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25 Macro & Micro Inspection
25 Macro & Micro Inspection
2 Micro-examination
This is performed on samples either cut to size or mounted in a resin mould.
The samples are polished to a fine finish, normally one-micron diamond
paste and usually etched in an appropriate chemical solution prior to
examination on a metallurgical microscope. Micro-examination is performed
for a number of purposes, the most obvious of which is to assess the
structure of the material. It is also common to examine for metallurgical
anomalies such as third phase precipitates, excessive grain growth, etc.
Many routine tests such as phase counting or grain size determinations are
performed in conjunction with micro-examinations.
Metallographic weld evaluations can take many forms. In its most simple
form, a weld deposit can be visually examined for large-scale defects such
as porosity or lack of fusion defects. On a microscale, the examination can
take the form of phase balance assessments from weld cap to weld root or a
check for non-metallic or third phase precipitates. Examination of weld
growth patterns is also used to determine reasons for poor mechanical test
results. For example, an extensive central columnar grain pattern can cause
a plane of weakness giving poor Charpy results.