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9500 Premium Series

Benchtop pH/Conductivity Meter


User Manual

PH9500 Benchtop pH Meter

EC9500 Benchtop Conduct ivity Meter

PC9500 Benchtop pH/ Conductivity Meter

APERA INSTRUMENTS, LLC


aperainst.com
1 Introduction ............................................................................................................................................................... - 1 -

1.1 Parameters ..................................................................................................................................... - 1 -

1.2 Basic Features and Functions ........................................................................................................ - 1 -

1.3 Features of pH Measurement ......................................................................................................... - 1 -

1.4 Features of Conductivity Measurement .......................................................................................... - 2 -

2 Technical Specifications ......................................................................................................................................... - 2 -

2.1 Technical Parameters ..................................................................................................................... - 2 -

2.2 Others ............................................................................................................................................. - 3 -

3 Meter Illustration ..................................................................................................................................................... - 3 -

3.1 Main Interface ................................................................................................................................. - 3 -

3.2 Measurement Interfaces ................................................................................................................. - 4 -

3.3 Keypad ........................................................................................................................................... - 6 -


3.3.1 Keypad Operation ........................................................................................................................................................ - 6 -
3.3.2 Function ........................................................................................................................................................................... - 7 -
3.3.3 Manual temperature compensation ...................................................................................................................... - 7 -

3.4 Meter Sockets ................................................................................................................................. - 8 -

3.5 Reading Mode ................................................................................................................................ - 9 -

3.6 Meter Installment .......................................................................................................................... - 10 -


3.6.1 Connect Test-Bench..................................................................................................................................................- 10 -
3.6.2 Install flexible electrode holder .............................................................................................................................- 10 -
3.6.3 How to use Test-Bench............................................................................................................................................- 10 -

3.7 Magnetic Stirrer Operation ........................................................................................................... - 11 -


3.7.1 Technical Specifications ...........................................................................................................................................- 11 -
3.7.2 Operation ......................................................................................................................................................................- 11 -
3.7.3 Notes ..............................................................................................................................................................................- 11 -

4 Meter Setup .............................................................................................................................................................- 11 -

4.1 Setup before Use.......................................................................................................................... - 11 -

4.2 Screen Display Setup ................................................................................................................... - 11 -

4.3 Parameter Settings ....................................................................................................................... - 12 -


4.3.1 Main Menu and Sub-menu ....................................................................................................................................- 12 -
4.3.2 Operation ......................................................................................................................................................................- 13 -
4.3.3 Parameter Settings Content ...................................................................................................................................- 13 -

4.4 Calibration Password .................................................................................................................... - 14 -

5 pH Measurement ...................................................................................................................................................- 14 -

5.1 About pH Calibration .................................................................................................................... - 14 -


5.1.1 Standard pH Calibration Buffer Solutions ..........................................................................................................- 14 -
5.1.2 5-point Calibration ....................................................................................................................................................- 15 -
5.1.3 Calibration Frequency ...............................................................................................................................................- 16 -
5.1.4 Check calibration record..........................................................................................................................................- 16 -
5.1.5 pH Calibration Reminder .........................................................................................................................................- 16 -

5.2 pH Meter Calibration..................................................................................................................... - 16 -

5.3 User-Define Calibration (take 2.00 pH and 7.30 pH as an example) ........................................... - 19 -

5.4 Self-Diagnosis .............................................................................................................................. - 20 -

5.5 Sample Measurement .................................................................................................................. - 21 -

5.6 About pH Measurement................................................................................................................ - 22 -


5.6.1 pH Stability Criterion .................................................................................................................................................- 22 -
5.6.2 pH Reading Alarm......................................................................................................................................................- 22 -
5.6.3 pH Isothermal Measurement Principal ...............................................................................................................- 23 -
5.6.4 Back to Factory Default Settings ...........................................................................................................................- 23 -

5.7 pH Electrode Maintenance ........................................................................................................... - 23 -


5.7.1 Daily Maintenance .....................................................................................................................................................- 23 -
5.7.2 Calibration Solutions .................................................................................................................................................- 24 -
5.7.3 Cleaning.........................................................................................................................................................................- 24 -

6 mV Measurement...................................................................................................................................................- 24 -

6.1 ORP Measurement ....................................................................................................................... - 24 -

6.2 ORP Measurement Notes ............................................................................................................ - 24 -

6.3 ISE Measurement ......................................................................................................................... - 25 -

7 Conductivity Measurement .................................................................................................................................- 25 -

7.1 Conductivity Electrode Information ............................................................................................... - 25 -


7.1.1 Default Electrode ........................................................................................................................................................- 25 -
7.1.2 Conductivity Cell Constant ......................................................................................................................................- 25 -

7.2 Conductivity Calibration Information ............................................................................................. - 25 -


7.2.1 Conductivity Standard Calibration Solutions ....................................................................................................- 25 -
7.2.2 Calibration Frequency ...............................................................................................................................................- 26 -
7.2.3 Check Calibration Record ........................................................................................................................................- 26 -
7.2.4 Conductivity Calibration Reminder ......................................................................................................................- 26 -
7.2.5 Reference Temperature ...........................................................................................................................................- 26 -
7.2.6 Temperature Compensation Coefficient ............................................................................................................- 27 -
7.2.7 Prevent Contamination of Standard Solutions ................................................................................................- 27 -

7.3 Conductivity Meter Calibration (Take 1413μS/cm as an example) .............................................. - 28 -

7.4 User-Define Calibration (Take 10μS/cm as an example) ............................................................. - 29 -

7.5 Self-Diagnosis .............................................................................................................................. - 30 -

7.6 Sample Measurement .................................................................................................................. - 31 -

7.7 TDS and Conductivity ................................................................................................................... - 31 -


7.8 Salinity Types ............................................................................................................................... - 32 -

7.9 Back to Factory Default Settings .................................................................................................. - 32 -

7.10 Conductivity Electrode Maintenance ............................................................................................ - 32 -

8 Data Processing Modes (Save, Recall, Print, Delete) ....................................................................................- 33 -

8.1 Data Processing Flowchart .......................................................................................................... - 33 -

8.2 Log Data in Meter ......................................................................................................................... - 34 -


8.2.1 Setup...............................................................................................................................................................................- 34 -
8.2.2 Data Storage ................................................................................................................................................................- 34 -
8.2.3 Data Logging Modes ................................................................................................................................................- 34 -
8.2.4 Save, Recall, Delete ....................................................................................................................................................- 34 -

8.3 Print Data ...................................................................................................................................... - 35 -


8.3.1 Setup...............................................................................................................................................................................- 35 -
8.3.2 Install Printer ................................................................................................................................................................- 35 -
8.3.3 Printer Information ....................................................................................................................................................- 36 -
8.3.4 Data logging and printing.......................................................................................................................................- 36 -
8.3.5 Delete Data...................................................................................................................................................................- 36 -

8.4 Data logging via PC ...................................................................................................................... - 37 -


8.4.1 Install Software ............................................................................................................................................................- 37 -
8.4.2 Software Interface ......................................................................................................................................................- 37 -
8.4.3 Operation Keys of PC-Link .....................................................................................................................................- 38 -

9 What’s in the Kit .....................................................................................................................................................- 38 -

10 Other Parts and Accessories ...........................................................................................................................- 39 -

11 Warranty ..............................................................................................................................................................- 40 -

Notes
• When the meter is connected to PC, do not pull out the USB cable until
the meter is turned off. Otherwise a system crash could occur. To fix the
crash, pull out the power cord, put it back in, and reboot the meter.
• Please do NOT pull out the power cord when the meter is turned on.
1 Introduction

Thank you for choosing Apera 9500 Premium Series Benchtop pH/Conductivity Meter. Before using this
product, please read this manual carefully.

9500 Series Benchtop Meter is an outstanding combination of advanced electronic technology, sensor
technology and intuitive software design, made for laboratory pH and conductivity measurement in
scientific research and quality control, fully meeting GLP (Good Laboratory Practice) standards.

1.1 Parameters

Measurement parameter PH9500 EC9500 PC9500

pH/mV √ √

Cond./TDS/Salinity/Resistivity √ √

Temperature √ √ √

1.2 Basic Features and Functions


• Large TFT color display with a user-friendly navigation system.
• Self-diagnosis function reminds users of electrode invalidity, incorrect calibration solutions, or
incorrect operation.
• Fully meets GLP (Good Laboratory Practice) Standard. Users can attach a keyboard to set up
calibration password, sample ID, electrode ID, user ID, and company name.
• Users can attach a printer (sold separately) to print out data meeting GLP/GMP standard.

• button to check on the built-in instructions of the meter

• Multi-language operation system, including English, German, Spanish, and Chinese.


• Equipped with a multi-functional Test-Bench, composed of a flexible electrode holder, buffer
organizers, and an intelligent magnetic stirrer.
• A variety of measurement modes for different requirements, including stable display mode, auto. hold
mode, auto. data logging mode, and dial mode
• USB data output for printing and further analysis, auto. data logging in the 9500 PC-Link desktop
software.
• PC9500 meter can measure and display pH & conductivity value at same time.

1.3 Features of pH Measurement


• 1 to 5 points of automatic calibration with calibration instruction and automatic checking functions.
• Automatically recognize pH buffer solution. 3 series buffer solution selectable: USA series, NIST
series and CH series, as well as User-Define solutions (any pH standard solutions).
• pH high/low value alarm function

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1.4 Features of Conductivity Measurement
• 1 to 4 points of automatic calibration with calibration instruction and automatic checking functions.
• Automatically recognize conductivity standard solutions. 2 series standard solution available:
Standard Series and CH Series, as well as User-Define solution (any conductivity standard solutions).
• Measurement modes include conductivity, TDS, salinity, and resistivity.

2 Technical Specifications

2.1 Technical Parameters


Applicable
Technical Parameters
Models
Range -2.000 to 20.000 pH

Resolution 0.1/0.01 /0.001pH

Accuracy ±0.002 pH ±1 digit


pH
Temp. Compensation Range 0 to 100°C (auto. or manual)
PH9500
Calibration Points 1 to 5 points
PC9500
Buffer Series Options USA, NIST, CH, and User-Define

Range ±2000.0mV

mV Resolution 0.1mV

Accuracy ±0.03% F.S ±1 digit

Range 0.00 μS/cm to 2000 mS/cm

Resolution 0.01/0.1/1μS/cm; 0.01/0.1/1 mS/cm

Accuracy ±0.5% F.S ±1 digit

Temp. Compensation Range 0 to 50°C (auto. or manual)


EC9500
Conductivity Cell Constant 0.1/1/10 cm-1
PC9500
Reference Temp. 15 to 30°C (adjustable)
Temp. Compensation
0.00 to 10.00% (adjustable)
Coefficient
Calibration Points 1 to 4 points

Standard Series Options Standard, CH, User-Define

Range 0.00 mg/L to 1000 g/L

Resolution 0.01/0.1/1mg/L; 0.01/0.1/1 g/L


EC9500
TDS Accuracy ±1.0% F.S ±1 digit
PC9500
Temp. Compensation Range 0 to 50°C (auto. or manual)

TDS Factor 0.40 to 1.00 (adjustable)

-2-
Range 0.00 to 100 ppt

Resolution 0.01/0.1 ppt


EC9500
Salinity Accuracy ±1.0% F.S ±1 digit
PC9500
Temp. Compensation Range 0 to 50°C (auto. or manual)

Salinity Type Linear / NaCl / Saltwater

Range 0.00 Ω·cm to 100MΩ·cm


0.1/1 Ω·cm; 0.01/0.1/1KΩ·cm; 0.1
Resolution EC9500
Resistivity MΩ·cm
Accuracy ±1.0% F.S ±1 digit PC9500

Temp. Compensation Range 0 to 50°C (auto. or manual)

Range -10.0 to 110.0°C; 14.0 to 230°F


PH9500
Temperature Resolution 0.1°C; 0.1/1°F EC9500
PC9500
Accuracy ±0.5°C±1 digit

2.2 Others

Data Storage PH9500/EC9500: 1000 groups; PC9500: 2000 groups

Power Supply DC9V/600mA

Dimensions and Weight Meter: (360×235×100) mm / 1.7kg

3 Meter Illustration

3.1 Main Interface


Diagram-1 is the complete pH measurement interface.

Diagram-1

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① Measurement Mode ⑪ Measurement Unit

② pH Measurement ⑫ Auto. Hold

③ mV value of pH electrode ⑬ Stable reading

④ Electrode ID ⑭ Date and time

⑤ Completed calibration(s) ⑮ Current stirring Saved stirring


speed speed

⑥ Sample ID ⑯ Manual data log Auto. data log

⑦ User ID ⑰ Printer

⑧ Used data storage ⑱ Meter memory PC

⑨ Temperature value and unit (°C°F) ⑲ Calibration reminder

Temperature compensation: ATC –


Automatic Temperature Compensation; Alarms of readings exceeding min/max
⑩ ⑳
MTC – Manual Temperature values
Compensation

3.2 Measurement Interfaces

pH Measurement Interface
applicable models: PH9500/PC9500
①-- pH measurement mode
②-- pH measurement
③-- mV value of pH electrode
④-- completed pH calibration(s)
⑤-- Temperature measurement
⑥-- Stable reading
⑦-- Date and time

mV (ORP) Measurement Interface


applicable models: PH9500/PC9500
①-- mV measurement mode
②-- mV measurement
③-- Temperature measurement
④-- stable reading
⑤-- Date and time

-4-
Conductivity Measurement Interface
applicable models: EC9500/PC9500
①-- Conductivity measurement mode
②-- Conductivity measurement
③-- Conductivity parameters (see section 7.1.2,
7.2.5, 7.2.6)
④-- Completed conductivity calibration(s)
⑤-- Temperature measurement
⑥-- Stable reading
⑦-- Date and time

TDS Measurement Interface


applicable models: EC9500/PC9500
①-- TDS measurement mode
②-- TDS measurement
③-- TDS conversion factor (see section 7.7)
④-- Temperature measurement
⑤-- Stable reading
⑥-- Date and time

Salinity Measurement Interface


applicable models: EC9500/PC9500
①-- Salinity measurement mode
②-- Salinity measurement
③-- Salinity type (see section 7.8)
④-- Temperature measurement
⑤-- Stable reading
⑥-- Date and time

Resistivity Measurement Interface


applicable models: EC9500/PC9500
①-- Resistivity measurement mode
②-- Resistivity measurement
③-- Temperature measurement
④-- Stable reading
⑤-- Date and time

pH/Conductivity Measurement Interface


applicable models: PC9500
①-- pH/conductivity measurement mode
②-- pH stable reading
③-- pH measurement
④-- Temperature for pH
⑤-- Completed pH calibration(s)
⑥-- Completed conductivity calibration(s)
⑦-- Temperature for conductivity
⑧-- Conductivity measurement
⑨-- Conductivity stable reading
⑩-- Date and time

-5-
3.3 Keypad

Diagram-2

3.3.1 Keypad Operation


Short press – Press key and hold for less than 2 seconds, buzzer makes a beep;
Long press – Press key and hold for more than 2 seconds, buzzer makes a beep when short pressing
the button, another beep will ring after holding the key for 2 seconds.

Table-1 Keypad Operation and Functions

Key Operation Functions

Short
press ● Power on/off

Press to switch among different measurement modes:


Short ● PH9500:pH→mV
press ● EC9500: Conductivity→TDS→Salinity→Resistivity
● PC9500: pH→mV→Conductivity→TDS→Salinity→pH/conductivity

Long
press ● Enter manual temperature compensation

Long
press ● In measurement mode, press to enter calibration

Short
press ● End all current operations and go back to measurement mode

-6-
• In measurement mode: press to enter parameter set-up main menu;
• In calibration mode: press to perform calibration;
• In main menu: press to enter submenu;
Short
press • In submenu: press to enter parameter set-up;
• In parameter set-up mode: press to confirm parameter;
• In manual temperature compensation: press to confirm temperature
value.

• In measurement mode: press key to store measurements,


• press key to recall saved data;
Short
press
• In recall (RM) mode: press or key to turn pages;
• In menu mode: press key to select items;
• In manual temperature compensation: press to change temperature
value, hold the key for fast changing.

Short
• Check quick guide
press

Short
• Turn on/off magnetic stirrer
press

Long
• Save the current stirring speed
press

Short
• Switch between current speed and the saved speed
press

Short
• Press to change stirring speed. Hold the key to change speed quickly.
press

3.3.2 Function
Press key to check the quick user guide of the meter,
including keypad operation information, icon information,
calibration illustration, calibration notes, electrode
maintenance, parameter settings, etc. Diagram-3 is the
index of content, which is only in English or Simplified
Chinese.

3.3.3 Manual temperature compensation


When no temperature probe is connected to the meter, long press to enter manual temperature
compensation mode. Press or to adjust temperature value. Hold the key to quickly
change values. Short press to confirm and go back to measurement mode.

-7-
3.4 Meter Sockets

Diagram-4
Table - 2 Meter Sockets Information
Socket Type Information

① BNC Connect pH or ORP combination electrode

② Ф2 power supply Connect magnetic stirrer

③ RCA Connect temperature sensor (for pH)

④ USB Connect printer

⑤ USB Connect PC

⑥ Ф4 banana Connect reference electrode

⑦ BNC Connect conductivity electrode

⑧ RCA Connect temperature sensor (for conductivity)

⑨ USB Connect keyboard

⑩ Ф2.5 power supply Connect DC9V adaptor

-8-
3.5 Reading Mode

3.5.1 Stable Reading Mode


When reading is stable, shows up. If you don’t see
the smiley face or it’s flashing, it means the reading is not
fully stabilized and it’s not the right timing to record or
calibrate.

3.5.2 Auto. Hold Mode


Choose “on” in parameter setting 4.6 to turn on Auto. Hold
mode. When stays on for more than 10 seconds, the
reading will be automatically locked, and HOLD icon will
show up. Short press to unlock.

3.5.3 pH dial display mode


Turn on the pH dial display mode in parameter setting 1.7.
This mode is featured with a vivid, stable, and continuous
display. The bottom right is the digital value.

3.5.4 Auto. timing mode


Setup auto. timing data logger in parameter settings 3.2 to
record measurements in long-term. When connected to
PC, a measurement curve can be formed in the PC-Link
software as shown right.

Note The icon will be displayed when the reading gets stabilized, but the measurement will continue.
When the measured value changes beyond a certain range, the icon will flash or disappear until it
stabilizes again. The stability of the reading is related to many factors:
• Measurement time -- the longer the measurement time, the more stable the icon will be;
• Nature of the test solution – the solution with low ionic strength (such as distilled or deionized water),
or the solution with unstable chemical nature, the measurement will not be easy to stabilize.
• The following three methods will help improve reading stability.
• (a) Turn on Auto. Hold Mode (parameter setting 4.6), refer to section 3.5.2.
• (b) Select the appropriate “pH stability standard” for different test solutions (parameter setting 1.5),
refer to section 5.6.1.
• (c) Select the right pH electrode for each specific application, see section 10.

-9-
3.6 Meter Installment
3.6.1 Connect Test-Bench

Before installment After installment

Test-Bench Meter

Stirrer cable Connecting board

Diagram-5
3.6.2 Install flexible electrode holder

Align the hole and


bar, then press
down with force.
Diagram-6
3.6.3 How to use Test-Bench

(a) Use in a connected manner (b) Use in a separated manner

Diagram-7

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3.7 Magnetic Stirrer Operation
3.7.1 Technical Specifications

Speed Range 0 to 2300 RPM (no load)


Working area diameter Ф100mm
Max. stirring volume 1000mL
3.7.2 Operation
(a) Insert the stirrer cable to the corresponding sockets in meter and stirrer.
(b) Short press to power on stirrer, will show up on the top of the display. Press or to
adjust stirring speed. Short press the key to adjust slowly; Hold the key to adjust quickly. Icon
indicates that the stirrer is powered on and it’s stirring at the current speed.
(c) How to use :After stirring speed is adjusted, hold for about 3 seconds until the buzzer
makes a beep. The adjusted speed is now saved. Next time, if you want to use this saved speed,
just short press , and icon will show up on top.
(d) Switch between two speeds: After saved speed and current speed are adjusted, short press
again to alternate between the saved speed ( ) and the current speed ( )

3.7.3 Notes

• If the bottom surface of the beaker is not flat, it will vibrate or even stop stirring. In this case, replace
a more qualified beaker.
• At zero speed, do not hold button, otherwise zero speed will be stored. If this is the case, just
re-adjust the speed and store it by holding again.

4 Meter Setup

4.1 Setup before Use


Before first-time use, please check the following settings and make adjustments: temperature unit, date
format, date, time, system language, pH resolution, pH buffer series, conductivity standard series, etc.
For details, refer to section 4.3.

4.2 Screen Display Setup


In parameter settings 4.5, choose Simple or Complete display mode. Complete display mode includes
electrode ID, user ID, and sample ID as shown in Diagram-8 (b). For setting up ID, refer to section 8.3.3-
(c).

(a) Simple Display Diagram-8 (b) Complete Display


- 11 -
4.3 Parameter Settings
4.3.1 Main Menu and Sub-menu
Main Menu pH sub-menu

Conductivity/TDS sub-menu

Data management Sub-menu

Settings Sub-menu

Diagram-9

- 12 -
4.3.2 Operation
For detailed operation, please follow the instruction at the bottom of screen.
4.3.3 Parameter Settings Content
Main
# Parameter Settings Content Default Info
Menu
Refer to
1.1 pH buffer standard USA/NIST/CH/User-Define /
section 5.1.1
1.2 Resolution 0.001/0.01/0.1 0.01 /
Refer to
1.3 Calibration info View/Print Check
section 5.1.4
Refer to
1.4 Calibration reminder Off/Hour/Day Off
section 5.1.5
Refer to
1.5 Stability standard Low/Medium/High Medium
pH section 5.6.1
Max/min reading Refer to
1.6 Off/Max/Min Off
alarm section 5.6.2
Refer to
1.7 Display mode Digital/Dial Digital
section 3.5.3
Refer to
1.8 Electrode ID --------- / section 8.3.3-
(c)
Back to factory Refer to
1.9 No/Yes No
default section 5.6.4
Refer to
2.1 Cell constant 10/1.0/0.1 1.0
section 7.1.2
Calibration solution Refer to
2.2 CH/Standard/User-Define /
standard section 7.2.1
Refer to
2.3 Calibration info Check/Print Check
section 7.2.3
Refer to
2.4 Calibration reminder Off/Hour/Day Off
section 7.2.4
Refer to
2.5 Reference temp. 15 to 30°C 25°C
Cond./ section 7.2.5
Temp. compensation Refer to
TDS 2.6 0.00 to 10.0% 2.00%
coefficient section 7.2.6
Refer to
2.7 TDS factor 0.40 to 1.00 0.71
section 7.7
Refer to
2.8 Salinity type Linear/NaCl/Saltwater Linear
section 7.8
Refer to
2.9 Electrode ID --------- / section 8.3.3-
(c)
Back to factory Refer to
2.10 No/Yes No
default section 7.6.4
Refer to section
3.1 Logging data to Memory/Printer/PC /
8.2.1/8.3.1.
Refer to
3.2 Logging mode Manual/Auto. /
section 8.2.3
Data Refer to section
3.3 Printing format Simple/Complete /
8.3.3(a)to(b)
Refer to
Delete data in
3.4 Yes/No / section 8.2.4-
memory
(d)
Refer to
Settings 4.1 Sample ID --------- / section 8.3.3-
(c)

- 13 -
Refer to
4.2 User ID --------- / section 3.3.3-
(c)
Refer to
4.3 Company name --------- / section 8.3.3-
(c)
Refer to
4.4 Calibration password --------- /
section 4.4
Refer to
4.5 Display info Simple/Complete /
section 4.2
Refer to
4.6 Auto. Hold On-Off /
section 3.5.2
4.7 Temperature unit °C - °F / /
YYYY-MM-DD/MM-DD-
4.8 Date format / /
YYYY/DD-MM-YYYY
4.9 Date setting --- / /
4.10 Time setting --- / /
Chinese-English-German-
4.11 Language / /
Spanish-French-Italian
4.4 Calibration Password
• The factory setting of the calibration password is “None” and the initial password is 000000. To set
the calibration password, connect the keyboard, enter parameter setting 4.4, press key, and
then enter the initial password twice as prompted;
• To set the new password, enter the old password first, then enter the new password twice. The
password is up to 8 English letters or numbers;
• Cancel password: Enter the old password in parameter setting 4.4 and press key to confirm,
then ignore the prompt to enter the new password, just press key twice to cancel password.
• There is a confidential envelope comes with the meter that has a set of “super password”. Please
make sure to properly save it. In case you have forgotten your password, you can use this super
password to unlock it, or contact your supplier.

5 pH Measurement

5.1 About pH Calibration


5.1.1 Standard pH Calibration Buffer Solutions
The meter has 3 series of standard pH buffers: USA, NIST, and CH; plus user-define buffers. Users can
make the selection in parameter setting 1.1 (buffer solution standard). The 3 standard series are as shown
in Table-3. For User-define buffers, refer to section 5.3.

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Table-3 pH Standard Buffer Series

pH Standard Buffer Series


Calibration Icon
USA NIST CH

1.679 pH 1.680 pH 1.680 pH

4.005 pH 4.003 pH 4.003 pH

5-point
Calibration 7.000 pH 6.864 pH 6.864 pH

10.012 pH 9.182 pH 9.182 pH

12.454 pH 12.454 pH 12.460 pH

Note: the calibration icons are examples of USA standard series. In practice, these icons will change
according to the series selected by users.

5.1.2 5-point Calibration


Users can choose 1 to 5 points of calibration. The 1st point of calibration must be 7.00 pH (or 6.86 pH in
NIST and CH Series). Then choose other buffers to calibrate 2nd point to 5th point. There are a variety
of combos of calibration points. The most commonly used combos are the 3-point one: 4.00 pH, 7.00 pH,
10.01 pH, and the combos that are suitable for strong acid/alkaline samples as shown in Table-4.
Generally, make sure the estimated pH range of your sample solutions falls in the two points of calibration.

Table-4 Commonly Used Calibration Combo (Take USA Series as an example)


Applicable
USA Series Calibration Icons
Scenarios

1-pt calibration 7.00pH accuracy≥±0.1pH

7.00pH and 4.00pH <7.00 pH

7.00pH and 10.01pH >7.00 pH


2-pt calibration
Strong acid
7.00pH and 1.68pH
samples
Strong alkaline
7.00pH and 12.45pH
samples

3-pt calibration 7.00pH, 4.00pH, and 10.01pH 0 to 14.00pH

- 15 -
5.1.3 Calibration Frequency
The frequency that you need to calibrate your meter depends on the tested samples, condition of
electrodes, and the requirement of the accuracy. For High-Accuracy measurement (≤ ±0.02pH), the meter
should be calibrated before test every time; For general-accuracy measurements (≥±0.1pH), once
calibrated, the meter can be used for about a week or longer. In the following cases, the meter must be
re-calibrated before next use:
a) The electrode hasn’t been used for a long time or a new electrode is connected.
b) After measuring strong acid (pH<2) or strong alkaline (pH>12) solutions.
c) After measuring fluoride-containing solution and strong organic solution.
d) There is a significant temperature difference between the test sample and the buffer solution.

5.1.4 Check calibration record


In parameter setting 1.3 (Calibration info), users can choose
to view or print. When choosing “view”, press to
display the last calibration record as shown in Diagram-10.
When choosing “print”, press to print out the last
calibration data (the meter’s data logging mode must be in
printer mode, and the printer’s status must be online. Refer
to section 8.3.4 for details).
Diagram-10
5.1.5 pH Calibration Reminder
Users can set up pH calibration reminder in parameter
setting 1.4. When time is due, the red reminder icon will
show up as shown in Diagram-11. This will not affect the
normal operation of the meter. After calibration or choosing
none in parameter setting 1.4, the reminder icon will
disappear.
Diagram-11

5.2 pH Meter Calibration


The following calibration process takes 4.00 pH, 7.00 pH, and 10.01 pH as an example. Put LabSen 211
pH Combination Electrode and MP500 temperature electrode on the flexible electrode holder and connect
to the meter.

Note: the electrode mentioned in Table-5 and Table-6 refers to pH combination electrode and temperature
electrode.

- 16 -
Table-5 pH Meter 3-point Calibration

1. Long press to enter calibration mode. Rinse off the


electrode with distilled or deionized water. Shake-dry or dry
with filter paper. Then insert the electrode into 7.00 pH buffer.
Press to continue.

2. Stir the electrode gently, let it stand in 7.00 pH buffer, and


wait for to show up and stay on screen (the buzzer will
make a beep). Then press to complete the 1st point
calibration.

3. When pH 7.00 is calibrated, the 7.00 icon will show up at the bottom left corner. The meter will automatically
enter the next point of calibration. Rinse off the electrode with distilled or deionized water. Shake-dry or dry with
filter paper. Then insert the electrode into 4.00 pH buffer. Press to continue.

4. Stir the electrode gently, let it stand in 4.00 pH buffer, and


wait for to show up and stay on screen (the buzzer will
make a beep). Then press to complete the 2nd point
calibration.

- 17 -
5. When pH 4.00 is calibrated, the 4.00 icon will show up at the bottom left corner. The meter will automatically
enter the next point of calibration. Rinse off the electrode with distilled or deionized water. Shake-dry or dry with
filter paper. Then insert the electrode into 10.01 pH buffer. Press to continue.

6. Stir the electrode gently, let it stand in 10.01 pH buffer,


and wait for to show up and stay on screen (the buzzer
will make a beep). Then press to complete the 3rd
point calibration.

7. When pH 10.01 is calibrated, the 10.01 icon will show up at the bottom left corner. The meter will
automatically enter the next process. Now the 3-point calibration is completed. Press to exit
calibration mode.

8. The meter will automatically go back to measurement mode after displaying calibration data for a few seconds.

Notes
a) The meter can perform 1 to 5 points of calibration. After all 5 points are calibrated, the meter will
automatically display calibration record and go back to measurement mode; if it’s 1 to 4 points
calibration, after completing any point, press to go back to measurement mode.
b) The meter can automatically recognize pH buffers. During calibration, if the buffer is incorrect, pH
electrode is not submerged in solution, or operation is incorrect, the buzzer will make a beep and
display self-diagnosis information. For details, refer to Table-7.

- 18 -
5.3 User-Define Calibration (take 2.00 pH and 7.30 pH as an example)
Table-6 pH Meter User-Define Calibration

1. In parameter setting 1.1, select User, press to


confirm. Then press to go back to measurement
mode.

2. Long press to enter calibration mode. Rinse off the


electrode with distilled or deionized water. Shake-dry or dry with
filter paper. Press to continue.

3. Insert the electrode to 2.00 pH solution, stir gently and let


it stand. Wait for to stabilize, press or
to adjust the measurement value to 2.00. Then press
to complete calibration.

4. After 2.00 pH is calibrated, the meter automatically enters the


next point of calibration. Rinse off the electrode with distilled or
deionized water, shake-dry or dry with filter paper.
Press to continue.

5. Insert the electrode to 7.30 pH solution, stir gently and let


it stand. Wait for to stabilize, press or to
adjust the measurement value to 2.00. Then short press
to complete calibration.

- 19 -
6. After 7.30 pH is calibrated, the meter will display calibration record for a few seconds and go back to
measurement mode. The calibration icons of 2.00 and 7.30 will show up at the bottom left. Note that in user-
define calibration, the icons are in black.

Notes
a) The meter can perform 1 to 2 points of user-define calibration. Press after the 1st point is
completed, the meter will exit calibration mode, which ends up being 1-point user-define
calibration.
b) The meter cannot automatically recognize user-define pH buffers, but requires that the difference
between two buffers is greater than 1.0 pH. Otherwise self-diagnosis will display error message.
c) pH value of user-define pH buffers is based at certain temperature. We recommend performing
calibration and measurement at the same temperature. Otherwise the error could be significant.
d) If it’s manual temperature compensation, temperature should be adjusted before calibration. It
cannot be adjusted during calibration.

5.4 Self-Diagnosis
The meter has a self-diagnosis function. When the electrode is not working properly, buffers are incorrect, or
operation is incorrect, relevant information will pop up at the bottom of the display as shown in Diagram-12. At
the same time, the buzzer will make two beeps. For detailed information of self-diagnosis, refer to Table-7.

Diagram-12
c

- 20 -
Table-7 pH Self-Diagnosis Information

Message Detailed information How to fix

1. Check if pH buffer is correct (1st


point must be 7.00 or 6.86).
2. Check if pH buffer is in good
Incorrect pH buffer, exceeding the
Buffer error quality (fresh and clean).
meter’s recognizable range
3. Check if electrode is properly
connected to meter.
4. Check if electrode is damaged.
User pressed before readings
Press after shows up and
Not stable yet are fully stabilized
stays on screen

1. Check if there is any air bubble


inside the glass bulb sensor. If
so, shake the electrode with
Reading hasn’t been stabilized for
Electrode Error force to remove it.
over 3 minutes
2. Electrode is aged (more than 1-
year of frequent use). Replace
the electrode.

5.5 Sample Measurement


Rinse off pH and temperature electrode in distilled or deionized water. Shake-dry or dry with filter paper.
Place electrodes into sample solution. Stir them gently, let them stand still, and wait for a stable reading
( shows up and stays on screen), which is the measurement you can record. Diagram-13 is the flowchart
for pH meter’s calibration and measurement.

Submerge the After the 1st point


electrode in 7.00 pH calibration is done, 1 st point
Long press to calibration
Press to power solution, press press to enter
enter calibration. when appears the measurement
on the meter
and stays. mode.

Submerge the After the 2nd point


electrode in 4.00 pH calibration is done, 2 nd point
solution, press press to enter calibration Sample
key when the measurement
Test
appears and stays mode.

Submerge the After the 3rd point


electrode in 10.01 pH calibration is done, 3r d point
solution, press the meter enters the calibration
when appears measurement mode
and stays. automatically.

Direct measurement

Diagram-13

- 21 -
5.6 About pH Measurement
5.6.1 pH Stability Criterion
pH stability criterion refers to the time it takes for pH readings to stabilize, which is related to the ion
concentration (iconic strength) of test samples. Generally, the higher the ion concentration, the faster the
readings get stabilized. In parameter setting 1.5, there are options for low, medium, and high. We
recommend setting as per Table-8. Factory default is medium.
Table-8
Stability Criterion Test Samples

Low Boiler water, steam condensate, deionized water, ultrapure water, etc.

Medium General water solutions

High Wastewater

5.6.2 pH Reading Alarm

In parameter setting 1.6, users can setup the pH reading alarm. The alarm range is 0 to 14.00 pH. The

alarm icons are (exceeding the preset maximum value) and (exceeding the preset

minimum value). At the same time, the buzzer will make a beep. There are four alarm modes available:

Diagram-14 Diagram-15

◆ No alarm
Set to none and there will be no reading alarm.
◆ Min alarm
If the reading is lower than the minimum value, reading alarm goes off. For example, if minimum value is
set to 6.20 pH, when measurement is lower than 6.20 pH, will show up and the buzzer makes a
beep. The range of 6.20 to 14.00 is good.
◆ Max alarm
If the reading is higher than the maximum value, reading alarm goes off. For example, if maximum value
is set to 8.60 pH, when measurement is higher than 8.60 pH , will show up and the buzzer makes
a beep. The range of 0 to 8.60 is good.

- 22 -
◆ Min-Max alarm
If the reading is lower than the minimum value or higher than the maximum value, reading alarm goes
off. For example, if minimum value is set to 6.50 pH, and maximum value is set to 7.60 pH, when
measurement is lower than 6.50 pH or higher than 7.60 pH, or shows up, and the
buzzer makes a beep. The range of 6.50 pH to 7.60 pH is good.

5.6.3 pH Isothermal Measurement Principal


According to pH isothermal measurement principal, the closer the temperature of test samples is to calibration
solutions’, the higher the measurement accuracy is. Therefore, keeping test samples and calibration solutions
at the same temperature is highly recommended.

5.6.4 Back to Factory Default Settings


The meter has the function of restoring factory settings. For details, see parameter setting 1.9 (see Diagram-
16). This function will clear all calibration data, return the instrument calibration to the theoretical value (zero
potential pH 7.00, slope 100%) and restore some of the function settings to their initial values (see Section
4.4.3 for details). When the instrument calibration or measurement is abnormal, this function can be enabled
to restore the instrument to the factory settings before calibration. Restoring the factory settings is irreversible,
so please pay special attention when enabling.

Diagram-16

5.7 pH Electrode Maintenance


5.7.1 Daily Maintenance
The protective vial at the front end of the pH electrode has an appropriate amount of 3M KCl solution (SKU:
AI1107), and the electrode tip is immersed therein to maintain the activation of the glass bulb and the junction.
When measuring, loosen the cap, pull out the electrode, and wash it with pure water. After use, insert the
electrode and screw the bottle cap to prevent the solution from seeping out. If the soaking liquid in the
protective vial is found to be turbid and moldy, it should be washed in time and replaced with new soaking
solution. The electrode should never be stored in pure water like distilled or deionized water, protein solution
or acidic fluoride solution, and should avoid contact with organic grease. Always keep the instrument clean
and dry. Pay special attention to keep the meter and electrode socket clean and dry. Otherwise, the
measurement will be inaccurate or invalid. If it is stained, it can be cleaned and dried with medical cotton and
anhydrous alcohol.

- 23 -
5.7.2 Calibration Solutions
To maximize the meter’s measurement accuracy, pH buffers should be fresh and clean. After multiple uses,
replace pH buffers in time.

5.7.3 Cleaning
pH electrodes must be thoroughly rinsed with pure water before and after each test. For tough contaminants,
users can use a soft brush and warm soap water to clean off. Then rinse with distilled or deionized water and
soak the electrode in 3M KCL storage solution overnight before next use. After measurement in viscous
samples, the electrode should be rinsed with distilled or deionized water multiple times to remove the adhesion
to the glass membrane.

6 mV Measurement

6.1 ORP Measurement


Press the to switch the meter to mV measurement mode. Connect the ORP combination electrode
(sold separately, SKU: AI1303), insert it into the test sample, stir gently and let it stand still. When
shows up and stays, it is the ORP value. ORP is an abbreviation for "Oxidation-Reduction Potential" and
indicates the redox potential of water solution. ORP is a measure of the redox capacity of water solution. The
unit is mV.

6.2 ORP Measurement Notes


6.2.1 The instrument does not need to be calibrated during ORP measurement, but if there is any doubt about
the test results or the quality of the ORP electrode, ORP standard solutions can be used to test its mV value
to determine whether the ORP electrode or instrument is accurate.

6.2.2 Cleaning and activation of ORP electrodes: After long-term use of ORP electrodes, the contamination of
the platinum surface may cause measurement inaccuracy and slow response. In this case, the following
methods can be used for cleaning and activation:
a) For inorganic contamination, the electrode can be immersed in 0.1 mol/L dilute hydrochloric acid for
30 minutes, rinsed with pure water, and then immersed in the electrode soaking solution for 6 hours.
b) For the contamination of organic oil and oil film, the surface of platinum may be rinsed with soap water,
and then immersed in the electrode soaking solution for 6 hours.
c) The platinum surface is heavily polluted, and an oxide film is formed on the surface. The platinum
surface can be polished with toothpaste, then rinsed with pure water, and then immersed in the
electrode soaking solution for 6 hours.

- 24 -
6.3 ISE Measurement
Connect the ion electrode, insert it in the test sample, stir gently and let it stand. Get the reading when
shows up and stays on screen, which is the potential value of the ion electrode. If the ion electrode is a
combination type, simply insert it to the pH/mV socket. If it is not a combination type, users should select a
suitable reference electrode and connect it to the REF socket, and the two electrodes must be tested at the
same time.

7 Conductivity Measurement

7.1 Conductivity Electrode Information


7.1.1 Default Electrode
The instrument is equipped with 2401T-F conductivity electrode, the cell constant K=1.0, and the built-in
temperature sensor enables automatic temperature compensation. The BNC plug of the electrode is
connected to the Cond socket; the RCA plug is connected to the Temp socket. After the conductivity electrode
is immersed in the solution, it should be stirred for a few times and then placed still to eliminate the bubble
interference, so that the reading will be fast and stable.

7.1.2 Conductivity Cell Constant


The meter can be equipped with 3 types of conductivity electrodes: cell constant K=0.1, K=1.0, and K=10.0.
The measurement ranges are shown in Table-9. Cell constant setting is in parameter setting 2.1.

Table-9 Cell constant and measurement range


Range <20μS/cm 0.5μS/cm to100mS/cm >100mS/cm

Cell constant K=0.1 cm-1 K=1.0 cm-1 K=10 cm-1

Calibration Solution 84μS/cm 84μS/cm 1413μS/cm 12.88mS/cm 111.8mS/cm

7.2 Conductivity Calibration Information


7.2.1 Conductivity Standard Calibration Solutions
The meter supports Standard and CH series conductivity standard calibration solutions, as well as user-define
solutions, which can be set up in parameter setting 2.2.

Table-10 Conductivity Standard Calibration Solutions


Icon Standard Series CH Series

84 μS/cm 146.6 μS/cm


1413 μS/cm 1408 μS/cm

12.88 mS/cm 12.85 mS/cm

111.8 mS/cm 111.3 mS/cm

Note: calibration icons are based on Standard series.

- 25 -
7.2.2 Calibration Frequency
a) The meter has been calibrated before leaving factory and can be used directly by the user.
b) It is recommended to calibrate once a month under normal circumstances.
c) If the accuracy requirement is high or the measured temperature is significantly different to the
reference temperature (25 °C), it is recommended to calibrate once a week;
d) Test the electrode performance with conductivity standard solutions, and perform calibration when the
error is large.
e) It is recommended to perform 3-point or 4-point calibration after a new electrode is used for the first
time or after the instrument is restored to the factory default settings. Generally, the calibration solution
with the conductivity close to the sample solution can be used for 1 to 2 points of calibration. For
example, in the 0 to 20mS/cm conductivity range, use the 1413 μS/cm solution to calibrate.
7.2.3 Check Calibration Record
In the parameter setting 2.3 (calibration information), you can select
“View” or “Print”. When you select “View”, press to display
the last calibration data, as shown in Diagram -17. Press
while selecting “Print” to print out the calibration information, but the
instrument's data processing mode must be "printer" and the printer
is set to online. See section 8.3.4 for details.
Diagram-17

7.2.4 Conductivity Calibration Reminder


Users can set up conductivity calibration reminder in parameter setting 2.4. When time is due, the red
reminder icon will show up as shown in Diagram-18. This will not affect the normal operation of the meter.
After calibration or choosing none in parameter setting 1.4, the reminder icon will disappear.

Diagram-18

7.2.5 Reference Temperature


The factory default reference temperature is 25 °C. Other reference temperatures can be set. The setting
range is 15 °C to 30 °C, and can be selected in parameter setting 2.5 (reference temperature).

- 26 -
7.2.6 Temperature Compensation Coefficient
The temperature compensation coefficient of the factory setting is 2.00%/°C, but the conductivity temperature
compensation coefficients of different kinds and different concentration solutions are different. Users can refer
to Table-11 and the data obtained from experiments. Set the setting in 2.6 (temperature compensation
coefficient).
Note: When the temperature compensation coefficient is set to 0.00, that is, there is no temperature
compensation when the instrument is measuring. The measured value of the instrument is the conductivity
value at the solution's temperature at the time.

Table-11 Temperature compensation coefficient of special solutions


Temperature Temperature
Solution compensation Solution compensation
coefficient coefficient
10% hydrochloric acid
NaCl solutions 2.12 %/°C 1.32 %/°C
solution
5% sulfuric acid
5%NaOH solutions 1.72 %/°C 0.96 %/°C
solution
Dilute ammonia
1.88 %/°C
solution

7.2.7 Prevent Contamination of Standard Solutions


The conductivity calibration solution is not buffered. Please take care to prevent contamination when using it.
The electrode should be cleaned and dried before being immersed in the calibration solution. In particular, the
low concentration 84μS/cm calibration solution should be paid special attention to prevent contamination. The
contamination of the calibration solution will affect the accuracy of the calibration.

- 27 -
7.3 Conductivity Meter Calibration (Take 1413μS/cm as an example)

1. Long press to enter calibration mode. Rinse off the


electrode with distilled or deionized water. Shake-dry or dry
with filter paper. Press to continue.

2. Insert the electrode to 1413μS/cm solution. Stir gently and

let it stand still. Wait for to show up and stay. Then

press to complete calibration.

3. Calibration process
a) Instrument calibration.
b) Display calibration data: date, time, temperature,
range, and cell constant.
c) Automatically returns to measurement mode.

(a)
4. Multi-point calibration, exit calibration and switching mode
- 11
4.1 Multi-point calibration can be selected as needed. For
example, repeat steps 1 to 3 above in 12.88mS solution.
Multi-point calibration should be performed according to the
concentration of calibration solution from low to high to avoid
contamination of low concentration solution. Calibration can
(b) also be repeated in the same calibration solution until the

- 11 displayed values are stable and have good repeatability.

4.2 To exit calibration mode, short press .

4.3 Press to switch the measurement mode:


conductivity → TDS→ salinity → resistivity.

(c)
- 11

- 28 -
7.4 User-Define Calibration (Take 10μS/cm as an example)

1. In parameter 2.2, select “user”, press to confirm.


Then press to return to measurement mode.

2. Long press to enter calibration mode. Rinse off the


electrode with distilled or deionized water. Shake-dry or dry
with filter paper. Press to continue.

3. Insert the electrode to 10.00 μS/cm solution, stir gently


and let it stand. Wait for to stabilize, press or
to adjust the measurement value to 10.00. Then
press to complete calibration.

4. Calibration is completed. The meter returns to


measurement mode. 10.00 icon shows up at bottom left.

● Conductivity user-define calibration has only 1-point calibration. User-define calibration has no
temperature coefficient or reference temperature. Therefore, it is recommended to perform calibration and
measurement at the same temperature. Otherwise, there will be a large error.
● The instrument does not automatically recognize user-define calibration solutions.
● If it's manual temperature compensation, the temperature value should be adjusted before calibration.
During calibration, temperature cannot be adjusted.

- 29 -
7.5 Self-Diagnosis
The meter has a self-diagnosis function for conductivity. When the electrode is not working properly, calibration
solutions are incorrect, or operation is incorrect, relevant information will pop up at the bottom of the display
as shown in Diagram-19. At the same time, the buzzer will make two beeps. For detailed information of self-
diagnosis, refer to Table-12.

Diagram-19

Table-12 Conductivity Self-Diagnosis


Self-diagnosis
Information How to fix
Message
1. Check if calibration solution is in good quality
Calibration solution has a (fresh and clean).
Solution error problem. The meter cannot 2. Check if the electrode is properly connected to
recognize it. the meter.
3. Check if the electrode is damaged.
User pressed before
Press after shows up and stays on
Not stable yet the reading is fully stabilized
screen

1. Shake the electrode with force to remove


The reading hasn’t been potential air bubbles.
Electrode error
stabilized for over 3 minutes 2. Electrode is aged (more than 1-year of frequent
use). Replace the electrode.

- 30 -
7.6 Sample Measurement

Rinse the conductivity electrode with distilled or deionized water. Shake-dry or dry with filter paper. Insert

it to sample solution, stir a few seconds and let it stand. Record the reading when shows up and

stays on screen. Diagram-20 is the flowchart for conductivity calibration and measurement.

Measure

Long press to Insert the electrode to 84 μS solution,


press when is fully stabilized. 1-pt Calibration
Press to enter calibration. 1st point calibration is completed and the
power on Rinse the electrode, meter goes back to measurement mode.
then press

Insert the electrode to 1413 μS solution,


2-pt
press when is fully stabilized. Calibration Sample
2nd point calibration is completed meter
goes back to measurement.
Test

Insert the electrode to 12.88 μS solution,


press when is fully stabilized. 3-pt Calibration
3rd point calibration is completed meter
goes back to measurement.

Insert the electrode to 111.8 mS solution,


press when is fully stabilized. 4-pt Calibration
2nd point calibration is completed meter
goes back to measurement.

Diagram-20

7.7 TDS and Conductivity


The conversion factor for TDS and conductivity is 0.40 to 1.00, which can be set in parameter setting
2.7, and the meter is factory set to 0.71. Users can adjust the conversion factor of TDS according to the
experimental data and experience in parameter setting 2.7. Table-13 lists some commonly used TDS
conversion factors according to the solution conductivity, for reference only. TDS doesn't need to be
calibrated. Calibrate conductivity and switch to TDS mode.

Table-13 Conductivity and TDS Conversion Factor


Solution’s conductivity TDS conversion factor
0 to 100 μS/cm 0.60
100 to 1000 μS/cm 0.71
1 to 10 mS/cm 0.81
10 to 100 mS/cm 0.94

- 31 -
7.8 Salinity Types
The salinity types are linear salinity, NaCl salinity and saltwater salinity. The linear salinity is calculated
according to the measured conductivity value (0.5 conversion factor). The NaCl salinity and saltwater salinity
are programmed based on 2 predetermined salt curves. The salinity type can be set in parameter setting 2.8
and the meter is factory set to “linear” salinity. Salinity doesn't need to be calibrated. Calibrate conductivity
and switch to salinity mode.

7.9 Back to Factory Default Settings


The meter has the function of restoring factory settings. For details, see parameter setting 2.9 (see Diagram-
21). This function will clear all calibration data, return the instrument calibration to the theoretical value and
restore some of the function settings to their initial values (see Section 4.4.3 for details). When the
instrument calibration or measurement is abnormal, this function can be enabled to restore the instrument to
the factory settings before calibration. Restoring the factory settings is irreversible, so please pay special
attention when enabling.

Diagram-21

7.10 Conductivity Electrode Maintenance


a) Conductivity electrodes must be kept clean. Rinse the electrode with distilled or deionized water and
dry it before measuring. It is best to rinse the electrode with the solution to be tested. After use,
clean it with distilled or deionized water.
b) When calibrating and measuring, stir the electrode in solution to eliminate potential air bubble
interference and make the measurement fast and stable;
c) The electrode head (platinum black plating part) is suitable for storage under humid conditions to
ensure a faster response. If the electrode is stored dry for a long time, the response may be slow. In
this case, immerse the electrode in the calibration solution of 12.88mS for 5 to 10 minutes, or soak
in tap water for 1 to 2 hours to restore the electrode to normal.
d) The surface of the sensing layer of the 2401T-F conductivity electrode is plated with platinum black
to reduce the polarization of the electrode and expand the measuring range. If the electrode is
contaminated, rinse it off with distilled water. For tough organic contaminants, use warm water or
alcohol to rinse off. Do not brush the surface of the sensor to prevent damage.

- 32 -
8 Data Processing M odes (Save, Recall, P rint, Delete)

8.1 Data Processing Flowchart


The data storage has three modes: “memory”, “printer” and “computer”, as well as “manual” and “auto.
timing” data logging modes. Diagram-22 is a flowchart explaining various storage and data logging modes.

In parameter setting
● Press to save;
3.2, select “manual”
shows up on top. ● Press to recall
Select “memory” in ● Connect meter to PC.
parameter setting 3.1. Export data to Excel file
shows up on top.
In parameter setting for printing;

3.2, select “timer” and ● Delete all saved data

set interval time. in parameter setting 3.4


3 data logging modes: shows up on top.
● Select “memory” or “printer” in meter;
● Enter PC mode when connected to PC
● Press to print
when printer is online
In parameter setting
● Press to save
3.2, select “manual”
shows up on top. data in printer when
Data Processing
Select “printer” in printer is offline. Press
● Save ● Recall
parameter setting 3.1. SEL to print all saved
● Print ● Delete
shows up on top. In parameter setting data altogether.
3.2, select “timer” and ● No data recall
set interval time. ● Saved data will be
shows up on top. deleted when printer is
Note: The meter can connect
powered off.
with PC and printer
simultaneously.

In parameter setting
3.2, select “manual”
● Press to save
shows up on top.
Connect computer, the data (displayed on PC).
meter automatically
● Export data as Excel
enters PC mode.
In parameter setting file for printing.
shows up on top
3.2, select “timer” and ● Press Clear to delete
set interval time. saved data.
shows up on top.

Diagram-22

- 33 -
8.2 Log Data in Meter
8.2.1 Setup
Select Memory in parameter setting 3.1. displays on top of the screen. All data will be stored in the
meter.

8.2.2 Data Storage


The PH9500 and EC9500 models has a storage capacity of 1000 sets, and the PC9500 can store 2000
sets. Single parameter display mode: 1 serial number corresponds to 1 set of measurement data; double
parameter display mode: 1 serial number corresponds to 2 sets of measurement data (pH + conductivity).
When the storage is full, if you press , “FULL” will flash under the number icon to remind you that the
storage is full and you need to delete it first. Saved data can be deleted in parameter setting 3.4.

8.2.3 Data Logging Modes


In parameter setting 3.2, you can select “manual” or “auto. timing” data logging mode. When manual is
selected, will be displayed on top of the display; when auto. timing is selected, will be
displayed on top of the display, as shown in Diagram -23.

(a) Manual data logging mode (b) Auto. timing data logging mode

Diagram-23
8.2.4 Save, Recall, Delete
(a) Manual data logger
Set “Manual” in parameter setting 3.2, press during storage, the display screen is as shown in
Diagram-24. indicates that the 8th group of data has been stored, press to display the
stored data page, as shown in Diagram- 25. If there are more than 8 sets of stored data, press or
to turn the page.

Diagram-24 Diagram-25
c

- 34 -
(b) Auto. timing data log
Select “Timer” in parameter setting 3.2 and set the data logging interval time (by every X seconds or
minutes), for example, 10 seconds, press to start auto. data logger, flashes, the first set of
measurement data is stored and shows up, then every 10 seconds one set of data will be stored
and the storage number will be automatically increased. Press again to stop auto. data logger.
press to display the stored data page, and then press or to turn the page.
(c) Print
The data stored in the meter cannot be directly printed. The stored data needs to be uploaded to the
computer via USB cable and then exported to an Excel document for printing. See section 8.4 for details.
(d) Delete
If the storage is full, delete it by selecting Yes in parameter 3.4. Otherwise, data logging can’t be continued.

8.3 Print Data

The meter is only compatible with Apera’s TH192G Pin-Type Mini Printer, which is sold separately.
8.3.1 Setup
Select "Printer" in parameter setting 3.1, and icon will show up on top of the display, indicating that
the data will be stored in the printer, and the real-time printing is completed by TH192G Pin-Type Mini
Printer. The data is stored in the printer and there are no data storage icons on the display and no data
recalling.

8.3.2 Install Printer


Connect the printer and the meter via the data cable first, then turn on the printer. The power switch is at
the bottom left of the printer. The buttons and indicators are as follows:
P (red light) — Power indicator, red light means power is on.
S (green light) — Green light on means the meter is in online status; Green light off means the meter is
in offline status.
SEL button — Press the button to switch between online (green light) and offline (green light off).
LF button — When the printer is offline, press the button to transfer printing paper. For printing paper
installation, refer to Diagram-26; printer ribbon replacement, refer to Diagram-27.


b ○
c


a


a Insert printing paper here

c Press here to remove printer ribbon.

b Press LF button when offline to transport paper
Diagram-26 Diagram-27

ccc
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8.3.3 Printer Information

(a) Complete format


Selecting “Complete” in parameter setting 3.3 to use the complete printing format. The printing information
includes device information, calibration information, and measurement data. The device information
refers to the instrument model number, serial number, electrode ID, company name, and operator ID; the
calibration information refers to the last calibration record; the measurement data refers to the numberings,
date, time, sample ID, measured value, and temperature.
Note: When selecting the complete format, each print contains a prefix for the device and calibration
information.

(b) Simple format


In the parameter setting 3.3, select “simple” to use the simple printing format. The first print after the
meter is turned on will include the device information and the calibration information. Afterwards, it will
only print out data information, including numberings, date, time, sample ID, measured value, and
temperature. If users require the device and calibration information again, just reboot the meter.

(c) ID Setup
To set the ID, insert the keyboard into the “Keypad” socket of the instrument, use the keyboard to input
up to 8 digits of English letters and numbers. The settings include sample ID, operator ID, company name,
pH electrode ID, and conductivity electrode ID. Calibration passwords can also be set (refer to Section
4.4 “Parameter Settings” for details).

8.3.4 Data logging and printing

(a) Manual Data Logger Printing


In parameter setting 3.2, select “manual”, will be displayed on top of screen. Set the printer to online
mode (green light on), short press to print out the measurements; if the printer is in offline mode
(green light is off), press to store the data in printer temporarily. According to your needs, after
storing enough data, press SEL button of the printer to print out the previously stored data altogether.

(b) Auto. Timing Printing


In parameter setting 3.1, select “Timer” and set the storage interval time (such as 3 minutes). will
be displayed on top of screen. Set the printer to online mode (green light on), press to print out
the measurements, and it will automatically print again by every 3 minutes; If the printer is in offline
mode (green light off), pressing to store the data in printer temporarily by every 3 minutes.
Then press SEL button of the printer to print out the previous stored data altogether.

8.3.5 Delete Data

In offline mode (green light off), the stored value will be deleted when the printer is turned off.

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8.4 Data logging via PC
8.4.1 Install Software
a) This instrument uses the PC-Link 9500 communication software, and the communication port is
USB. Copy the PC-Link 9500 program files to the computer from the flash drive, connect the USB
communication cable to the PC socket of the meter and the computer’s USB port. The software
will be automatically open. The instrument and the computer will be automatically connected, and
will show up on top of the display.
b) If manual data logger is selected, press , data will be uploaded to the computer; if auto.
timing data logger is selected, press , data will be uploaded to the computer by the certain
timing you set. All the data uploaded to the computer will not be saved in the meter. Auto-timing
data logger will generate a measurement curve in PC-Link software as shown in Diagram-28.
c) If the printer is connected at the same time, it can also print out the data while uploading them to
the computer.
8.4.2 Software Interface

Diagram-28
Note: In the pH measurement alarm mode, the curve area shows the maximum and minimum red
lines.

1
○ Model number and Serial number 5
○ Prompt for PC connection
2
○ Parameter setting information 6
○ Data area
3
○ Calibration information 7
○ Operation keys
4
○ Data logging type 8
○ Measurement curve area

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8.4.3 Operation Keys of PC-Link
Refresh — When the meter and the computer are not connected, press the button to connect again.
Download — Upload the data in the meter’s memory to the computer.
SyncTime — Sync the time and date of PC to the meter.
Clear — Clear the data.
Export — Export the stored data to a Microsoft Excel document for further analysis.
Exit — press to exit PC-Link.

9 What’s in the Kit

Content Quantity PH9500 EC9500 PC9500

1 PH9500 pH Meter 1 √

2. EC9500 Conductivity Meter 1 √

3. PC9500 pH/Conductivity Meter 1 √


606 Test-Bench (including a flexible electrode
4. 1 √ √ √
holder)
5. LabSen 211 glass pH combination electrode 1 √ √

6. MP500 temperature electrode 1 √ √

7. 2401T-F conductivity electrode(ATC, K=1.0) 1 √ √


pH standard pH buffers
8. 1 for each √ √
(4.00/7.00/10.01pH/50mL each)
Conductivity standard calibration solutions
9. 1 for each √ √
(84μS/1413μS/12.88mS/50mL each)
10. Stirrer cable 1 √ √ √

11. USB cable 1 √ √ √

12. PC-Link 9500 flash drive 1 √ √ √

13. Keyboard 1 √ √ √

14. 9V Adapter 1 √ √ √

15. Vials / 3 3 6

16. L200 stir beads / 3 3 6

17. User Manual 1 √ √ √

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10 Other Parts and Accessories

Models Name Information


Pin-type mini Printer×1, power adapter×1, data cable×1, printer ribbon×2,
1. TH192G
printer printing paper×2
2 TH5740 Printing paper 14 rolls per box

3 CRC-09 Printer ribbon 5 pieces per box


3-in-1 pH For general water solutions. Built-in temp. sensor, ATC
4 LabSen213
Electrode available.
Glass pH
5 LabSen231 For wastewater, emulsions, and suspensions
Electrode
Glass pH
6 LabSen221 For low-ion concentration samples and viscous samples
Electrode
For surface pH measurement like skin, fabrics, paper,
7 LabSen371 Flat pH Electrode
leather, etc.
Semi-micro pH Electrode width: Φ6×100mm, suitable for test tubes and
8 LabSen241-6
Electrode small volume measurement (<0.2mL)
Micro pH Electrode width: Φ3×70mm,suitable for micro-volume
9 LabSen241-3
Electrode measurement (<20μL)
Glass Spear pH
10 LabSen251 For soft-solid samples
Electrode
Pure water pH For pure water e.g. drinking water, distilled water, RO water,
11 LabSen801
Electrode etc.
Ultra-pure water
10. LabSen811 For ultra-pure water
pH Electrode
Food pH For soft-solid food samples e.g. cheese, meat products,
12 LabSen721
Electrode fruits, sushi rice, etc.
Blade Spear pH
13 LabSen761-B For meat and fish
Electrode
For strong acid solutions and solutions containing
14 LabSen831 HF pH Electrode
hydrofluoric acid
Strong alkaline pH
15 LabSen841 For strong alkaline solutions and high-temp solutions
Electrode
Viscous sample For highly viscous samples e.g. cosmetics, paints, resin,
16 LabSen851-3
pH Electrode etc.
Low-temp pH
17 LabSen881 For low-temp solutions
Electrode
Conductivity k=0.1, built-in temp. sensor, comes with a flow cell, for pure
18 DJS-0.1-F
Electrode water conductivity tests
Conductivity k=10, built-in temp. sensor, for saltwater and seawater
19 2310T-F
Electrode conductivity tests
Glass ORP Glass body, Φ6×2.5mm platinum ring, for ORP
20 3501Pt-C
Electrode measurement

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11 Warrant y

We warrant this instrument to be free from defects in material and workmanship and agree to repair or replace
free of charge, at option of APERA INSTRUMENTS, LLC, any malfunctioned or damaged product attributable
to responsibility of APERA INSTRUMENTS, LLC for a period of THREE YEARS (SIX MONTHS for the
electrodes) from the delivery.

This limited warranty does not cover any damages due to:
Transportation, storage, improper use, failure to follow the product instructions or to perform any preventive
maintenance, modifications, combination or use with any products, materials, processes, systems or other
matter not provided or authorized in writing by us, unauthorized repair, normal wear and tear, or external
causes such as accidents, abuse, or other actions or events beyond our reasonable control.

To submit a warranty request, go to support.aperainst.com and click “New Support Ticket” on the upper right
corner. Fill out the form, then click Submit. One of our customer support specialists will help you fulfill the
warranty in one business day.

APERA INSTRUMENTS, LLC


Address: 6656 Busch Blvd, Columbus, Ohio 43229
Tel: 1-614-285-3080
Email: info@aperainst.com
Website: aperainst.com

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