EUROPEAN STANDARD EN 12004-2 NORME EUROPEENNE. EUROPAISCHE NORM Febraary2017 es #100; 51.20030,9110030 Supersedes EN 12002:208, 6 120082008, EN "Som 2007 EN 1823 2007, 12242007 EX English Version Adhesives for ceramic tiles - Part 2: Test methods “Tiron Sanaa ave by CN 25 9 2016 no emp wthhe CENJCENELE ntl Repltn wich pl he contin fring “cea dad nn he ich rn (pth Fh rman ei nan at ie sero. a0. wore Ramona Sea Sa Slr pn Scden Surana cece, Ore seinen og nai nay iam ny no ned sein 096220978EvS-EN 12008-22017 Contents Page European foreword nme 53 53a 532 aa aia 812 aia aia aus, a2 a2 822 a2 a24 a3 aaa a2 B33 asa 83s a4 42 a4 aaa Aas as asa 852 B53, asa ass a6 861 62 SCOP van Normative references. Sampling Test conditions “Test materials. Generalenene Ceram ies ‘Test substrate Concrete sab. Other substrates TiTtl I TrETl Mixing ofthe adhesive Test Pep Pt erent “Test methOU enna Determination of open time -v-emvnenvvne ‘Test materials. ereniennnsooneooronn Determination of ipo enw “Test materi. gene rene Appatatls.one nnn Procedure. ow nwnna nner “Test report mene nets HO Determination of tensile adhesion strength for comentitous adhesives (C) wwe 1d Test materi nen nner Hh separates aan Procedure wsenn = Evaluation and expression of results ‘Testreport Determination of shear adhesion strength of dispersion adhesives (D) memo 14 Test materiale nen Apparat Procedure one AT Evaluation and expression of results mewn 1D Test porn anne nvsemnenmonrnyennwnnnnnnn nnn 1D Determination of shear sdnesion sirengtr of reaction resin adhesives (8) x-mo———— 19, Tee arta ee STE ee 8 [Apparatiswnosmsemnnneom==vosmmnnsvnnennnnn nnn AD ne eee 20. Evaluation and expression of FeSul-oe ener BB Test PpOF ene BR Determination of ransverse deformation of cementitious adhesives (C)oemwememvem= 22 PIMC enn BB ‘Test materiale BB iEVS-EN 12004-22017 863 Anporcte oe 864 Procedure sw w-nwnnnnnnenennennennnnnnnnnene m5. Resa reerenas ea “Annex (normative) Concrete Sl 1018 wnnnnernninnnrennnne DT ‘RAL Genera treet enennnenrnenersocomvocneovomenoonnm a 82 Teetconditions new once EINE AB ADP APRS penne E AA Concrete abn mmm nmnnmmnmnnnmnmmnnnnnen AAA Manufacture ofthe concrete slab E ‘ANZ. Conattoning ot me concrete slab ncnenececnonen oe ees ‘(AAS Water absorption at the surface... ee ‘AAA. Teasleadheston strength .vu-n-o-s-soemeomnomennennmmsennnn mae AAS Data recorded wenn AE [Annex B (normative) Fale Pa eyeenemewewevennenntenennne 1 BA Adhesion allure (APSF AF-T) --msv-snvosm=esvmnennonnennnnnee A 2 Cohesive allure within the adhesive (CF-A}ooscocon BB Cohesive lure inthe substrate orn the tile (CFS or CPT) nomenon 38 eam lleregliy cece eeeEVS-EN 120042:2017 European foreword ‘This document (EN 12004-2:2017) has heen prepared by Technical Commitee CEN/TC67 "Ceramic ‘es the secretariat of which is eld by UNT ‘This Buropean Standard shall be given the status ofa national standard, ether by publication ofan ‘dencal text or by endorsement, tte latest by Algust 2017, and conicting national standards shall bewithdrawn at he atest by August 2017, ‘Aenton is dren to the possibity that some ofthe elements ofthis document may be the subject of Daten ght CEN shal pot beheld responsible orienting ary oallsueh patent ight This document supersedes EN 1368-2007, EN1323:2007, EN1324;2007, EN 1346:2007, 28 1348:2007, EN 12002:2008, EN 12003-2008, EN 12004, Adhesives or es, s composed with he following pars — Part 1 Requirements evaluation of conformity, classification and designation; — Pare 2: Text methods ‘According to the CEN-CENELEC Internal Regulations, the rational standards organisations of the folloving countries are bound to implement this European Standard: Aust, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark. Estonia, Finland, Former Yugoslav Republi of Macedon, France, Germany, Greece, Hungary, Ieeland, Ireland, aly, Latwa, Lithuania, Loxembourg, Maka, Netheriands, Norway, Poland, Portugal, Romania, Sera, Slovakia Slovenia, Span, Sweden, Switzerland, ‘Turkey andthe United Kingdom. ik GEUSTENE TH AS. a Fon rondo an tbe lrg be Esenian Cane Santon. ‘Selon fern Order 7288, 2067 Fgh of Use is decvonc document: TEBAR TEST BELGELENDINNE ARABEVSEN 12008-22017 1 Scope ‘This European Standard species the methods for determining characterctice for adhesives used in (nternal and externa installation of crane tes. This European Standard doesnot contain performance requirements oF recommendations fr the design and installation of eramic es ‘The following test methods ae described = determination of open tine (8.1) — detertninaton of sp (82): 05 N/mm? is achieved or cohesive falure occurs in the substrate the ‘requirements considered satisfied iter Ue this deren ocumert TERAR TEST BELGELENDIAME ARAGTRN reEVS-EN 12004-22017 6 Mixing of the adhesive ‘The amount of water and/or guid admix required for preparing the cementitious adhesive shall be as stated by the manufacture in parts by mass ie igui wo dry powder (inthe case where a range of ‘alies ie pven te average shal be se Prepace a minimita quantity of kg ofthe adhesive na mixer ofthe typedesribed in EN 196-1:2016, 443, using the sow speed settings (1405) rotations por min and (#225) revolution planetary Carry ou the follwing procedure: ‘= pour the qi into the pans — seater the dry powder over the iui: = minfor305; — takeout the mining pale; = scrape downthepade and pan within 1 min replace the pe and miso 1 min, Let the adhesive mature as specified inthe manufacturer'sinstrctons, and then mie fora further 15. \Where ready-t-ase dispersion adhesives or reaction resin adhesives ar tv be used the manufacturer's Instructions shallbe allowed. 7 Test report ‘The est report sal provide the following information: 8} thenumber and year ofissue ofthis European Standard, ie. EN 120042, and dat of ssue 1b) thepace, date and time of sampling ©) type of adhesive commercial designation and manufacturer 4) sdeniteation of test sample: «) handling and storage of samples before testing: test ondions 8) daeoftese 1) amount of wate gud uted for preparing the adhesive (For cements adhesives) 3) anyother far that could have infuenced the result 4)testressndvdual and mean values and mode offal where required 1) opentime: 2) sip: i 3 | : } i A i 2 5EVS-EN 1200622017 23) tense adhesion strength 49) shear adhesion strona: 5) transverse deformation 8 Test methods 8.1 Determination of open time an ‘Testmatertals 8.1.14 Coram les “Thetles used for this method shal be glazed porous hody le complying with EN 14411, group BI of water absorption (15 £3) by mass, with a thickness inthe range ? mum to 10 am anda rai back Pattern ess than 0.25 mm dep, cut to fcial dimensions of (50 & 1) mmx (S01) mm, 8.1.12 Test substrate “The concrete slab shall compl wit the vequlrements given in 531. 8.1.2 Apparatus 8.1.21 Notched trowel, ‘A notched rowel having 6 mum x6 mm notches at 12 mm centres. 812.2 Weight (Mass). ‘A. mass capable of exerting a force of (204105) N, with a cross-sectional area of less than Somm 30 0m. 8123 Pull-ead plates, Square metalic plates, with dimensions of (50 1) mi x (50 1) mm and a minimum thickness of 30mm witha sutable tingfor connection tthe est machine 8124 Testmachine ‘test machine for direct pl tensile force test and with suitable capacity and sensitivity fr the est “The machine shal be capable of applying the lad to the pullhead plate tthe rate of (250 +50) N/s through a siable iting that does not exert any bending free. 8.13 Procedure ‘Apply a thin layer ofthe adhesive, mixed in accordance with Clause 6, tothe conerete lab with a "aight edge trowel Then apply a thicker layer and com with the notched trowel (81.22) “The trowel shall be held at an ane of approsimately 60° to he substrate ata right angle to one ee of the slab and drawn aero the i pall to tha edge (i sualght ne). ‘Aer Simin, 10 min, 20 min and 30 min pace a east 10 es les (8.1.1.1 50 mm apart onthe adhesive Wein 30s. The tes ae placed on no more than four ibe for all adhesives Load each tle with (202005) ror30s (8122) [Alter 27 storage under standard condition, bond the pullhend plates (0.1.2.8) to the tes with a ‘ultable high strength adhesive (eg, epoxide aahesie). ‘tora further 24 h storage under standard conditions determine the tensile adhesion strength ofthe fahesive by applying afore ineeasing ata constant rae of (250 +50) N/sEVS-EN 12008-22017 ‘8.1.4 Bvaluationand expression of results “The individual tensile adhesion strengths are quoted to the nearest 0,1N/mmé using the flowing orm o where ‘Ass the individual tensile adhesion strength in Newton per square millimetre; 1 sthe cal tensile load in Newton; A. Isthe bondingarea in square millimetre (2 500 mm?) “The tensile adhesion strength foreach ie intervals determined 3 follows = determine he mean of the 10 values = scar the vals fling outside the range of = 209% ofthe mean valu — ttiveor more values remais determine the new mean; — les than ie values remain repeat the test — determine the mode offre ofthe test units acordingo Annex B asthe predominant mode ‘The open time in minutes, i the maximum time interval at which the adhesive meets the tense adhesion strength reqeirement defined EN 2004-1 8115 Testreport ce. dre, S736, 3207 “The information sted in Clause 7, tems.) to) shall be provided plus tem) 1: open ie in minutes 8.2 Determination of slip 82. Test materials eng ee 82.1.1 Ceramic tiles “The tes used for this method shal be dry pressed ceramic tein accordance with EN 14411, group Bl with a water sleoeption «05% by macs, angiszed, with plane adhering surface and wth facial ‘limensions of (100 )mmx(100~ 1} mm, a mass of (200'2 10) ganda thickness in the range of ‘Brum to 10mm 82.1.2 Test substrate ‘Te concrete si shall comply with the requirments glen nS. 822 Apparatus 8221 Steelstralghtodge. 8222 clamps8223 Masking ape. |A25 mm wide masking ape 8224 Notched trowel, ‘notched trowel having 6 mm x 6 mm notches a 12mm centres. 8225 spacers. ‘Two (25+ 05) mm x(25- 0,5) mm (10 #5) mim thick spacers made from stainless tech 822.6 Weight (Mass). ‘A: mass capable of exerting 2 force of (5020.1) N with a cross-sectional area of less than (Goo 1) mm (100 #1} mm 822.7 Vernlercaliper Vernier caliper acurate to 001 mm, 8223 Procedure Secure the sel stralght edge (8.2.2.1), with the clamps (822.2), 3 the top ofthe concrete slab so that its botom edges horizontal when the la eased is verti postion, Position 25 mm wide masking ape (822.3) immediately below the sel stralght edge and apply a thin layer ofthe adesive mixed in acordance with Clase 6 to the concrete slab witha straight ede trowel ‘Then apply a ticker layer of adhesive tothe surface ofthe concrete slab so that t Just overlaps the bottom edge of the masking tape. Comb the adhesive stright angle tothe straightedge withthe notched trowel (82.24), ‘The wowel shall beheld at an ange of approximately 60° to the substrate and parle othe straight cee. Immediately remove the masking tape, position 25 mm spacers (8.2.25) agaist the straight edge and ater to minates place the ile (8211 aginst the spacers, as shown in Figue I and lo with the ‘mass 50+ 0) N (822.6). Measure the gap between the straight edge and the tle, in three points with the Verner caliper (6227) towthins 04 mm. [ter (50-5) remove the weigh and the spacers and immediatly an carefully Mt the slab into 3 ‘vertical positon, Aer (20 #2) min remeasure the gap, as Delor, inthe same the pln ‘The maximum sip ofthe tile under ts own mas isthe diference between the two readings Carry ou the test foreach of 3 es, for each adhesive, Report the results in millimetres and the mean value 82.4 Test report ‘The information listed in Clause 7, tems a) to) shall be provided plus Kem J) 2: Sp in milimetre (individual and mean values) i i i : ;EVS-EN 12008-22017 i el straight dge 25mmx25 mmx lO mmc spacers onctete sab Figure 1— Sliptest ‘83 Determination of tensile adhesion strength for cementitious adhesives (0) 1834 Test materials 83.1.1 Ceramic les “The tls used for this tt shall be dry pressed ceramic tile in accordance with EN 14411, Group Bl fully vitrified, with a water absonption of 05 % by mass, nglazed and with plain, mat, adhering ‘surface, with faa mensons of (50 = 1) mm x (50+ 1} mm, ‘83.1.2 Test substrate ‘The concrete test substrate shall conform to requirements given in S2. 83.2 Apparatus 83.21 Weight (as), u pote an te telong the Estrin Cone Sandon,EvS-EN 12008:2:2017 A mass capable of exerting a force of (202005)N, with a cross section area of less than Somm:x50™mm. 832.2 Pullhead plate. Square metalic plates, with dimensions of (504 1) mim x (5021) mm and a minimum thickness of 10mm witha sulable iting for connection tothe est machine 832.3 Tensile esting apparatus A test machine for direct pl tensile fore test and wit suable capacity and sensitivity for the test ‘The mochine shall be capable of applying the load tothe pulchead plate 3 the rate of (250 250) N/s ‘rough suitable ting tht does not exert any beading ace. 832.4 Alrciculating oven. An arcrclating oven capable of cooling the temperature to within 3". 832.5 Notched trowel, ‘Anotched trowel having 6 mm x6 mm notches at 12.mm centres. 83.3 Procedure 183.3. Preparation oftestunlts “Apply a thin layer ofthe adhesive, mised in accordance with Clase 6, tothe concrete slab with a _Sraight edge trowel Then apply a thicker ayer and comb witha notched trowel (3.25). “The trowel shal be held at an ange of approximately 60" tothe substrate ata ig angle to one edge of {heslab and drawn aeross he slab parle to that ede (in astaght ne). [After min place 10 ties (83.1.1) on the adhesive at distance apart of $0 mm and load each le with (2020.05) for 30, £83.32 Initial tensile adhesion strength Prepate the tes units in accordance with 833.1 ‘After 274 storage under standard conditions bond the pull-head plates (83.22) tothe ties with ‘table high strength adhesive (eg. epoxide}. ‘After a farther 24 h storage under standard conditions determine the tenslle adhesion strength ofthe dhesive by appvinga fore ata onstant rate of (250 250) N/s If fast-seting properties of adhesives are tobe tested, determine the tensile adhesion strength after six hours under standard conditions the pl ea plates shall be bonded 2 minimum of two hours before determining the tensile adhesion strength Report the result in Newton 83.3.3 Tensile adhesion strength after water immersion Prepare the test units accordance with 33.1 Condition the test unite under standard conditions for 7d, and immerse in water atthe standard temperature [After 20 d remove the test units fom the water, wipe with a cloth and bond the pullhead plates (832.2) to theses, Aer further ? hin standard conditons Immerse the Lest unts in Water a he Standard temperature “The following day remove the test units rom water and immediately carryout he tensile adhesion test inaceordance with 8232 2