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Composites Science and Technology 168 (2018) 448–459

Contents lists available at ScienceDirect

Composites Science and Technology


journal homepage: www.elsevier.com/locate/compscitech

Modelling race-tracking variability of resin rich zones on 90° composite 2.2 T


twill fibre curved plate
Spiridon Koutsonas
Ulster University/NIACE (North Ireland Advanced Composites Engineering Centre), Faculty Computing and Engineering / NIACE Advanced Composites and Engineering,
Belfast, NI, UK

ARTICLE INFO ABSTRACT

Keywords: Resin rich zone along component edges is a common phenomenon during composites liquid infusion with the
Finite element/control volume modelling resin transfer moulding process. The challenge in the present work is to be able to predict the realistic race-track
Liquid composite moulding flow behaviour along a 90° edge in order to manufacture high-quality composites materials for aerospace or
90° curved plate other applications. To that end, there is a lack of an advanced simulation tool capable to predict the manufacture
2/2 twill fibers
of multi-layer textile composites. The issue of 2D, 3D racetrack prediction on this paper was investigated along a
2D, 3D race-track permeability
90° edge for a composite textile. A novel numerical approach for a three-dimensional Finite Element Control/
Volume modelling was developed in order to predict race-tracking permeability for any composite structure. The
model was experimentally verified for a 2/2 twill carbon fibre geometry. All experiments and simulations used
1 bar pressure and 300 mPa s viscosity.

1. Introduction prediction. Schell et al. [4] published on numerical prediction and ex-
perimental characterization of mesoscale voids in Liquid Composites
Continuous fiber reinforced composites are widely used for aero- Moulding process. Simacek and Advani [5], provided a numerical
space, automotive, marine and civil applications due to their light model in order to predict fibre tow saturation during LCM. Long [6]
weight and enhanced mechanical properties. The Liquid Composite [14], gave a description of race-tracking and what may happen during
Moulding (LCM) processes are one of the most common manufacturing the composites manufacturing process. Lawrence et al. [7] character-
routes for composites. The resin flow behaviour during impregnation ized the preform permeability in the presence of race-tracking. Bick-
affected by the preform properties, which are fibres orientation, and erton et al. [8,9] researched fabric structure and mould curvature ef-
textile volume fractions, that can vary locally. Local variations induced fects on preform permeability and mould filling during the RTM
by moulders' geometry and fabrics’ architecture the forming process. process. Endruweit et al. [10] [21], showed firstly the influence of
Advanced Composites Structures made of 2D or 3D woven geome- stochastic fibre angle variations on the permeability of different di-
trically complex preforms, thus making the impregnation process hard rectional textile fabrics and secondly on random discontinuous carbon
to control and potentially causing defects in the manufacturing of the fibre preforms. Babu and Pillai [11], presented an experimental in-
final component. Industrial experience has shown that during mould vestigation of the effects of fibre-mat architecture on the unsaturated
filling, due to race-tracking and stochastic variability in the material flow during the LCM process. Frederick and Phelan [12], provided
properties, the filling patterns and arising cycle times are rarely the further insights into computational modelling, Trochu, et al. [13] used
same between a given set of apparently identical mouldings. Therefore the Finite Element (FE) method for numerical analysis of the RTM
we will model race-tracking variability of resin rich zones on 90° process. Devillard et al. [15] provided an on-line characterization of
composite fibre curve plate is a very important issue and will be pre- bulk permeability and race-tracking during the RTM process filling
sented on this paper. stage. Andersson et al. [16] provided a numerical model for vacuum
Approaches to estimating race-track and local permeability during infusion manufacturing of polymer composites. Hammami et al.
the impregnation of a composite have been studied by Rudd et al. [1]. [17,18] modelled the edge effect in LCM and the vacuum infusion
Li et al. [2] used a stochastic simulation based approach for statistical moulding process analysis. Lawrence et al. [19] studied automated
analysis and composites characterization. Liu et al. [3] for modelled manufacturing in order to address bulk permeability variations and
Resin Transfer Moulding (RTM) gate control, venting and dry spot race-tracking in RTM with auxiliary gates. Weimer et al. [20] provided

E-mail addresses: spiros_koutsonas@hotmail.com, s.koutsonas@ulster.ac.uk.

https://doi.org/10.1016/j.compscitech.2018.08.001
Received 30 April 2018; Received in revised form 1 August 2018; Accepted 1 August 2018
Available online 06 August 2018
0266-3538/ © 2018 Published by Elsevier Ltd.
S. Koutsonas Composites Science and Technology 168 (2018) 448–459

a research on an approach to net-shape preforming using textile tech- volume. Therefore a fill factor of zero shows that the control volume is
nologies on the edges. Pillai et al. [22] modelled the heterogeneities empty and a factor of one show that it is fully saturated. An inter-
presented in preforms during RTM during mould filling where the in- mediate value indicates that the flow front passes through the control
fluences of various race-tracking situations on the flow pattern have volume in question. Nodes within these flow front control volumes are
been addressed. 90° composite fibre curve plate presented by various assigned the appropriate boundary condition. With this method, the
researchers. Dong [24] presented a model development for the forma- mass conservation is achieved locally at the expense of a slight increase
tion of resin-rich zones in composites processing on a 90° composite in geometric feature complexity.
fibre curve plate. Devillard, Hsiao, Advani [25] presented a Flow sen- The 3D form of Darcy's law equation (1)
sing and control strategies to address race-tracking disturbances in the 1
resin transfer moulding process. u¯ = [K ] P
(1)
u
Bickerton and Advani [26] presented a paper Characterization and
modelling of race-tracking in liquid composite moulding processes. may be combined with the assumption of conservation of fluid volume:
Finally, Koutsona [27] measured the compaction and bending varia-
1
bility with measurements on a novel 3D woven layer to layer interlock [K ] P = 0
µ (2)
composite textile around a 90° curve plate 3.2 mm radius. Addressing a
problem of high relevance in the composite manufacturing of complex In the general case, the permeability [K] tensor in eq. (2) and its
geometry, therefore this research study aims at the description of shape components in three-dimensional space may be written as (3):
of gaps forming at 90° bends in the mould modelling of related through-
Kxx Kxy Kxz
thickness variations in the effective preform permeability, and numer-
ical simulation of impregnating resin flow with particular focus on the [K ] = Kyx Kyy Kyz
racetrack in the gap. K zx K zy K zz (3)
For a woven fabric, considering the axes of coordinates oriented
2. Theory along the principal directions of anisotropy, for an anisotropic forma-
tion Kx ≠ Ky ≠ Kz, and the permeability as a tensor with 3 components
2.1. Control volume finite element method (CV/FE) one on each x, y, z-axis: The permeability tensor is orthotropic where
Kxy = Kyx , Kxz = K zx , Kyz = K zy , and there exists a principal coordinate
The combination of the finite element method with the control system with a principal permeability tensor so eq. (3) can be written:
volume technique in order to determine the pressure field for flow front
advancement is called the Control Volume/Finite Element method (CV/ Kxx 0 0
FE). Frederick, and Phelan [12], researched simulations of the injection [K ] = 0 Kyy 0
process in resin transfer moulding with the use of CV/FE. Trochu et al. 0 0 K zz (4)
[13] presented a paper on the numerical analysis of the resin transfer
So eq. (4) may be reformulated with (2) as eq. (5):
moulding process by the Finite Element Method. Long [14], presents in
details the CV/FE method. Initially, the entire flow field is discretized Kxx 0 0
into a finite element mesh. Each element is sub-divided by lines con- 1
0 Kyy 0 P =0
necting the centroid, to the midpoint of each side as shown in Fig. 1. A µ
0 0 K zz (5)
control volume is composed of several sub-areas surrounding a single
node. A fill factor is associated with each control volume, which re- The computational approach may be summarised as followed ac-
presents the degree of resin saturation of the region and is equal to the cording to Rudd et al. [1]:
volume of the resin divided by the original pore volume of the control The control volume is generated by the FE model. Control volumes

Fig. 1. CV/FE method (left), CV/FE method moving flow front (right) [1].

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S. Koutsonas Composites Science and Technology 168 (2018) 448–459

enclosing inlet nodes are assumed to be filled with resin and the filled 2.3. Material properties for simulations
region is identified by the control volume fill factors. The pressure
equation (5) at nodes within the filled domain is solved by the FE When the preform bends around an edge (inside the mould) it is
method by applying the appropriate boundary conditions. The pressure compacted radially. Modelling on elastic compression of a fiber net-
gradients at the flow front are calculated by differentiating the element work was done by Toll and Manson [37] and reported on their 1995
shape functions and the velocity field is then determined by Darcy's paper. This is due to the stiffness of the preform and forces of friction
law. Hence the volumetric flow rate between control volumes is cal- between the preform and the mould wall. As a result of this behaviour,
culated by multiplying the connecting area with the normal fluid ve- a gap between the preform and the mould wall along the edge will be
locity. The appropriate time increment is calculated to fill at least one created. This can lead to resin rich zones, along with the edges of the
control volume each time and the fill factors are updated at the flow composite part. The existence of race-tracking is able to affect the filling
front. The whole process is repeated as a second step for the newly filled and final mechanical properties of the composite. Resin rich zones are
domain and so on until the mould cavity is completely filled with resin. difficult to predict due to the height gap variation as studied by Dong
The approximate flow front position at any time may be determined by [24] with a model on VARTM experiments. Bickerton et al. [8,9] pro-
identifying nodes within control volumes which are between 0 and 1. vided a series of experimental investigations on racetrack modelling,
and mould curvature effects during the RTM process. Curvature effects
on preform permeability during filling on a closed mould were studied
2.2. Race-tracking for a non-planar geometry. Numerical modelling of flow channel effects
in RTM was studied as well. Devillard et al. [15,25] provided an on-line
After the mould filling stage of the RTM process, the textile must be characterization of bulk permeability and race-tracking during the
completely saturated with resin. Race-tracking and local permeability filling stage in the RTM process. A paper with flow sensing and control
may alter the flow pattern and cause the resin to reach the vent before strategies was presented. Hammami et al. [17] presented a research on
the entire preform has been saturated. Therefore it follows that char- edge effects modelling for composites.
acterization of the preform local permeability and race-tracking loca- Therefore an FE/CV modelling in order to predict the formation of
tions are key elements in order to apply simulation tools for the com- resin rich zones of the enclosed curve angle φ = 90° is presented in this
plete filling of any composite part. Thus, with the study of race-tracking paper. The relationship between gap thickness and edge radius is also
and variability one may optimise gates, vent locations and flow control investigated. This modelling is validated against experimental data
strategies to minimise the change of defect deformation as mentioned taken from the experimental study with a 2/2 twill fabric. The 2/2 used
by Lawrence et al. [7]. The characterization of preform permeability in for this investigation as shows Fig. 2 i) provided by Carr reinforcements
the presence of race-tracking is repeated by Bickerton et al. [9], giving Ltd made of Mitsubishi Rayon Carbon Fibres & Composites Grafil
fabric structure and mould curvature effects on preform permeability 34–700 12 K × 12 K in warp and weft 42 ends/mm, 42 pic/mm 0.9 mm
and mould filling in the RTM process.
Considering that gates and vents have been placed appropriately in
order to ensure complete saturation, without any air entrapments inside
the mould, the next step is to increase the yield of successful parts by
taking into account phenomena such as preform variability and race-
track as mentioned by Hammami et al. [17], Anderson, et al. [28],
Sozera, et al. [29].
A race-track channel may exist because of the fabric compaction
across an angle at the edges of the preform. Racetrack may also be
introduced as galleries to deliberately expedite mould fill. On this gap
area, the fluid usually meets lower flow resistance than the textile
preform; hence permeability along a race-tracking channel is higher.
For a complex geometry part like a truss structure, more complexity
also introduces a higher probability of variability and race-tracking of
the resin during impregnation along preform radii. This may lead to
incomplete saturation, forming dry spots in the composite. The strength
and existence of race-tracking is a function of the fabric architecture
and their placement in the mould. The race-tracking and preform
variability are random phenomena and may vary from part to part due
to fabric different volume fractions or gaps that may arise from the
textile bending in the angles, and are therefore generally not repeatable
from one part to the next. Therefore the optimization of the race-
tracking phenomenon is of high importance for the manufacturing
process of any composite material. Over the past few years an extensive
amount of experimental and modelling research around the race-
tracking flow phenomenon has been performed by Lawrence et al. [19],
Pillai, et al. [22] paper on modelling the heterogeneities present in
preforms during mould filling in RTM, Devillard, et al. [25], Gokce and
Advani [30], Lawrence, et al. [31], Bickerton, Advani [32,33], papers
on characterization and modelling of race-tracking in liquid composite
moulding processes.
On the other hand, the fabric's compaction behaviour may be based
on an empirical power law discussed in detail by Robitaille, F. et
Gauvin, R. [34–36], with their three papers study that gives the fabric Fig. 2. 2/2 Twill textile, ii): Design of the 2/2 twill textile used for compaction
thickness variation (H) against pressure. and bending measurements. Image generated using Tex-Gen Software
(University of Nottingham).

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S. Koutsonas Composites Science and Technology 168 (2018) 448–459

Table 1 the channel flow apparatus which is the most common method to
Experimental Compaction tests power law fitting. measure permeability in the through-thickness direction. Darcy's law
Preform Layers H height (mm) plays a governing role in measuring the permeability as for two-di-
mensional flow. Inside the through-thickness permeability measure-
2.2 Twill 3-layers 1.8637 P(−0.078) ment cylinder, there are two circular plates with holes to support the
specimen. The specimen is first weighed with a high precision balance
in order to calculate accurately the Vf and is then fixed inside the
of thickness the areal density of this textile measured 0.686 (Kg/m2) 80 mm cavity. Spacers with different thickness are used in order to
areal mass. achieve the desired fibre volume fraction Vf. The Vf calculation was
done in the same way as for in the in-plane permeability measurements
2.4. Fabric compressibility with equation (13). A piston pump with constant flow rate supplies
through one side (upper side) inside the cylindrical cavity and the oil
The through-thickness compressibility of the 2/2 twill fabric was flows through the porous medium into the other side of the sample
performed in a similar fashion as reported by Koutsona [27] on an chamber in order to ensure continuous fluid flow rate inside the spe-
Instron 5500 machine according to equation (6) cimen. Near the upper and lower side of the steel, cylinder there are two
pressure transducers to measure the pressure difference along the flow
Hfabricthickness = P (6)
direction. The numerical difference information of the two pressure
Where the preform thickness H is related to a given compaction pres- transducers is then transferred to a PC with LABVIEW software and two
m 1
sure P, where = A and are empirical material constants. graphs of pressure against time are automatically plotted. When the two
c
Through-thickness compressibility power law curve fitting is presented curves show that there is a constant pressure drop the test is stopped.
in Table 1. Thereafter from Darcy's law eq. (1), K3 is calculated since all the other
factors such as fluid velocity (constant) and the used Trent HDX30 oil
2.5. Experimental permeability measurements viscosity are known.
Therefore with the above mentioned experimental method in un-
Bidirectional flow experimental method was used for the in-plane saturated radial flow the in-plane permeabilities (K1, K2) and flow or-
permeability K1, K2 measurements: With this method, the test fluid was ientation (θ) were measured. In saturated unidirectional flow at a
injected from the centre of the mould cavity and the analytical solution constant flow rate, the through-thickness permeability K3 was de-
was based on Darcy's law eq. (1). For an isotropic scenario, the flow termined from the pressure variation across the specimen thickness
front would advance in a circular shape, and the following solution has with the use of Darcy's law. This technique has the advantage of the
been proposed eq. (7): need for only one preform to measure the permeability of all the fibre
volume fractions desired. In-plane permeability power law curve fitting
2
Rf Rf 4tK P for three different volume fractions 0.44, 0.5, 0.58 is presented in
2 ln 1 +1=
R0 R0 µR20 (7) Table 2 a), Through-thickness permeability power law curve fitting is
presented in Table 2 b).
where: Rf is the flow front radius at time t, R0 inlet radius, i.e. the radius
of the hole where the reinforcement stack at the centre injection point,
2.6. Description of the instrumentation flow analysis on a 90° curved plate
ΔP is the pressure gradient, t is the elapsed time, μ the fluid viscosity, Φ
the porosity and K the isotropic permeability (K = Kx = Ky).
In order to analyze the race-track modelling, a prototype trans-
For the anisotropic case, Kx ≠ Ky results in the flow front having an
parent tool with a 90° curved plate mould cavity was designed and
elliptical shape. Several simplification methods exist in the literature as
fabricated.
reported by Endruweit, A. et al. [38]. The procedures for one of the
The transparent rig was made of two pieces; one male and one fe-
simplified solutions are shown, which transforms the anisotropic per-
male. The uniform cavity on the male part was manufactured with di-
meability into an equivalent isotropic system, where the Laplace
mension 150 mm along the race-track section and 2.75 mm height
equation is utilized. A point in the original domain is transformed to a
along a 90° curved plate. The radius of the male part was set at 3.2 mm
new coordinate system: (x) (y)= > (xe ye) by the relations eq. (8):
while the radius of the female part was set at 5.95 m m to maintain a
1 1 constant cavity thickness.
Ky 4 Ky 4
xe = x and ye = y The experimental setup of the apparatus for the racetrack image
Kx Kx (8) visualization is shown in Fig. 3 and consisted of:
In this equivalent isotropic system, the flow front is represented by a
circular shape with R = Rxe = Rye. Along with the relationship between (i) The Perspex rig.
x and y in the original domain, the solution for permeability can be (ii) An appropriately modified table that was hollow in the centre in
obtained by the following set of equation (9): order to visualise the flow from underneath.

Ke = Kx Ky
Table 2
1
Experimental preform permeability K1, K2, K3 against Vf that may be
Ky 4 used in simulation tools.
Rx 0, e = R0
Kx (9) a) In-plain K1, K2 fitting equations:

2 K1 fitting eq.(m2) K2 fitting eq.(m2)


µR x20, e Rx Rx Preform
Ke = 2 ln 1 +1
4t P R0 R0 2/2 Twill 0.001 Vf (−11.28)
0.0012 Vf (−10.73)

where Rx is the semi-major axis of the flow front ellipse at time t, Ke the
b) Through thickness K3 fitting equations:
tested preform permeability and Rx0,e, is the equivalent injection gate
dimension in direction Rx for a circular injection gate in elliptical co- Preform K3 fitting eq.(m2)
ordinates reported by Endruweit et al. [38]. (−6.644)
2/2 Twill 0.0593 Vf
Experimental through thickness permeability K3 was measured with

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S. Koutsonas Composites Science and Technology 168 (2018) 448–459

Fig. 3. Set up of the apparatus for preform infusion. The displayed instrumentation was used for the race-track image visualization along the 90° curved plate on a
hollow table.

(iii) A personal PC with MATLAB software installed. 3. Race-track modelling


(iv) A vacuum pump.
(v) A pressure pot indicator. 3.1. Race-track modelling procedure
(vi) Metallic fixtures and two webcams, with one positioned above the
mould and the other below. Macro-flow models consider flows through a fibre preform with a
(vii) Commercial motor oil type HDX30 (with measured viscosity defined permeability in the present work the race-track effect was
Appendix B) modelled, by grouping different zones on 90° curved plate reinforce-
(viii) A tripod with a light ment and by assigning to each of them a single local permeability. The
modelling software used was PAM-RTM® developed by ESI group [23].
The objective was to create a transparent apparatus with gates, However despite its many advantages, this software is also quite time-
vents, preform cavity and fluid delivery that would reproduce experi- consuming making 3D computations long enough and complex parts
mentally the 90° preform bending simulations referred to in Figs. 9 and (such as the Advanced Composites Truss Structures) with multiple in-
10 iii), iv) on this article. jection ports and vent gates, required high-speed processing power to
be used.
2.7. Experimental methodology Within PAM-RTM® the saturated, partially saturated and un-
saturated flow regions are modelled using the Finite Element Control
The set up for experimental flow visualization instrumentation used Volume method, where each node is assigned a fill factor one (filled
for the experimental comparison with numerical simulations was pre- node), between zero and one (partially filled node) and zero (unfilled
sented in Fig. 3. Image visualization of the flow front propagation on node).
both sides of the Perspex (top and bottom side) provided information
about race-track along the 90° curved plate preform during liquid in- 3.2. FE CAD 90° curved plate race-track modelling
fusion with oil type HDX30 with a known viscosity.
The methodology followed here was similar to that reported by 3.2.1. Two-dimensional FE CAD 90° curved plate race-track modelling
Bickerton et al. [8,9]. All experimental results were obtained according As soon as the resin flow front arrives in the mould at the 90° curve
to the experimental setup Fig. 3. plate edges, (where gaps often exist between the preform and mould
All specimens were cut to the same dimensions as the Perspex wall), the resin will tend to flow faster than elsewhere in the mould as
cavity. Thereafter each fabric specimen was weighed with a precision reported for example by Liu et al. [3]. Bickerton et al. [8,9] reported the
scale ( ± 0.1 g) and placed inside the Perspex cavity. When the two mould curvature effects on preform permeability during mould filling
webcams, PC, and lights were set up the liquid infusion of known in RTM with his experimental work. By taking into account this effect
viscosity, oil type HDX30 started and so the image data collection. For and in order to model the variability the following approach will be
visualization purposes, a MATLAB view interface code was used used: Firstly the critical variability areas (gap channels) of a component
(Appendix A). All experimental image visualization output files were must be considered. At edges during the filling process, the local per-
collected on the PC. meability may differ from the rest of the component. This is because of
Following the above method, a number of 2/2 twill 3-layers a free channel between the mould wall and the fabric Dong [24]. Thus
weaving architecture were experimentally tested. Thereafter the race- the local permeability may be given from the empirical equation re-
track behaviour of experimental results are presented for comparison ported by Endruweit et al. [21] and Pillai et al. [22] as shown equation
with the modelling results in Figs. 9 and 10 iii), iv). (10):

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S. Koutsonas Composites Science and Technology 168 (2018) 448–459

Fig. 4. Curved plate model injection gate (group 1, indicated by blue line left)
and vent (group 2, indicated by the green line right end). Red arrows shown the
resin through thickness flow direction for all 2D, 3D 90° curve plate CAD
models. (For interpretation of the references to colour in this figure legend, the
reader is referred to the Web version of this article.)

Fig. 6. 3D FE CAD 90° curved plate models meshed with seven zones geometry
Fig. 5. 2D FE model with 9800 triangular elements (due to PAM-RTM) on a 90° of different permeability, three hgap zones (green, yellow, purple) see red ar-
curved plate, geometry with five zones you may see red arrow (green, yellow, rows, three compressed zones with different Vf (turquoise, orange, pink) and
purple, turquoise, orange) colours of different local permeability for race-track blue colour zone with the fabric's permeability (a) with 154350 tetrahedral
modelling and blue colour zone with the fabric's permeability. (For inter- elements and hmax 0.85 mm (b) with 300600 tetrahedral elements and hmax
pretation of the references to colour in this figure legend, the reader is referred 0.35 mm. (For interpretation of the references to colour in this figure legend,
to the Web version of this article.) the reader is referred to the Web version of this article.)

h2 height and hgap is the gap height between the preform and the mould
K=
12 (10) wall. So for an anisotropic preform, the in-plane permeability will be
Trochu et al. [13] as shown equation (12):
Where K in (m2) is the permeability of the gap and h is the gap between
the fabric and mould wall. For all 2D, 3D curve plate models a linear (hfabric K1 + hgap K gap)
K1aver =
injection gate (inlet) from one end and linear vent (outlet) from the hfabric + hgap (12)
other end were used as shown in Fig. 4.
Firstly a 2D CAD model of 90° curve plate was designed and meshed and
with triangular finite elements in Altair Hyper-mesh software as shown
(hfabric K2 + hgap K gap)
in Fig. 5. K2aver =
Along the 90° curved plate a number of five different zones were hfabric + hgap
generated. Element properties were determined by taking into account
Furthermore, K1aver, K2aver were used as local permeability input
the weighted averaged permeability of the compacted preform and the
data along with the material experimental properties presented with a
gap and by assuming good in-plane flow behaviour as suggested by
power law in Tables 1 and 2 The FE modelling in 2D provided an
Trochu et al. [13] according to equation (11):
average estimation about how much local permeability may be affected
(hfabric Kfabric + hgap K gap) by fabric's bending along a 90° angle during infusion in RTM process.
K2D = As an input for 2D flow simulations, thickness-weighted averaging
hfabric + hgap (11)
of the equivalent gap permeability and the permeability of the com-
2
where K2D in (m ) is the average 2D-element permeability, Kfabric is the pressed fabric allows the effective permeability for each segment of the
fabric permeability, Kgap is the gap permeability, hfabric is the preform bend to be estimated.

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S. Koutsonas Composites Science and Technology 168 (2018) 448–459

3.2.2. Three-dimensional FE CAD 90° curved plate race-track modelling


2.2 Twill fabric of the same size was laid down with parallel edges
on moulder and therefore with reduced fibre on the outside side of the
90° corner. Experimental analysis of localized fabric compression in-
dicated as reported by Koutsona [27] that the gap height along the 90°
bend can be modelled as a parabolic equation with preform thickness H
equation (6), Table 1 related to a given compaction pressure P as pre-
sented in equation (10). Based on this model, the bend has been seg-
mented into materials zones (layer by layer) with different compaction
force P, average gap height and fabric thickness as shows Table 1 Fig. 6
(a), (b). The equivalent permeability of the gap can be estimated, and
the permeability of the compressed reinforcement can be determined by
through interpolation of the permeability measured at different com-
paction levels coloured zones.
To model three-dimensional flow (with the through-thickness per- Fig. 7. Permeability vector orientations K1 (red arrows), K2 (green arrows) on a
meability K3), 3D FE CAD models were designed and meshed with bend 3D curved plate model. (For interpretation of the references to colour in this
zone segmentation. For each zone, the average fabric thickness Hfabric figure legend, the reader is referred to the Web version of this article.)
was determined with the equivalent preform permeability in relation to
the fibre volume fraction Vf and the gap thickness hgap with equivalent
gap permeability according to equation (10). In this case, a mesh with For the flow behaviour during RTM, fluid mass conservation and
tetrahedral finite elements was used allowing higher geometrical de- equations of unsaturated flow of a viscous liquid through a porous
tails in comparison to other types of finite elements. However, the use medium were solved by PAM-RTM®, based on an adaptive mesh as
of high element mesh density leads to an FE model which requires in- presented by Trochu et al. [13]. All the 2D, 3D FE CAD model simu-
tensive computation. Therefore for practical reasons, it was preferable lations were scaled in the same dimensions as the experiments with a
to limit the mesh refinement on the FE CAD model and the number of Perspex cavity tool that has been used subsequently for the modelling
zones along the curved plate. verification.
Thus 3D race-tracking was studied by creating a series of FE 3D CAD
models of different gap heights (hmax). In Fig. 6 (a), (b) the 2.75 mm 3.3. Permeability vector orientations inside 90° 3D curved plate
radius height was divided into two sections:
For all the FE 3D CAD curved plate geometry models, (one of which
(i) a blue colour zone 1 with the fabric's permeability, is shown in Fig. 7, permeability vector orientations were incorporated
(ii) an outer gap section with measured maximum gap height (hmax) of for each tetrahedral element. For this, onto all tetrahedral elements
resin rich zones 2, 3 and 4 (green, yellow and purple), assigned and the warp in-plane K1 permeability orientations and the
(iii) a compressed bent fabric section along the 90° curved plate zones weft in-plane K2 permeability orientations. These are shown in Fig. 7.
5, 6 and 7 (pink, orange and turquoise), under the racetrack The through-thickness K3-permeability orientation was automatically
channel of higher volume fraction Vf and with compressed fabric considered by the PAM-RTM® software, to be perpendicular to K1 and
permeability. K2 accordingly.

Within the zones, the permeability of the gap was assigned ac- 3.4. 2/2 twill volume fractions for simulations
cording to equation (10). The gap height was derived from stochastic
modelling based on experimental observations by Koutsona [27]. On In order to evaluate the areal density (d) of the tested 2/2 Twill
the bent preform and along the 90° angle, the material properties fabric a series of experimental measurements of mass (Kg) and area
(Tables 1–3) were assigned with the appropriate volume fraction Vf. (m2) were done for each preform. Thereafter the average aerial density
Thereafter a series of six FE 3D CAD models were designed and con- of each preform was defined as the division of mass (Kg) against area
structed with hmax = 0.35, 0.45, 0.55, 0.65, 0.75, 0.85 mm, i.e. values (m2) and shown in Table 3. With the use of equation (13)
within the range of those measured with Coordinate Measurement m
Machine (CMM) experimental observations. Gaps with hmax less than Vf =
AH (13)
0.35 mm have not been modelled due to the stochastic variability of the
tested preform that made it impossible to quantify experimentally a where m is the specimen mass, A is the specimen area, and ρ is the
small gap. The experimental behaviour of each of the tested fabrics was density of the carbon fibres and H the mould height, the fibre volume
thereafter compared with the closest behaviour of the above generated fraction was calculated as a function of the above-mentioned para-
FE 2D and 3D CAD models. meters.
FE modelling in 3D provided more detailed information about how Volume fraction eq. (13) numerical calculation for 2/2 twill 3-layer
much local permeability may be affected by fabric's bending along a 90° preform for 2.75 mm thickness: Vf 3layer = 42.6% .
angle during infusion in RTM process. Fibre volume fractions calculated have been used as simulations
input data with PAM-RTM® firstly for FE CAD 90° curve plate models in
Table 3 this paper.
2/2 twill aerial density measured experimentally for the average value.
3.5. Mesh sensitivity
Mass (Kg) Area (m) d (m/A)

0.343 0.7 × 0.7 0.7 In this section the 2D, 3D 90° curved plate mesh sensitivity studies
0.0668 0.36 × 0.28 0.663 are presented. All sensitivity studies were performed for linear injection
0.0675 0.36 × 0.28 0.67 gate and vent along the preform bend geometry in 2D, 3D as shown
0.064 0.4 × 0.23 0.696
Tables 4–9 in sections 4.6, 4.7. The fill time (s) of each model was
0.0658 0.4 × 0.235 0.7
0.12142 0.686 provided by the simulation. Analytical filling time was calculated with
the use of equation (14)

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S. Koutsonas Composites Science and Technology 168 (2018) 448–459

Table 4 Table 8
2D 90°curve plate sensitivity with 6899 triangular elements. 3D 90°curved plate upper side racetrack sensitivity.
K Principal Permeability (m2) Filling Time (s) Analytical Filling Time (s) No of Tetrah. Racetrack fill Edge fill Δy-lag position Racetrack
elem. time (s) time (s) edge (mm) zones
3.40E-10 8.79 8.82
2.22E-10 5.77 5.75 22680 0.736 2.13 61.7 3 out of 6
5.21E-12 13.36 13.5 154350 0.755 2.15 62.0 3 out of 6

Table 5 Table 9
3D 90°curve plate sensitivity with 169892 tetrahedral elements. 3D 90°curve plate lower side racetrack sensitivity.
K Principal Permeability (m2) Filling Time (s) Analytical Filling Time (s) No of Tetrah. Racetrack fill Edge fill Δy lag position Racetrack
elem. time (s) time (s) edge (mm) zones
3.40E-10 8.69 8.82
2.22E-10 5.76 5.75 22680 0.818 2.13 27.0 3 out of 6
5.21E-12 13.29 13.5 154350 0.839 2.15 32.0 3 out of 6

Table 6 elements.
2D 90°curved plate with one segment racetrack zone. Due to mesh refinement of the gap geometry which required a 3D
No of Triag. Racetrack fill Edge fill Δy lag position Racetrack zones structured mesh (highly time-consuming and intensive computation-
Elem. time (s) time (s) (mm) ally) race-tracking mesh sensitivity was only considered for two 3D
models like those presented in Fig. 6.
22320 1.69 2.13 16.7 1 zone gap
The calculation of race-tracking was done at the end of the vent of
the upper side of the 3D curved plate model.
The Δy lag racetrack position was calculated at the injection point of
the opposite side (lower part) 3D curved plate model: Table 8 shows
µ
t ff = x ff2 racetrack sensitivity for the upper side 3D curved plate models.
2KPinj (14) Table 9 shows lower side Δy lag racetrack sensitivity.
Results of filling time of the edge for increasing number of tetra-
for rectilinear flow presented by Rudd et al. [1] where Φ is the bed
hedral elements comply well in both 3D and 2D cases with a small
porosity, μ is the fluid viscosity, K is the permeability (m2), P the in-
variation which demonstrates an acceptable level of mesh convergence.
jection pressure (bar), xff is the filling distance (m). All models had the
All results 3D, 2D cases “include theory and simulation” agreed closely
same dimensions as the Perspex tool cavity used for the FE/CV mod-
with the analytical fill time and so the above models may use for ex-
elling verification.
perimental comparison.

3.6. Two-dimensional and three-dimensional 90° curved plate sensitivity 4. Results and discussion

2D, 3D 90° curved plate models without the racetrack gap seg- The experimental flow behaviour was captured through imaging
mentation were studied for sensitivity verification using K principal with a Mat-Lab software code web cameras presented on Appendix A.
permeability (m2) as shown in Tables 4 and 5. All results “include Therefore, in the following sections, the simulation which was the
theory and simulation” agreed closely with the analytical fill time and closest match to a particular experiment is presented. From this, the
so the above models may use for experimental comparison. racetrack gap height used in the simulation is presumed to determined
represent that present in the experiment. This comparison yielded the
3.7. Two-dimensional and three-dimensional with segment zones race- racetrack behaviour of the tested fabrics along the 90° angle.
tracking 90° curved plate sensitivity Considering different mould materials and testing the simile pre-
forms, some small flow variations were expected, from the previously
For example in Table 6, racetrack fill time represents the fill time tested 2/2 twill fabrics. This was due to:
along the racetrack zone, edge fill time is the fill time at the edge of the
mould, and Δy lag position the distance between them. • Stochastic fabric variability that has not introduced on the 90°
2D racetrack sensitivity was verified for a series of models as shown curved plate FEA model.
in Table 6 (first with one segment on bend geometry), Table 7, using, • Local variation of the friction-compression coefficient, of the pre-
the permeability data presented in Tables 1 and 2 for the 2/2 twill forms.
fabric i) 2D 90° curved plate models with five segment racetrack zones • Lateral race-tracking on edges and corners of the model during in-
as per Fig. 5. Table 7 shows racetrack fill time against a number of fusion was not considered as well on FE/CV Analysis modelling.
elements, illustrating that convergence was seen for 93.600 triangular
The experimental flow behaviour was captured through imaging by
the web cameras. Therefore, in the following sections, the simulation
Table 7 which was the closest match to a particular experiment is presented.
2D 90°curve plate 5 gap zone racetrack sensitivity studies. From this, the racetrack gap height used in the simulation is presumed
to determined represent that present in the experiment. This compar-
No of Triag. Racetrack fill Edge fill Δy lag position Racetrack zones
ison yielded the racetrack behaviour of the tested fabrics along the 90°
Elem. time (s) time (s) (mm)
angle.
9800 1.77 2.12 12.9 5 zones
28800 1.77 2.13 13.3 5 zones
4.1. 2/2 twill race-tracking
50400 1.74 2.132 14.2 5 zones
93600 1.74 2.135 14.4 5 zones
In this section two-dimensional 2D, 3D FE curved plate models via

455
S. Koutsonas Composites Science and Technology 168 (2018) 448–459

presents y fit race-track analysis for Fig. 8.

4.1.2. Results discussion 2D 2/2 twill 0.85 mm gap FE model


The simulated 2D average flow front position showing race-
tracking, with lagging pressure gradient shapes reflect the dominating
effect of race-tracking in the gap as shown in Fig. 8 and numerically
presented in Table 10.
For the 2D case simulated y fill position centre measured at 0.05,
0.10, 0.15 (m) from the inlet at this point y fill position top-left and
down-right was found to be 0.0242, 0.0598, 0.0999 m respectively in-
creased Δy race-tracking flow front for 0.0258, 0.0402 and 0.0501 m at
the outlet.

4.1.3. Three-dimensional 2/2 twill race-tracking for 0.85 mm gap FE model


In order to obtain more accurate results, through-thickness varia-
tions in permeability have to be taken into account in 3D FE model flow
simulation.
3D 2/2 twill weave FE model shown in Fig. 9 for a 0.85 mm gap
height along the 90° angle compared with Perspex experiment revealed
about the same fluid flow behaviour and so a gap of about the same
height for the upper side bend of the tool.
Shape analysis on resin flow simulation based on 2/2 twill along the
90° angle on Fig. 9 presented in following Table 11.
Comparing 3D modelling race-track results on Fig. 9 and Table 11 i)
with 11 ii), Table 11 iii) with 11 iv) give close relation to the experi-
mental results than those on 2D modelling on Table 10 as expected due
to more realistic Vf along the 90° curved plate bending.

4.1.4. Results discussion 3D 2/2 twill 0.85 mm gap FE model


In this situation (case 1) the simulated flow front pressure gradient
shapes reflect the dominating effect of race-tracking in the gap.
This observation indicated that the volume fraction modelling along
the 90° angle with the 2/2 twill textile was correctly evaluated and that
the fluid flow between the mould and the 2/2 twill fabric have been
predicted more accurately with 3D FE modelling.
Modelling results of fluid flow agree well with the experiment as
shows Fig. 9 and Table 11.
Considering that the local variability of the fabric and the others
phenomena in section 4.8 bullet points did not take on to account for
the 3D FE model these are satisfactory results.

4.1.5. Three-dimensional 2/2 twill race-tracking for 0.35 mm gap FE model


A further 2/2 twill weave Perspex experiment revealed a fluid flow
behaviour filling similar to 3D FE (PAM-RTM®) 0.35 mm gap height for
the upper side bend of the tool.
The shape analysis on Fig. 10 3D model with 2/2 twill race-tracking
for 0.35 mm gap FE model presented on following Table 12.
Fig. 8. i), ii), iii) 2D 2/2 twill Δy racetrack evaluation for 0.85 mm gap mod- 3D modelling race-track results on Fig. 10 and Table 12 i), ii),
elled with the PAM-RTM software (red coloured filled area, blue unfilled, other Table 12 iii), iv) are more realistic due to more realistic Vf along the 90°
colours half filled). (For interpretation of the references to colour in this figure
curved plate bending.
legend, the reader is referred to the Web version of this article.)

4.1.6. Results discussion 3D 2/2 twill race-tracking for 0.35 mm gap FE


model
the PAM-RTM® software shown in Fig. 8 i), ii), iii), 9 i), ii), 10 i), ii) 3D simulation modelling results from PAM-RTM® with 2/2 twill
were compared with the experimental results for the 2/2 twill fabric properties, 0.35 mm gap observed similar flow behaviour compared
Fig. 9 iii), iv), Fig. 10 iii), iv). with a Perspex tool experiments (with the same dimensions).
In this situation, the through-thickness permeability K3 is less
4.1.1. Two-dimensional 2/2 twill race-tracking for 0.85 mm gap FE model dominant and therefore there is only a small racetrack on top of the tool
As input for 2D flow simulations, thickness-weighted averaging of along the bend angle and small lag of flow front at the opposite side of
the equivalent gap permeability shown in Fig. 5 and the permeability of the tool.
the compressed fabric allow the effective permeability for each segment Similar flow behaviour was obtained with the 3D FE CAD model for
of the bend to be estimated. In the 2D racetrack model, the flow front a 0.35 mm gap with 2/2 twill material properties as shown in Fig. 10
(red colour filled area) is symmetrical as shown in Fig. 8. Table 10 and Table 12 and in modelling the results of fluid flow are in agreement

456
S. Koutsonas Composites Science and Technology 168 (2018) 448–459

Fig. 9. 2/2 twill racetrack evaluation (at y = 100 mm of race-track) for 0.85 mm gap size, firstly obtained with the PAM-RTM software 3D FE CAD model (top images
i), ii)) and secondly with the Perspex transparent tool (lower images iii), iv)).

with the experiment. Experimental results observation of the 2/2 twill preform with the
Perspex tool on a 90° curved angle bend, suggested that during infusion
4.1.7. Results discussion 3D 2/2 twill race-tracking there may be a centre gap of 0.85 mm between reinforcement and tool,
Experimental observations with the Perspex transparent tool sug- which results in race-tracking at the upper radius of the bend.
gested that the racetrack gap on the upper part of the bend angle may In this case, the through-thickness permeability K3 is reasonable
vary between 0.85 and 0.35 mm. high and therefore may allow an effective through thickness fluid ex-
The variation of the through-thickness permeability K3 against vo- change on both sides of the bend. The flow front shape at the top and
lume fraction Vf provided different shapes of race-tracking, which were the opposite side was dominated by the racetrack zone of the upper
modelled with the PAM-RTM® software. part. A similar behaviour was obtained for the 2/2 twill material

Fig. 10. 2/2 twill racetrack evaluation for the 0.35 mm gap size, obtained with the PAM-RTM software 3D FE CAD model (top images i), ii)) and with the Perspex
transparent tool (lower images iii), iv)).

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S. Koutsonas Composites Science and Technology 168 (2018) 448–459

Table 10
2D 2/2 twill racetrack flow shape analysis from inlet for a 0.85 mm gap FE model of Fig. 9.
y-fill position 90° centre (mm)a y-fill position upper (mm) y-fill position lower (mm) Δy race-track (fill 90° centre (−) fill average upper/lower) (mm)

50 24.2 24.2 25.8


100 59.8 59.8 40.2
150 99.9 99.9 50.1

a
For briefly in the future only images y-fill presented.

Table 11 Table 12
2/2 twill racetrack flow shape analysis from the inlet for a 0.85 mm gap FE 2/2 twill racetrack flow shape analysis from the inlet for a 0.35 mm gap FE
model against 2/2 twill Perspex exp. i), ii) upper sides, iii), iv) lower sides model against 2/2 twill Perspex exp. i), ii) upper sides, iii), iv) lower sides
related to Fig. 9. related to Fig. 9.
y-fill position 90° y-fill position y-fill position Δy race-track (fill 90° y-fill position 90° y-fill position y-fill position Δy race-track (fill 90°
centre (mm) upper (mm) lower (mm) centre (−) fill average centre (mm) upper (mm) lower (mm) centre (−) fill average
upper/lower) (mm) upper/lower) (mm)

i) 3D 2/2 twill FE (PAM-RTM) model shape analysis upper side: i) 3D 2/2 twill FE (PAM-RTM) model shape analysis upper side:
50 14.3 14.3 35.7 50 39.4 39.4 10.6
100 33.3 33.3 66.7 100 87 87 13
150 63.6 63.6 86.4 150 137 137 13
ii) 2/2 twill Perspex exp. shape analysis upper side: ii) 2/2 twill Perspex exp. shape analysis upper side:
50 13.8 18.6 33.8 50 48.6 42 4.7
100 27.5 28.3 72.1 100 89.3 88.2 11.3
150 40.3 57.5 101.1 150 134.5 126 19.7
iii) 3D 2/2 twill FE (PAM-RTM) model shape analysis lower side: iii) 3D 2/2 twill FE (PAM-RTM) model shape analysis lower side:
50 33.2 33.2 16.8 43.9 50 50 −6.1
100 67.4 67.4 32.6 93.8 100 100 −6.2
150 112 112 38 141 150 150 −9
iv) 2/2 twill Perspex exp. shape analysis lower side: iv) 2/2 twill Perspex exp. shape analysis lower side:
50 31.1 30.1 19.4 47.9 49.7 50.7 −2.3
100 68.7 68.2 31.6 93.6 98.7 100.5 −6
150 113.1 114.1 36.4 141.9 149 150 −7.7

and variability data can complement experimental data in order to


properties of gap size 0.85 mm, but with the 3D FE CAD model as enhance flow simulations at the component scale. The future scope on
shown in Fig. 9. this research adds the racetrack behaviour in Advanced Composites
For a 0.35 mm centre gap observed (transient behaviour) the Structures CAE/CAD geometries which include the 90° composite fibre
through-thickness permeability K3 is less dominant therefore there is curve plates in order to be able to predict the racetrack and flow be-
only a small racetrack on top of the tool along the bend angle and small haviour in more advanced composites geometries like Advanced
lag of flow front at the opposite side of the tool as presented in Fig. 10. Composites Truss Structures.

5. Conclusions Acknowledgement

A novel numerical approach for 3D CV/FE CAD modelling was de- The work reported in this article was carried out under the Innovate
veloped in order to predict race-tracking and variability for advanced UK collaborative research through Advanced Composites Truss
composites structures. A stochastic analysis technique was developed to Structures (ACTS) project TP/8/MAT/6/I/Q1505D with industrial
account for the effect of variability during the fabrication process by partners Airbus, Bentley Motors Ltd, Composites Integration Ltd,
RTM. The study based on this technique provided important insights Network Rail, NP-Aerospace, Pipex, QinetiQ, Tony Gee, Sigmatex Ltd,
into flow filling variations, void formation and optimization on a gen- Oxford Brooks University, and The University of Nottingham. JEC
eric 90° curved angle bend composite 2/2 twill textile. Composites winner innovation award was given for the ACTS project
The model technique developed from this work can be used to ac- which includes the racetrack modelling. Gratuitous mentions of
count for the effects of race-tracking and variability on any other Sigmatex Ltd woven performs. Special thanks to my supervisor of ACTS
composite component at the macroscale level. The predicted race-track project Prof Andy Long.

458
S. Koutsonas Composites Science and Technology 168 (2018) 448–459

Appendix A. Supplementary data

Supplementary data related to this article can be found at https://doi.org/10.1016/j.compscitech.2018.08.001.

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