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International Journal of Impact Engineering 48 (2012) 107e115

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International Journal of Impact Engineering


journal homepage: www.elsevier.com/locate/ijimpeng

On designing structures for extreme environments


Neil K. Bourne
AWE, Aldermaston, Reading, Berkshire RG7 4PR, United Kingdom

a r t i c l e i n f o a b s t r a c t

Article history: Structures designed for extreme environments must be designed not only for the magnitude of the load
Received 25 March 2011 that they will experience, but also time for which that load acts upon them. At the core of the problem
Received in revised form lies the loading impulse experienced by materials and the operating deformation mechanisms that are
20 November 2011
excited. Our experience of materials’ physics, gathered by investigating response to mechanical loads, has
Accepted 21 November 2011
suggested a series of descriptive constructs within which we build our picture of behaviour. This paper
Available online 30 January 2012
suggests a framework by which to interpret data collected on the response of metals. It suggests that
strength is a quantity that decays over time and that fundamentally approaches zero in the limit of
Keywords:
Extreme
infinite time. Controlling this decay is the business of engineering, to design structures that will survive
Shock in the environments for the time windows of importance.
Metals physics Crown Copyright Ó 2012 Published by Elsevier Ltd. All rights reserved.
Impulse
Akrology

1. Introduction environments and longer service lifetimes without failure [3]. To


counter security threats, defence agencies require the technological
Materials and structures are loaded to extremes in everyday means to field protection for the populace against terrorist attack
environments and across nature. The loadings are both static and and to protect critical facilities against human or atmospheric
dynamic; static high pressure exists at the centre of all massive extremes. Finally, exploitation of deep sea or space environments
objects within the cosmos, as a result of the gravitational forces that demands technologies constructed from materials capable of
drive matter to agglomerate over time. This pressure exerts forces withstanding the range of operational conditions found in these
on condensed materials, driving structural change and forming locations [3].
new states which differ from those familiar at ambient conditions This paper aims to explain the principal mechanisms that
on the surface of the Earth [1]. The speed with which the loading reorder a material’s structure and changes the mechanical and
occurs drives these changes but also heats the material to high physical properties it exhibits. Such a material may be a metal,
temperature as a result of the work done by the impulse and this polymer or a brittle solid; it may also be reactive. Whilst each of
too takes materials to new extremes to which they must respond. these cases deserves discussion in its own right this paper will
The shock wave represents the most rapid application of concentrate on metal deformation. Understanding the mechanisms
compression to a solid, vaporizing the material in the ultimate case. at work and the mathematical descriptions of the behaviour
The physics of shock processes also controls earthbound explosive observed, allows the principles of material response to be used to
effects, as well as carving Earth’s morphology. These concepts design engineering structures and to do so requires a means of
govern complex geophysical processes which can also be decon- choosing materials and selecting tests to track response. These
structed to illustrate principles of these extreme loading modes [2]. steps are necessary to iterate to a design that can respond under
Materials are central to every one of the technologies available extremes of loading. Finally the structure itself will respond to
to meet performance requirements in a range of mechanical loadings with defined responses which integrate the effects on
extremes. In transportation, future vehicles will require lighter components experienced as the impact proceeds.
weight components with increased strength and damage tolerance An individual engineering design problem may be decomposed
to decrease fuel consumption. Next-generation nuclear fission into a series of steps allowing the response of metals to be pre-
reactors require materials capable of withstanding higher dicted or a material chosen for use in a particular environment. The
temperatures and higher radiation flux in extremely corrosive first step in the process requires the characterization of the
impulsive load to which the metal is subject. This defines the
mechanical threat to which the material must respond. Delivery of
E-mail address: neil.bourne@mac.com.

0734-743X/$ e see front matter Crown Copyright Ó 2012 Published by Elsevier Ltd. All rights reserved.
doi:10.1016/j.ijimpeng.2011.11.011
108 N.K. Bourne / International Journal of Impact Engineering 48 (2012) 107e115

this to a target then allows the material response to be tracked difficult, thus increasing the strength of the material. Once
using suitable sensors. This process will be illustrated with exam- unloading occurs such dislocation structures relax and the
ples of metal response mechanisms to incident impulses in what remaining relaxation morphologies may be observed in samples
follows. recovered from targets loaded in idealized experiments where
a square impulse is applied (see Fig. 1) [8e10].
2. Mechanisms The effect of structure on the observed plasticity results from
differences in classes that different elements adopt to stack the unit
Materials may fail by a variety of deformation modes. These are cell. In general terms most metals (there are exceptions) adopt one
generally a suite of mechanisms grouped into an integrated form to of the three principal stacking groups; face centred cubic (FCC),
define the various processes. Each takes different times to act on body centred cubic (BCC) and hexagonal close packed (HCP). Slip of
the material since there is a single or an integrated set of operating planes of atoms requires the breaking of a number of bonds within
deformation mechanisms operating at any one time. In order of the lattice and the structure favours particular planes for slip within
temporal duration they may be listed as; impact, yielding, thermal grains. The integrated forces required to overcome the interatomic
shock, fracture, shear failure, buckling, creep, fatigue, corrosion, bonding determine the Peierls stress for slip on close-packed
fouling and wear. In each case the process acts over longer times planes in particular unit cell geometries. Whilst BCC structures
and the results apply over a larger region of space. The impact have a large number of potential systems, there are no easily acti-
phase overcomes the strength of a material to begin the processes vated ones so that there is a greater energy required to start the slip
of inelastic flow; plasticity in metals. Yielding occurs when the process reflected in a higher Peierls stress. This results in a high
stress reaches a threshold at which plastic flow starts to occur. This density of dislocations and their rapid propagation in FCC struc-
process occurs at lower levels as time progresses since the material tures, with low dislocation density and slower propagation speeds
substructure is developing over time. Thermal shock represents an in BCC metals.
instantaneous load but such insults are not considered further here. Fig. 1 shows loading in three classes of metal up to 10 GPa
Fracture represents a later part of the process where (in metals) amplitude, each pulse lasting 1 ms. Different material classes show
ductile failure occurs in tension with the creation of new free differing characteristic behaviours behind the shock front; yet all
surface. Once localization of deformation has occurred within show shock strengthening with pressure up to ca. 30 GPa [11]. FCC
a material, a plastic zone can act as a hinge which allows structural metals such as Cu and Ni harden (a), while pure BCC metals (Ta here
collapse of components where a large part of the bulk stays in the in b, but also Nb and W) soften over the microsecond taken for the
elastic state. Finally creep processes at long time scales represent microstructure to develop (stress histories to the right). Tie6Ale4V,
the flow of the material under all the previous failures where the composed primarily of the HCP a-phase, shows planar slip in the
strength has been rendered less again by virtue of the time for square pulsed specimens. There were no twins when targets were
which the material has been left. The other mentioned mechanisms loaded to 5 GPa but in the 10 GPa pulsed samples about 3% of the
take longer and involve other (e.g. chemical, corrosion) insults and grains twinned [8,9]. Twinning is a rapid plastic process and this
while what is discussed here applies in a general sense, individual results in the shear stress equilibrating quickly on loading as can be
details are specific to the mechanism. seen in the stress histories to the right. Differences in the Peierls
Let us first look at the deformation of crystalline solids under stress show contrasting substructure evolution in the metals.
mechanical loading. The initial mechanisms operating do not break Materials with higher values have greater resistance to defect
bonds and thus may be regarded as compression in a purely elastic motion in the lattice and show a greatly reduced ability to cross-slip
state as the first planes of atoms within a microstructure compact. and to store additional line defects. Metals (such as Ta) that possess
The unit cell minimizes its potential energy and if it can rearrange higher Peierls stress, show restricted dislocation motion when
interatomic packing at this stage, a denser phase may quickly form there is insufficient thermal activation (such as is found with short
around nucleation sites within the structure. In regions where the impulses or at low temperatures). If twinning can occur, the shear
material has no point or larger defects, the lattice responds with its stress equilibrates rapidly as strain is accommodated by the plastic
theoretical strength, controlled only by the forces due to inter- processes [8].
atomic bonding within the atomic environment [4]. This initial In microstructures where defect densities are lower, disloca-
phase occurs regardless of loading amplitude since some motion is tions do not become close and thus do not lock to form barriers to
imparted to the first layers of the solid at the start of the process further motion. Crystal plasticity is composed of group atomic
when a mechanical insult is applied. interactions that are best treated to illustrate the nature of the
Local deformation can begin at inhomogeneities within the response with molecular dynamics (MD) [12], until effects from
lattice, and nucleation of slip, via dislocations occurs at defect sites. second phases (which are on a larger dimension than can interact
Slip along interatomic planes begins and plastic deformation is within the shock front) become important. At this time, the stress
established around the nucleation site. At later times interactions of states become ill-defined within each phase until equilibration by
travelling dislocations will nucleate further line defects in crystal- wave propagation has occurred within a representative micro-
line domains which then proceeds under the shear stresses present structural volume element. Thus atomic interactions control this
in the material behind the compression front [5]. These processes length scale of deformation and plastic processes occur to relieve
transit the purely elastic state at the first moments of impact to the shear stresses applied to the crystal boundaries. The defect
inelastic flow at a lower stress since work is expended in breaking length scale in this region is controlled by atomic scale point or line
bonds to accommodate the applied strain. The defined plastic state defects found within the crystalline demains.
takes time to establish but once these processes have been The microstructural scale has inhomogeneities at different
completed the descriptions developed using quasistatic loadings scales controlling processes which equilibrate by wave propagation
from the developments of mechanics through from the nineteenth between new phases. One may consider the time taken for infor-
century can be applied [6]. mation to travel from areas of differing impedance to interact with
Slip is arrested by the interaction of dislocations with solid processes within the crystal to define a temporal and a physical
particles (precipitates) or when they interact with one another boundary between scales within the material. The impedance may
pinning their motion and locking crystals into states that resist be greater (second phase particulate inclusions) or lower (voids)
further slip within the lattice [7]. This makes deformation more than the primary phase of the material under investigation. The
N.K. Bourne / International Journal of Impact Engineering 48 (2012) 107e115 109

Fig. 1. Recovery of targets loaded in 1D strain; plate hits sectioned target from the rear, loading a sample recovered for metallographic analysis. Left: as received and TEM of
recovered microstructures from shock-loaded targets. Right: longitudinal and lateral (dashed) and shear stress components (solid) in (a) Ni, (b) Ta and (c) Ti64 loaded to 10 GPa for
1 ms. Details in [8e10].

wave propagation process may be modelled successfully by localize deformation as operating kinetics play against thermal
considering equilibration between these different phases using conduction away from the deformation zone within the solid.
continuum quantities for each component along with transport At greater length scales again the material has further surfaces
properties derived from continuum measurements of the phase. within, and when waves have travelled around the components of
Such mesoscale simulations using continuum hydrocodes solve the structure it has now adopted a defined stress equilibrated state
conservation of relations across component phases in the where local inhomogeneities and non-deforming regions obey the
composite microstructure. The continuum response can then be defined mathematical assumptions of continuum mechanics. In
reconstructed by reconstructing integral components by statistical particular, critical mechanistic times for shear localization allow
averaging across the defined areas relevant to the structure or plastic hinging to occur within the structure. This time is the
problem of interest. Such wave processes equilibrate stresses minimum that is required to plastically deform a local region but
within large parts of the structure but also localize deformation on the formation of a hinge is further determined by wave equilibra-
planes of principal shear determined by the geometry of the tion of the structure defining the shear state of the loading in
problem and evolution of the strain field in the deforming solid. a defined geometry at nucleated shear sites. Once formed, the
Local regions of lower strength may begin to localize plastic morphology responds structurally with jointing around the local-
deformation and heat forming the onset of shear banding within ized regions of plastic deformation induced in the equilibration
the solid. In dynamic tension (related to the shear applied to phase [6]. The structure slips as a homogeneous mass around the
microstructure) local failure will again localize at regions where hinges formed at regions of intense plastic deformation defined by
which will first nucleate and then grow voids within the material. the wave phase in the material beyond this critical time and strain.
Thus the defect distribution at the mesoscale, determined by the Having discussed a suite of mechanisms, tracking through
nature of the methods adopted in production, will characterize the crystal deformation to structural mechanics, it is worth adding
series of mechanisms which equilibrate stress on the one hand and times and corresponding length scales that one must resolve to
localize failure on the other. According to the material and its observe these processes in operation in representative single-phase
properties, this deposition of plastic work within the solid may metals. Table 1 shows a suite of typical mechanisms with
110 N.K. Bourne / International Journal of Impact Engineering 48 (2012) 107e115

corresponding order of magnitude estimates of time scales for such equilibrated, the connection to spatial scales comes through wave
processes and length scales over which they operate. The times speeds in the materials (which are of order thousands of m s1 in
themselves clearly vary markedly between metals of differing these metals).
structure and density and with the applied compression in indi-
vidual impulses so that these values are for ranking purposes only. 3. Platforms
This is since the wave speeds that drive the faster mechanisms are
defined by the atomic mass of the atoms that are displaced. It is In order to investigate and characterize the operating mecha-
possible to group the mechanisms listed into groups that act at nisms for a particular material under a particular load, the defor-
different times and scales and show that these are driven by the mation of a target must be tracked with application of a defined
defect distributions at each scale that exist in the material and the impulse which can be used to excite the deformation mechanisms
structure constructed from it. For the purposes of this paper which outlined above. Each impulse has some activation stress in order for
will focus on the response of a single-phase metal, these groupings it to operate and some characteristic relaxation time determined by
will be labelled nucleation mechanisms, inelastic flow, wave the operating physics. In order for the process under investigation
equilibration and localization and a regime that is governed the to be complete in a particular experiment, impulses of greater time
mechanics of the engineering structure. than that of the mechanism will be required to observe the corre-
Nucleation mechanisms operate at the atomic scale around sponding deformation. If one is going to construct continuum
point or line defects within the material or by shearing the unit cell material models from observations in an experiment, the platforms
to change the phase of the material. These processes have a relax- used to investigate each mechanism need to have suitable capa-
ation time of order a nanosecond within the metal. If the threshold bility to deliver the correct impulses (amplitude and pulse length)
for them to be activated is reached these will be the first operating in order to observe the required response. The grouping of the
mechanisms within the solid during loading nucleating the deformation mechanisms made on the basis of their regimes of
generation of dislocations and establishing inelastic processes operation and described above can be related to the impulse
within the solid. applied by individual platforms as well. Some isolate the nucleation
Once defects are activated, inelastic process can occur on atomic phase where the defects start atomic processes, others include the
planes around these sites and their propagation and interaction inelastic flow phase where slippage of planes can occur to accom-
determines the plastic flow relieving the stresses within the grain. modate the applied strain. This is part of a wave-dominated phase
In some metals at later times, effects such hardening may occur where equilibration occurs across the structure localizing defor-
where the dislocation density is high and the resistance to slip is mation to geometrical zones. Finally there is a mechanical loading
low. These processes equilibrate strain states within crystals and response where the structure with its component parts obeys
define a state for a crystalline element between lower impedance mechanics concepts around continuum features such as shear
boundaries which show disorder in the boundary regions. zones or hinges.
The third scale relies on slower operating mechanisms accom- There are several platforms used to investigate mechanical
panying processes driven by surface creation or deformation and response in the laboratory environment. They range from
tracks the achievement of stress state equilibrium within the solid. compression presses found in most engineering laboratories to the
Alternatively strain localization occurs which increases plastic most intense laser platforms constructed in investigate nuclear
work in regions deforming the material as well heating it. This physics including fusion [14,15]. Table 2 lists a number of these
equilibration and localization regime achieves stress equilibrium platforms and ranks them according to several parameters to
and defines slip boundaries within the solid. characterize their response. Quasistatic loading devices include
Finally a demain is achieved in which the material is equili- diamond anvil cells capable of achieving high pressure in small
brated and plastic hinge and slip zones are defined. This regime is (tens of microns) targets, as well as Hopkinson bars which extend
defined here as the mechanics regime in which continuum loading to the limit at which measurement can made of continuum
concepts can truly be applied within the material to determine properties. This group of devices yields data concerning the
structural scales for design and analysis. Research by Dear et al. [13] continuum loading of the material under investigation since in all
has shown that specimen dynamics during mechanical testing can case stress states have equilibrated before data is extracted from
have significant effect on recorded material property evaluations. the deforming target. The other devices in the table work in the
In each regime, the temporal estimates for typical single-phase wave regime where equilibration processes are underway. In the
metals indicated reflect the speed at which the mechanisms case of single and two stage launchers (SSL and TSL) a step impulse
operate. In the regimes where the microstructure is not is applied to the impact plane. Z pinch loading applies a more
gradually rising stress impulse to target. In this mode different
Table 1 mechanisms are accessed at different stress thresholds and proceed
Characteristic length and time scales for observing typical crystalline deformation
with different kinetics, energy sinks and work done on the target.
mechanisms in a single-phase metal after applying step compression loading at
t ¼ 0.

Mechanism Representative
Table 2
time scale
Commonly used mechanical test beds. The table gives generic loading conditions for
Defect activation 100 ps each device.
Phase transformation 1 ns Nucleation
Twinning 1 ns P (GPa) Loading Pulse rise Target Impulse
Slip 10 ns Inelastic flow time (ms) (ms) (mm) (GPa ms)
Dislocation interaction 100 ns Large press 0.01 QS e 50 N
Pinning at boundaries 1 ms DAC 300 QS e 0.1 N
Void growth 1 ms Equilibration and Drop weight 0.1 100,000 10 50 10,000
Nucleation adiabatic shear band 10 ms Localization SHPB 0.1 100 10 5 10
Stress state equilibration 100 ms SSL 150 10 0 100 1500
Localization at plastic hinges 1 ms TSL 300 3 0 50 900
Buckling 1s Structural Z Sandia 500 0.1 0 10 50
Creep 10 s Mechanics Large lasers 1000 0.001 0 1 1
N.K. Bourne / International Journal of Impact Engineering 48 (2012) 107e115 111

However the magnetic interaction may also be used to accelerate relaxation time for completion. Clearly if there are several mecha-
plates to impact applying shock loading to the target [16]. In this nisms operating simultaneously, then each occurs in parallel with
mode it can apply ca. 100 ns pulse loading and this is plotted as the the other and dissipates energy at a rate determined by the nature of
datum Z in Fig. 2. Finally laser pulses apply ns loading but to the the processes. In this model an idealized pulse applied to the
highest amplitudes. This overview of platform impulse delivery material is filtered by its properties so that the result output after
shows the relative abilities of different platforms to excite defor- some travel through it can be deconvolved to deduce the material
mation mechanisms within a material. The impulse delivered by mechanisms operating during the process. The measurement of
launchers is considerably higher than the laser platforms although states with suitable sampling rate at varying locations within it is
the amplitude achieved is less. Thus only the highest thresholds can thus a necessary part of the process which must be matched to the
be accessed by lasers although the impulse delivered can only nature and kinetics of the mechanisms operating. An ideal form for
couple to nucleation processes within the lattice. The plastic state a mechanical impulse in such an investigative process is a shock
achieved in materials with high defect concentration or within pulse with defined amplitude and duration since is ensures activa-
liquids or gases allows determination of the equation of state tion of all processes present at its maximum stress level at the same
parameters using these platforms. time. Thus input step with a defined duration is a necessary input
To design for an application where structures are fielded in impulse for experiments designed to probe material mechanisms.
extreme environments requires a series of steps to be followed. In order to determine the utility of experimental platforms in
Firstly the mechanical insult itself needs to be defined in terms of order to match material models to deformation it is necessary to
the amplitude and duration of the loading experienced. This find some means to characterize their usefulness for the derivation
defines an impulse experienced by the structure during the event. of models to design structures for future use. To do so, a dimen-
Each material has a potential suite of operating available defor- sionless constant, F, has been introduced which offers a means of
mation mechanisms in response to that impulse which are trig- determining the totality of the deformation mechanism [17]. It is
gered by the event as it occurs. Knowledge of these responses for defined to represent the extent to which a mechanism is driven to
a range of materials fielded in a device allows the design of completion by a stress or temperature excursion during the time for
a structure optimized for an application. This includes suitable which the impulse is active in the following manner
material types for particular component geometries as well as
a range of jointing strategies between those components within the trelax
F ¼ ; (1)
structure. At the level of the device it is the defects at each length timpulse
scale within it that determine the strength of the whole. The
principle defects activated by the insult relate to the jointing where trelax refers to the characteristic relaxation time for the step
between components and then with the material during the load. in the rate limiting process and timpulse is the length of the impulse
Both of these features must be understood in idealized tests before applied to the structure. Thresholds in stress, pressure or temper-
design can occur successfully. This the construction of mathemat- ature need to be exceeded in order that the mechanism is activated
ical representations of the device response must include adequate and further when the critical process (since there will in general be
material characterization tests over the impulse range to be expe- a suite of them) is complete long before the impulse releases back
rienced including the correct stress amplitudes but also the oper- to an ambient state, the stable final form will be an equilibrium
ating kinetics in the deforming material. state of the material under loading. If this is the case F will be small
Thus any test programme that wishes to cover a particular regime and the state will be defined. Conversely if the impulse is short
of mechanical behaviour must view a target material as a body that relative to the completion time of a mechanism assumed to act (or
must be excited with pulses that isolate each kinetic effect in turn to the shortest available at that stress level) then F will be large and
properly represent it within a mathematical description. Pulse the state observed will be transient and similar to the initial state of
lengths of different duration at similar thresholds can then be used the material at the start of the process.
to map out the material response and construct valid models over Such a criterion can be used to rank experiments to derive the
the stress range applicable. In this view, each mechanism can be quantities necessary to construct an equation of state for a material
investigated to determine its threshold for operation and its since it measures the degree to which loading has reached an
equilibrium state within it. Thus it represents a litmus test of the
ability of an experiment to excite a response to investigate a process
on the one hand and provides a means of tailoring an impulse to
optimize a material’s properties for resisting dynamic deformation
on the other.
Fig. 3 shows the form of F for a series of impulse and relaxation
times. There is a region in which it exceeds one and one where it is
less than it which is represented as colored regions in the contour
map to the left of the figure. Individual characteristic times (from
Table 1) are used to indicate regions occupied by devices along the
ordinate whereas individual mechanistic groups are indicated
schematically up the abscissa. Since experiments aim to occupy
a space in which they are complete and F should be less than one,
the experiments sit below and to the right of the diagonal indicated.
An example shows wave equilibration and localization processes
which can be studied using launchers and the Hopkinson bar to
construct descriptions of the operating mechanisms.
The completion of processes defines a time scale which matches
to a length scale swept by a pulse. These are connected by some
Fig. 2. The impulse delivered by platforms to excite deformation mechanisms in propagation velocity which depends upon the process but is
targets as function of pulse length compression is delivered for. limited in the fastest processes driven at the highest amplitudes by
112 N.K. Bourne / International Journal of Impact Engineering 48 (2012) 107e115

Fig. 3. F as a function of kinetic times for mechanisms and impulse times delivered by various platforms. The impulse and mechanism times are measure in ns.

a wave speed in the material. This region defines a minimum The first example examines plastic deformation within recov-
volume element for the completion of the mechanism under ered targets of copper after shock loading to two stress levels (ca. 30
investigation. It also defines a voxel over which measurement must and 60 GPa) [18]. Different platforms were used to compare
be achieved within the loading time of the experiment. All response at the same shock amplitudes with impulse durations of
measurements of state evolution are integrated over some 1 ms for plate impact and 3 ns for laser loadings. In the experiments,
temporal and spatial domains and account of these defines recovered targets were examined to identify a series of features in
necessary equipment and region sampled at the relevant scale. the microstructures of loaded single-crystal copper targets. These
Finally it is worth noting that the processes of scaling can be included stacking faults, twins, recrystallized regions and micro-
assessed quantitatively using this methodology. Reducing the shear bands. The results showed dislocation structures and twin-
geometrical size of a test also scales the loading impulse. Since ning within the crystals regardless of the length of the loading
material deformation is a nested suite of operating mechanical pulse. However, the recrystallization and micro-shear were not
mechanisms, scaling will only be valid where particular mecha- present in the target subject to laser loading. Ranking mechanisms
nisms relevant at one scale are reproduced at the lower one. If this describing the processes defining plasticity in metals (Table 1) has
is not the case, the kinetics and amplitudes of the deformation will shown representative times for dislocation nucleation and twin-
not match those in the alternate case and the behaviours will not be ning. This gives F around one for the laser case and the plate impact
analogous. In particular, damage mechanisms will be seen to case gives F  1. Clearly the mechanisms were complete in both
occupy a defined length and time scale which relates to defect cases as seen in the recovered microstructures. However shear
activation and growth but which can be turned off by the incorrect banding was not fully developed in either case with F  1 in the
choice of impulsive loading. laser case and around five for plate impact loading.
Recrystallized regions in the recovered plate impact targets
reflect the greater energy deposited by the longer impulse over that
4. Examples in the laser loading. The pulse length is ca. 5000 times longer in the
former case making the impulse delivered the same factor greater.
At the shortest pulse lengths, metals respond to the nucleation The consequent extra heating results in greater temperature rise
processes which start dislocation motion from defects at the lattice and thus much greater microstructural effect on cooling back to the
scale and seed the rapid motion which twins grains to accommo- ambient state as observed in the grains in the recovered targets.
date the strain applied at the impact face. In the later inelastic flow These pure FCC metals show dislocation substructures which
phase, slip proceeds to relieve yet further shear stress. At later follow the development of the impulse as it loads the target. Since
times, second phase particles and grain boundaries can commu- these mechanisms are driven by the applied shear, when the pulses
nicate and the stress equilibration processes within the target are relieved, inelastic processes cease and the duration of the pulse
proceed with attendant strain localization beginning within the freezes the development of the plasticity observed in the
inhomogeneous material. In all these processes the shock impulse microstructure.
heats the material by performing plastic work expended in the A second mechanism of importance relates to high-rate tensile
compression of the target during the impulse. To illustrate these failure of a target by localization of deformation and growth of new
mechanisms in action, processes occurring during the pulse free surface at defects within the microstructure. Inception of new
showing examples of deformation are presented. These provide voids growing from such sites is embodied in the nucleation and
examples of pulse length effects in action but also that mechanisms growth model (NAG) [19]. Such a mechanism has a series of
can be frozen at an incomplete stage by removal of driving shear sequential operating timescales with the nucleation phase followed
stress. This may be used to track the development of such processes by growth of the void from its origin. As the duration of that pulse
within the metals. Whilst it is not exactly the case, the assumption becomes smaller, observed voids reduce as the time for the growth
that a mechanism can only be driven whilst a shear stress is applied phase is reduced. In a series of experiments two different pulse
can be shown to be operating in the case of metals. durations, an order of magnitude different, were introduced to
N.K. Bourne / International Journal of Impact Engineering 48 (2012) 107e115 113

cavitate SS316 at three different stress levels [25]. The void size was induced impulses offer a means of accessing the limits of
observed to reduce until voids were barely visible in the target. The strength in a material in a manner not possible using other tech-
measured tensile strength of the material starts to increase once niques [15].
the point at which there is no free surface is reached. Other work on The tensile failure of metals occurs on timescales which will
copper using HE loading has shown that there was no evidence of couple with whatever the dominating mechanical processes oper-
void formation but only intense sheared layers in the metal at the ating during the loading impulse are. The pulse interacts with
location of the spall plane [19]. defect populations existing in the material in compression in its as
There has been considerable work over the years on the tensile received state or induced as a result of interactions within the solid
or dynamic spall strength of materials. It has been possible to trace due to inelastic processes resulting from the compressive drive. The
shock experiments conducted on pure aluminum, on different defect volumes at the atomic scale accessed as the pulse length
platforms, across work published over many years [15]. The results decreases are so small that the observed strength of the metal
are collated and presented in Fig. 4. The dynamic tensile strength is approaches the theoretical strength as the pulse length tends to
taken as is conventional for this field by recorded the height of pull- zero. At the mesoscale the corresponding loading times access
back signals recovered from stress histories. These are plotted for nucleation and growth mechanisms which can fail the material at
each tensile pulse length delivered to the target. It can be seen that a lower stress. At longer times again the failure moves from a wave
the nucleation and growth of voids is consistent with delivering to a bulk dominated process and the surfaces of the metal and its
a signal which implies an constant value of tensile strength (given surroundings become significant. Localization occurs first within
that these were not the material or in the same preparation state). the material at a population of sites and then appears within the
There is an increase in the value recovered when the pulse length bulk resulting in necking of the target before subsequent ductile
drops below 10 ns and it rapidly grows larger as the shorter pulses fracture ensues. As timescales and the volume of material accessed
delivered by laser loading are approached. Further, the recovered increase, tensile strength falls to lower and lower values as larger
targets show no evidence of void nucleation and formation of spall defects in the material are accessed.
planes in the manner observed in the long pulse cases. The onset of plasticity and localization in an FCC metal like
The plot collates experiments across all the different launchers aluminum to increasing impulse duration has been tracked through
used to assemble the data that in turn deliver differing square earlier examples. Finally, consider the response of a structure
pulses into targets before wave interaction subsequently fails them. constructed from aluminum (a tube) under the application of
Plotting the data as a function of the logarithm of the pulse dura- a dynamic load from a dropping mass. In this case the processes of
tion, allows regions of the response to be assigned an F number for plastic localization and buckling occur over a different series of
the NAG mechanisms assumed to describe the spallation process in time and length scales which again follow similar behaviours
ductile metals. The boundary between the two behaviours comes at driven by physical mechanisms in the material.
the 10 ns pulse length discussed above. The stress levels at later times required to fail the structure are
The point at which free surface becomes increasingly difficult to now very much less than the theoretical strength of the material.
create corresponds with F becoming large and this results in the Inertia is the single dominating factor which drives failure at
observed spall strength rising. This relates to the defect population shorter times to require higher stresses than at later ones and the
from which failure ensues at the mesoscale on the one part, but also forms of this will be described below for a simple example. In an
since the trade between energy of the surface created and work experimental and theoretical analysis, previous work has shown
done growing the void does not favour cavitation at this length that the axial failure of the cylinder was due to the yielding and
scale (of order 1 mm). If the pulse is sufficiently short that it cannot folding of the cylinder into a series of segments with discrete
open voids significantly, then the energy required to open a new geometry and features (Fig. 5) [20,21]. The cylinder yields at plastic
surface increases bounded by the theoretical shear strength of the hinges and folds at these to accommodate the applied load. This
solid. This value is taken here to the shear modulus, G/2p, which, in localization of plastic deformation into discrete zones allows strain
the case of aluminum, is ca. 4.5 GPa (the asymptote to the values to be accommodated by buckling, inversion and splitting when
recorded at the smallest pulse lengths). Thus these short laser- stress is applied to the cylinder. The accommodation of such large
strain however has many practical uses since it acts as an efficient
way to use deformation to absorb large amounts of energy in plastic
work in the cylinder collapse.
In the first moments, material interfaces are not accessible by
a volume element within the bulk and the strength of the material
is governed by an ever-greater accessed volume that evolves from
atomic scale effects to wave interactions between the mesoscale
defect structure over the first microsecond. As wave propagation
equilibrates the material state over the component volume, global
strain rate becomes defined for the deformation of a component.
The dislocation which propagates compression within the lattice is
replaced by a population of developing shear bands within the
structural component. As time progresses the mechanical defor-
mation proceeds to accommodate the imposed strain from the
drive. The deformation is controlled by the equilibration time for
the wave transmission through the elements of the structure and
these are observed as inertial effects within the components. This
inertia has microstructural effects observed in metals which affect
slip within the metallic lattice. A low dislocation density and high
Peierls stress makes slip in BCC metals a slower process than in FCC
materials where fast motion and tangling occur readily. This leads
Fig. 4. Spall strength as a function of pulse length in pure aluminum [16]. to the observation of strain rate dependence in the strength in these
114 N.K. Bourne / International Journal of Impact Engineering 48 (2012) 107e115

Fig. 5. The plastic deformation of a cylinder crushed within a load frame (a) radial, (b) axial crush and (c) crushed cylinder; external diameter 51 mm and wall thickness 1.6 mm
[20,21].

two classes of materials which is different and reflected in different produce a larger compressive plastic strain [20]. At some time into
constitutive descriptions to describe strength. The discussion that the deformation the longitudinal compressive strain rate becomes
follows assumes a regime for structural response in which the zero and a second phase begins in which transverse bowing
timescales of the loading impulse are much longer than those of increases further by means of the rotation of plastic hinges until
elastic and plastic wave propagation in the structure. eventually the motion ceases.
This wave precursor phase results defines differences in the The time for stress state equilibration of a metal grain is tens of
time taken for a structure to respond to dynamic deformation, with nanoseconds, that of grains of different orientation or similar scale
the controlling mechanical components occurring in the earliest defects of order hundreds of nanoseconds to a microsecond. The
part of the compression. Thus it is these early processes which equilibration of the stress state within the structural component in
define the progression to a final state of equilibrium. This is the direction of the loading may take microseconds for a thin plate
reflected in Perrone’s rule which states that the single level of strain and hundreds of microseconds for a rod, and once the stress state
rate which best characterises the process of deformation as a whole has equilibrated and a strain rate has been defined for the
is that which occurs in the initial stages of deformation. component, transverse accelerations develop shear localizations in
The mode of deformation of the structure will thus be different the structure and plastic hinges develop; these processes together
from the quasistatic case until stress state equilibration has take tens of milliseconds. Finally the structure accommodates the
occurred within individual loaded components. At the micro- strain over hundreds of milliseconds until the stress state is
structural length scale, wave equilibration between grains and equilibrated with the incoming driver and the relative deformation
second phase particles must occur before a state of continuum ceases. The stressestrain response of the structure under dynamic
strain exists within the bulk. This substructure, known as the load may be mapped to a stress-time one. At the earliest times and
mesoscale, refers not to a specific measurement scale such as the smallest strains the strength is the theoretical maximum of the
a micron for microstructure, but to one based on the dimension of metal under load. After a microsecond it adopts the strength of the
an inhomogeneity within the substructure which delineates the microstructural volume element sampled. When wave equilibra-
regime at which three dimensional strain is observed for a loading tion occurs the stress state in the component is uniaxial stress and
which is imposed as one-dimensional at the continuum. In this yields at the flow stress of the metal. Finally the structure defines its
respect it refers to the scale at which inhomogeneity is explicitly deformation mode with plastic hinges and the stress state required
considered. Equally, at the scale of elements of the macrostructure, is at a lowered state until it reaches a maximum locking strain or
the compression must develop until mechanical deformation has the driving impulse is absorbed.
equilibrated to the state observed in quasistatic loading. This is Fig. 5 shows deformation of a cylinder (a) radially and (b) axially.
engineered through the action of inertial forces developed within The case illustrated in (b) requires a phase establishing plastic flow
the structure by rapid acceleration which parts of it experience in the cylinder before plastic hinges are defined. It may be con-
during the impact. These mechanisms result in two behaviours trasted with the analogous case in (a) where the same cylinder is
which have been ascribed by Calladine [20] to two classes of loaded radially, the plastic state is established within microseconds
structure. The dividing characteristic between these two groups is and the response occurs at a constant rate with strain accommo-
the difference in the times required to establish stress state stability dated by hinging. The latter deformation is classified by Calladine as
in the loading direction (and uniform strain during the deforma- Type I behaviour for structural response and the former as Type II
tion). Mechanically this reflects the time (which is directly related [21]. Type II behaviour illustrates the transition between stress
to the strain) to localize shear zones at positions within the struc- state-limited and structure-limited response whilst in Type I,
ture, followed by the growth of motions in resolved planes structural response is attained very quickly and deformation occurs
perpendicular to the loading direction, to accommodate the strain uniformly at lower stress values. Application of the concepts
imposed by the load. Further all of the lateral deformation must be described earlier would define the relaxation time for acquisition of
compatible with the motion of the falling mass during its retar- this state to be the time required to reach this state and a load could
dation [20]. In such as case it can be shown that the transverse be conceived in which F > 1 for radial loading (a) but F < 1 for
acceleration of structural components is independent of the a longitudinal loading (b) where the weight was arrested. Further
velocity of the impact and that a higher impact velocity will one can see from this example that a relaxation time for
N.K. Bourne / International Journal of Impact Engineering 48 (2012) 107e115 115

a mechanism might equally be substituted for a relaxation strain connections over phenomena and disciplines. A term is required to
which the drive acting on the component might easily also be re- unite these concepts; Akrology the science of the extreme [17].
expressed in terms of an applied strain.
These three examples of deformation in a pure FCC metal show
Acknowledgments
the ability of a solid to exhibit strength at its theoretical maximum
derived from that required to overcome the interatomic potential at
These ideas have developed over my time working in this varied
the bond scale in the first case, through to the buckling character-
field. I would particularly thank the referees who stimulated some
istic of structural deformation modes at the laboratory scale. These
of the discussion on structural collapse in the text. I thank all of the
processes track localized deformation over fifteen orders of
colleagues and students who have contributed particularly from
magnitude in time scale and similar in length scale. The failure in
my groups in Cambridge, RMCS Shrivenham, Manchester and
each case rests with the dimension and the scale of the defect at the
across AWE. Neither could these ideas have progressed without the
operating scale. It is here that one needs to address accurate
many friends at the US national labs and academia who have dis-
measurement techniques focused on the determination of the
cussed these concepts with me and I thank them for their patience.
critical scale of that at which failure will occur.
In particular to Steve Reid to whom the papers in this volume are
dedicated. His patient help and guidance has assisted and encour-
5. Conclusions
aged a great many of workers in the area of impact mechanics
across the UK community and abroad. We hope he remains active
Plastic deformation in nature is the response of composite
over the coming years and remains a pin of the community and the
structures to arbitrary mechanical and radiative loads. The
field.
mechanical ones described here show that design at a particular
British Crown Copyright MoD/2012.
length scale must integrate the macroscopic response of processes
that equilibrate the stress state at that scale. This paper has
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