Professional Documents
Culture Documents
1965
Recommended Citation
Hu, Kuo-Chu, "Epoxy resin admixture for concrete" (1965). Masters Theses. 5242.
https://scholarsmine.mst.edu/masters_theses/5242
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-·.. 11
I'
BY
KUO-CHU HU I I t{z.,?;
THESIS
Rolla, Missouri
1965
APPROVED BY
~'~ ~~...._(Advisor)
~-q"'1 \Z ~
ii
ABSTRACT
ACKNOWLEDGEMENT
TABLE OF CONTENTS
Page
ABSTRACT . . . . . . . . ii
ACKNOWLEDGEMENT • lll
LIST OF ILLUSTRATIONS . . . . . . . . . . . vi
I. INTRODUCTION . . . . . . ..
. . . . . . . 1
A. Resins . . . . . . . . . . . . 7
Curing . . . . . . . . .
'
B. . . . 8
A. Test Apparatus . . . . . . . . . . . . . . . . 10
1. Sieves and Sieve Shakers . . . . . . . . . 10
2. Concrete Mixer . . . . . . . . . . . . . . 10
3. Compression Testing Machines . 10
4. Los Angeles Abrasion Testing Machine . ll
5. Ames Dial Gage . . . . . . . . . . . . 11
B. Materials Used In Tests . . . 12
1. Cement . . . . . . . . . . . . . . 12
2. Aggregate . . . . . . . . . . . . 12
3. \-'later . . . . . . . . . . . . . . .
. 14
4. Admixture . . . . . . . . 14
c. Mixing Procedure . . . . . .
. 14
1. Design of the Mixtures . . . . . . .
. 14
2. Mixing Concrete . . . . . . . . . .
. 15
3. Handling Precautions . . . . . . . .
. 18
D. Test Procedure . . . . . . . . . . . . .
. 18
1. 'rest Procedure for Compressive Strength 18
2. Test Procedure for Flexural Strength . .
. 19
3. Test Procedure for Modulus of Elasticity . 21
TABLE OF CONTENTS
Page
APPENDIX . . . . . . 35
BIBLIOGRAPHY . 42
VITA . . . . . . . 43
Vl
LIST OF ILLUSTRATIONS
Figures Page
LIST OF TABLES
Table Page
I. INTRODUCTION
its high strength but little research has been done in this
direction.
retained.
2
1:18 by weight.
sists of:
Epoxy resin 10 parts by weight
Filler Variable
concrete pipe for sewers can be coated with epoxy. The re-
service.
bond.
A. RESINS
cured system.
resins become permanently hard once they cure and will not
melt at elevated temperatures. Cured epoxy resins are char-
B. CURING
used, and also its mass and temperature. The use of shallow
9
A. TEST APPARATUS
sizes was used: 1", 3/4", 1/2", 3/8", No.4 and No.8.
a set of sieves 8 11
in diameter made by W. S. Tyler Company,
2. Concrete Mixer
This machine has two scales, the low range of 0-60,000 pounds
with 200 pound graduations and the high range of 0-350,000
pounds with 1000 pound graduations.
mixer.
inch.
12
1. Cement
2. Aggregate
No. 8 0
3/8 inch 20 55
No. 4 0 - 10
No. 8 0 - 5
13
that the coarse aggregate used in the mixes met the require-
No. 4 99
No. 8 82
No. 16 66
No. 30 55
No. 50 18
No. 100 3
No. 4 95 - 100
No. 8 80 - 100
No. 16 50 - 85
No. 30 25 - 60
No. 50 10 - 30
No. 100 2 10
14
3. Water
4• Admixture
by weight.
C. MIXING PROCEDURE
2. Mixing Concrete
------------------------------------------------------------------·
Type of Coarse Fine Epoxy Curing
Mix Aggregate Aggregate Cement Water Resin Agent
(lb.) (lb.) (lb.) (lb.) (lb.) (lb.)
1-'
0'\
~I
and C as follows:
added.
(4) The curing agent was added to the water, and then
the premixed curing agent and water and cement were added to
concrete mixer.
(5) Mixing was continued for two minutes.
fine aggregate. The epoxy and sand were mixed for two min-
utes in the concrete mixer, and then half of the coarse
aggregate was added and mixed for three minutes. The rest
of the coarse aggregate, cement and water was then added and
mixing was continued for two minutes.
3. Handling Precautions
D. TEST PROCEDURE
specimen
p
f = A
where
f = unit stress in pounds per square inch
P = ultimate load in pounds
A - cross-sectional area of the cylinder in square
inches
used and the beams were supported over a span of 15". The
follows:
3PL
R - 2bd2
where
concrete was not very large. The slump for the two batches
of Mix A was 1 1/2" and 1". The slumps for Mix B, Mix c and
Mix D were 2", 1 1/2" and 1 1/2" respectively. The test re-
particles.
Mix B and c is 81.5 per cent and 93.5 per cent of Mix A re-
spectively.
24
conditions.
1 1
l--+-+-+-+---l-+-+-l-+--1--t-l--+-i-+
.... "'---1'H-"'+t-11-t-+H-++-H++-H--t--HH--t-H---t--t-\rt=t-I"J • t-!,
'"'I -i-!-ii-+-+--+--+-+-+-l
+---l-l-+-1-~-++-l--+++-H-+t-li-++H-++H++-H--t-iiH--t-H--t--t-N-ri'l.::::~- 1 _bP~~:=-i-+-+---t-t-++--t--+--t--+--I---+--+---+-H--I
~~--
H-+--1-1-1-- :;==-= --i----i-\-+--l---i-lr-+---1,H+H-++-H++-H++-H-+H-++-t:;=:::±--H-n~-- (i~da~~--r+-+--+-+----+--+-l+--+--t-+--t--HH--1,H
--- I I
j- i . kl=
1---1----+---!-!- r --;-- - 1--1--t-t-+-J-l+-il - -I !
-1-- - f- 1 -- -l-H--+--HH-+H-++-H-+--t-t-t-t-
1-f- · - -- t 1-r--r--- -- '--+--+--1---+-t--t--cl-- --
--+--H+--+--H-l--+-t-t-+-+-1-t--t-H-t-+ Urda -i--+-+-1-++-+-t --l---i-H--+-~-+-+---1-1
!/'' -
1- -- - 1 -t-t-t--t-t-- i --+--t-1---+=t-=,n+ln=-tl---- -+-+--1-+--t--+-1---+--+-I-+-H-+-t-H-t----t-·t-:r'-f--t--+--t-: -rj .,..--!·-,... 1 4~1-4+--1-4+--1-4+--1-~l--1-+t--t1~+-1~+-1~+--l--l
f-t-1--- --+-f- -1--hl-+--+--t-f- -1-t-t-1- -~'-+--+-1-++-i-1---l--~-i-l-++-H++-H-+'-t---t-t--+-!-8' ,-- I I L-l-
-t~
+- , ~ti~~1-
- :==-:t-~~1-~~t~-+-f-+-t-t--t-:-t-+-1
I I I
:=:-=t- _i_-
:=;:JI-_+1---+--+--1--+++--1-f--f-H-1-+ _l,_'i- ++ -++_(_-++_(_-++---1-t--++--1-t-+f--t-+-+t--1-t--t-f--++ ++-t'-++--11--+t--i--t_--tt--- :- -
I
i I
I
;
1
1-t++-!-t++-r-+-++-H-+-HY-+t-1'-++kilht=;;iv;siF'.;;;i,·-~7'~rt
1
-r•r:;;l;;;tJI'~__j-+ +-- -I--H-++-+--+-+-+-+-+-+-+-~---+-+--t-+
1
H-t--1-t--+-+--t-t-t-t---t--<H--t--t-" -t-t---t-t --r- L.la1 :rat- p ·:::-rvt "": h rr _ 'h h H 1- li bh S H-L--t- -+-t-t-t---+-1-t--t--+-i-t--t-H-t--t-H
H++-H++-H++-H-++- ·1-f- - -1--l--l-+--l--l-+-• .
H--+-+-H++--l-+-++-H--+-+-1-++-+-l-t--t-H-t- - · -r- .. -~ \-
I!
-
r
\"" -!-"- t- --1--f-f- · !- - 1-+--1-+-1-t--t-H-t--t-H-t--t-H--t--t--i
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H--+--!-H++-+-++-+-H---+--HH-+-t-i-+-t-1--- H- H - '. . ;_:+-r-+-+--Hr-l-+H-++H-+--t-H-+--1-l
I --+-1-+--+-+-+-+-+--t-t-+-+-t-t-t-tl-+
1++-+-+++--H--+--H-+-+-H-+-t-H--l
~4-~-+~-t-~--t-~4-t--t-~-t-~-t-~,_rr~~~_i~~
~--+-~~-1-++-t-~~-~-~-rr+-~
J
_l
L I
27
-- i+--l-1-'----+-+-+-+---
__j I '
J--l--+-1---+-1------l--+--+--l---l
I I '
F-R :
i
! I
I i I
I
i I I .. j_ I i I -- --i - ~ --+'---+1-+-i--J-+----1'- _J__ I I
I
t-- +--+--H4-f-W-l-+-H-+-H-++H++-iH-+H+-hH-+H--t-HH-+H-t--HH--t-Hi
I t-+H+-1--1!-t-+-H++-:f-i---il-+-
. - t- l-r-+-+-t
.·--+---J-+--1
30
r-r--r--r-+_:~1+ ~±~
: I
+--+-t--t-+-1----'- :-~ t-~ I ~~-
l-: , "
--f--+---H-+.-f---l-1---<--L 1-r-- - r--'-- ---i---1--t-i--
I
-r--r-t-H~. --~.-'-,-, 1--j-;-ri !
-r-- -r- -~~-· E-i 1-' _, __ . ;I]
·-'-- --t - - --- • H t- i
I
-L;-+-+--i-l--+-+--t
. I I I c
-h
I i I I I
I
I I
I I
I
._
I ' t1
t-t-- J _I -l ~-~~- - --+1-i----+---+-f--+-+-+-!
I .......
-res=
I
1, I
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Lr----ft-------+t---,if----+:-_-.1_- i ~ ~ - --1,--+-+-H---+-3~,_---1-+;_-...~i·----~t------+•--r-t·-+---++-H-+-+--''--+---++-t----j-l---t--+--l-H---+--+-+1---+---'
--++-f--+-+--+-+-+-+-+-~+-~-+--+-+-+--t-f-+-+--+-+-+--+,-+1----i' -~-~~+-~+--+-+-J-4-~+--+-+1~~4-~
LH-t-++-H-++HH++-t-+-+-l--1-f-----l
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,- I
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I
--+---+-t--1--+-,-,-
1-+-+-+--+-!-+-+-+-1---+--+-!-+-+---"---++++-l-f--+--t-! -l-!--1 H-t----'H--t++--++--11++,+++-1--+-+---rl!
t- ~~-- 1--i I I ' I
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I
t- -~ - -1-r I h +-~---: I I
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_lj
I I
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+ I'" Li-+ ++-+++----+++-++-H-+-f--l-1--il-+---+-+-+-+
+-1-l I ' _i
-' -~-r -+-- r!
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l-
I I I
j I
31
f---t-
f---t-t--~~~-+~~~+-~~~~~-~-+4-~-r+-~~~~i-H-rt-rt-r~-ti-t-r ~,_~~+-r+-r~l-+~i-t~-~r+~
~++--+++--t++--t+-Hf--++-H-+--f-l+H+H+t-t+H+H+H--t-H---t-M--t---!1 - t-,-
~~- ~-f-t~-+-+,~~~+-~-+~+-t-t-+~+-~-+~+-~-+~+-~-+~+-~-t~~~t~1 --r-
I '
32
VI. CONCLUSIONS
with Mix A.
cap which had a low elastic modulus itself and the extension
and the same measuring method was used for all mixes, the
gate. The mixing time was limited for Mix D because the
34
epoxy resin had been mixed with curing agent before it was
mixed with aggregate thus shortening the pot life. However,
epoxy resin and sand can be mixed as long as desired for
Mix C and B because the curing agent was added in the last
step.
APPENDIX
! .
·l·
• t ••.
·t·.
:1:
.. ;
_._
--- --~ ·-··_· ~;~:-.
"' "
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..
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,~ :--- ., L , :_ -
J·t f-1-
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_, • ~ t l t·
-~r- t· _::+- - t .... l-t1 ' 1· t _t _ - - --+ r-r w • t- - ~-+ + t.-t-++ ~ .,. ~ ...... · · t -~ .......
· · ·, •-•,
.... t
rl+f- -H-
~t--tl· .,~+t~tr-- t- ·t•r-1
--~--+ +tfl t: r; _f,_ t
+H '+ H--+ f_;,.;.. ~+...:-~_ -·_, -••-t-l
· •--- ~~+---t
~-''.......... __1..., •-
t.' '
'-~' t 1 ' - ~-t - t-f- .1-f j' -t I -~-f + t -4 0 • + • • ,__....._
.... -· ' .!j -'• t:-ft++ ~·-' ,. - i-t +f-+ -· :± •':_-±_ .n:j ·-·t· t. .... .. .n-
• . . . • . - ' 11''•
•-···t·•·· • ' ' I~- H -·-
• 'l' . 'c1·- ;t-t£·" -
~- -C
·- ~-'+ .- - •-~--m~-1-i- I I ~ •• ' l'!.f' .. • .......
' • • .•• '. 0
f •'
H-:.::.,_;~ + ' 't ' I
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..;. -it · !' •• -,j·,. I. .·r··• -
T , _ t Jr . LL !.~ '- ~..~ +
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~ •
t. - . H-r -q
-
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• t
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-
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1T'' L.l· t
'··' .···· ••• . , •I• r-4- H+- tt'· .I.J-fo 't-'f• I • -t ........ 1'tt ~., - r+r :-t 1·- t t Jj t•·· .,, •!•t --;-:-;,
., . . .:--;--;--~~
....... . ~ tT-"~'
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1 • • • r •
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t , ,. • t
•_-•~_!
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....,
i ~ •. .. r • 1 • • i'~~
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,,...,,t t·"- ·r ,.,,
• t • t , ;
[[-~-T. . '1'•1"''
, ~ • • • r [@.'' • ~ t
•-f1'1.- .,.-~l~···
t 1- -
. . • '-+ • • r H.,, -
r-~ · • •
.. , ! " ' I•· ....... . 1- •
,...,., r- 4 +- t ' 1 • • • • • • .. , •••
t . . . ·- • • • ; • • - t
• . . ' . . I ' . . 1 • l . I t • ,_ 1 I I I ' "I l: . l ; . i I I . It; r - 1-ft I 1. •·I 1 I' t lr
t +I•"r~~ L +-. ., f l J •- ' .. • I J• t ! r ' ... ' .. .. .. .. " . :
~..:.:.:,w_: ::.:: :.:.....tl.tful-':ITft··_;--=-t-:- :•.;: ::: -t+L- ;_~t~J-+.:. :~.- - ;,:.i ~-i-! .l:.i-h .r;_±_,- t±: lf. .:-::l.lt~-4-B- r..:..;_:.~-~~: ·:~ :.;..:._;_
...........
•r• ·••
j,,L,. r·r t+I t~ ••1' ,t,.
•·• ·-t•· .. -r- ~.,. •·
,, •tt·
·-1•· .r,
••• •
··;~T!:j.~:fi· N~~.;rcot'~FF· ~-t r- •r
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·-+ -
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r •• · ·-~· ., •• +- t-' ._
1
+-t • •• 1
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' ,. ~ 0 t ' ' ' I I ' t I < • j ~ t r• •~ 11 • • • j < t • I I f ! t 1 ~ 1
+ r ' '
I t • t t r I • t j.. t r-t t- ·· r t ' rt1_·
r-r ~ 1~q- t ...... t- t' t ~ I + I ·t· i :+- I j" ' ' I • ' ' • • t • • l •
, .•. ·~·· .... '~!· ·~~- ~~~· ·j·· •• ··_·· till:l't' .. ,. ~~.~· ~~ru·1 ··!+ ·+tl " .• , .• ,. I I · · • . • . •_ . . . . . . . . -·+!-: 1r·r ·r-··
tr~:J.:"r•: ·-·~o;.i ·t f· tt:i-:t t!;; :::::.::::::.
. :;; :.:: :;:; ;:.: ··&· :.;: :· 1-'ttH~:n·~n>}H~ t 1
+·:r,·r· l;::
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H -r- ~b I++ r " t-
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1' •' 'r •! ' 1• t-1
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Ljt ,.,! T' - - I' t' ,"'r t~ 1--,.
j: -II·
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• •·t·t· -t · ·-H- ~
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·
+Lt ttf~
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·t:·jr·•· ·n;:tW
+tt:- .' -. .. '
t
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'rt T•
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·tt'
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t~l· •t-+•
I . , • • • - ....... ~ , . . . .,,.:
. . . .!-···
. . .. .tr. .; .. KJ!-1
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tj·tr '1' ft1J t•j;·f-:tni 1
t ~~j·t·td•-Tt·" -tt•··t++•t ··;;· •-t•• ... , '''" ' ' "
Lt;! ~-·.: ; l: ~ r·i t t~-f.Lt- -lT~i ~ ~ ~. t: ;-;; ~ i-:; ~.
t"~-H~ ·-[i_, t-H-t -~-t~t-- -+ - --.--.
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L:.J..i_;_.
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f; h l -:-;--;--, '.!' . j •-t ,. +t- •.,_,.. ~n-:-' TT;. ' +-+- . . L ' . L LL
;.++-> i-+ H-i 4 -:::\+ -t I ·;· I L, l; • . . ;-:-:-:--- ' ' . - • ' ••••
'1;1-·· , ...._I·Ji' 1->·· ·-+•· , .•...••
·t·t··' 1'' ·~· +-it q: rt
+ t' ,.t ,_j_;.
~rtl ±t'ffli+t-t-t-r-r_' ,,. lfr- 1;1
rnr-r;~ ::;:J~'il :;~;:-::; .....
1;: .• 1:-.n:
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rt'r:t flrm-tt-!:t;::::-;t-rrrt.:•:tJ:-t.n
~ T.
I rl
•••·•!~·'·· '•i•-
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·'••t·c," 1I·. - ,,.~- -~ : ·r .- -·
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80.
t:-~·:rtt•tr. ,1 nt-~~~r~• r•j++" 7!,., '. ', ' ' I .. ' .
>- H-:1 •It•
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" :T .. " t.~-~~·-..-.-tLr.:_t-l-t
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.... ~1-.....;-,. ;.
~. ' c. 1-i
T·tl' •. ' "tt-- Hn=··t
·t t
1-r~lltf
J•-+-t-- -·
'lt11 -•- ·-tf •i~·~I t-t· t-t
i-r-ft -t-r I;., ' t·r•'-
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42
BIBLIOGRAPHY
7. 1
'Good Industrial Floors - Chemical Resistant Epoxy
Floor Toppings", Civil Engineering, August 1962,
p. 4 0.
43
VITA
Hong Kong.