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Iq Oq PQ
Iq Oq PQ
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D. Gowrisankar et al / J Biomed Sci and Res., Vol 2 (2), 2010,89-99
90
D. Gowrisankar et al / J Biomed Sci and Res., Vol 2 (2), 2010,89-99
PQ Relationships
System Name:
System ID No.:
Installation site:
Performer_______________Signature _______________Date:______
Reviewer_______________Signature________________Date:______
Manager_______________Signature________________Date:______
91
D. Gowrisankar et al / J Biomed Sci and Res., Vol 2 (2), 2010,89-99
25°C ± 2°C
92
D. Gowrisankar et al / J Biomed Sci and Res., Vol 2 (2), 2010,89-99
93
D. Gowrisankar et al / J Biomed Sci and Res., Vol 2 (2), 2010,89-99
94
D. Gowrisankar et al / J Biomed Sci and Res., Vol 2 (2), 2010,89-99
Vial equilibrium 22 m
Vial pressure 0.5 m
Loop fill 0.5 m
Loop equilibrium 0.05 m
Inject 1.00 m
GC cycle time 38 m
Oven temperature 80°C
Loop temperature 100°C
Vial pressure 10.8 psi
Acceptance criteria: The %RSD of System precision for head space auto
retention time should be not more than sampler:
1.0%& peak area should be not more than Preparation of standard solution: Prepare
5.0%. a standard mixture solution by taking
Methylene dichloride (0.6g), Chloroform
95
D. Gowrisankar et al / J Biomed Sci and Res., Vol 2 (2), 2010,89-99
96
D. Gowrisankar et al / J Biomed Sci and Res., Vol 2 (2), 2010,89-99
97
D. Gowrisankar et al / J Biomed Sci and Res., Vol 2 (2), 2010,89-99
98
D. Gowrisankar et al / J Biomed Sci and Res., Vol 2 (2), 2010,89-99
99