of 5%–7% and RAP content of
0%–50%. Compressive Strength
It was found that the compressive strength of the sample decreased
Checking the Validity of Models with Results of Other with an increase in RAP content. At 7 days of curing, the sample
Researchers showed an overall compressive strength more than 7 MPa, up to
To verify the equation, the results of dry density obtained by Singh 20% of WRAP addition, which is the recommended benchmark
et al. (2018b), the results of two different water content, and RAP value per IRC SP-49 (BIS 2014), and was not found in DRAPC.
content were checked with the proposed equation in the paper. On The overall reduction percentage in compressive strength for 30%,
comparing the results for the 6.5% water content and 50% RAP, the 40%, and 50% of the 7-day sample was about 40%, 60%, 64%, 38%,
variation in result obtained was 3.3%; also, for the 7% water con- 58%, and 60% for DRAP and WRAP, respectively, as compared to
tent and 50% RAP, the variation obtained was 2.15%. Also, com- Natural Aggregate Incorporated Concrete (NAC). However, the
paring the results of Settari et al. (2015) for the 5.5% and 6% water individual cube strength for 30% WRAPC was found to be more
content with 50% replacement of NA with RAP shows only 2.47% than 5.5 but less than 7.0 MPa. Also, for a 28-day sample, the bench-
and 3.22% variation in results, respectively. No other studies have mark strength of 10 MPa was attained by 20% WRAP addition
used only RAP as a replacement of NA in DLC, thus validating the whereas 30%, 40%, and 50% showed its strength than 10 MPa.
equation. The values obtained for all the compressive strength corresponding
to the curing days is shown in Fig. 8. Table 4 presents the change in
compressive strength after addition of DRAP and WRAP in concrete
Workability for 7, 14, 21, and 28 days. From the values obtained, it is evident
Generally, DLC is zero slump concrete. However, the incorporation that compressive strength decreased by 50%–60% as compared
of RAP in DLC increases the slump value. It was observed that the to NAC. The findings of Huang et al. (2005, 2006) stated that at
slump value of 50% RAP concrete was more than 100% NA con- 100% coarse RAP replacement to NA, the reduction in strength
crete. The increment in the slump value for DRAP and WRAP is was up to 75% for a binder content of 396 kg=m3 . However, Abraham
shown in Fig. 7 for the mixes containing 10%, 20%, 30%, 40%, and and Ransinchung (2019) found that the reduction of strength was
50% DRAP and WRAP content. On comparing DRAP and WRAP, 4.85% for 25% RAP addition for a water-cement ratio of 0.44. This
WRAP showed higher slump value as shown in Fig. 6. This in- variation of strength reduction depends upon the amount of dust
crease in slump value is due to the absence of water absorbing dust and asphalt content and age of the RAP aggregates. Moreover, the
in WRAP aggregates. However, the overall increase in slump value compressive strength of the concrete can be increased by increasing
in comparison with NA concrete is due to the presence of asphalt its density. The best method of increasing the density of RAPC is by
coating (Brand and Roesler 2014). In India, the milling of RAP adding or increasing the cement content (Singh et al. 2018b);
Fig. 8. Compressive strength of mixes with various percentages of RAP addition for various curing days.
Table 4. Change in compressive strength with addition of RAP for various curing days
% of coarse aggregate added
S. No Aggregate Day 0 10 Δ 20 Δ 30 Δ 40 Δ 50 Δ
1 DRAP 7 9.57 6.70 30 6.02 38 5.90 40 3.88 60 3.47 64
2 14 10.89 8.54 22 7.92 28 7.01 36 4.96 55 4.54 59
3 21 12.04 9.04 21 8.76 21 7.03 37 5.82 48 4.98 55
4 28 12.86 10.25 21 9.89 21 8.76 32 7.90 39 6.31 51
5 WRAP 7 9.57 7.33 23 7.24 25 5.98 38 4.04 58 3.92 60
6 14 10.89 8.59 22 8.24 25 7.04 36 5.94 46 5.20 53
7 21 12.04 9.92 18 9.06 24 7.78 36 6.63 45 6.23 49
8 28 12.86 12.08 7 11.03 15 9.16 29 8.32 36 7.21 44
however, it was not possible in this study due to economic consid- mix, the compressive strength attained was 9.7 MPa, which is al-
eration because DLC itself is a lean concrete that does not allow most equal to the benchmark of 10 MPa. Hence, 21 days is taken as
higher cement ratio with aggregate content. the optimum curing period.
From Fig. 8 it is evident that the optimum compressive strength The maximum 28-day compressive strength attained by
attained by the WRAP mix is 20%. At 21 days of 20% of WRAP WRAPC is 12.08 for 10% of WRAP addition. But it is evident that
even 20% of WRAPC also attends the benchmark of 10 MPa. y ¼ −0.0155x2 þ 0.7158x − 2.4098 ð6Þ
Hence, the optimum WRAP addition is taken as 20%.
where x = compressive strength in MPa; and y = flexural strength
in MPa. This equation has been derived from data obtained from
Flexural Strength five varying water contents (5%–7%) with varying percentages
Similar to the compressive strength, 100% NAC gave a maximum of WRAP (0%–50%) concrete mixes. The R2 value obtained
flexural strength of 2.65 MPa, but as the RAP addition increased, was 0.9618.
the flexural strength decreased. On comparing DRAP and WRAP,
for the 7-day cured sample the flexural strength attained by the Splitting Tensile Strength
WRAP was found to be 33%, 35%, 50%, 52%, and 57%, while At 7 days of curing the tensile strength attained by the DRAPC was
DRAPC showed 47%, 64%, 72%, 75%, and 85% less than NAC found to be 27%, 32%, 44%, 54%, and 63%, while WRAPC was
for 10%, 20%, 30%, 40%, and 50%, respectively. Similarly, the found to be 15%, 22%, 31%, 47%, and 50% less than 100%
28-day flexural strength attained by the WRAP sample was found (0.65 MPa) NAC for 10%, 20%, 30%, 40%, and 50% DRAP
to be 16%, 22%, 33%, 52%, and 56%, while DRAPC showed and WRAP addition, respectively.
35%, 55%, 69%, 78%, and 79% less than NAC (4.67 MPa) for Similarly, the 28-day splitting tensile strength attained by the
10%, 20%, 30%, 40%, and 50%, respectively, as shown in Table 5. WRAP sample was found to be 6%, 17%, 29%, 35%, and 40%,
A decrease in flexural strength was reported by Abraham and while for DRAP it was found to be 23%, 25%, 40%, and 58% less
Ransinchung (2018) for all curing ages. The reduction of strength than 100% (0.9 MPa) NAC for 10%, 20%, 30%, 40%, and 50%
varied in the range of 6%–25%. Moreover, for 20% of RAP RAP replacement, as shown in Table 6 and Fig. 10. Similar to com-
addition, Hossiney et al. (2010) found that the variation in reduc- pressive strength, Huang et al. (2005, 2006) found a reduction in
tion of flexural strength was 20%–22% with the control mix. The splitting tensile strength as well. The percentage of reduction was
reason for the reduction of strength is same as the reduction in com- found to be 79.1% and 49.5%, respectively, for the water- cement
pressive strength. The asphalt present in WRAP does not allow the ratio of 1∶2. However, according to the findings in Abraham and
cement to form a bond with aggregates, thus failing at lower loads. Ransinchung (2019), the splitting tensile strength had a greater re-
However, in the present study, WRAPC showed better results com- duction compared to the findings in compressive and flexural
pared to DRAPC, as shown in Fig. 9. strength. The reason behind the reduction in tensile strength of
Eq. (6) is the best-fitting equation considering WRAP- WRAPC is similar to that of the flexural and compressive strength.
incorporated DLC and shows the relationship between compressive However, with WRAP, the results obtained were better than tensile
strength and flexural strength strength with DRAP aggregates.
Fig. 10. Splitting tensile strength of mixes at various percentages of RAP addition.
Eq. (7) is the best-fitting equation considering WRAP- resisting crack propagation (Huang et al. 2006). However, in the
incorporated DLC and shows the relationship between compressive present study, WRAP showed less variation in the formation of
strength and splitting tensile strength the transition zone as compared to DRAP. Also, more ettringite for-
mations are seen in the DRAP sample as compared to the WRAP
y ¼ 0.0028x2 –0.0127x þ 0.5127 ð7Þ sample. The same concept has been demonstrated by Abraham and
Ransinchung (2018) using the mercury intrusion porosimetry
where x = compressive strength in MPa; and y = splitting tensile (MIP) technique in which more CH concentration is found in fresh
strength in MPa. This equation has been derived from data obtained RAP or clean RAP as compared to the aged RAP.
from five varying water contents (5%–7%) with varying percent-
ages of WRAP (0%–50%) concrete mixes. The R2 value obtained
Acidic Environment
was 0.9755.
The other reason for overall reduction in mechanical strength is Fig. 12 shows the condition of the sample after being exposed to
the stress concentration, which is induced in the soft asphalt binder 2.5% and 3% HCl solution. Fig. 13 shows the loss in weight of
and causes microcracking within the cement concrete matrix. This various concrete mixes after being exposed to a concentrated
mechanism of failure is explained by Huang et al. (2004), who in- HCl solution. The loss in weight of concrete when exposed to 2.5%
corporated rubber as an aggregate in cement concrete. The trend of concentrated HCl was noted as 3.53%, 4.75%, 4.94%, 4.96%,
interfacial transition zone (ITZ) of reduction in mechanical strength 5.76%, and 6.88% for mixes containing 0%, 10%, 20%, 30%, 40%,
was found to be similar; however, less variation was found in the and 50% WRAP. Further, when exposed to 3.0% of concentrated
reduction for RAP aggregate in terms of mechanical strength. HCl, the loss in weight was noted as 4.95%, 5.25%, 5.40%, 6.60%,
Moreover, the reduction in strength is because of the ITZ built be- 8.1%, and 9.31% for mixes containing 0%, 10%, 20%, 30%, 40%,
tween aggregate and cement matrix, as shown in Fig. 11. The zone and 50% WRAP. Thus, it is noted that with the incorporation of
built with RAP aggregate is found to be larger than the compared WRAP the loss in weight of concrete increases. This increase in
NA because of the asphalt present in aggregate. Findings from pre- weight loss with increase in WRAP is due to the increase in water
vious studies suggest that the concrete with RAP aggregates has absorption (i.e., formation of permeable voids). A similar trend was
more large and porous ITZ, which is the major reason behind initial also observed by Singh et al. (2017), where the loss in mass when
crack initiation. It was also observed that the amount of calcium exposed to 2.5% HCl was found to be 14.10% for 25% of ARAPC
hydroxide (CH) formation within the asphalt cement paste interface (abrasion and attrition). Also, it was observed that the presence of
was less compared to overall CH formation in the sample dust in RAP-incorporated concrete results in an increase in weight
(Sebastian 2015). Although the addition of RAP in cement aggre- loss (Singh et al. 2018a), and as per research findings, it was ob-
gate initiates initial crack formation, it also improves toughness by served that a loss in mass for a 100% RAP-incorporated mix was
Fig. 11. Surface demonstration of 20%: (a) WRAP; and (b) DRAP.
Fig. 12. 28-day specimen exposed to (a) 2.5% HCl; and (b) 3.0% HCl.
Fig. 13. Loss in weight of concrete mixes after being exposed to HCl.
Fig. 14. 28-day compressive strength of concrete mixes after being exposed to concentrated HCl.
Fig. 15. 28-day water absorption value with increase in WRAP content.
found to be 19% as compared to the control mix, while a loss in mass incorporation of WRAP the water absorption of concrete mixes
with fine RAP-incorporated concrete was found to be 46% when the ncreases significantly. Increments in the water absorption value
sample was fully saturated. The 25% ARAPC showed comparable compared to the control mixes were noted to be 40.74%, 69.81%,
performance when the sample was fully dried. However, for 20% 76.81%, 78.08%, and 78.6% for mixes containing 10%, 20%, 30%,
WRAPC, the loss in weight when exposed to 2.5% HCl was found 40%, and 50% WRAP. A similar increase in water absorption was
to be much less compared to the preceding research studies. observed by Singh et al. (2017); however, the absorption rate de-
Fig. 14 shows the loss in compressive strength after being creased when 75% of abrasion-treated RAP was added in a mix. On
exposed to the concentrated HCl solution. The reduction in com- the contrary, Settari et al. (2015) found comparable water absorp-
pressive strength for the 2.5% and 3.0% concentrated HCl solution tion for 50% RAP and 50% fine RAP with respect to reference mix,
as compared to the 28-day compressive strength was noted to be while the addition of fine RAP in concrete showed 20%–60% of
2.06% and 3.34%; 11.02% and 11.67%; 10.17% and 14.85%;
water absorption. Hence, we can conclude that from the above find-
14.76% and 20.13%; 3.63% and 4.12%; and 2.98% and 4.36%
ings the dusts present within the RAP aggregate are a major source
for mixes containing 0%, 10%, 20%, 30%, 40%, and 50% WRAP.
that increases water absorption. Increasing the water absorption of
various varying concrete mixes leads to a reduction in the compres-
Water Absorption sive, flexural, and tensile strength of concrete. The water present
Fig. 15 shows the water absorption value of various varying con- in the concrete will evaporate when exposed to atmosphere and
crete mixes after 28 days of curing. It was found that with the form voids, which in turn will be responsible for the reduction
of strength. Higher water absorption of concrete reduces resistance same as the 10% mix to NAC. However, the values increased the
to sulphate attack. addition of WRAP further, as shown in Table 7. Singh et al. (2017)
Eq. (8) is the best-fitting equation considering WRAP- found the same results. Comparing the results of present study with
incorporated DLC and shows the relationship between compressive Singh et al. (2017), the value of 50% treated RAP aggregate was
strength and water absorption found to be 1.3%.
y ¼ 0.0003x3 –0.0091x2 þ 0.0894x–0.1978 ð8Þ
Nondestructive Tests
where x = compressive strength in MPa; and y = water absorption Nondestructive tests on concrete were done using two methods.
in %. This equation has been derived from data obtained from
five varying water contents (5%–7%) with varying percentages Ultrasonic Pulse Velocity (UPV) Test
of WRAP (0%–50%) concrete mixes. The R2 value obtained The test was done on a 28-day cured concrete sample. The normal
was 0.9756. concrete with 0% WRAP showed the highest velocity of all sam-
ples with 3.8 km=s. However, the UPV value of a concrete sample
slightly varied until 30% of WRAP-added concrete with 3.4 km=s
Coefficient of Sorptivity for 10%, 3.2 km=s for 20%, and 3.0 km=s for 30%. The increase in
The coefficient of sorptivity increases with the addition of WRAP the percentage of WRAP after 30% showed significant change in
aggregate as compared to the NAC after 28 days of curing period, UPV value. For 40% and 50%, the UPV values determined were
as shown in Fig. 16. The increase in the value of the coefficient of 2.4 and 2.1 km=s, respectively. Similar UPV results were obtained
sorptivity is due to the increase in the value of water absorption. by Al-Mufti and Fried (2017), and it was found that up to 25%
Eq. (9) is the best-fitting equation considering WRAP- of RAP addition in UPV travelling through concrete remained un-
incorporated DLC and shows the relationship between compressive affected, while during higher addition the UPV value decreased.
strength and coefficient of sorptivity However, the value increased when the addition was made in
mechanically-treated form for longer hours of treatment, whereas
y ¼ −0.0997x2 þ 0.9732x þ 7.5241 ð9Þ the UPV value did not show much influence for the aggregate
treated with chemical solvent. This reduction in value is due to
where x = compressive strength in MPa; and y = coefficient of the nonbonding of the cement matrix and aggregates, which is a
sorptivity. This equation has been derived from data obtained from major factor for the ultrasonic pulse to take a longer route to travel
five varying water contents (5%–7%) with varying percentages the concrete sample.
of WRAP (0%–50%) concrete mixes. The R2 value obtained Dynamic Young’s modulus of elasticity was calculated using
was 0.9586. Eq. (2). From the values obtained, it was found that NA possessed
Alkalinity
Table 7. Alkalinity of various concrete mixes after 28 days of curing
The pH of a concrete signifies its deterioration level. The pH of
a concrete for rigid pavement should not be less than 9.0 and % of incorporated aggregates in concrete Observed pH values
for durable concrete it should lie between 12.0 and 13.0. The 100NAC 12.07
pH of concrete greater than 9.0 can withstand salting in winter and 10WRAPC 12.07
other variable climatic conditions. Table 7 represents the pH value 20WRAPC 12.22
of various concrete mixes. 30WRAPC 12.44
With the incorporation of WRAP the pH increased up to 50% 40WRAPC 12.75
50WRAPC 12.93
WRAPC as compared to NAC. The increase in the pH is noted the
Conclusion
higher values of modulus of elasticity (2.95 × 104 MPa) as com-
pared to any other mix. However, there was a slight variation be- The present study describes a possible way to use RAP in DLC.
tween 10%, 20%, and 30% of WRAPC with values of 2.35 × 104 , RAP obtained from a stockpile that had gone through the oxidation
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2.05 × 104 , and 1.79 × 104 MPa. At 40% and 50% of WRAP in- process were used to study the fresh and mechanical properties to
corporation, the modulus of elasticity values reduced drastically to satisfy the DLC criteria as given in IRC SP-49 (BIS 2014). Given
1.14 × 104 and 0.87 × 104 MPa, respectively. This reduction in that WRAPC satisfied the DLC conditions of achieving a 7-MPa
dynamic modulus of elasticity in the mix is due to the variation benchmark for a 7-day curing period compared to DRAPC, the
of density, given that WRAP has a lower specific gravity as com- durable property of WRAPC was investigated. Some inferences
pared to NA. experimentally investigated in the present study are as follows:
• With the incorporation of WRAP, the workability of concrete
Rebound Hammer Test increased compared to DRAPC and NAC. This implies that
Table 8 shows the effect of the replacement of WRAP after 28 days the concrete containing WRAP will not settle rapidly and thus
curing. After 28 days of curing, no effect on the hardness of con- increases travel time of mix to site.
crete has been noticed for 10% WRAPC. Further, increasing the • Density decreased due to the lower specific gravity of RAP. How-
replacement of WRAP by 20%, 30%, 40%, and 50% resulted in ever, WRAPC showed higher density as compared to DRAPC.
a reduction of rebound number (RN) surface hardness after 28 days Thus, this decrease in density of concrete decreased the compres-
of curing. Al-Mufti and Fried (2017) observed that for 7-day sive, flexural, and splitting tensile strength of concrete.
curing, 25% of RAP addition had no effect on surface hardness. • With the increase in the WRAP content, the mechanical prop-
Beyond that, there was slight reduction compared to control mix. erty (compressive, flexural, and splitting tensile strength) tends
Moreover, an increase in the addition of RAP aggregate decreased to decrease gradually. 50% replacement of NA by WRAP and
the surface hardness with age. The replacement of NA with WRAP DRAP shows a maximum reduction in strength compared to
having lower water absorption will not allow NA to obtain moisture 10%, 20%, 30%, and 40% WRAP and DRAP addition. The
from the surrounding cement matrix, which will thus result in most noticeable part of the present study was that when 20%
reduction of stiffness and lower surface hardness. WRAP aggregate was used, the reduction in the mechanical
property was found to be less than 25% after 28 days of curing.
It was also noted that 20% replacement of NA by WRAP pro-
Discussion and Recommendations duces a 11.039-MPa compressive strength, which is more than
the benchmark for the construction of DLC as per IRC SP-49
An attempt was made to enhance the properties of DLC by washing (BIS 2014); however, this was not achieved by DRAPC.
the RAP aggregates as studied from the literature, and the dust • With the incorporation of WRAP, the loss in weight of concrete
present in RAP was the major reason for decrease in strength. and compressive strength tends to decrease significantly. The
The results from the present study indicate that washing RAP water absorption of the concrete increased with the addition
aggregate played a pivotal role with the fresh properties of RAP in- of WRAP, which reduced resistance to sulphate attack. Simi-
clusive concrete. Because water-absorbing dust was washed away, larly, the alkalinity of concrete also increased, which signifies
the WRAP mix showed better workable characteristics compared concrete can withstand salting in winter and other variable
to DRAP. The incorporation of WRAP in DLC performed better climatic conditions.
in terms of mechanical and durability aspects compared to DRAP. • From the present study it has been investigated that 20% of
IRC SP-49 (BIS 2014) recommends a minimum benchmark of WRAP replacement can be used for construction of DLC in
7 MPa for 7 days of curing. The 20% optimum WRAP addition cal- rigid pavement without affecting the mechanical and durable
culated in this study is mainly focused on higher quality pavement property of hardened concrete.
base course, like national highways and express ways, while for low-
volume roads a higher dosage of WRAP aggregate can be added.
Moreover, the benchmark for 10 MPa was attained by 20% in 21 days
of curing; hence, this means further construction like the PQC layer Data Availability Statement
can be started after 21 days of curing the DLC course. This DLC can
Some or all data sheets related to experimental results and models
be used as subbase for road pavements or other projects such as traf-
developed, or codes that support the findings of this study are avail-
fic pavements for rural roads and large areas of pedestrians.
able from the corresponding author upon reasonable request.
Taking into account the environmental aspect of using water to
wash the RAP before using in DLC, according to the Ecoinvent
database (version 3.0), approximately 657 L=m3 of water is used
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