Date and time: 04/08/2021 10:47:15

Operator: Administrator
Workstation: HPG2-PC
NIRWare version: 1.5
Instrument: NIRFlex N500 Measurement cell: Solids
Instrument serial No.: 1000250955 Cell serial No.: 1000250952
No. of scans: 32
Application: RM & Feed Ruminant, Pig, Sheep, Goat,Horse
Version: 5 GUID: {A73A8D3A-4EB6-4E62-8378-7D016D6750E3} State: not approved
Jenisa Sample tepung ikan
AnalysisID 058/PO/04/2021 (Tepung Ikan)

1 tepung ikan_058/PO/04/2021 Value Residual

(Tepung
Ikan)_2021-04-08_10-46-35

1 20.04 % ^^
ok
x 0.003939 ok

2 20.02 % ^^
ok
x 0.004043 ok

n: 2
Moisture 20.03 % vok
^^
v^v
x ok StdDev: 0.014

1 3.76 % ok
x 0.004002 ok

2 3.59 % ok
x 0.004097 ok

n: 2
Fat 3.68 % vok
xv
v ok StdDev: 0.120

1 21.22 % ok
x 0.003689 ok

2 21.64 % ok
x 0.003775 ok

n: 2
Protein 21.43 % vok
xv
v ok StdDev: 0.297

1 13.09 % ok
x 0.000478 ok

2 13.82 % ok
x 0.000491 ok

n: 2
Ash 13.46 % vok
xv
v ok StdDev: 0.516

1 7.44 % ok
x 0.000189 ok

2 7.56 % ok
x 0.000196 ok

n: 2
Fibre 7.50 % vok
xv
v ok StdDev: 0.085

1 19.83 % ok
x 0.003337 ok

2 19.58 % ok
x 0.003429 ok

n: 2
Neutral Detergent Fibre 19.70 % vok
xv
v ok StdDev: 0.177

1 28.92 % ok
x 0.003413 ok

2 29.82 % ok
x 0.003500 ok

n: 2
Starch 29.37 % vok
xv
v ok StdDev: 0.636

1 1.14 % ok
x 0.004855 ok

2 1.15 % ok
x 0.004949 ok

n: 2
Phosphorus 1.14 % vok
xv
v ok StdDev: 0.007

1 4.36 % ok
x 0.000157 ok
x

2 4.40 % ok
x 0.000163 ok
x

Printed: 04/08/2021 10:54:37 Page 1 of 6

C:\Program Files\Buchi\NIRSolutions\Report\Buchi.Operator.ResultQuantitative.rpt
 Acid Insoluble Ash vok
^^
v^v
x ok
x

1 1.07 % ok
x 0.002360 ok
x

2 1.12 % ok
x 0.002395 ok
x

Alanine vok
^^
v^v
x ok
x

1 0.69 % ok
x 0.005693 ok

2 0.74 % ok
x 0.005780 ok

n: 2
Arginine 0.72 % vok
xv
v ok StdDev: 0.035

1 2.04 % ok
x 0.006515 ok

2 2.15 % ok
x 0.006640 ok

n: 2
Aspartic acid 2.10 % vok
xv
v ok StdDev: 0.078

1 0.34 % ok
x 0.000535 ok
x

2 0.35 % ok
x 0.000542 ok
x

Cystine vok
^^
v^v
x ok
x

1 0.86 % ok
x 0.000020 ok

2 0.94 % ok
x 0.000020 ok

n: 2
Glycine 0.90 % vok
xv
v ok StdDev: 0.057

1 3.14 % ok
x 0.005509 ok
x

2 3.08 % ok
x 0.005591 ok
x

Glutamic Acid vok

^^
v^v
x ok
x

1 0.24 % ok
x 0.003793 ok

2 0.27 % ok
x 0.003827 ok

n: 2
Hystidine 0.26 % vok
xv
v ok StdDev: 0.021

1 1.01 % ok
x 0.002542 ok
x

2 1.02 % ok
x 0.002565 ok
x

Isoleucine vok
^^
v^v
x ok
x

1 1.86 % ok
x 0.004051 ok

2 1.88 % ok
x 0.004064 ok

n: 2
Leucine 1.87 % vok
xv
v ok StdDev: 0.014

1 0.94 % ok
x 0.000693 ok
x

2 1.05 % ok
x 0.000704 ok
x

Lysine vok
^^
v^v
x ok
x

1 0.61 % ok
x 0.000735 ok

2 0.59 % ok
x 0.000748 ok

n: 2
Methionine 0.60 % vok
xv
v ok StdDev: 0.014

1 0.94 % ok
x 0.002317 ok
x

2 0.93 % ok
x 0.002350 ok
x

Phenylalanine vok
^^
v^v
x ok
x

1 1.51 % ok
x 0.006468 ok

2 1.47 % ok
x 0.006595 ok

n: 2
Proline 1.49 % vok
xv
v ok StdDev: 0.028

1 1.11 % ok
x 0.006654 ok

2 1.11 % ok
x 0.006750 ok

Printed: 04/08/2021 10:54:37 Page 2 of 6

C:\Program Files\Buchi\NIRSolutions\Report\Buchi.Operator.ResultQuantitative.rpt
 n: 2
Serine 1.11 % vok
xv
v ok StdDev: 0.000

1 1.05 % ok
x 0.000740 ok
x

2 1.05 % ok
x 0.000750 ok
x

Threonine vok
^^
v^v
x ok
x

1 0.21 % ok
x 0.002948 ok

2 0.23 % ok
x 0.002967 ok

n: 2
Tryptophan 0.22 % vok
xv
v ok StdDev: 0.014

1 1.44 % ok
x 0.002375 ok

2 1.44 % ok
x 0.002399 ok

n: 2
Tyrosine 1.44 % vok
xv
v ok StdDev: 0.000

1 1.46 % ok
x 0.000854 ok

2 1.48 % ok
x 0.000868 ok

n: 2
Valine 1.47 % vok
xv
v ok StdDev: 0.014

1 26.70 % ok
x 0.000777 ok
x

2 26.28 % ok
x 0.000787 ok
x

ADF vok
^^
v^v
x ok
x

1 -1.44 % x 0.002581 ok
x

2 -1.49 % x 0.002611 ok
x

Calcium vok
^^
v^v
x ok
x

Printed: 04/08/2021 10:54:37 Page 3 of 6

C:\Program Files\Buchi\NIRSolutions\Report\Buchi.Operator.ResultQuantitative.rpt
 Calibration
Moisture Calibration name: Moisture-Feed-09-14 Version: 1

Calibration range: 4.60 - 16.06 [%] Method: PLS

Action range: 4.60 - 16.06 [%] SEP: 0.451237

Warning range: 4.60 - 16.06 [%] Bias: 0.000000

Max. Residual: 0.013585 Slope: 1.000000

GUID: {B48788FC-ECD9-4602-85EB-36ADC6A0629D}

Fat Calibration name: Fat-Feed-09-14 Version: 1

Calibration range: 0.20 - 16.10 [%] Method: PLS

Action range: 0.20 - 16.10 [%] SEP: 0.419541

Warning range: 0.20 - 16.10 [%] Bias: 0.000000

Max. Residual: 0.013452 Slope: 1.000000

GUID: {3B74CA1E-3142-413A-82B8-0E282CEF1B5E}

Protein Calibration name: Protein-Feed-09-14 Version: 1

Calibration range: 1.34 - 68.58 [%] Method: PLS

Action range: 1.34 - 68.58 [%] SEP: 0.744332

Warning range: 1.34 - 68.58 [%] Bias: 0.000000

Max. Residual: 0.015801 Slope: 1.000000

GUID: {8393209B-B9AF-4542-93B2-6FA1183FCB02}

Ash Calibration name: Ash-Feed-09-14 Version: 1

Calibration range: 1.20 - 36.70 [%] Method: PLS

Action range: 1.20 - 36.70 [%] SEP: 1.016663

Warning range: 1.20 - 36.70 [%] Bias: 0.000000

Max. Residual: 0.001268 Slope: 1.000000

GUID: {C18A1162-1EEC-4FBB-9F52-8D18AF4763D1}

Fibre Calibration name: Fibre-Feed-09-14 Version: 1

Calibration range: 0.54 - 32.31 [%] Method: PLS

Action range: 0.54 - 32.31 [%] SEP: 0.654759

Warning range: 0.54 - 32.31 [%] Bias: 0.000000

Max. Residual: 0.001108 Slope: 1.000000

GUID: {86CD8E85-2CE0-49B7-A4CC-1D051B371A57}

Neutral Detergent Fibre Calibration name: NDF-Feed-09-14 Version: 1

Calibration range: 10.18 - 39.21 [%] Method: PLS

Action range: 10.18 - 39.21 [%] SEP: 0.401037

Warning range: 10.18 - 39.21 [%] Bias: 0.000000

Max. Residual: 0.006358 Slope: 1.000000

GUID: {55D3CAEE-B9C2-4640-84C9-F4B8454ACD4A}

Starch Calibration name: Starch-Feed-09-14 Version: 1

Calibration range: 3.93 - 66.87 [%] Method: PLS

Action range: 3.93 - 66.87 [%] SEP: 1.080547

Warning range: 3.93 - 66.87 [%] Bias: 0.000000

Max. Residual: 0.006373 Slope: 1.000000

GUID: {A68F4027-8E23-4539-8ED5-BD8239DB51C9}

Phosphorus Calibration name: Phosphorus-Feed-09-14 Version: 1

Calibration range: 0.16 - 1.59 [%] Method: PLS

Action range: 0.16 - 1.59 [%] SEP: 0.075398

Warning range: 0.16 - 1.59 [%] Bias: 0.000000

Max. Residual: 0.006632 Slope: 1.000000

GUID: {31A5B508-7532-4AD9-BD1A-A4245196EE27}

Acid Insoluble Ash Calibration name: Acid Insoluble Ash-Feed-10-12 Version: 0

Calibration range: 1.70 - 6.45 [%] Method: PLS

Action range: 1.70 - 6.45 [%] SEP: 0.365209

Warning range: 1.70 - 6.45 [%] Bias: 0.000000

Max. Residual: 0.000097 Slope: 1.000000

GUID: {4050B4BC-CF01-4236-BFD4-30073756B89D}

Alanine Calibration name: Alanine-Feed-01-13 Version: 1

Calibration range: 0.03 - 4.58 [%] Method: PLS

Printed: 04/08/2021 10:54:37 Page 4 of 6

C:\Program Files\Buchi\NIRSolutions\Report\Buchi.Operator.ResultQuantitative.rpt
 Action range: 0.03 - 4.58 [%] SEP: 0.070401

Warning range: 0.03 - 4.58 [%] Bias: 0.000000

Max. Residual: 0.001783 Slope: 1.000000

GUID: {7684A560-62A5-47D8-BC8A-B1FB14CC69EC}

Arginine Calibration name: Arginine-Feed-01-13 Version: 1

Calibration range: 0.23 - 6.12 [%] Method: PLS

Action range: 0.23 - 6.12 [%] SEP: 0.243210

Warning range: 0.23 - 6.12 [%] Bias: 0.000000

Max. Residual: 0.014606 Slope: 1.000000

GUID: {084D8E77-3D59-4449-B916-70FE0D3ADC57}

Aspartic acid Calibration name: Aspartic-Acid-Feed-01-13 Version: 1

Calibration range: 0.09 - 8.44 [%] Method: PLS

Action range: 0.09 - 8.44 [%] SEP: 0.324546

Warning range: 0.09 - 8.44 [%] Bias: 0.000000

Max. Residual: 0.007997 Slope: 1.000000

GUID: {6AA1CB6E-98E8-4F18-B656-4501FC33C16E}

Cystine Calibration name: Cystine-Feed-01-13 Version: 2

Calibration range: 0.05 - 2.84 [%] Method: PLS

Action range: 0.05 - 2.84 [%] SEP: 0.083462

Warning range: 0.05 - 2.84 [%] Bias: 0.000000

Max. Residual: 0.000514 Slope: 1.000000

GUID: {C26631FF-C009-4E6C-8AD4-00CA9BFF44ED}

Glycine Calibration name: Glycine-Feed-01-13 Version: 1

Calibration range: 0.06 - 4.84 [%] Method: PLS

Action range: 0.06 - 4.84 [%] SEP: 0.100994

Warning range: 0.06 - 4.84 [%] Bias: 0.000000

Max. Residual: 0.000024 Slope: 1.000000

GUID: {25132A94-431A-45F8-B6B2-E5E4F2CCB06E}

Glutamic Acid Calibration name: Glutamic acid-Feed-01-13 Version: 1

Calibration range: 0.22 - 29.56 [%] Method: PLS

Action range: 0.22 - 29.56 [%] SEP: 0.340717

Warning range: 0.22 - 29.56 [%] Bias: 0.000000

Max. Residual: 0.005422 Slope: 1.000000

GUID: {7D51E061-3BAA-4E7E-8611-8C31C509EBA4}

Hystidine Calibration name: Hystidine-Feed-01-13 Version: 1

Calibration range: 0.13 - 3.48 [%] Method: PLS

Action range: 0.13 - 3.48 [%] SEP: 0.173173

Warning range: 0.13 - 3.48 [%] Bias: 0.000000

Max. Residual: 0.006469 Slope: 1.000000

GUID: {403B6E7C-AC31-4D12-9702-43C5B8DCAAFA}

Isoleucine Calibration name: Isoleucine-Feed-01-13 Version: 1

Calibration range: 0.04 - 4.81 [%] Method: PLS

Action range: 0.04 - 4.81 [%] SEP: 0.107470

Warning range: 0.04 - 4.81 [%] Bias: 0.000000

Max. Residual: 0.002259 Slope: 1.000000

GUID: {7F158BD8-9A18-4C40-BE4B-497570203DDC}

Leucine Calibration name: Leucine-Feed-01-13 Version: 1

Calibration range: 0.77 - 8.65 [%] Method: PLS

Action range: 0.77 - 8.65 [%] SEP: 0.152363

Warning range: 0.77 - 8.65 [%] Bias: 0.000000

Max. Residual: 0.004935 Slope: 1.000000

GUID: {5182E8EA-0FA2-44E4-ADC1-3252A0FAE261}

Lysine Calibration name: Lysine-Feed-09-13 Version: 1

Calibration range: 0.05 - 7.89 [%] Method: PLS

Action range: 0.05 - 7.89 [%] SEP: 0.227895

Warning range: 0.05 - 7.89 [%] Bias: 0.000000

Max. Residual: 0.000568 Slope: 1.000000

GUID: {1C088AFD-DC78-415F-AB03-411ED60FECC8}

Methionine Calibration name: Methionine-Feed-01-13 Version: 1

Calibration range: 0.14 - 2.05 [%] Method: PLS

Printed: 04/08/2021 10:54:37 Page 5 of 6

C:\Program Files\Buchi\NIRSolutions\Report\Buchi.Operator.ResultQuantitative.rpt
 Action range: 0.14 - 2.05 [%] SEP: 0.051369

Warning range: 0.14 - 2.05 [%] Bias: 0.000000

Max. Residual: 0.000846 Slope: 1.000000

GUID: {8EADAA52-50B5-4C05-ACED-6A49A1EF0FA0}

Phenylalanine Calibration name: Phenylalanine-Feed-01-13 Version: 1

Calibration range: 0.03 - 6.55 [%] Method: PLS

Action range: 0.03 - 6.55 [%] SEP: 0.100573

Warning range: 0.03 - 6.55 [%] Bias: 0.000000

Max. Residual: 0.002183 Slope: 1.000000

GUID: {7FBBCF92-8645-4C62-9F20-EE1BDCCCFCD4}

Proline Calibration name: Proline-Feed-01-13 Version: 1

Calibration range: 0.61 - 12.84 [%] Method: PLS

Action range: 0.61 - 12.84 [%] SEP: 0.254579

Warning range: 0.61 - 12.84 [%] Bias: 0.000000

Max. Residual: 0.006723 Slope: 1.000000

GUID: {B6BC9DD6-1899-4F46-81E6-4AA02327A002}

Serine Calibration name: Serine-Feed-01-13 Version: 3

Calibration range: 0.04 - 5.31 [%] Method: PLS

Action range: 0.04 - 5.31 [%] SEP: 0.099997

Warning range: 0.04 - 5.31 [%] Bias: 0.000000

Max. Residual: 0.012202 Slope: 1.000000

GUID: {CCB18FB5-689F-489A-AA09-4A1FDE16182A}

Threonine Calibration name: Threonine-Feed-01-13 Version: 1

Calibration range: 0.03 - 5.34 [%] Method: PLS

Action range: 0.03 - 5.34 [%] SEP: 0.089249

Warning range: 0.03 - 5.34 [%] Bias: 0.000000

Max. Residual: 0.000583 Slope: 1.000000

GUID: {AEC40521-40B4-4A14-8A03-73007F9BD1E0}

Tryptophan Calibration name: Tryptophan-Feed-01-13 Version: 1

Calibration range: 0.03 - 1.48 [%] Method: PLS

Action range: 0.03 - 1.48 [%] SEP: 0.043045

Warning range: 0.03 - 1.48 [%] Bias: 0.000000

Max. Residual: 0.004243 Slope: 1.000000

GUID: {BCF21EFF-817D-4A22-ADB8-8F35516C29A2}

Tyrosine Calibration name: Tyrosine-Feed-01-13 Version: 1

Calibration range: 0.17 - 4.99 [%] Method: PLS

Action range: 0.17 - 4.99 [%] SEP: 0.111532

Warning range: 0.17 - 4.99 [%] Bias: 0.000000

Max. Residual: 0.002430 Slope: 1.000000

GUID: {05938F80-E635-46CE-B103-8144D8E180F7}

Valine Calibration name: Valine-Feed-01-13 Version: 1

Calibration range: 0.05 - 5.49 [%] Method: PLS

Action range: 0.05 - 5.49 [%] SEP: 0.159980

Warning range: 0.05 - 5.49 [%] Bias: 0.000000

Max. Residual: 0.001100 Slope: 1.000000

GUID: {F67F6C00-D1AD-4CC5-B1AB-29E8FCC20372}

ADF Calibration name: ADF-Dry Silage-11-14 Version: 1

Calibration range: 16.96 - 55.50 [%] Method: PLS

Action range: 16.96 - 55.50 [%] SEP: 0.881520

Warning range: 16.96 - 55.50 [%] Bias: 0.000000

Max. Residual: 0.000338 Slope: 1.000000

GUID: {CF199764-8381-4EDD-AB3C-DAFD05B9F5E5}

Calcium Calibration name: Calcuim-Dry Silage-11-14 Version: 1

Calibration range: 0.13 - 1.82 [%] Method: PLS

Action range: 0.13 - 1.82 [%] SEP: 0.087143

Warning range: 0.13 - 1.82 [%] Bias: 0.000000

Max. Residual: 0.001425 Slope: 1.000000

GUID: {38316942-83ED-4B1D-93C1-D572CE6D85F4}

Printed: 04/08/2021 10:54:37 Page 6 of 6

C:\Program Files\Buchi\NIRSolutions\Report\Buchi.Operator.ResultQuantitative.rpt