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Certificate of Analysis

Ordered Quantity: 48.000 DR

Shipped From: AIE US CALVERT CITY PLT

PVP IODINE DRUM 49.9KG 1

POVIDONE-IODINE, USP, EP, JP | PVP Iodine
Ashland Material Number: 831093

Characteristics Specification Results

Appearance @ 25 deg. C - Free PASS PASS

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flowing reddish brown powder
Identification Tests - USP, EP PASS PASS
& JP (W1125) Pass equals Meets
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all ID tests
Clarity and Color of Solution PASS PASS
(CCLM478) Pass equals Clear and
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brown
% Available Iodine (anhydrous 11.0 - 12.0 11.3
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basis, W404)
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% Iodide (anhydrous basis, W404) <= 6.0 5.2
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% Loss on Drying, (W1126) <= 5.0 1.9
pH of 10% soln. w/v of CO2 free 1.5 - 3.5 1.6
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water (Q231)
% Nitrogen (anhydrous basis, 10.0 - 11.5 10.3
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W1118)
% Ash (Residue on Ignition or <= 0.025 0.000
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Sulphated, W1381)
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ppm Heavy Metals (W1494) <= 10 0
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ppm Arsenic (W1494) <= 1.5 0.0
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ppm Free Iodine (CCLM088) <= 30 3
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Iodine/Iodide Ratio (W404) 1.8 - 2.2 2.2
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Date of Manufacture January 15, 2015
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Retest Date January 14, 2017
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Ordered Quantity 48.000 DR
Notes:
Meets the requirements of Povidone, Iodinated and Povidone - Iodine in
the current EP, JP and US Pharmacopoeias respectively. Precursor meets
the requirements for Povidone in the current EP, JP and US
Pharmacopoeias.

Printed: February 11, 2015 11:47:42

 Page 2 of 2

Certificate of Analysis

Ordered Quantity: 48.000 DR

Shipped From: AIE US CALVERT CITY PLT

PVP IODINE DRUM 49.9KG 1

POVIDONE-IODINE, USP, EP, JP | PVP Iodine
Ashland Material Number: 831093

Characteristics Specification Results

Responsible Manufacturing Facility:

ISP Chemicals LLC
Affiliate of Ashland Inc.
455 N. MAIN ST. (HWY 95)
CALVERT CITY KY 42029

Printed: February 11, 2015 11:47:42