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Fluidised catalytic cracker

hydrotreater revamp
Primary revamp of reactors, exchangers and other FCC pretreater components
provided return on investment for a complex refining facility

Raj Patel Haldor Topsoe Inc


Howard Moore, Harrell Duff and Brian Hamari Marathon Ashland Petroleum LLC

A
s part of the Marathon Ashland Petroleum sulphur to less than 50ppm sulphur and in some
LLC (MAP) clean fuels programme at the locations in the EU will actually start to require
Catlettsburg, Kentucky, refinery, the exist- zero sulphur gasoline with less than 10ppm
ing fluid catalytic cracker (FCC) feed sulphur. By 2009, zero sulphur gasoline will be
hydrotreating unit was revamped to allow required throughout the EU. Gasoline sulphur
increased capacity, processing of tougher feeds, specifications are also being reduced in the Far
and production of lower sulphur product. The East.
design rate increased from 40000 to 60000 To meet these specifications, refiners with an
bpsd and the blended feed to the unit will FCC will have two choices. One option is the
contain 15% deasphalted oil (DAO). The hydrot- post-treat option that requires treating the FCC
reated product sulphur specification is set at gasoline. The second option is the pretreat
750ppm to produce FCC gasoline that can be option, which requires reducing the sulphur in
blended directly into the gasoline pool and still the feed to the FCC. One problem with post-
meet the future low sulphur gasoline treatment is the potential loss of octane. This
specifications. can be addressed through advanced technology.
The primary revamp included addition of four The more fundamental problem of post-treat-
new reactors, additional exchangers, a new ment is that there is little chance for ROI. The
membrane unit for purifying hydrogen, and post-treat processes will meet the product
upgrading of the wash water system. The unit sulphur spec but will produce a product that is
modifications described here are part of an over- at best equal to the feed value while incurring
all restructuring of the Catlettsburg refinery and capital and operating costs.
will not only enable MAP to meets the require- The fundamental problem with pretreatment is
ments of the clean fuels project, but also provide the high capital cost. However, due to the
a return on the investment (ROI) with improved improvements in the feed, the yield structure
FCC operation. will be more favourable from the FCC and an
Gasoline sulphur specifications are tightening ROI is possible. This is especially true if costs
throughout the world. In the USA, a company can be minimised in a revamp of an existing
pool average gasoline sulphur specification of unit. In general, enhancing FCC feed hydrotreat-
120ppm was begun in January this year. In ing is economical when the combination of
January 2005, this is to be reduced to 90ppm improved FCC yields, heavier feedstocks, and
and an additional refinery specification of 30ppm environmental credits are available.
will also begin. In January 2006, a per-gallon MAP faced the challenges of meeting future
limit of 80ppm will be required in the USA gasoline sulphur specifications and turned this
generally, with an even more stringent standard adversity to an advantage. MAP chose to revamp
in California. their FCC feed pretreater as well as to restruc-
In 2005, the European Union will cut gasoline ture the refinery operations.

www.digitalrefining.com/article/1000155 PTQ Q2 2004 1


gasoline pool sulphur. Discussions
60 Mbd with technology vendors, internal
Sour heavy Gasoline
High
pool
pilot plant evaluations, and available
gas oil pressure 0.075 FCC
2.54% S HTU wt% S gasoline Gasoline 24 ppm S literature information were used to
FCCU
41 ppm S blending provide a cat feed (FCC feed) sulphur
97.1%
HDS target of 660ppm. This level of
0.05
sulphur would be provided by two
35 Mbd Other stocks
Sour heavy Low
wt% S 10 ppm S units producing 60000bpd of heavy
gas oil pressure feed at 750ppm sulphur and
1.34% S HTU 35000bpd of lighter feed at 500ppm
96.3% sulphur, as shown in Figure 1.
HDS
The revamp of the existing cat feed
hydrotreater to a high severity heavy
Figure 1 FCC pretreater system with a high-pressure hydrotreating cat feed hydrotreater, dubbed high-
unit (HTU) for processing up to 60000bpd heavy feed (2.5 wt%S) pressure virgin gasoil (HPVGO)
and a low-pressure HTU processing up to 35000bpd lighter feed hydrotreating unit, is described in
(1.34 wt%S) further detail.

Objectives Pre-revamp
The Catlettsburg refinery has operated since Based on an alliance between MAP and Haldor
1917, and was the origination of Ashland Oil and Topsoe, the technology requirements for all of
Refining Company. Two additional refineries the FCC feed pretreaters in the MAP refining
have been integrated into the facility since that system are provided by Haldor Topsoe. To date,
time and petrochemical facilities were added that designs have been completed for four units, in
make it a very complex refinery. This FCC project addition to three revamps and one grassroots
originally began to increase the severity of an unit. Two of the four units have successfully
existing catalytic feed hydrotreater and was started up, including the Catlettsburg refinery
combined with other projects for refinery stream- HPVGO hydro-treater. In addition, reactor inter-
lining and simplification, as well as gasoline nals have been provided for other hydrotreating
desulphurisation. units.
The overall refinery objectives were to meet At the Catlettsburg refinery, two hydrotreating
existing and future gasoline sulphur require- units were revamped for FCC feed hydrotreating
ments while improving refinery economics. service. The existing unit had a name-plate
Specifically, the objectives were: capacity of 40000bpsd using two reactor trains
• Improve FCC economics by hydrotreating all with two, single-bed reactors in each train. The
of the FCC feed, including all DAO production. unit was typically operated at 1050psi, which
• Avoid post-treating cost/investment by reduc- was significantly less than the 1500psi original
ing FCC gasoline sulphur to a level allowing design due to hydraulic and equipment limita-
direct blending to the gasoline pool while meet- tions. The unit contained an amine scrubber to
ing 2006 requirements. remove the H2S from the recycle gas. Product
• Reduce fixed and operating costs, and improve from the high-pressure loop was sent to the
overall refinery reliability, by reducing refinery stripper before being sent out to the FCC unit.
complexity and multiplicity of equipment. The feed was straight run gas oil with some
• Avoid major turnaround (TAR)/ revamp costs DAO. However, the quantity of DAO that was
on existing FCC unit. added was limited due to high deactivation rates.
• Expand distillate hydrotreater, and reduce The feedstock typically averaged 1.7% sulphur
2006 ultra low sulphur diesel (ULSD) revamp and product sulphur averaged 0.4 wt% for a little
costs by reducing the quantity and sulphur less than 80% desulphurisation. At these rela-
content of light cycle oil (LCO). tively low sulphur conversions, the nitrogen
An FCC gasoline sulphur content of 45ppm, conversion was also low at less than 30%. The
when blended with the existing gasoline compo- gravity improvement averaged on the order of
nents, was determined to produce the targeted two API numbers with about 24 API in the feed

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and 26 API in the product. Reactor temperature The existing high- pressure piping was also
rise averaged about 30°F in the lead reactor and determined to be inadequate for future operation
20°F in the lag reactor. and much of it had to be replaced with larger
diameter piping. The pressure drop in the heat-
HPVGO revamp ers was estimated to be excessive, but
The scope of the revamp included a name-plate replacement of the heater tubes was avoided by
capacity increase from 40000bpsd to 60000bpsd adding a treat gas bypass around the heater.
with a substantially lower product sulphur target Excessive pressure drop in the reactors was
of 750ppm. The target operating cycle is 24 avoided by selecting the proper diameter that
months. As part of the overall refinery reconfig- minimised pressure drop but still provided
uration, the feed to the HPVGO pretreater would proper flow distribution, even at turndown
be substantially more difficult to process. The conditions.
design feed properties are provided in Table 1. The most cost effective option for meeting the
Significant modifications to the unit were heat requirement of this unit was to add new
required. These modifications are identified as feed effluent exchangers, two shells per train
part of six key areas, including reactors, hydrau- while maintaining the fired heater duty. The only
lics, preheat limitations, hydrogen partial change to the fired heaters was to replace the
pressure limitation, isolation of each train and existing burners with low NOx burners. Due to
wash water system upgrade. the expected higher preheat temperatures in the
In order to increase throughput, increase exchangers, facilities were provided to add
conversion, increase cycle length and process hydrogen “soker gas” to the feed upstream of the
tougher feeds, it was necessary to increase the exchangers. The purpose of the soker gas is to
reactor catalyst volume. The following four provide some source of hydrogen to minimise
options were considered for each of the two reac- fouling of the exchangers. With the addition of
tor trains: the four new exchanger shells, the total heat
• Replace existing reactors with two new recovery increased by almost 80 million Btu/hr.
reactors In order to treat much tougher feed, including
• Replace existing reactors with a single large 15% DAO in the feed, it was necessary to increase
reactor the hydrogen partial pressure in the unit. The
• Replace existing reactor with a single large primary method was simply to replace the bottle-
reactor and a guard reactor necks that prevented the operation of the unit at
• Reuse existing reactors in parallel and add
single reactor in series. Revamp design feed properties
The first of the four options (two new reactors)
was selected. Considerations that went into the Revamp design feed properties for 60000bpd HPVGO
decision making process not only included the pretreater with 750ppm sulphur in product specification
cost, but also the ease of catalyst loading and
unloading during operation. By replacement of Composition Units Design
Deasphalted oil %vol. 15
the existing two reactors with two larger diame- Lube aromatic extract %vol. 10
ter reactors, the reactor volume was more than Heavy VGO %vol.
doubled. 66
Unit hydraulic limitations had to be overcome Light VGO %vol 10

due to the 50% increase in the feed rate. The Properties
first item was the feed pumps. The unit had Gravity °API 20
three feed pumps, one for each train and a Sulphur %wt. 2.4
shared spare. New impellers were added to each Nitrogen Wppm 1070
Metals, Ni + V Wppm 3.3
pump. The recycle and makeup gas compressors Ramsbottom carbon res %wt. 1.4
were inadequate for the revamp conditions. The Distillation, % °F
existing compressors were replaced with two IBP/30/50 539/759/849
new 70% capacity reciprocating machines. 70/90/FBP 943/1131/1308
It was envisaged that both compressors would
be operating but one would be only 50% loaded. Table 1

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addition, with the replacement of the recycle gas
compressors, higher treat gas rates were main-
tained, which minimised the impact of the higher
hydrogen consumption on the hydrogen partial
pressure at the lag reactor outlet. The presence
of the recycle gas scrubber also helped maintain
higher hydrogen partial pressures in the reactor
system.
One of the requirements of the revamp was to
maintain operation of one train while catalyst
change-out activity takes place in the other train.
This involved re-piping and addition of isolation
valves. Due to the addition of the isolation
valves, relief valves also needed to be added at
appropriate locations.
Due to the higher rates and higher conversion
of the sulphur and nitrogen in the feed to hydro-
Figure 2 New reactor in fabrication shop prior to delivery gen sulphide and ammonia, much higher content
of ammonium bisulphide is produced and higher
the design pressure of 1500psi. The second quantities of wash water are required. The
requirement was to increase the makeup gas targeted sour water ammonium bisulphide
purity and increase the gas bleed rate from the concentration was set at 4%, requiring replace-
high-pressure loop. Since hydrogen was in short ment of the wash water pumps. Additional
supply, adding a membrane hydrogen recovery instrumentation was also added at the injection
unit and increasing the capacity of the make-up points to ensure proper flow distribution to each
compressor to handle the higher make-up rates bay.
met both of these requirements. Additionally,
the high-pressure piping was rerouted to allow Project time line
addition of higher purity makeup gas selectively Conceptual studies began in early 1998 with the
at the lead reactor inlet while the quench gas observation that Catlettsburg could improve FCC
requirement was preferentially supplied by the economics by processing a higher percentage of
lower purity recycle gas. This improved the FCC feed at a higher severity than the existing
reactor average hydrogen partial pressure. In 80% desulphurisation target. A parallel project
to streamline Catlettsburg was underway and
when gasoline sulphur regulation projects were
added, it became clear that there was synergy
between the projects. Formulation of the concept
of the combined project began in 2000, and
approval to proceed with engineering was
obtained in February 2001. The kickoff meeting
was held with Haldor Topsoe in March 2001,
and MAP rapidly moved into front end engineer-
ing design (FEED) with Fluor.
Because compressors and reactors are known
to be long lead-time issues, the official ordering
date for the reactors was December 2001. The
compressors were ordered from MAP’s alliance
partner, Dresser-Rand, in November 2001. The
reactors (Figure 2) were shipped in August 2002,
from the Far East and were erected in October
Figure 3 Final reactor configuration incorporates two- and loaded with catalyst in March 2003.
reactor design (lead and lag reactor) for each train Almost all of the new equipment was

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fabricated and installed (even the
catalyst was loaded early) with the old 700
equipment operating. The old cat
690
feed unit was shut down in May 2003, TC 1
and tie-ins to the new equipment 680 TC 2

Temperature, °F
TC 3
were accomplished in the time 670 TC 4
normally required for a catalyst TC 5
660 TC 6
change. Sulphiding and startup took TC 7
Bed 3
place in June 2003. Startup and 650 TC 8
normal operation were attained with Bed 2 TC 9
640 Bed 1 TC 10
few problems other than plugged TC 11
strainers. A test run at the design 630 Reactor 1 Reactor 2
TC 12
TC 13
conditions was performed in 620
September 2003. 0 20 40 60 80 100
Catalyst, %

Reactor and internals design


As previously indicated, the final reac-
tor configuration selected was a Figure 4 Test run temperature profiles
two-reactor design for each train.
The lead reactor is a two-bed reactor and the lag MAP performed a test run at the design rate of
reactor is a single-bed reactor. Since there are 60000bpsd in September 2003. During the test
two trains, the total number of reactors added is run, the unit was operating at design rate with
four. A picture of the new reactors is shown in close to design feed and at the design conver-
Figure 3. sion. The temperature profiles in the reactor are
The reactors were fabricated by Kobelco and presented in Figure 4 for the first train. Similar
the reactor specifications were provided by observations were made in the second train. The
Haldor Topsoe, who also provided the reactor x-axis shows percent catalyst volume from zero
internals design, including design of the inlet to 100% representing the top of the lead reactor
diffuser, distribution tray, catalyst support gird, to the outlet of the lag reactor. The drop-in
quench section (including quench ring), mixing temperature at 27% represents the quench
chamber and redistribution tray, and the outlet section in the lead reactor and at 58% represents
collector design. Haldor Topsoe also specified the quench in the line between the reactors.
the thermocouple arrangement. The plot shows that the performance of the
The indicator of reactor internals technology is distribution trays is good based on the +5°F
in the performance of the unit. Primary perform- temperature difference at the outlet of the top
ance indicators are the temperature distributions bed and +2°F at the outlet of each reactor. There
in the reactor. Temperature mal-distribution at are 13 temperature measurement points at the
the bottom of the bed will indicate performance outlet of the reactors. The performance of the
of the distribution tray. There are a multitude of quench section is also excellent based on the
reasons that can cause temperature maldistribu- radial temperature difference of +1°F at the inlet
tion at the outlet of a reactor bed, including poor of the second bed.
reactor internals.
However, good temperature profiles observed Benefits
at the outlet of reactor beds indicate good Expectations for the FCC pretreatment projects
performance of the distribution trays. The more were to significantly improve FCC gasoline yield
temperature measurements at the outlet of each and produce low gasoline sulphur content.
bed, the more confidence there is in the perform- During the design, pilot plant tests were
ance of the distribution tray. performed to confirm these expectations.
The performance of the quench section is Hydrotreating pilot plant tests were performed
obtained by observing the temperature distribu- at Haldor Topsoe’s facility in Denmark as well as
tion at the inlet of the bed downstream of the testing at the Catlettsburg refinery. Both facili-
quench section. ties carried out the testing on similar feed

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agreement with the design basis when corrected
Comparison of pilot plant results and design basis
for feed properties. The design basis, and pilot
Design
plant results obtained from facilities are
Feeds basis Topsoe MAP Test Run presented in Table 2.
°API 20.5 20.5 20.6 21.6 Differences in feedstock properties are prima-
Sulphur, % 2.43 2.69 2.71 1.54 rily due to the lack of availability of the
Nitrogen, ppm 1071 1043 1174 1058
Ni + V, ppm 3.3 2.7 2.6 3.5
post-revamp refinery component streams.
RBC, % 1.4 1.3 – 1.1 Several of these materials were simulated by
Distillation: blending. Pilot plant operating conditions were
5 602 515 517 adjusted based on the experience of the individ-
10 651 590 590
50 849 837 825
ual laboratory in simulating commercial
90 1131 >1151 1114 operations. The differences in results between
laboratories are primarily due to the differences
Operating conditions in operating pressure. The differences in hydro-
Catalyst TK 557 TK 557 TK 557 TK 557
LHSV, hr-1 Base* Base Base Base*
gen partial pressure also accounts for a majority
Temperature, °F 695 690 701 671 of the observed differences in the catalyst desul-
Inlet pressure, psig 1533 1276 970 1560 phurisation and denitrogenation activity.
Hydrogen purity, % 82 100 100 – Confirmation of hydrogen consumption and
H2/HC, SCFB (100% H2) 2438 2089 2265 2458
total liquid yield was excellent.
Chemical H2 The pilot FCC tests were the first opportunity
consumption, SCFB 610 617 614 to validate predicted relationships between FCC
feed and product sulphur, and to verify the yield
Total liquid product Stripper
properties bottoms benefits of the conversion. Additional pilot tests
Yield, wt% 98.0 97.8 97.7 96.6 were performed on the LPVGO unit and prod-
°API 26.5 27.3 27.5 27.3 ucts from both units were blended in anticipated
Sulphur, ppm 713 721 753 640 mass balance proportions to provide FCC pilot
Nitrogen, ppm 247 194 288 276
feedstocks. These blends averaged 700ppm
*Equivalent TK 557 activity basis. sulphur, with a range of 670-730, compared to a
design-basis FCC feed sulphur level of 660ppm.
Pilot FCC gasoline yields were excellent, with
Table 2 yields at the “knee” exceeding 67 vol% and gaso-
line selectivities well above 80%.
utilising Topsoe’s TK-557 tri-metallic high activ- The difference between the design point and
ity NiCoMo desulphurisation/denitrogenation the curve is primarily due to light material in the
catalyst. The Catlettsburg tests were designed to feeds (gasoline components produced in the
produce a quantity of feedstock for FCC pilot hydrotreating step were not removed from the
plant testing. Hydrotreating results were remark- feed). The pilot data also confirm the design
ably similar between the pilot plants and in good value for location of the gasoline knee. The knee
Gasoline sulphur, ppm

45
Gasoline yield, vol%

70 Design
40
68
35
66
64 Design 30

62 25
60 20
74 76 78 80 82 84 79 79.5 80 80.5 81 81.5 82
Conversion, wt% Conversion, wt%

Figure 5 Pilot FCC gasoline yields at the “knee” Figure 6 High severity hydrotreating produces gasoline
exceeding 67 vol% and gasoline selectivities well above well below 40ppm sulphur, even at high conversion
80% levels

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20 70
Feed
60
15 Product
Sulphur, ppm

Composition, wt%
50
10 40
Benzo
thiophene 30
5
Thiophene 20
0 10
RSH Sulphide Methyl Mt Bz
thiophene thiophene 0
Saturates 1 Ring 2 Ring 3 Ring 4 Ring Polars

Figure 7 Sulphur speciation values for the pilot plant Figure 8 Aromatics conversion data
test at the gasoline knee

is relatively flat, as shown in Figure 5, which of the test run were to validate hydraulic capa-
should provide good operability for the FCC in bility of the unit at the 60000bpd revamp rate
this region with limited sensitivity to minor and to verify that 750ppm sulphur product
changes in operating variables. would be produced at design conditions.
FCC gasoline sulphur design for the project Overall results are shown in the right-hand
was slightly over 40 ppm. All of the pilot gaso- column of Table 2, under Test Run, compared to
line data were below 40 ppm, even though the the earlier design and pilot plant information.
feedstock had more sulphur than design (700 vs Feed sulphur was lower than desired due to a
660ppm). As shown in Figure 6, this is a strong larger proportion of sweet crude in the crude
confirmation that FCC gasoline sulphur can slate, but high rates of DAO were processed. A
confidently be prepared at these levels with high full 60000bpd feed rate was attained, resulting
severity hydrotreating. in product sulphur of 640ppm at a relatively low
To further confirm the sulphur values, sulphur 671°F weighted average bed temperature
speciation was performed by GC–AED in the (WABT). The test run showed the normalised
Catlettsburg laboratories. Figure 7 shows the desulphurisation and denitrogenation activity of
sulphur speciation values for the pilot plant test the catalyst was higher than the design.
at the gasoline knee. Few mercaptans, sulphides, The maximum capacity of the unit was tested
and/or thiophenes were present. These materi- and the bottleneck was found to be the feed
als may, at least in part, be recombinant products pump motors at a rate of 61000bpsd. This issue
that are a function of H2S partial pressure, resi- is under evaluation. It is believed that kinetically
dence time and reactor effluent cooling curves. the revamped unit will be able to process signifi-
The data demonstrate that for a unit with low cantly more than the 60000 bpd design rate.
residence time and H2S partial pressures, these Aromatics conversion data are good indica-
values should be low. tions of FCC performance improvement. As
Benzothiophenes are also remarkably low and shown in Figure 8, multi-ring aromatics are
significant levels of sulphur compounds only converted roughly at a 50% conversion rate, with
begin to occur with methyl benzothiophenes and the saturation products resulting in increases in
heavier compounds. This provides the refiner one-ring aromatics and saturates. A total
with yet another control point in case of hydrot- aromatics saturation rate (increase in paraffins)
reater upsets. Even with high severity of 9% is excellent, as most one-ring species are
hydrotreating, EP control can be used for prod- difficult to saturate with a base metal catalyst.
uct sulphur adjustment if needed. Not all of the refinery projects have been
completed in time to provide commercial results
Test run at 60000bpd on the new units at the design conditions.
An acceptance test run was performed on 30 However, interim operations on the HPVGO
September 2003. A post-refinery revamp feed- when providing about 90 percent of the feed to
stock was not available since all of the overall the old FCC resulted in:
project changes had not been accomplished, so a • Dramatic shift in yields with a 2.5 vol%
simulated feed was used. The primary objectives increase in gasoline, 4.2 vol% increase in

www.digitalrefining.com/article/1000155 PTQ Q2 2004 7


saturate C4s, and a 0.9 vol% increase in saturate Raj Patel is a principal hydroprocessing specialist for Haldor
C3s Topsoe Inc at Orange, California, USA, where he is responsible
• An overall increase in conversion of over 5 for project management and process design for licensed
vol% and a 1.5 vol% increase in volume gain hydroprocessing projects. He has been working in the
• Overall 0.5 vol% increase in propylene with hydroprocessing field for 22 years. He has an MS degree in
chemical engineering from Stanford University and MBA from
the same butylene yield
California State University in Fullerton.
• Cracked gasoline octane was down 1.5 research
Email: rhp@topsoe.com
octane number clear (RONC) for the same reac- Howard F Moore is a principal engineer with Marathon Ashland
tor temperature. Gasoline RONC has been Petroleum LLC in Catlettsburg, Kentucky, USA. He is the
between 91.5 and 92.0 RONC hydroprocessing technologist for MAP, responsible for oversight,
• Slurry make is down 1.6 vol% expert services, and best practices for all hydroprocessing units
• Light cycle oil (LCO) yield is down 4 vol% with in MAP’s refineries. Before formation of the joint venture, he was
LCO gravity declining from 19.5 to 17.5 with a 2 manager, process R&D, for Ashland Petroleum Company. He has
cetane index decrease MS and BS degrees in chemical engineering from the University
• Higher activity FCC catalyst was utilised to of Kentucky.
allow the regenerator temperature to stay above Harrell L Duff is a principal engineer with Marathon Ashland
Petroleum in Catlettsburg. He works in the asset development
minimum.
group and is responsible for development of large capital
Finally, the most recent operations on the
projects, primarily for the Catlettsburg refinery. Before formation
HPVGO and the existing FCC have been at high of the joint venture, he was the process technologist for Ashland
severity due to plant requirements/constraints Petroleum Company. He has a BS degree in chemical engineering
incurred during the RCC conversion. FCC gaso- from the University of Missouri at Rolla.
line sulphur levels have been as low as 15ppm, Brian Hamari is a refining engineer with Marathon Ashland
although gasoline EP during this period is only Petroleum. He is responsible for monitoring and optimisation of
on the order of 360°F. various process units at the Catlettsburg refinery. He holds a BS
degree in both chemical engineering and business administration
Acknowledgements from Michigan Technological University.
The authors wish to thank Marathon Ashland Petroleum LLC
and Haldor Topsoe AS for permission to release these data. The
contributions of Harrell Duff, Glen Puzey and Mike Skurka are
Links
gratefully acknowledged for their contributions of data, evaluation
and critique. Pilot plant data was provided by Don O’Donnell More articles from the following categories:
and Ron Cordle of MAP, and Per Zeuthen and Angelica Vivas of Fluid Catalytic Cracking
Topsoe. Fluor was the design and construction contractor for the Revamps, Shutdowns and Turnarounds
project, and their contributions to the successful project also are
appreciated.

7 PTQ Q2 2004 www.digitalrefining.com/article/1000155

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