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Original Article

Proc IMechE Part B:


J Engineering Manufacture
2016, Vol. 230(7) 1295–1308
Measurement of forced surface Ó IMechE 2015
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DOI: 10.1177/0954405415599928

deposition additive manufacturing pib.sagepub.com

Jarred C Heigel1, Pan Michaleris1,2 and Todd A Palmer3

Abstract
The accurate modeling of thermal gradients and distortion generated by directed energy deposition additive manufactur-
ing requires a thorough understanding of the underlying physical processes. One area that has the potential to signifi-
cantly affect the accuracy of thermomechanical simulations is the complex forced convection created by the inert gas
jets that are used to deliver metal powder to the melt pool and to shield the laser optics and the molten material. These
jets act on part surfaces with higher temperatures than those in similar processes such as welding and consequently have
a greater impact on the prevailing heat transfer mechanisms. A methodology is presented here which uses hot-film sen-
sors and constant voltage anemometry to measure the forced convection generated during additive manufacturing pro-
cesses. This methodology is then demonstrated by characterizing the convection generated by a PrecitecÒ YC50
deposition head under conditions commonly encountered in additive manufacturing. Surface roughness, nozzle config-
uration, and surface orientation are shown to have the greatest impact on the convection measurements, while the
impact from the flow rate is negligible.

Keywords
Additive manufacturing, finite element analysis, convection measurement, heat transfer, directed energy deposition

Date received: 22 August 2014; accepted: 13 July 2015

Introduction found in welding. FEA has been used extensively to


simulate welding processes,1–3 and many aspects of
In additive manufacturing (AM), components are pro- these studies are useful in defining models of the DED
duced in a layer-by-layer manner directly from a digital process. Unfortunately, the convection models used to
file. Directed energy deposition (DED) is a major sub- simulate shielding gas flows in welding may not be use-
set of currently available AM processes, in which a ful. During welding, the rate of convective heat transfer
high-energy density heat source, such as a laser, elec- from the weld bead to the environment is low com-
tron beam, or arc, is used to create a melt pool into pared to the rate of conductive heat transfer from the
which metal powder or wire is injected. The localized bead into the part.4 As a result, convective heat loss has
heat input and the heat removed through conduction, been excluded in some models,5 while natural convec-
convection, and radiation create complex thermal gra- tion has been applied to all free surfaces in others.6–10
dients. When combined with the contraction of the However, weld models are not very sensitive to convec-
melt pool during rapid solidification, plastic deforma- tion because of the comparatively short processing
tion and residual stress are induced and negatively
affect the finished part, causing it to crack or distort. 1
Department of Mechanical and Nuclear Engineering, The Pennsylvania
Finite element analysis (FEA) is often used to simulate State University, University Park, PA, USA
the thermal cycles and distortion experienced by dis- 2
Pan Computing LLC, State College, PA, USA
crete components during DED and similar processes. 3
Applied Research Laboratory, The Pennsylvania State University,
However, useful FEA results can only be achieved University Park, PA, USA
when the underlying physical processes are accurately
Corresponding author:
captured. Jarred C Heigel, National Institute of Standards and Technology,
The high-energy density heat source and the result- Gaithersburg, MD 20899, USA.
ing distortion modes in DED are very similar to those Email: jarred.heigel@gmail.com
1296 Proc IMechE Part B: J Engineering Manufacture 230(7)

times, low bulk temperatures, and the relatively small which is directly affected by the geometry of the nozzle.
amount of filler material addition compared to the size Researchers have also investigated how the impinge-
of the existing part. ment angle affects the heat transfer on a plate.25–28
Even though there are similarities with welding, Others have studied the velocity field and heat transfer
DED processes have unique characteristics that com- resulting from two coaxial jets29–33 and the effect of
plicate the convective heat transfer conditions. For particles in the flow.34 However, these studies are typi-
example, laser-based processes utilize inert gas jets that cally performed using nozzles that are designed to
are much more concentrated than those used in weld- achieve desired flow characteristics, not using nozzles
ing. These jets are used to shield the melt pool, protect designed for industrial applications. The complexity of
the laser optics, and deliver powder to the melt pool. the laser deposition process introduces a number of
Consequently, localized forced convection is generated other considerations when attempting to quantify coef-
on the surfaces of the melt pool and the rapidly solidi- ficients of convection for improved simulation results.
fying material. In addition, the long processing times For example, the interaction of the shielding and pow-
and high bulk temperatures prevalent during DED pro- der delivery jets, the effect of the metal powder in the
cesses allow a great deal of heat to be evacuated jet, and the effect of the deposited surface roughness on
through convection.11 Furthermore, the role of forced the rate of heat transfer have unknown impacts on the
convection becomes more significant when the large predicted convection and the accuracy of these deposi-
surface area of the deposition and the localization of tion process models.
the convection are considered. Measurements of the convection generated during
Michaleris4 demonstrated that the thermal results of deposition processes are required to produce accurate
FEA models of DED process are sensitive to surface FEA thermal models.4 A technique based on the use of
convection. Despite this sensitivity, convection has been hot-film constant voltage anemometry is developed
inconsistently applied to FEA models of the process. here to measure the heat transfer from the forced con-
For example, surface convection has been neglected12–15 vection produced by laser deposition heads.
or assumed to be equal to natural convection,16–18 Calibrations are made to then extract the coefficient of
much like the conditions used in the welding literature. convection from the heat dissipated from the sensor.
Dai and Shaw19 use an atypically high value of The forced convection is then characterized at multiple
60 W/m2/K for natural convection, although the moti- locations around the deposition head to generate a
vation for this choice is unclear. Some of the results map of the forced convection acting on the surface.
from these studies were not validated with experiments, This technique is demonstrated by characterizing the
while others were validated with small builds that did forced convection from a PrecitecÒ YC50 deposition
not allow sufficient time for the convective heat loss to head. An integrated distribution of these measurements
become significant. is compared to the average convection measured using
Other researchers have included forced convection the lumped capacitance method. Convection resulting
models in their simulations of laser-based DED pro- from jets impinging onto a flat surface or being
cesses. Qi et al.20 considered forced convection when bisected by a wall is measured to demonstrate the effect
modeling laser cladding; however, the value of the coef- of different surface orientations which are common in
ficient of convection was not reported. Michaleris4 AM. In addition, the effects of changes in gas flow rate,
approximated the forced convection as a sphere of nozzle configuration, and surface roughness are investi-
higher convection surrounding the melt pool, while free gated to illustrate how convection is affected by
convection was applied on all surfaces outside of this changes in common processing parameters.
sphere. Ghosh and Choi implemented forced convec-
tion from the shielding jet using the empirical equation
defined by Gardon and Cobonque21, 22 and natural Methodology
convection on all free surfaces not affected by the gas
flow.23 Zekovic et al.24 included the forced convection A new method is presented here that utilizes hot-film
on a thin wall and substrate caused by four radially sensors and constant voltage anemometry to obtain the
symmetric nozzles blowing an argon gas carrying pow- coefficient of convection from heat transfer measure-
der onto the deposition zone. Flow modeling software ments at locations on a flat surface relative to the
was used to calculate the velocity contours of the gas deposition head. Typically, these sensors are used to
around the wall and substrate, and analytical relations measure gas velocity based on empirically derived rela-
were used to calculate local coefficient of convection tionships that are dependent upon the gas properties.
for the velocity. However, none of these convection In the method presented here, the coefficient of convec-
models have been validated for the processes being tion is extracted from the direct measurement of the
modeled. heat transfer from the sensor. When a voltage is sup-
Heat transfer resulting from gas jets has been experi- plied by a Constant Voltage Anemometer (CVA) to a
mentally and numerically studied.25–34 Many of these hot-film sensor, the heat generated through resistive
works have concluded that the heat transfer is depen- heating is dissipated into the environment through con-
dent upon the velocity of the jet and its turbulence, vection and radiation and into the substrate through
Heigel et al. 1297

The total convective heat flux (qconv ) is defined by


ð
qconv dA = Ae qconv = hAe ðTe  Tamb Þ ð5Þ
Ae

The variables Te and Tamb are the temperature of the


element and the ambient temperature, respectively. The
total heat flux through radiation (qrad ) is
ð
 
Figure 1. Energy balance of the sensor element. qrad dA = Ae qrad = esAe T4e  T4amb ð6Þ
Ae

where s is the Stefan–Boltzmann constant and e is the


conduction. Each sensor must be calibrated to deter-
surface emissivity of the element. The total amount of
mine the conductive heat transfer and the effective area
qcond ) is
heat transferred through conduction (~
over which the radiation and convection occur. The
ð
results allow the coefficient of convection (h) to be
qcond dA = q~cond ð7Þ
extracted from the measurements. The distribution of h
on a surface resulting from a gas flow is then character- Ae

ized by taking measurements at incremental locations The total conductive heat transfer is derived empiri-
relative to the deposition head. cally in section ‘‘Conduction into the substrate.’’ As a
result, the total energy balance of the sensor is
Calculating h from hot-film anemometry
I2 Re  Ae qconv  Ae qrad  q~cond = 0 ð8Þ
measurements
The total energy balance is maintained despite
Constant voltage anemometry is used to measure the
changes in the heat transfer acting on the sensor ele-
steady-state heat transfer from the element of a hot-film
ment because its resistance changes in response. For
sensor into its surroundings, as shown in Figure 1, and
example, an increase in the convection acting on the
defined by the following energy balance
element decreases its temperature. In turn, both the ele-
ð ð ð ð
ment resistance and the total resistance of the circuit
QdV  qconv dA  qrad dA  qcond dA = 0 decrease, causing the current flowing through the ele-

Ve Ae Ae Ae ment to increase and leading to more resistive heating
ð1Þ that balances the increase in convective heat transfer.
The following equation relates the temperature and
where Q is the heat source generated within the element resistance of the element
with a volume ( Ve ) that is dissipated through convec-
Re
tion, conduction, and radiation. The corresponding sca- Reamb 1
lar heat fluxes (qconv , qrad , and qcond ) are assumed to be DT = Te  Tamb = ð9Þ
a
uniform over the effective area of the element (Ae ) as
derived empirically in section ‘‘Effective surface area of The resistance increases from its initial value (Reamb )
the element.’’ Applying an electric current to the ele- at ambient temperature to the value during the mea-
ment generates heat within it, as defined by surement according to the increase in temperature (DT)
ð and the temperature coefficient of resistance of the ele-
QdV = I2 Re ð2Þ ment (a). The initial resistance of the element must be
determined before the measurement. The total resis-

Ve
tance of the circuit during the measurement is calcu-
where the variables Re and I are the resistance of the lated from the anemometer output signal.
element and the current flowing through it, respectively. Based on these measurements, the coefficient of con-
The current is calculated using vection can be determined using the following
relationship
Vc
I= ð3Þ h=
R  
 Vc  2
where Vc is the constant voltage applied to the circuit. R ðR  Rl  Rw Þ  es ðTamb + DTÞ4 T4amb  q~cond
The total resistance of the circuit (R) equals the sum- Ae DT
mation of the resistances of the element (Re ), the sensor ð10Þ
leads (Rl ), and the wires connecting the sensor to the
anemometer (Rw ) The standard deviation of the coefficient of convec-
tion (sh ) is calculated using the propagation of error
R = Re + Rl + Rw ð4Þ formulation35
1298 Proc IMechE Part B: J Engineering Manufacture 230(7)

sffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
   2      
∂h 2 2 ∂h ∂h 2 2 ∂h 2 2 ∂h 2 2
sh = sV c + s2R + sq~cond + sA e + sDT ð11Þ
∂Vc ∂R ∂~ qcond ∂Ae ∂DT

where sVc and sR are the standard deviations of the Effective surface area of the element. Resistive heating
applied constant voltage and the calculated circuit resis- within the sensor element generates a greater tempera-
tance during the measurement, respectively. The stan- ture in the element than in the leads. This temperature
dard deviation of the element temperature (sDT ) is also gradient effectively spreads the heat over a greater area
derived using the propagation of error formulation than the nominal area of the element, as demonstrated
sffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi by O’Donovan et al.36 using a FEA model of a sensor.
  ffi In the method presented here, the effective surface area
∂DT 2 2
sDT = sR e ð12Þ is empirically derived (as a function of DT) by perform-
∂Re
ing a series of measurements of the heat transfer at a
where sRe is the standard deviation of the element resis- variety of constant voltages while the substrate is placed
tance during the measurement. The variables sq~cond and in a steady and uniform gas flow, hereafter known as
sAe are the standard deviations of the differences the reference flow. The convection generated by the ref-
between the calibration data and the empirically erence flow is measured using the lumped capacitance
derived functions for the conduction (~ qcond ) and the method.37 In this method, a thin plate of a known mate-
effective area (Ae ). rial and geometry is heated to a uniform temperature
and then placed in the reference flow. The temperature
of the plate is measured as it cools and is used to calcu-
 acting over
late the average coefficient of convection (h)
Sensor calibration
the plate. The cooling of the plate with a known volume
Conduction into the substrate. Conduction from the sensor (
V), density (r), and heat capacity (c) subjected to con-
element into the substrate is complex and cannot be vection and radiation is described as
easily calculated. Both the thin film onto which the sen-  
 ðT  Tamb Þ + esA T4  T4
sor element is deposited and the adhesive used to mount hA amb =  rc  VdT
dt
ð14Þ
the sensor to the substrate impact the conduction in
unknown ways. Empirically derived functions must, where A is the exposed surface area of the plate through
therefore, be developed to take into account the varia- which convection and radiation occur. Since equation
tions within the sensors, adhesives, and substrates. (14) is nonlinear, h is calculated using an iterative pro-
In order to measure the conduction, the sensor must cess to achieve a decay in T that matches the measured
be insulated from convection and radiation. Insulation temperature decay. Once the average coefficient of con-
is used to eliminate the convective and radiative heat vection is found, it can be substituted for h, so that the
transfer components and allow conduction to be mea- effective surface area can be calculated.
sured using the following relationship The lumped capacitance method is valid when the
ratio of convection to internal conduction is sufficiently
I2 Re  q~cond = 0 ð13Þ small. This ratio is described by the nondimensional
Biot number (Bi)
A range of constant voltages are applied to the sen-
sor to heat the element to different temperatures. h 
V
Bi = ð15Þ
Measurements of the heat transfer from the element Ak
are made at each constant voltage increment once the where k is the thermal conductivity of the plate. The
element temperature has stabilized. It is assumed that lumped capacitance method is a valid way to measure
the substrate temperature is equal to the ambient tem- the average coefficient of convection only when Bi is
perature (Tamb ) and does not change during the calibra- less than 0.1.37 The Biot number is calculated from all
tion since its thermal mass is orders of magnitude lumped capacitance measurements to prove their
larger than the thermal mass of the element. validity.
The average values of the constant voltage and the
output signal during the steady-state measurement at
each increment are used to calculate the increase in sen- Map the distribution of convection
sor element temperature (DT). These values are calcu- The distribution of the localized forced convection gen-
lated using the CVA supplied function to calculate the erated by a deposition head is characterized using mea-
circuit resistance from the output signal and equation surements made at incremental locations, as shown in
(9). Conductive heat transfer is calculated using equa- Figure 1. When the gas flow is begun, the sensor is
tion (13). A function is then fit to the data to relate con- allowed to achieve equilibrium, as defined in equation
ductive heat transfer to DT. The standard deviation of (8). The time required for this to occur is dependent
the difference between the data and the fit is used to cal- upon the sensor and substrate. Once the output signal
culate sq~cond . from the CVA becomes steady, the constant voltage
Heigel et al. 1299

Figure 2. Cross-sectional view of the PrecitecÒ YC50 head


and nozzles.

Figure 3. SenflexÒ SF9902 hot-film sensor with dimensions of


and the sensor output are recorded and then the mean the nickel element and copper leads: (a) sensor and (b)
values and standard deviations of these signals are used schematic diagram of sensor with dimensions.
to calculate the coefficient of convection (h) and the
standard deviation of this measurement (sh ) at this deposition head. The sensors are chosen because their
location. The relative position of the deposition head small element size results in a fine resolution of the mea-
to the sensor is then incrementally changed, and time is surement distribution. Figure 3 shows a schematic dia-
allowed for the signals to become steady once again gram of a characteristic sensor that consists of a nickel
before the signals are recorded, allowing h and sh for element and copper leads. The nickel element, which is
the new location to be calculated. This procedure is nominally 0.20 mm thick, 0.1 mm wide, and 1.4 mm
repeated until the convection distribution acting over long, has been deposited onto 0.2-mm-thick UpilexÒ
the desired surface area is mapped. polyimide film. Copper leads that are nominally 12 mm
thick and 0.76 mm wide are also deposited onto the
Validation of the methodology film. Copper wires with diameters of 0.25 mm and
lengths between 3.3 and 3.6 m are used to connect the
Equipment sensors to a four-channel Tao of Systems Integration,
Demonstration of the convection measurement method Inc. Model 4-600 CVA. The relationship between the
is performed using a commercially available Precitec output voltage (Vo ) and the total resistance of the cir-
YC50 clad head and nozzles, which are schematically cuit (R) is given as37
depicted in Figure 2. In this specific design, argon gas
flows through the center of the clad head to shield the 1
R= ð16Þ
melt pool and to protect the laser optics positioned a VVoc +b
upstream from the head. The inner nozzle constricts
the flow from a diameter of 42.0 mm at the interface where a and b are channel-specific variables that are
with the head to a diameter of 10.4 mm at the nozzle provided with the CVA.38 The voltage signals from the
exit over a length of 60.1 mm, allowing the shield flow CVA are acquired using a National Instruments NI
to exit the nozzle through an 85-mm2 area. Powder and 9205 module. Type K thermocouples are used to moni-
argon gas are delivered to the part through a 2.5-mm- tor the ambient temperature of the environment and to
wide circumferential channel in the clad head. The measure the temperature of the argon jets at the nozzle
clearance between the outer nozzle and the inner nozzle outlet. The jet temperature is measured before the con-
is 0.7 mm, and the powder delivery flow exits through vection measurements so that the thermocouple does
a 65-mm2 area between the inner and outer nozzles. not affect the flow during those measurements. It is
During processing, the bottom of the outer nozzle is found that the jet temperature is equal to the ambient
positioned at a constant height of 10 mm above the tar- temperature of the deposition environment. A National
get surface. Instruments NI 9213 module is used to acquire the ther-
SenflexÒ SF9902 single-element hot-film sensors mocouple signals. The acquired thermocouple and vol-
from Tao of Systems Integration, Inc. are used to mea- tage signals are recorded in a LabVIEWÒ environment
sure the convective heat transfer generated by the at a rate of 20 Hz.
1300 Proc IMechE Part B: J Engineering Manufacture 230(7)

Figure 4. Schematic diagram of the plexiglass substrate and the three hot-film sensors mounted on it.

100 100 100


sq =0.2 mW sq =0.2 mW sq =0.1 mW
cond cond cond
80 80 80
qcond (mW)

qcond (mW)

qcond (mW)
60 60
60
40 40
Data Data 40 Data
20 20
Fit Fit Fit
0 0 20
0 100 200 300 0 100 200 300 0 100 200 300
ΔT (°C) ΔT (°C) ΔT (°C)
(a) (b) (c)

Figure 5. For each sensor, the heat loss through conduction is dependent on the element temperature: (a) sensor 1, (b) sensor 2,
and (c) sensor 3.

Three sensors are attached to a 222-mm-long, 123- increment. Figure 5 presents the results from these
mm-wide, and 3.2-mm-thick plexiglass substrate using measurements. A second-order polynomial function
MACfilmÒ IF-2012 adhesive, as shown in Figure 4. produced the best fit to the data for each sensor, as
This configuration allows the convection acting on a shown in the following relationships
wall to be measured at different distances from the top
edge when the substrate is mounted vertically. A plexi- q~cond, sensor 1 =  2:428e7 DT2 + 3:854e4 DT  2:876e3
glass substrate was chosen because it has a lower ther- ð17Þ
mal conductivity than the metallic materials typically q~cond, sensor 2 =  2:174e DT + 4:072e DT  3:491e3
7 2 4

used in cladding operations. This selection decreases


ð18Þ
the energy transfer through conduction. A 45° edge is
ground into the back edge of the substrate, so that this q~cond, sensor 3 =  4:489e7 DT2 + 5:241e4 DT  1:149e3
edge has a minimal impact on the gas flow when the ð19Þ
substrate is mounted vertically to bisect the flow.
The quality of these fits is described by the difference
Sensors 1 and 2 are placed 0.8 and 5.4 mm from this
between the calculations and measurements at one stan-
edge, respectively. Sensor 3 is mounted near the middle
dard deviation. These values are less than 1% of the
of the substrate, 108.7 mm from the ground edge.
rate of conduction into the substrate from each sensor.

Heat loss through conduction. The process described in Effective surface area. The effective area of each sen-
section ‘‘Conduction into the substrate’’ is used to sor is found using the process described in section
empirically derive functions that describe the conduc- ‘‘Effective surface area of the element’’ using aluminum,
tive heat loss from each sensor into the plexiglass sub- copper, and steel plates. Different plates are used to
strate. Fiberglass insulation, 90 mm thick, is placed on demonstrate that this calibration is independent of the
top of the substrate. Measurements are made using chosen plate material. Table 1 presents the properties
constant voltages between 0.3 and 1.0 V, in 0.1-V incre- of these plates. Each plate is heated and then placed on
ments, to heat the nickel elements. At each setting, the an insulated fixture, to restrict the heat loss to one side
energy balance is allowed approximately 30 s to reach of the plate, and cooled in four different airflows. The
equilibrium before Vc and Vo signals are recorded over chosen reference flows have average velocities that are
a period of approximately 30 s. The mean values of similar to the output from the deposition head. Three
these signals are used to calculate DT and q~cond at each of the reference flows, with velocities of 1.3, 1.8, and
Heigel et al. 1301

Table 1. Properties of the plates used in the modified lumped capacitance analysis to determine the effective surface area of each
sensor element.

Al 6061-T6 Commercially pure Cu A36 steel

r (kg/m3) 2710 8470 7833


cp (J/kg/K) 896 397 465
k (W/m/K) 167 386 54
A (m2) 20:5e3 19:8e3 19:5e3
V (m3)
 65:2e6 62:8e6 124e6
Lc (mm) 3.18 3.17 6.36
e 0.09 0.038 0.79

Table 2. Results of the modified lumped capacitance measurements to determine the effective surface area of each sensor element.

Parallel to a Parallel to a Parallel to a Perpendicular to a


1.3-m/s airflow 1.8-m/s airflow 2.5-m/s airflow 2.8-m/s airflow
Plate Al Cu Steel Al Cu Steel Al Cu Steel Al Cu Steel
h (W/m /K)
2
27.5 25.4 26.6 32.5 29.4 30.4 39.5 36.8 38.5 25.4 22.5 23.6
Bi 5e24 2e24 4e23 7e24 3e24 4e23 8e24 3e24 5e23 7e24 3e24 4e23
Average h (W/m2/K) 2761 3162 3861 2461

7 7 7
6 Data 6 Data 6 Data
5 Fit 5 Fit 5 Fit
Ae (mm2)

Ae (mm2)

Ae (mm2)

4 4 4 sA =0.1 mm2
3 3 3 e

2 2
2 2
1 sA =0.3 mm 1 sA =0.3 mm
2
1
e
e
0 0 0
0 100 200 300 0 100 200 300 0 100 200 300
ΔT (°C) ΔT (°C) ΔT (°C)
(a) (b) (c)

Figure 6. Measurement data and the corresponding second-order exponential fit used to calculate the effective area for each
sensor: (a) sensor 1, (b) sensor 2, and (c) sensor 3.

2.5 m/s, are parallel to the plate. A fourth reference to 1.0 V in 0.1-V increments, to heat the element to a
flow with a velocity of 2.8 m/s is perpendicular to the range of temperatures. The mean value of each signal
cooling plate. and the average coefficient of convection from Table 2
Table 2 presents the results of the modified lumped are used to calculate the effective area using equation
capacitance measurements. The negligible differences (5) for each flow condition. Figure 6 presents the result-
between the measurements made using each plate indi- ing data to which second-order exponential equations
cate that the plate material has no impact on the cali- are fit to the data to develop functions to describe Ae
bration. The mean and standard deviation of the for each sensor, as well as the standard deviations of
average coefficient of convection is calculated for each the difference between the data and these functions
airflow. Considering the difference in properties of the
three plates, the small standard deviation in each air- Ae, sensor 1 = 5:66 exp0:017DT + 4:15 exp0:003DT ð20Þ
flow illustrates the consistency of the lumped capaci- Ae, sensor 2 = 22:45 exp 0:065DT
+ 5:48 exp 0:005DT
tance method to determine the average convection
ð21Þ
resulting from each reference flow condition.
After the average convection resulting from each ref- Ae, sensor 3 = 3:02 exp0:013DT + 0:56 exp0:001DT ð22Þ
erence flow is determined, measurements are made
using the hot-film sensors with the substrate placed in
the insulated fixture. Measurements are made in each Measurement cases. Table 3 presents the hot-film con-
airflow using constant voltages (Vc ), ranging from 0.3 stant voltage anemometry measurement cases, and
1302 Proc IMechE Part B: J Engineering Manufacture 230(7)

Table 3. Cases used to measure the distribution of h resulting from different argon flow conditions.

Case Jet Surface Shielding flow (L/min) Powder delivery flow (L/min)

1 Impinging Smooth 9 9
2 Impinging Smooth 19 19
3 Impinging Smooth 9 0
4 Impinging Smooth 19 0
5 Impinging Rough 9 9
6 Parallel Smooth 9 9

Figure 7. Illustrations of the experimental setups: (a) the distribution of h resulting from an impinging argon jet is measured in
cases 1 through 5 and (b) the distribution of h on a vertical wall when it bisects the argon jet is measured in case 6.

Figure 7 illustrates the different measurement setups surface area of the element makes the actual resolution
used to map the convection generated by the deposition slightly larger. Both the shielding and powder delivery
head. Powder is not included during these hot-film flows are used in cases 1 and 2, with rates of 9 and 19
measurements because its abrasive nature could dete- L/min, respectively. Cases 3 and 4 are performed to
riorate the nickel element, changing its resistance and investigate the heat transfer when the head is used for
affecting the calculation of the coefficient of convection laser processes that do not require powder to be
according to equation (10). injected into the melt pool, such as wire-based deposi-
The hot-film measurement method is used to map tion. The rate of the shielding flow in case 3 is 9 L/min
the distribution of h resulting from the argon jet and the rate in case 4 is 19 L/min. Measurements are
impinging onto a surface in cases 1 through 5. The performed along the X- and Y-axes in case 1 to identify
experimental setup is presented in Figure 6. The plexi- any axial asymmetry in the distribution of the convec-
glass substrate is placed on the horizontal X-Y plane, tive cooling, and all other case measurements are per-
with the sensor 3 located at the origin of the reference formed only along the X-axis to simplify the analysis.
frame. In this orientation, the dimensions of the nickel In case 5, ShurtapeÒ anti-skid tread tape is applied
element limit the nominal spatial resolution to 0.1 mm to the plexiglass substrate to simulate the rough surface
in the X-axis and 1.45 mm in the Y-axis. The effective typically produced in a powder-based deposition.
Heigel et al. 1303

Figure 8. Images of (a) the clad surface produced in Heigel et al.11 using a laser power of 2.5 kW, a travel speed of 10.6 mm/s, a
hatch spacing of 2 mm, and a powder flow delivery rate of 19 g/min and (b) the ShurtapeÒ anti-skid tread tape that is applied to the
surface around the sensor to approximate the clad surface.

Table 4. Values of h measured using the lumped capacitance method, resulting from an impinging jet created by a 9-L/min shield
flow and a 9-L/min powder delivery flow (case 1).

Material Al 6061-T6 Commercially pure Cu


Dimensions (mm) 49.33 3 46.43 3 3.12 50.01 3 50.08 3 3.18

Powder rate (g/min) 0 19 0 19


h (W/m2/K) 65.6 65.1 66.5 65.4
Bi 1e23 1e23 5e24 5e24

Figure 8 shows the similarity of a powder-clad surface11


and the tread tape. The roughness of these two surfaces
was measured by Gouge et al.39 using optical profilo-
metry. The roughness average (Ra ) values of the clad
and tape are 26.91 and 25.62 mm, respectively.
Although these averages are similar, the standard devia-
tion of the tape measurement (11.17 mm) is larger than
the measurement of the clad (1.17 mm). Furthermore,
the undulations visible in the clad surface generated by
successive clad tracks are not represented in the tape.
However, for the purpose of this study, the roughness
of the tape does not need to be identical to that of a
clad surface; it is only used to demonstrate the potential
Figure 9. Illustration of the modified lumped capacitance
difference between a rough surface, similar to the one
method.
produced through powder cladding, and a smooth
surface.
In case 6, the distribution of h on the face of a verti-
are used to create an impinging jet to cool the plates,
cal wall resulting from a parallel jet is measured using
and the rate of each flow is 9 L/min. Each plate is
the hot-film method. As shown in Figure 7(b), the
heated to a temperature greater than 100 °C and then
shielding and powder delivery jets are emitted by the
placed on an insulated fixture under the deposition
nozzle while the top edge of the substrate, with the 45°
head, as shown in Figure 9. Measurements are made
edge, bisects the argon jet. The convection acting at
with and without the inclusion of powder in the flow to
increasing distances from the top edge is measured
determine its impact on the measurement of the aver-
using the three sensors. In this orientation, the plexi-
age coefficient of convection.
glass substrate is fixed in the vertical X-Z plane. The
dimensions of the sensors limit the nominal resolution
to 1.45 mm in the X-axis and 0.1 mm in the Z-axis. Effect of metal powder in the flow. It is necessary to deter-
mine the impact of powder on the coefficient of convec-
tion because it cannot be used during the hot-film
Comparison with the lumped capacitance method anemometry measurements. Table 4 presents the aver-
Modified lumped capacitance measurements are per- age coefficient of convection (h)  measured using a mod-
formed, using copper and aluminum plates, to verify ification of the lumped capacitance method, for the
the hot-film measurement method. Both argon flows coaxial jets impinging upon the surface of each metal
1304 Proc IMechE Part B: J Engineering Manufacture 230(7)

140 140
120 120
100 100

h (W/m2/K)

h (W/m2/K)
80 80
60 60
40 40
20 20
0 0
−100 −75 −50 −25 0 25 50 75 100 −100 −75 −50 −25 0 25 50 75 100
X (mm) Y (mm)
(a) (b)

Figure 10. Results from case 1 in which the shielding and powder delivery jet impinge upon the substrate. The rate of each flow is
9 L/min. Measurements are performed in 3-mm increments along (a) the X-axis and (b) the Y-axis.

plate. The jets are produced by the two argon flows,


each with a rate of 9 L/min (case 1). When no powder 140
Case 2, 19 L/min
is included in the argon flow, the measured values of h 120
100 Case 1, 9 L/min

h (W/m2/K)
are 65.6 W/m2/K using the aluminum plate and 66.5
80
W/m2/K using the copper plate. When InconelÒ 625
60
powder, with a particle size distribution between 44 40
and 149 mm, is delivered at a rate of 19 g/min, the mea- 20
sured values of h are 65.1 and 65.4 W/m2/K. The inclu- 0
sion of powder changes h by only 0.7% and 1.6% for −100 −50 0 50 100
X (mm)
each plate, indicating that the powder has a negligible
effect on the average convective heat transfer. Figure 11. Comparison of the convection generated by two
different flow rates for each argon flow.
Comparison between the methods. The surface convection
resulting from an impinging jet is characterized by tak-
ing measurements at discrete points on the X- and Y- upon the metal plate, causing the gas to deflect and
axes. By compiling these individual measurements, the flow across its surface. As it flows over the surface, the
distribution of the coefficient of convection can be temperature of the gas increases as it extracts heat from
compared to the average coefficient of convection mea- the plate, reducing the rate of heat transfer acting
sured using the lumped capacitance method. Figure 10 nearer the edges of the plate. In the anemometry mea-
presents the hot-film measurement results from case 1 surements, the gas does not extract heat from the plexi-
in which both the shielding and powder delivery argon glass substrate as it flows toward the heated sensor
jets impinge upon the substrate at a rate of 9 L/min. element at each measurement location.
Figure 9 shows that h decays from a maximum value of
10569 W=m2 =K at the impingement point (X = 0 mm)
Measurement results and discussion
to a value of 3263 W=m2 =K at the edges. The decrease
in h is more gradual on the negative X-axis than on the The impact of flow rate on convection is investigated
positive X-axis. Figure 9 shows that two local maxima by first comparing the two cases along the X-axis with
of 9667 and 11768 W=m2 =K, separated by 12 mm, different argon flow rates supplying each jet. Figure 11
occur on the Y-axis. A minimum value of compares the results measured in case 1 with those
7566 W=m2 =K is measured between these two obtained in case 2, in which both the shielding and
maxima. powder delivery argon jets impinge upon the substrate
The hot-film measurement results are compared to at a rate of 19 L/min. This flow rate is approximately
those obtained using the lumped capacitance method. twice the flow rate used in case 1. The value of h result-
To make this comparison, the average coefficient of ing from the 19-L/min flows decays from a value of
 acting over the area corresponding to
convection (h) 10768 W=m2 =K to a value of approximately 34 W/m2/
the surface of each metal plate is calculated. First, a K at the outermost measurement locations. The
quadratic polynomial fit is applied to the data, and h is decrease in h is more gradual on the negative axis than
calculated as the average of this surface fit. The anemo- the positive axis.
metry measurements produce values that are 3%–5% Increasing the flow rate supplying each jet has little
greater than those measured using the lumped capaci- effect on the convection generated by the deposition
tance method. This small difference can be attributed head. Figure 11 shows that increasing the rate of each
to the nature of the two measurement methods. During flow from 9 L/min in case 1 to 19 L/min in case 2
the lumped capacitance method, the argon jet impinges increases the maximum measured value of h by only 2
Heigel et al. 1305

140 140
120 Case 3, 9 L/min 120 Case 5, rough
100 Case 4, 19 L/min 100 Case 1, smooth
h (W/m2/K)

h (W/m /K)
2
80 80
60 60
40 40
20 20
0 0
−100 −50 0 50 100 −100 −50 0 50 100
X (mm) X (mm)

Figure 12. Comparison of the convection generated only by Figure 14. Effect of surface roughness on convection.
the shielding jet using different flow rates.

indicating that changes in the flow rate have no impact


140 on the convection acting away from the deposition
120 Case 4, 1 flow
head.
100 Case 1, 2 flows
h (W/m /K)

Figure 13 presents a comparison of the heat transfer


2

80
caused by a single impinging jet compared to two coax-
60
40
ial impinging jets. The combined flow rate of the two
20 jets in case 1 is 18 L/min, and the flow rate of the shield-
0 ing jet in case 4 is 19 L/min. Despite these similar flow
−100 −50 0 50 100 rates, the distribution of h in these two cases is very dif-
X (mm)
ferent. The two coaxial jets in case 1 create an asym-
Figure 13. Convection generated by both the shielding and
metric distribution of h with a single peak. The single
powder delivery jets compared to the convection generated jet in case 4 creates a symmetric distribution with two
only by the shielding jet. peaks. The values of h measured at the peaks in case 4,
which uses only the shielding flow, are 50% less than
the peak when both flows are employed in case 1.
W/m2/K. In addition, the values of h measured at the Although the flow rates of the shielding and powder
outermost locations also increase by 1 W/m2/K. These delivery jets are the same in case 1, the average velocity
differences are within the uncertainty of the of the shielding jet as it exits the inner nozzle is 1.8 m/s,
measurements. whereas the average velocity of the powder delivery jet
Figure 12 presents the results from cases 3 and 4 in as it exits the outer nozzle is 2.3 m/s. This difference in
which only the shielding jet impinges upon the substrate velocity creates a shear between the jets that alters the
at a rate of 9 and 19 L/min, respectively. In case 3, two flow structure, as shown by Hwang et al.33 In that
local maxima with values of 3964 and 4164 W=m2 =K study, two coaxial jets with different exit velocities cre-
are separated by 15 mm with a local minimum of ated vortices, so that their effect on heat transfer could
2863 W=m2 =K between them. The convection decays be investigated. It was shown that the induced vortices
from these maxima to approximately 19 W/m2/K at the could increase the rate of heat transfer on the surface.
outermost locations. For case 4, values of 5264 and This effect explains the increased distribution of h when
5365 W=m2 =K are measured at the two local maxima. both jets are used in case 1 compared to when only the
These maxima are separated by 15 mm, in which a local shielding jet is used in case 4.
minimum of 3464 W=m2 =K is measured. The convec- The impact of surface roughness on convection is
tion decays from these peaks to approximately 21 W/ investigated by comparing cases 1–5, as shown in
m2/K at the outer measurement locations. The local Figure 14. In each case, both argon jets impinge upon
minimum at the impingement point in these cases is the surface at a rate of 9 L/min. In case 5, in which the
likely a result of the boundary between laminar and tur- surface surrounding the sensor is rough, the value of h
bulent flows within the jet, which has been shown in the decays from 8867 to approximately 21 W/m2/K.
literature to create maximum values away from the Compared to the smooth surface in case 1, the rough
impingement point.40 surface in case 5 decreases the maximum value of h by
Increasing the rate of the shielding flow from 19 W/m2/K compared to the maximum value in case 1.
9 L/min in case 3 to 19 L/min in case 4 increases the In addition, the rough surface causes h to decrease
values of h measured at the peaks by 12 W/m2/K. This more rapidly from the peak value. Finally, the rough
increase exceeds the measurement uncertainty. surface decreases the measured values of h at the outer
The minimum value between the peaks increases by locations by 11 W/m2/K. It should be noted that the
6 W/m2/K. However, there is no difference in the mea- rough surface in case 5 is approximated using the tread
sured values of h at the measurement extremes, tape, as discussed in section ‘‘Measurement cases,’’ and
1306 Proc IMechE Part B: J Engineering Manufacture 230(7)

70 70 70
60 60 60

h (W/m /K)

h (W/m2/K)

h (W/m2/K)
50 50 50

2
40 40 40
30 30 30
20 20 20
10 10 10
0 0 0
−40 −20 0 20 40 −40 −20 0 20 40 −40 −20 0 20 40
X (mm) X (mm) X (mm)
(a) (b) (c)

Figure 15. Convection acting on a vertical wall in case 6: (a) sensor 1, 0.8 mm below top edge; (b) sensor 2, 5.4 mm below top
edge; and (c) sensor 3, 108.7 mm below top edge.

maximum value of h in case 1 is 81% greater than the


140
Case 1, impinging jet maximum value in case 6. The distribution of h is dif-
120
Case 6, bisected jet ferent between these two cases. A double peak is cre-
100
h (W/m /K)

ated by the parallel flow in case 6, whereas a single


2

80
60 peak is created by the impinging jet in case 1. In the lit-
40 erature, impinging jets which impinge directly onto a
20 surface have been found to induce a greater rate of heat
0 transfer compared to parallel jets or those with a shal-
−100 −50 0 50 100
X (mm) lower impingement angle.25–28 The jet in case 1 is
deflected by the surface and spreads radially from the
Figure 16. Comparison of the convection on a horizontal impingement point, which results in a higher value of h
surface compared to the convection near the top edge of a spreading over a greater area. In contrast, the wall
vertical wall. bisects the parallel jet and does not disrupt the flow to
the same extent. Although the results in case 6 could
vary depending on the different in geometry between
consequently, the results may vary for an actual clad the ground edge of the substrate and the top of a
surface. deposited wall, the comparison is still noteworthy.
The distribution of convection acting on a vertical
wall is found by analyzing the results of case 6.
Figure 15 presents the results from case 6 in which Conclusion
both argon jets flow parallel to the substrate at a rate
of 9 L/min. The jets flow parallel to the wall surface A method using hot-film constant voltage anemometry
and are bisected by the top edge of the wall. The coeffi- to measure the heat transfer from the sensor into the
cient of convection is measured at three locations on environment is developed to characterize the surface
the wall. The maximum value of h measured by sensor convection contribution from the shielding and powder
1, which is located only 0.8 mm from the top edge of delivery systems used in laser-based AM processes.
the wall, is 5864 W=m2 =K. At sensor 2, which is Calibrations are performed, so that the coefficient of
5.4 mm below the top edge, the maximum measured convection can be extracted from the heat transfer mea-
value is 4066 W=m2 =K. The distribution measured by surement. The distribution of the forced convection is
each of these sensors exhibits a second peak of a signifi- mapped by incrementally taking measurements at dif-
cantly lesser value than the maximum. The value of h ferent locations relative to the deposition head. By com-
measured by sensor 1 at the extreme locations is paring its results to those obtained using a modified
2562 W=m2 =K, and the value measured by sensor 2 is lumped capacitance measurement, the method is shown
2263 W=m2 =K. The distribution of h measured by sen- to be valid. The modified lumped capacitance measure-
sor 3 exhibits a different trend. A maximum value of ment is also used to demonstrate that excluding powder
3664 W=m2 =K, which decays to values of approxi- during the hot-film anemometry measurement has little
mately 21 and 32 W/m2/K, is measured by sensor 3. impact on the results.
Figure 16 compares the distribution of h resulting The method is then demonstrated by characterizing
from an impinging jet (case 1) and from a bisected par- the convection generated by a Precitec YC50 deposition
allel jet (case 6). The flow rate of each jet in both cases head. It is found for this application that the distribu-
is 9 L/min. The comparison is made using sensor 1 in tion of convection is affected by a variety of factors:
case 6, which is closest to the top edge of the plate. The
impinging jet causes a greater rate of heat transfer than 1. Increasing the flow rate minimally affects the sur-
the parallel jet, which is evident by the fact that the face convection.
Heigel et al. 1307

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Declaration of conflicting interests
14. Pinkerton AJ and Li L. The development of temperature
The author(s) declared no potential conflicts of interest fields and powder flow during laser direct metal deposi-
with respect to the research, authorship, and/or publi- tion wall growth. Proc IMechE, Part C: J Mechanical
cation of this article. Engineering Science 2004; 218(5): 531–541.
15. Vasinonta A, Beuth JL and Griffith M. Process maps for
predicting residual stress and melt pool size in the laser-
Funding based fabrication of thin-walled structures. J Manuf Sci
The author(s) disclosed receipt of the following finan- E: T ASME 2007; 129(1): 101–109.
cial support for the research and/or authorship of this 16. Labudovic M, Hu D and Kovacevic R. A three dimen-
article: J.C. Heigel is supported by the National Science sional model for direct laser metal powder deposition and
Foundation under grant no. DGE1255832. This article rapid prototyping. J Mater Sci 2003; 38(1): 35–49.
17. Jendrzejewski R, Śliwiński G, Krawczuk M, et al. Tem-
is based upon work supported by the Office of Naval
perature and stress fields induced during laser cladding.
Research through the Naval Sea Systems Command
Comput Struct 2004; 82(7): 653–658.
under contract no. N00024-02-D-6604, delivery order 18. Plati A, Tan JC, Golosnoy IO, et al. Residual stress gen-
no. 0611. Any opinions, findings, and conclusions or eration during laser cladding of steel with a particulate metal
recommendations expressed in this article are those of matrix composite. Adv Eng Mater 2006; 8(7): 619–624.
the authors and do not necessarily reflect the views of 19. Dai K and Shaw L. Distortion minimization of laser-
the Office of Naval Research or the National Science processed components through control of laser scanning
Foundation. patterns. Rapid Prototyping J 2002; 8(5): 270–276.
20. Qi H, Mazumder J and Ki H. Numerical simulation of
heat transfer and fluid flow in coaxial laser cladding pro-
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