Nama : Rizki Nurjanah

NIM : 061830400285
Kelas : 4 KA
Dosen Pengampu : Dr.Ir.H.Muhammad Yerizam,M.T.
OPERASI TEKNIK KIMIA 1
28 Juli 2020
1. A slury of flake soybens weighing a total of 100 kg contains 75 kg of inert solids and 25 kg
of solution with 100 wt % oil and 90 wt % solvent hexane. This slurry is contacted with 100
kg of pure hexane in a single stage so that the value of N for the outlet underflow is 1,5 kg
insoluble solid/kg solution retained. Calculate the amounts and compositions of the overflow
V1 and the underflow L1 leaving the stage
2. A treated ore containing inert solid gangue and copper sulfate is to be leached in counter
current multistage extractor using pure water to leach the CuSO4. The solid charge rate per
hour consists of 10000 kg of inert gangue (B), 1200 kg of CuSO4 (solute A), and 400 kg of
water (C). The exit wash solution is to contain 92 wt% water and 8 wt% CuSO4. A total of
95% of the CuSO4 in the inlet ore is to be recovered. The underflow is constant at N = 0,5 kg
inert gangue solid/kg aqueous solution.calculate the number of stage required.
JAWABAN

1. Jumlah dan komposisi dari overflow V1 and underflow L1 meninggalkan stage masing-
masing 75kg dan 125kg

Penyelesaian :
Kita misalkan

A= solvent (hexane)

B= solid (inert solid)

C= solvent (oil)

= massa solvent + massa minyak (i.e A+C)

Fase Umpan:
Total umpan (yaitu slurry of flakes soybeans) = 100kg
B= mass of solid =75 kg
 F= massa solvent + massa minyak (i.e A+C)

= 25kg

Rasio massa minyak terhadap larutan =

masssa minyak (C) =25 × 0.1 wt = 2.5kg

massa hexane di dalam umpan = 25 × 0.9 =22.5kg + 2.5 =25kg

Oleh karena itu =

= 0.1

Rasio massa padat terhadap larutan

=3

Fase pelarut (solvent):

C= Massa minyak = 0 kg

A= Massa hexane = 100kg

mass of solutions = A+C = 0+100kg

pelarut (solvent ) = 100kg

Underflow:
underflow = L₁ = ???

L₁ = E₁ + B

nilai N untuk outlet dan underflow adalah 1.5 kg

yaitu N₁ =

solution in underflow E₁ = Mass (A+C)

Overflow:
Overflow = V₁ = ???

solution in overflow V₁ = Mass (A+C)

ini karena , B = 0 di dalam overflow

 Neraca massa solid : ( Karena solid adalah inert, Maka bisa dikatakan sama di dalam

umpan (feed) dan underflow )

solid dalam umpan = solid dalam underflow = 75

75= E₁ × N₁

75 = E₁ × 1.5

E₁ = 50kg

Underflow L₁ = E₁ × B

= 50 + 75

=125kg
Neraca massa total : Umpan + Solven = underflow + overflow

100 + 100 = 125 + V₁

V₁ = 75kg

2. Diketahui :
B (gangue inert) = 10000 Kg/h
A (solute CuSO4 ) = 1200 Kg
C (air) = 400 Kg
Ditanya : Jumlah stage yang dibutuhkan

Jawab :

L0 = 1200 kg/jam

yA0 = 1

B = 10000 kg/jam

N0 = 10000 / 1200 = 8.33 kg insoluble solid/kg solution

VN+1 = 400 kg, xAN+1 = 0, xCN+1 = 1

L0 + VN+1 = LN + V1 = M …(1)

M = 1200 kg/jam + 400 kg/jam = 1600 kg/jam

L0 . yA0 + VN+1 . xAN+1 = M . xAM …(2)

1200 (1) + 400 (0) = 1600 . xAM

xAM = 1.33

B = N0 . L0 = NM . M … (3)

8.33 (1200) = NM . 1600

NM = 6.2475