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    ams 4945 E-2011 - eng. - УПМС

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    Tetiana

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    of 10
    SAE Aerospace AEROSPACE SAE ams4sa5 REV. E SSA eto Grp MATERIAL —_ SPECIFICATION = Jrevisee 2011-08 ‘Superseding AMS4945D Titanium Alloy Tubing, Seamless, Hydraulic 3Al- 2.5V, Controlled Contractile Strain Ratio. Cold Worked, Stress Relieved (Composition similar to UNS E5320) RATIONALE AMS4945E results from a clarification of furnace classes (3.3.1) and an update of this specification 1. SCOPE 4.41 Form This specification covers a titanium alloy in the form of seamless tubing, 1.2. Application This tubing has been used typically for parts, such as hycraulic lines, requinng high fatigue strength and oxidation resistance up to 600 *F (316 *C) and weldability, but usage is not limited to such applications. 2. APPLICABLE DOCUMENTS The issue of the following documents in effect on the date of the purchase order forms a part of this specification fo the extent specified herein. The supplier may work to @ subsequent revision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no superseding document has been specified, the last published issuo of that document shall apply. 2.4 SAE Publications Available from SAE International, £00 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or 724-776-4970 (outside USA), www.sae.or0. AMS2244 Tolerances, Titanium and Titanium Alloy Tubing AMS2249 Chemical Check Anaiysis Limits, Titanium and Titanium Alloys AMS2634 —_Ulrasonic Inspection, Thin Wall Metal Tubing AMS2750 — Pyrometry AMS2809 _Identtfication, Titanium and Titanium Alloy Wrought Products AS4076 Contractile Strain Ratio Testing of Titanium Hydraulic Tubing AS33611 Tube Bend Radi ‘SAE Tecra] Sandnse Bos Res poise hats repr publsnedby SAEs savanca he sine ol ec snd mghewing ceneas_ The wee Os pOT 3s pea ah sy fray parce cng any ua genetarang ero, se soe rape ee yeh’ © S011 SAE inemstonal = = Arges No sr. pbiaton may pace, stan arava stem oan nay oy ny nese Seon, neha TOPLACE ADOCUMENT ORDER: Tel: 877-606-7528 (inside USA and Canada) Tek 1724-76910 (outside USA SAL value i i wines on this Technical Report, please visit Ensit Costner Se vioeQzae ory | tto./iwun.sce.crattechnicalstandards/ANS<945E SAE WEB ADDRESS: hepulww.sse org ; SAE AMS4945E Page 2 of 10 2.2 ASTM Publications Available from ASTM Intemational, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www astm.org. ASTME8/E 8M Tension Testing of Metallic Materials ASTME 1409 Determination of Oxygen and Nitrogen in Titanium and Titanium Alloys by the Inert Gas Fusion Technique ASTME 1447 Detormination of Hydrogen in Titanium and Titanium Alloys by the Inert Gas Fusion Thermal Conductivity/infrared Detection Method ASTME 1941 Determination of Carbon in Refractory and Reactive Metals and Their Alloys ASTME 2371 Analysis of Titanium and Titanium Alloys by Atomic Emission Plasma Spectrometry 2.3. ASME Publications Available from American Society of Mechanical Engineers, 22 Law Drive, P.O. Box 2900, Fairfield, NJ 07007-2900, Tel: 973-882-1170, www asme.org. ASME B46.1 Surface Texture (Roughness, Waviness and Lay) 3. TECHNICAL REQUIREMENTS 3.1. Composition Shall conform to the percentages by weight shown in Table 1; carbon shall be determined in accordance with ASTM E 1941, hydrogen in accordance with ASTM E 1447, oxygen and ritrogen in accordance with ASTM E 1409, and ther elements in accordance with ASTM E 2371. Other analytical methods may be used if acceptable to the purchaser. TABLE 1 - COMPOSITION Eement iin max Auminum 3.60 Vanadium 3.00 Iron 0.30 Oxygen 0.12 Carbon 0.05 Nitrogen 0.020 (200 ppm) Hydrogen (3.1.2) 0.015 (180 ppm) Yitrium (3.1.1) 90.005 ( 50 ppm) Other Elements, each (3.1.1) 0.10 Other Elements, fotal (3.1.1) 040 Titanium __temainder 3.1.1 Determination not required for routine acceptance. 3.12 When using ASTM E 1447 for hydrogen analysis, sample size may be as large as 0.36 gram. 3.13. Check Analysis Composition variations shall meet the applicable requirements of AMS2249. SAE AMS4945E Page 3 of 10 8.2 Melting Practice Alloy shall be muttile melted. The fist melt shall be made by consumable alectrode, nanconsumable electrode, electron Joeam cold hearth, or plasma arc cold hearth meting practice. The subsequent melt or mells shal be made under vacuum using vacuum arc remelting (VAR) practoe, Alloy additons are not permitted in the final melt cycle. 3.2.1 The atmosphere for nonconsumable electrode melting shall be vacuum or stall be argon andior helium at an absolute prossure not highar than 1000 mm of mercury. 32.2. The electrode tip fornonconsumable electrode melting shail be water-cooled copper. 33° Condition Cold worked and stress relieved by heating to a temperature not lower than 700 °F (371 °C) and holding at heat for not less than 90 minutes. Tubng that '$ ‘olary staightened after final reduction shall be stress relieved ala minimum temperature of 700 *F fornot less then 2 hours alter straightening, Pyromety shell be in accordance with AMS27£0. 3.1. Furnaces shall meet the requirements of AMS2750. Furnaces shall be a minimum Class 5 (425 “F/4t4°C), with ‘a minimum of Type D instumentation 3.4 Properies Tubng shall conform tb the following requirements: 3.4.1 Tensile Properties Shall be ae shown in Table 2, determined in accordance with ASTME 8 / E 8M with the rato of strain set at 0.066 inchiinchiminute (0.005 mmimm/minute) and maintained within a tolerance of +0002 inchfinchiminuta (0.002 mm/mmiminute) through the 0.2% offset yreld stain, TABLE 2 - MINIMUM TENSILE PROPERTIES Proparty Value Tensie Strength 725 wi (862 MPa) Yield Strength at 0.2% Offset 105 ksi(724 MPa) Elongation in 2 Inches (608 mm) Nominal Wall Thickness Upto0.01€ineh 0.41 mm), incl 8% Over 0,016 inch (0.41 mm) 10% 342 Flarabilty ‘Specimens as in 43.3 shall withstand flaring at room temperature, without formation of cracks of other visibie defects, by being forced axially, with steady pressure, over a hardened and polished tapered steel pin havng a 74-degree inciuded angle to produce a flare having a permanent expanded OD nat less than 1.20 tmes the original nominal OD. 3.43 Prossurs Testng ‘Tubing shall show no bulges, leaks, pin holes, cracks, or othar defects when subjected to an internal hydrostatic pressure (P) sufficient to cause a tensile stress of 105 ks (724 MPa) in the tubing wall, except that a diametric permanent set of 0.02 inclvinch (0002 mmvmm) of diameter is acceptable. The hydrostatic pressure (P) shall be determined from Equation 1 (4.1) SAE AMS4945E Page 4 of 10 where Festprossure in ksi (MPe) S= 105ksi(724 MPa) D= Nominal OD 4 lominal ID 3.44 Banding Tubing shall not develop cracks, tears, breaks, or other flaws when bent 180 degrees around a suitable bend die having a centering radius equal to three times the nominal OD of the tubing. soid rod or bal-type retractatle mandrel inserted to tne tangent of the Dend shall be used to support the inside of the tube curing bending lo restictfletlening to a value that does not exceed 3% of the nominal OD of the tube. Flattening shal be measured in accor danice with AS33011 3.45 Flattening ‘The inside and outside surfaces of tubing shall show no cracks, tears, breaks, opened die marks, or opened polishing marks when a full section of the tube is flattened between parallal plates under a load appied gradually and perpendiculerly to the longitudinal axis unl the distance between the plates is not greater than shown in Table 3. After examination of the outside surfaces, the samples shall be split longitudinally and the inside surfaces. examined. Examinaton of tube surfaces shall be at 5to 10X magnification, TABLE 3 - FLATTENING TEST Outside ameter b Wall Thickness Rato Distance Between Plates opt (t= Wall Thicknoss| Upb @, ne Not Required Over 12 10 16, nc) 12t Over 16 10 20, nc) 15t Over 30 to £0, inc! a7 3.4.5.1 Asan attemate flattening test, a half-tube sample shal be pressed to produce a flat surface approxmatey 3/8 inch (9.5 mm) wide on the tubing ID. 2.48 Mioroetucture Shall be predominantly an elongsted wrought structure, wth some areas of patialy transformed beta structure permissible, Standards shall be acceptable to purchaser, Tubing shall be free of any oxygenwich layer, such as alpha case (Ses 8.2), or other surface contamination, determined by microscopic examination at not lower than 400K magnifcation or by otner method agreed upon by purchaser and vendor. 3.47 Contractile Stain Ratio. The contractio strain ratio (CSR), when testod in accordance with AS4076, shall be not loss than 13 for tubing sizos with wall thicknesses up fo and including those indicated in Tabla 4 Tha CSR for tubing sizes up to and including thasa indicated in Table 5, shal be not less than 1.5. SAE AMS4945E Page 5 of 10 ‘TABLE 4 - TUBING SIZES FOR 1.3 MININUM CONTRACTILE STRAIN RATIO Maximum Maximam Nominal OD —NominalOD — Wall Thickness Wall Thiskness Inch Millimeter Inch Milimeters 36 48 0.920 Ost 44 64 0.022 0.55 38 95 0.032 081 We 127 9.043 1.09 5/8 159 0.054 137 314 19.0 0.085 1165 78 22 0077 168 4 26.4 0.088 224 TABLE 5 - TUBING SIZES FOR 1.5 MINIMUM CONTRACTILE STRAIN RATIO Maximum Maximum Nominal OD —NominalOD Wall Thickness Wall Thickness Inch Nillimeters Inch Milimeters la 318 0.087 221 2 33.1 0.980 220 3.5 Quality Tubing, as received by purchaser, shall be uniform in quality and condition and shall have a finish conforming fo the best practice for nigh auaity aircraft tubing. It shall be smooth and free from scele or oxide, burrs, seams, tears, grooves, laminations, slivers, pits and other imperfections detrimertal to usage of the tubing. Surface imperfections, such as handling marks or staightering marks, will not be considered injurious if the imperfections are removable within the tolerances specified for val thickness tut removal of such imperfectiens is notrequired, 3.8.1 Each tube shall be ultrasonically inspecied in accordance wilh AMS2634, Class AA, for ID, OD, and subsurface imperfections of al types and orientaton (longitudinal and transverse). 3.52 Surface Condition 3.62.1 OD Surface Shall show a uniformly acd-pickied surface finish; not less tan QOCt inch (0,025 mm) shall have been chemically Temoved trom the wal thickness as a finishing operation. Soft, Delt polisning frior to the Pking operation is permissible ‘races of the polishing marks may remain after the pickling operation. Centerless grinding or other mechanical operations ‘aro nol permitted. 3.522 ID Surface Shall show a uniform matte finish, produced by abrasive blasting with grit nat larger than 100 mash (150 jm) followed by forcedflow, acid pickling to remove not less than 0.0005 inch (0.013 mm) fram the wall thickness, 3.523 Surface Roughness Shall bo not greater than 63 microinches (16 im) on the ID and 32 microinches (08 jim) on the OD, determined in accordance with ASME B46.1 3.52.4 The ID and OD surlaces of the tubina shall be free from arease and other foreign matter. Metalic fakes or Pattices stall not be collected by a cean, white cloth drawn through the length cf the bore of a test sample Discoloration cf the cloth, without the presence of fakes or particles, is acceptable, SAE AMS4945E Page 6 of 10 36 jerances Shall conform to all applicable requirements of the following! 3.61 Outer Diameter Shall be as specified in Table 6; tolerances shown include ovally. TABLE 6A TOLERANCES, OUTER DIAMETER, INCH/POUND UNITS Tolerance Tolerance Nominal OD Inch neh Inches Plus. Minus ‘Over 0.093 t00.187, incl 0.002, 0000 Qver 0.187 100.499, incl 0.008 ‘9.000 Over 0.499 100.749, incl 0.004 ‘9.000 Qver 0.749 100.989, incl 0.004 ‘9001 ‘Over 0.98810 1.498, incl 0.004. 9002 Over 1.499 104,999, incl 0.006 0.002 ‘TABLE 6 -TOLERANCES, OUTER DIAMETER, SI UNITS ———_______Teterance Tolerance Nominal 0D Milimater Millimeter Millimeters Plus Minus Over 23610 475, inal 0.08 ‘0.00 Quer 475101267. incl 0.08 00 Over 12.87 1018.02,incl «0.10 G00 Over 19.02 1028.37, incl 0.10 0.025 Over 25.37 1036.07, incl 0.10 aos Over 38.07 105077,incl 0.13. 08. 3.6.4.1 Diameter tolerances for tubing 0.093 inch (2:38 mm) and under or over 1,999 inches (80.7 mm) in nominal OD shall be as agreed upon by purchaser and vencor. 3.62 Inner Diameter Shall be as specified in Table 7, The nominal inner diameter is defined as being equal to tne nominal OD minus twice the nominal wall thickness, TABLE 7A- TOLERANCES, INNER DIAMETER, INCH/POUND UNITS Tolerance Tolerance: Nominal 1 Inch Inch Inchas Plus. Minus Upto 0.338, iret 00018 00015 ver 0,338 10 0.48, incl 0.002, 0,002 ver 0.449 10 0.673, incl 0.0028 0,025 Over 0.875 00.900, incl 0.003 (0,003, ver 0,900 and above 0,004 0,004, SAE AMS4945E Page 7 of 10 ‘TABLE 7B - TOLERANCES, INNER DIAMETER, SI UNITS. Tolerance Tolerance Nominal 1D Millimeter Milimeter Milimeters. Plus. Minus Upto 8.59, inal 0.038 C038 Over 8,59 1011.40, incl 005 08 Over 11,40 to 17.08, incl 0.064 0.064 ver 17.09 10 22.86, incl 0.08 0.08 Over 22.86 and above 010 010 3.63. Wall THiness ‘Altubng 1, £00 inches (38, 10 mm) end under in nominal OD shallhave a wall thickness not les than @5% of nominal 3.64 Length and Straighness Shall conform to AMS2244, 4. QUALITY ASSURANCE PROVISIONS 4.1. Responsbiliy for nspection ‘The vendor of tubing shall supply all samples for vencor’s tests and shall be responsible for the performance of al required teste, Purchaser reserves the right to sample and to perform eny confirmatory testing deemed necessary ‘ensure that the luting confarms to specified requirements 4.2. Classifcation of Tests 4.24 Acceptance Tesis All lechnical requirements except pressure testing (3.43) are acceptance tests and shall be performedon each heat or lt ‘98 applicable, 4.22 Periodic Tasts Pressure testing (3.43) is a periodic test end shall be performed at a frequency selected by the vendor unless frequency ‘of testing is specified by purchaser, 4.23. Preproduction Tests All technical raquiremenis ara preproduction tests and shall be perfarmed pricr to or on the initial shipment of tubing to a purchaser, when a change in material andior processing requires reapproval as in 44.2, and when purchaser deems confirmatory testing to be requred, 4.3. Sampling and Testing Shell be in accordance with the following; a lot shall be all tubing of the same nominal size from the same ingol, same processing and finsshing oporations, and sirace ralieved in the eame furnace charge. 4.31 Composition One sample from each heat, except that for hydrogen determinations one sample from each lot obtained after thermal ‘and chemical processing is completed. An ingot analysis obiained from the alloy producer may be utlized to substantiate heat requrements, SAE AMS4945E Page 8 of 10 4.32 Tensile Properties (One sample for each 1000 feet (305 m) or three samples from each Ict, whichever is greater. 4.33 Farabiliy (One sample por tube for lot sizos of four or loss tubes and four samples for lot sizas of § to 30 tubes, Forlot sizes af 40 er more tubes, one sample from one end of 10% of the tubes. 4.33.1 Specimens for flarabilty (3.4.2) test shall be full tubes or sections cut from a tube, The end of the specimen to be flared shall be cut square, with the cut end smooth and free from burrs, but net rounded, 434 Pressure Test {As agreed upon by purchaser and vendor 435 Bending “Two samples from each lt 435 Pattening One ample for cach 195 foot (41 m) of tubing or 10 samplas from each lot, whichever is loss. Each specimen shall bo not less than 2 inches (51 mm) long, cut in haff with the cuts parallel to the axis ofthe tude 4.37 Microstucture One sample from each let 4.98 Contractile Stain Ratio “Three perlot 4.39. Utrasonic inspection and Tolerances Each tube 4.9.40 Surface Condon Each hibe, e

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