Professional Documents
Culture Documents
1Department of Nanotechnology, Medicaps Institute of Science & Technology, Madhya Pradesh, India,
2Head of Department of Chemistry, Medicaps Institute of Science & Technology, Madhya Pradesh, India,
----------------------------------------------------------------------------------------------------------------------------
Abstract: The present work describes synthesis and biosynthetic and environment friendly approach has
characterization of Titanium dioxide (TiO2) nanoparticles. added much importance because of its eco-friendly
TiO2 nanoparticles prepared by eco-friendly green synthesis products, biocompatibility and economic viability in the
method using Moringa oleifera leaves extract. The synthesized long run and also to avoid adverse effects during their
TiO2 nanoparticles were characterized by X-ray diffraction application especially in medical field.
(XRD). Anatase phase TiO2 nanoparticles with mean
crystalline size 12.22 nm and Band gap of 3.9 eV was obtained Biosynthesis of nanoparticles is a bottom up approach
by UV-Visible spectroscopy. where the main reaction occurring is reduction/oxidation.
The plant phytochemicals with antioxidant or reducing
Keywords: TiO2, XRD, Moringa oleifera, Band gap, properties are usually responsible for the preparation of
Crystalline size. metal and metal oxide nanoparticles [4]. The three eco-
friendly and green chemistry perspective for the
nanoparticle synthesis are the choice of the solvent
medium, reducing agent and non-toxic material for the
1. INTRODUCTION stabilization of nanoparticles.
Recently nanoparticle synthesis were achieved using plant
Nanotechnology is a branch of science which deals with extract such as azadirachta indica, camellia sinensis,
matter having at least one dimension sized from 1-100 nm. Nyctanthes arbor-tristis, coriandrum, nelumbo nucifera,
Nanomaterials are classified into organic and inorganic ocimum sanctum and several others which is compatible
material. The synthesis of inorganic metal oxide with the green chemistry principles. Among the various
nanoparticles has attracted considerable attention in biosynthetic approaches, the use of plant extract has
physical, chemical, biological, medical, optical, mechanical advantages such as easily available, safe to handle and
and engineering sciences where novel techniques are possess a broad viability of metabolites. The main
being developed to probe and manipulate single atom and phytochemicals responsible for the synthesis of
molecules [5]. Metal and metal oxide nanoparticles have nanoparticles are terpenoids, flavones, ketones, aldehydes,
high surface to volume ratio which is responsible for their amides [1]. In this paper we have reported green synthesis
fascinating properties such as antimicrobial, magnetic, using Moringa oleifera leaves. Moringa has chosen because
electronic and catalytic activity. Generally properties of of its antibacterial, anti-septic, antifungal and anti-
nanoparticles depend on size, shape, composition, inflammatory activities.
morphology and crystalline phase. Among the various
metal oxide nanoparticles, TiO2 nanoparticles have wide
applications in air and water purification, Dye sensitized
2. EXPERIMENT DETAILS
solar cell (DSSC) due to their potential oxidation strength,
high photo stability and non-toxicity.
Traditionally metal oxide nanoparticles were synthesized The healthy leaves of Moringa oleifera were collected from
by various physical and chemical methods. Some Agar District, Madhya Pradesh, India. The collected leaves
commonly used synthetic methods are non-sputtering, were washed to remove dust. Leaves were shade dried at
Solvothermal, reduction, sol-gel technique and room temperature for about 7 days in normal atmosphere.
electrochemical technique. But these methods are costly, Dried leaves were cut into fine pieces, grinded to get the
toxic, high pressure, high energy requirement and finest powder. Ten gram of the dried leaves were mixed
potentially hazardous [2]. Hence developing of reliable with 100 mL of ethanol and extracted under reflux
condition at 50oC. After one hour, the ethanolic leaf extract
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 470
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395 -0056
Volume: 04 Issue: 3 | Mar -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 471
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395 -0056
Volume: 04 Issue: 3 | Mar -2017 www.irjet.net p-ISSN: 2395-0072
4. CONCLUSION
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 472
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395 -0056
Volume: 04 Issue: 3 | Mar -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 473