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Whereas the Parliament of India has set out to provide a practical regime of right to
information for citizens to secure access to information under the control of public authorities,
in order to promote transparency and accountability in the working of every public authority,
and whereas the attached publication of the Bureau of Indian Standards is of particular interest
to the public, particularly disadvantaged communities and those engaged in the pursuit of
education and knowledge, the attached public safety standard is made available to promote the
timely dissemination of this information in an accurate manner to the public.

“जान1 का अ+धकार, जी1 का अ+धकार” “प0रा1 को छोड न' 5 तरफ”

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“The Right to Information, The Right to Live” “Step Out From the Old to the New”

IS 11802 (1986): Method of determination of diffusible

hydrogen content of deposited weld metal from covered
electrodes in welding mild and low alloy steels [MTD 11:
Welding General]

“!ान $ एक न' भारत का +नम-ण”

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“Invent a New India Using Knowledge”

“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता ह”

है”
ह
Bhartṛhari—Nītiśatakam
“Knowledge is such a treasure which cannot be stolen”
 1 3 JAN
.. fW9
IS : 11802 - 1988
((Reaffirmed
Reaffirmed1997)
2003 )

Indian Standard
METHODS FOR DETERMINATION OF
DIFFUSIBLE HYDROGEN CONTENT OF
DEPOSITED WELD METAL FROM COVERED
ELECTRODES IN WELDING MILD AND
LOW ALLOY STEELS
( First Reprint OCTOBER 1998 )

UDC 621.791.053 : 543 [ 546.11 ]

0 Copyright 1987
BUREAU OF INDIAN STANDARDS
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002

Gr 4 May 1987
 IS : 11802- 1986

Indian Standard

METHODS FOR DETERMINATION OF

DIFFUSIBLE HYDROGEN CONTENT OF
DEPOSITED WELD METAL FROM COVERED
ELECTRODES IN WELDING MILD AND
LOW ALLOY STEELS

Welding General Sectional Committee, SMDC 14

Choirmon Representing
SHRI D. S. HOWAVAR D & H Sechcron Electrodes Pvt Ltd, Indore
Members
SHRI S. R. JANA ( Alternate to
Shri D. S. Honavar )
SHRI R. S. AGGARWAL Association of Indian Engineering Industry, New
Delhi
SHRIJ. K. AHLTJWALIA Stewarts & Lloyds of India Ltd, Calcutta
SHRIT. K. BASU ( Alternote )
SHRI H. N. AHUJA Directorate General of Employment and Training,
New Delhi
DR S. BALASUBRAWNIAN Peico Electronics and Electricals Ltd. Bombay
DR S. BHATTACHARYYA ( Alternate )
SHRI K. BALUANOHAR Hindustan Shipyard Ltd, Vishakhapatnam
SHR~ R. V. KALE ( AIterncte )
SHRI R. BANERJFE Indian Oxygen itd, Calcutta
SHRI S. K. DAS (Alternate )
SHRI S. C. BHAWAL National Test House, Calcutta
SHRJ K. L. BARUX( Alternate )
SHRJ S. K. BUR!.IAN M. N. Dastur & Co Pvt Ltd, Calcutta
SHRI B. B. GHOSH ( Alternate )

( Continued on page 2 )

Q Copyright 1987
BUREAU OF INDIAN STANDARDS
This publication is protected under the Indian Copyright Act ( XJY of 1957 ) and
reproduction in whole or in part by any means except with written permission of the
publisher shall be deemed to be an infringement of copyright under the said Act.
IS :11802- 1986
(Continuedfrompage 1)
Members
SHRI R. S. CHOUDWRY
DEPUTY DIRECTOR( CHEMICAL )
RDSO, Lucknow
PRODUCTIONENQINE~R
INTEGRALCOACH*FACTORY,
MADRAS ( Alternate )
SHRI S. C. DEY
SHRI C. R. GHOSH
SHRI D. B. MOHARIL ( Alternate )
SHRI I. P. KAPOOR
SHRI L. M. TOLANI ( Alternate )
SHRI S. MAJUMDAR
SHRI S. K. BHATIA ( Alternate )
SHRI R. S. MALLICK
SHRI N. MUMMOORTHY
SHRI H. S. DUGGAL ( Alternate )
SHRI J. D. PANDA
SHRI RAJISDRA NATH I Alternate
SHRI S. L. V. RANGAN‘( Alternate
SHRI K. M. POLE
SHRI G. D. APTE ( Alternate )
DR S. PRASANNAKUUAR
SHRI J. K. NANDA ( Alternate )
SHRI J. R. PRASHER
SHRIN. RADHAKRISHNAN
SHRIB. RAMASWAMY
SHRI S. M. KADAM ( Alternote )
DR V. RAMA~WAMY
DR S. K. CH~UDHURY ( Alternate )
SHRI P. H. MADHAVA REDDY
SHRI M. G. NARAYANA RAO ( Alternate )
REPRESENTAIIVE
SHRI RAMESHKUMAR ( Alternate I )
SHRI V. SREEMANNARAYANA ( Alternate II )
REPRESENTATIVE
SHRI N. K. ROY
SHRI P. K. ROY ( Alternate )
SHRI S. K. ROY
SHRI B. K. SINQH
SHRI A. V. MULEY ( Alternate I )
SH~UP. S. JOSHI( Afternate II )
SHRI V. K. SRIDHAR
SHRI R. C. SHARMA ( Alternate )
Representing
Steel Authority of India Ltd (Bokaro Steel Plant ),
Bokaro Steel City
Ministry of Railways
Central Boilers Board, New Delhi
Mukand Iron & Steel Works Ltd, Bombay
Department of Atomic Energy, Bombay
Directorate General of Technical Development,
New Delhi
Gas Authority of India Ltd, New Delhi
Engineer-in-Chief’s Branch, Ministry of Defence
Dalmia Institute of Scientific & Industrial Rese-
arch, Rajgangpur
I 1
li 1
%&handnagar Industries, Walchandnagar
Larsen & Toubro Ltd, Bombay
Engineers India Ltd, New Delhi
Binny Ltd. Madras
Indian Hume Pipes Co Ltd, Pune
Steel Authority of India Ltd ( Research and
;rnl;ipment Centre for iron and Steel),
Bharat Heavy Plate and Vessels Ltd, Vishakha-
patnam
Bharat Heavy Electricals Ltd, Hyderabad
Jessop & Co Ltd. Calcutta
Projects & Development India Ltd, Dhanbad
Mini&y of Defence ( DGI )
Tata Engineering and Locomotive Co Ltd.
Jamstiedpur
Directorate General of Supplies and Disposals,
New Delhi
( Continued on page 13 )
2
 IS:11802-1986

Indian Standard
METHODS FOR DETERMINATION OF
DIFFUSIBLE-HYDROGEN CONTENT OF
DEPOSITED WELD METAL FROM COVERED
ELECTRODES IN WELDING MILD AND
LOW ALLOY STEELS

0. FOREWORD

0.1This Indian Standard was adopted by the Indian Standards Institution

on 14 August 1986, after the draft finalized by the Welding General Sec-
tional Committee had been approved by the Structural and Metals Division
Council.
0.2 This standard covers the methods for determination of diffusible
hydrogen of deposited weld metal by mercury and glycerin method. The
correlation of mercury and glycerin methods is given in Appendix A for
information.
0.3 In the preparation of this standard, assistance has been derived from
the following publications:
IS0 3690-1976 Welding - Determination of hydrogen in deposited weld
metal arising from the use of covered electrodes for welding mild and
low alloy steels. International Organization for Standardization.
BS 639 : 1976 Covered electrodes for the manual metal arc welding of
carbon and carbon manganese steels. British Standards Institution.
JIS : Z 3113- 1975 Method for measurement of hydrogen evolved from
deposited metal. Japanese Standards Association.
Rules and regulations for classification of ships - 1981. Lloyd’s Register
of Shipping, United Kingdom.

1.SCOPE
1.1 This standard covers the procedures for determination of content of
diffusible hydrogen in deposited weld metal arising from the use of shielded

3
IS:11802 - 1986

metal arc electrodes for welding mild and low alloy steels by mercury and
glycerin methods. For glycerin method, the values reported shall be in
terms of evaluation by mercury method using the formula given in
Appendix A. The glycerin method shall be used as a routine method. The
mercury method shall be used as a referee method in case of disputes, in
addition to being used as a routine method.

2. TERMINOLOGi’
2.1 For the purpose of this standard, the definitions given in IS : 812 - 1957*
shall apply.

3. PRINCIPLES OF MEASUREMENT
3.1 Mercury Method - The diffusible hydrogen content of the weld metal
sample is made to collect over mercury at room temperature for sufficient
time. The amount of hydrogen thus released is measured by volumetric
methods.
3.2 Glycerin Method - The diffusible hydrogen content is made to collect
over glycerin in a bath maintained at 45 ‘C for sufficient time. The amount
of hydrogen thus evolved is measured volumetrically.

4. MATERIALS REQUIRED FOR TEST

4.1 Parent Plate Material - The test assembly shall be prepared from steel
conforming to IS : 226-19751 or IS : 2002-1982~ or IS : 2062-1984s or
equivalent material.
4.2 Electrodes - The electrodes to be tested shall be of 4.0 mm core wire
diameter, or of 3.15 mm diameter in case of iron powder electrodes having
more than 130% metal recovery.
4.2.1 The electrodes shall be dried before testing as per recommendations
of the manufacturer. If no recommendation ii provided by the manu-
facturer, the electrodes shall be dried as per the schedule given below:

4 Hydrogen controlled electrodes - 250°C for two hours or 350°C for

one hour.
b) Other than hydrogen controNed electrodes - 125°C for 2 hours, ex-
cepting cellulosic electrodes.
4 Ceilulosic electrodes - no drying.

*Glossary of terms relating to welding and cutting of metals (first revision ).

tSpecification for structural steel ( standard quality ) (flfrh revision).
$Specification for steel plates for pressure vessels for intermadiate and low tempera-
ture service including boilers (firsr revision).
$Qxcification for weldable structural steel ( fhird revision ).

4
 IS:11802-1986

5. MERCURY METHOD
5.1 Apparatus - An audiometer type gas burette shown in Fig. 1 may be
used for the test. Burettes of other design my be employed provided that
the following criteria are fulfilled:
a) Mercury is used as the confining fluid.

/-- 69 SPHERICAL JOfNT

HIGH VACUUM HOLLOW KEY

SINGLE OBLIQUE STOP-COCK
+4 BORE

a
0 TO 10 ml BURETTE
GRADUATED TO 0.05 ml VACUUM
ABOUT 30 mm LENGTH
PER ml.OR 10 TO 11 00
5
HIGH VACUUM HOLLOW KEY
DOUBLE OBLIQUE STOPCOCK
6 ’
*L BORE

CONICAL JOlNf

120 STRAIGHT
- - SECTION --I
‘_A+-MERCURY

BOROSILICATE GLASS
THROUGHWT

All dimensions in millimetres.

FIG. 1 DIFFUSABLEHYDROGENMETER
IS :11802 - 1986

b) It is possible to maintain sample under vacuum for a brief period as

specified in 5.4.1 (d) to remove entrapped gases in the fractured
surface before the sample is subjected to vacuum in the measuring
burette. In burettes consisting of single limb, this may be achieved
through manipulation of mercury level and the stopcock: any gas
released during the brief period of surface degassing being swept out
of the burette before the measurements.
c) The value of collected gas is measured to an accuracy of at least 0.05
ml under normal temperature and pressure.

5.2 Welding Jig - A copper jig shown in Fig. 2 shall be used in preparing
the specimens.

SECTIONAA

All dimensions in millimetres.

FIG. 2 TEST PIECE ASSEMBLY FOR HYDROGEN SAMPLING

OF WELD DEPOSIT

6
 IS:11802 -1986

5.3 Preparation of Test Specimens

53.1 Triplicate sets of test pieces conforming to 4.1 and having a cross
section of 10 x 15 mm and length of 30 mm shall be used for each type of
electrode being tested. The test pieces shall be degassed at 650°C for one
hour and then kept in a desiccator in dry condition prior to use.
5.3.2 The test piece a’ssembly shown in Fig. 3 consists of run-on and
run-off pieces and a central sample section of 30 mm length. The 30 mm
centre portion shall have a length tolerance of & O-25 mm and shall be
weighed nearest to. IO mg before testing.

All dimensions in millimctres.

FIG. 3 SPECIMEN ASSEMBLY

5.3.3 Welding - The temperature of the ji,0 shall be 30 .-t 10°C before
testing. The welding current shall be 15 amperes less than the maximum
recommended by the manufacturer, the Fachine setting being controlled to
within -& 5 amperes. The speed of welding shall be adjusted to an elect-
rode consumption between 12 and 13 mm per IO mm of bead length. The
time spent on the deposition shall be noted.
5.3.4 A bead of 100 mm length shall be deposited along the centre-line
of each test assembly. No burning off of the tip of the electrode prior to
testing is allowed.
5.3.5 Three seconds after extinction of the arc, the jig shall be released
and the test piece assembly shall be quenched in iced water and subsequently
in alcohol or acetone saturated with carbon dioxide at a temperature
of - 50°C or below. The sample pieces shall be broken apart while cold,
using brief intermittent periods of cooling; the intervals spent outside the
cooling bath in these operations shall not exceed IO seconds each. The
samples may now be stored at or below -WC for a period upfo 3 days
before analysis.

7
IS :11802 - 1986

5.4 Test Procedure

5.4.1 Preparation of Sample for Analysis -When transferring the sample
to gas burette, a shield of dry nitrogen shall be applied to avoid condensa-
tion of atmospheric humidity. The sequence of operation and the time
spent in each shall be as follows:
The sample shall be washed in alcohol for a period of 3 to 5 seconds.
The sample shall be washed in pure ether for a period between 3 to
5 seconds. (
The sample shall be dried in a blast of dry nitrogen supplied from
a nozzle, particular attention being paid to the fractured surface of
the specimen. The operation shall be accomplished in not less than
20 seconds and not more than 22 seconds.
While maintaining a blanket of dry nitrogen, the sample shall be
transferred to the outer limb of the burette (audiometer) where the
sample shall be held in position clear of the mercury surface by a
magnet. The outer limb of the burette shall then be evacuated down
to a pressure of approx 13Pa ( 0.1 mm Hg). The time spent in these
operations shall be not less than, 20 seconds and not more than 25
seconds.
The sample shall then be transferred through mercury air Ioek fo its
final position in the measuring limb of the burette. This operation
shall be accomplished within 5 seconds.
The total time spent in transferring the sample until meaqurements
commence shall not exceed 60 seconds.
5.4.2 Analytical Procedure - The sample shall be maintained under
reduced pressure at 25 & 10°C for a period of 72 hours when the final
volume shall be measured. The barometric pressure as well as the precise
temperature shall be recorded. The sample shall be removed from the
apparatus and thoroughly brushed to remove any oxide skin and then
weighed to an accuracy of 10 mg.
5.5 Calcniation and Expression of Results - The volume VI, of diffusible
hydrogen per 100 g of deposited metal shall be calculated from the follow-
ing formula:

vh = v,(B - W 273 100

760’ (273 + TR) ’ (Mz - M,)
where
VI, = volume of diffusible hydrogen in ml per 100 g of deposited
metal at NTP ( 0°C and 760 mm Hg ),

8
 IS : 11802 - 1986

I’, = volume of gas in burette in ml after 72 11,

B = barometric pressure in mm Hg,
TR = room temperature in “C when Vs is measured,
H =Z head of mercury in mm at which I’:: is measured,
MZ z= mass of sample in g after removal from apparatus, and
M1 = mass of sample in g before deposition of weld.
For the purpose of this standard, the average value of results from three
determinations shall be used.

6. GLYCERIN METHOD

6.1 Apparatus - A typical apparatus using glycerin as confining fluid is

shown in Fig. 4. The set up consists of the following:
a) A thermostatically controlled water bath with circulation and heating
arrangements to maintain bath temperature at 45 i 1 ‘C,
b) Perforated stand made of metal which will allow free circulation of
bath fluid around the glycerine container, and
c) Glycerine container and measuring burette wilh inverted chamber
which conhnes the sample in a bath of glycerin. The burette is
graduated to an accuracy of 0.02 ml.

6.2 Preparation of Test Specimens

6.2.1 Test specimen measuring 12 x 25 mm in cross section and approxi-
mately 125 mm in length conforming to plate material given in 4.1 shall
be used. The specimens shall be free from rust. For each test, four specimens
shall be prepared and weighed to 0.1 g accuracy.

6.2.2 Welding
6.2.2.1 The size of electrodes used for Jeposition of weld bead and the
drying of electrodes shall be in accordance with 4.2.
6.2.2.2 The welding is carried out with a short arc. The welding current
shall be 15 amperes less than the maximum specified by the manufacturer.
No burn-off of the tip is allowed before the test.
6.2.2.3 On the 25 mm surface of each test specimen prepared as per
6.2.1, a single bead of weld measuring approximately 100 mm in length shall
be deposited.

9
IS:11802 - 1986

All dimensions in millimetres.

FIG. 4 APPARATUSFORHYDROGENDETERMINATION
BYGLYCERIN
METHOD
DISPLACEMENT

6.3 Test Procedure - Within 30 seconds of deposition of the bead, the slag
shall be removed and the sample quenched in iced water having a tempera-
ture not exceeding 5°C for a p,eriod of 30 seconds. Within 10 seconds
thereafter, the sample shall be cleaned and then placed in the glycerin bath
for collection of hydrogen by displacement of glycerin. The total time spent
from the completion of the welding till the transfer of the sample to the
glycerin bath shall not exceed 70 seconds. The glycerin bath shall be
maintained at 45 f 1°C during the test. All the four specimens shall be
welded and placed in the glycerin bath within 30 minutes.

10
 IS :11802 - 1986

6.3.1 Hydrogen Measurenzent - The sample shall be kept immersed in

glycerin for a period of 48 hours. They shall then be removed from the
apparatus and cleaned with water followed by methanol/acetone and weigh-
ed to nearest 0.1 g to determine the amount of weld metal deposited. The
amount of gas evolved is measured to the nearest 0.05 ml and corrected to
20°C and 760 mm of Hg.

6.4 Calculation and Exprekion of Test Results - The volume VI, of diffusi-
ble hydrogen per 100 g of deposited metal shall be calcualted from the
following formula:
B 293 100
vh = VP x -7T ’ (274 + T,:) ’ (M2@;)
where
vh = volume of diffusible hydrogen in ml per 100 g of deposited
metal at NTP ( 0°C and 760 mm Hg ),
V, - volume of gas evolved in burette in ml after4S 11,
B = barometric pressure in mm Hg,
TK = room temperature in “C when V, is measured,
M2 = mass of sample in g after removal from apparatus, and
M, = mass of sample in g before deposition of weld.

APPENDIX A
( Clauses 0.2and 1 .l )

CORRELATJON OF MERCURY AND GLYCERIN METHODS

A-l. As glycerin absorbs some amount of hydrogen evolved by the sample,

the results obtained by using this method tend to be somewhat lower. The
method is nonetheless is easy to operate and does not involve hazardous
chemicals such as mercury, which is a known toxic material and needs
careful handling. The glycerin method therefore lends easily to quality
control and routine inspection.

11
1s:11802 - 1986

A.;l.teNowing correlation between glycerin and mercury methods may

Vhc?= 0.64 Vm - 0.93

where
VW A hydrogk measured by glycerin method in ml per 100 g of
deposited weld metal, and
VIM = hydrogen measured’ by mercury method in ml per 100 g of
deposited weld metal.

12
 Is:11802-1986

( Continued from page 2 )

Members Representing
SHRIH. K. TAF: Indian Register of Shipping, Calcutta
SHRIS. CHAN~RA ( Ahernute )
SHRIJ R. UPADHY~Y Apar Pvt Ltd. Bombay
SWRIB. S. PATEL( Alternote )
SHIUP. S. VI~VANATH Advani-Oerlikon Ltd. Bombay
SHR~N. VIVANATHAN National Hydroelectric Power Corporation Ltd,
New Delhi
SHR~K. RAOHAV~NDRAN, Director General, BIS ( Ex-officio Member )
Director ( Strut & Met )

Secretary
SHRI S. S. SETHI
Joint Director ( Strut & Metals ), BLS

Subcommittee for Welding Consumables, SMDC 14 : 1

Convener
SHRI D. S. HONAVAR D & H !&heron Electrodes Pvt Ltd, Indore
Members
SHRIS. R. JANA( Alternate
to Shri D. S. Honavar )
SHRI R. S. AOOARWAL Modi Arc Electrodes Co, Modinagar
SHRI A. V. DESHPANDE
( Alternate )
SHRI AWTARSINOH Irrigation Works, Chandigarh
SHR~S. K. BASU Indian Oxygen Ltd. Calcutta
Sxar R. BANERJEB
( Alternate )
DR S. BHATACHARYYA Peico Electronics and Electricals Ltd, Bombay
DR S. BALASUBIUMANIAN ( Alternate )
C~errrsr AND METAL~u~OIST-II Ministry of Railways
RDSO, LLJCKNOW
ASSISTANT
RESEARCH
OFFICER
RDSO, LUCKNOW( Alternate )
SHR~V. H. HA~LANI Ministry of Defence ( DGI )
SHRIK. S. SOUNDAPPAN ( Alternate )
SARIR. M. JAIN Special Machines, Karnal
SHRI A. K. GUPTA( Alternute )
SHIUS. KRISHNAMURTHY ACC Babcock Ltd. Durgapur
SHRI PREMKRISHNA( Alternute)
SXIU M. NAGESHWARARAO Mirhra Dhatu Nigam Ltd. Hyderabad
SARI VIWK S. MAYADEo ( Alternate )
SHRI K. NA~ASIMHAN Bharat Heavy Electricals Ltd. Hyderabad
SHRI RAMESHKUMAR ( Alternate I )
Smu V. SREEMANNARAYANA
( Alternate II )’

( Continued on page 12 t

13
IS:11802 - 1986

‘wdlers Representing
StmI ANIL PANDYA SteelB;;;hc$ty of India Ltd ( Bokaro Steel Plant ),

SHRI J. R. PRASHER Engineers India Ltd, New Delhi

SHRI M. R. C. NAGZRZJ.\N ( Alrernate)
~~_PXI.SENTATIVf. , Bharat Heavy Plate and Vessels Ltd, Vishakha-

IZ~PRJ~ESTAIIW PowgaEz$cts Division, BARC, Bombay

RF PRESESATIVE Dalmia Institute of Scientific and Industrial
Research, Rajgangpur
SIIRIJ. R. UPAOHYAY Apar Pvt Ltd. Vadodara
SCiRlP. S.VIsV4NATII Advani-Oerlikon Ltd, Bombay
SHKI M. P. DHA~UKA ( Alternate )

14
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