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Spectroquant® Prove
Spectroquant® Prove
Spectrophotometer 100 ● 300 ● 600
Contents 1 Safety
1 1
1 Safety......................................................................... 3 This Quick Guide contains basic instructions
that you must follow during the commissioning,
Safety instructions
Safety instructions in this operating manual are
1.1 Intended use............................................................................................................ 3
operation and maintenance of the spectropho- indicated by the warning symbol (triangle) in the
2 Overview.................................................................... 4 tometer. Consequently, all responsible person- left margin. The signal word (such as "CAUTION")
2.1 Scope of delivery...................................................................................................... 4 nel must read this Quick Guide carefully before indicates the danger level.
2.2 Overview of the instrument........................................................................................ 4 working with the meter. Keep this Quick Guide in The following warning symbols are used:
2.3 Display and user interface.......................................................................................... 5 the vicinity of the meter.
4 Operation.................................................................. 15 on, which may cause damage to the eyes. Never look directly in the radiation of this light
source without wearing proper eye protection. Protect your skin from the direct exposure
4.1 Switching the spectrophotometer on or off................................................................. 15 to UV light.
4.2 System setup ........................................................................................................ 17
WARNING
4.3 Zero adjustment for preprogrammed m ethods............................................................ 18
Dangerous electrical voltage.
4.3.1 Notes on zero adjustment ............................................................................... 19
4.3.2 When to repeat the zero adjustment? .............................................................. 19
3 4.4 Measurements........................................................................................................ 20 3
WARNING
4.4.1 Performing a measurement.............................................................................. 21 WARNING
Signifies instructions that must be followed precisely in order to prevent serious dangers
5 Appendix.................................................................. 23 to personnel.
NOTE NOTE
Signifies a notice drawing your attention to special characteristics.
4 REFERENCE 4
Used to indicate references to other documents.
1 2.1 Scope of Delivery 2.2 Overview of the Instrument 2.3 Display and User Interface
1
• Spectrophotometer Packaging
• Power adapter The spectrophotometer is shipped in protective NOTE
5 6 7 8
• Power connectors (3 pieces) transport packaging. The entire display is touch-sensitive. Make selec-
• Dust cover tions using a f ingertip or special touch pen. Do
• Zero cell CAUTION not touch the display with sharp objects (e.g. the
• Quick Guide (A4 format) Retain the original packaging including the inner tip of a ballpoint pen).
• Safety instructions packaging to p rotect the instrument against hard
• Certificate of final inspection knocks if it has to be transported. Please note
that damage caused by improper transport voids • Do not place objects on the display, as doing
all w
arranty claims. so may scratch it
2 • Touch buttons, words or symbols to select 2
them
Front of the instrument • Scrollbars are provided to assist quick move-
ment through long lists
1 Display and user 2 Flip-up cover Ports at the rear of the instrument • Touch the arrow in the scrollbar to scroll up-
interface 5 Socket for plug-in power supply unit wards or downwards through the list
6 LAN port • Following selection, the item is activated im-
7 USB Mini B port mediately
8 USB-A ports • Touching a main button outlines it in blue
• Selecting an item inverts it (with dark text be-
NOTE ing shown on a light background)
• Selecting a text inverts it (with dark text
3 All connections comply with SELV.
being shown on a light background), e.g. 3
method-specific settings for concentration
mode "Show Absorbance"
• "0" is OFF, "I" is ON – the active selection is
displayed light grey with dark figure, in this
case the Show Absorbance is ON
4 4
2
2 Methods System 2
Settings Setup
Ad hoc Login/Log-
out
AQA Timer
The main menu "Methods" comprises two main overview panels arranged as shown below:
the Concentration Measurement Overview and the Method List Overview.
3 3
Screen layout concentration measurement overview
2 Alerts
Normal
Remains static
7 Action
Active fields are always shown in bright color. buttons
11 Main
Pressed fields invert the color as long as the menu
chosen action is performed. selection
button: 10 Brief
infor- 9 Notification symbols/ 8 Info bar with
Disabled Switch be- mation settings Information
5 Draws 30 % of the normal state tween the button 5
two main
Inactive, disabled fields show faint color. menu
overviews
2
2 For performing measurements (absorbance/transmission, spectrum, kinetics)
Allows measurements to be performed without the need to create methods
2
Absorbance/Transmission Mode
Ad hoc submenu: perform absorbance or transmission measurements
6 Name of
Spectrum Mode
method 5 Scrollbar Ad hoc submenu: record spectrum
Method list: create methods -> Spectrum Mode
Kinetic Mode
Ad hoc submenu: perform kinetic measurement
Method list: create methods -> Kinetic Mode
AQA
3 Overview and list of all Analytical Quality Assurance (AQA) modes 3
AQA Status 1&2
AQA submenus: Status display of the period of validity and the outcome (passed/failed)
AQA1
AQA submenu: List of AQA1 methods
AQA2
AQA submenu: List of AQA2 methods
4 Pipette check
AQA submenu: List of pipette-checking methods
4
Result list
List of all stored results
System setup
This button is for optional instrument settings (e.g. date, time, updates etc.)
Login/logout
Log users in and out
5 Timer list 5
List of stopwatch functions
1 Overview of action & selection buttons 3.1 General Notes on Handling 3.2 Initial Setup
1
The Spectroquant® Prove spectrophotometer is Proceed as follows:
Action & Selection an optical precision instrument. It should always • Connect the power adapter (see section 3.2.1)
Description • Switch on the spectrophotometer (see section
Buttons be handled with care, especially when in mobile
Start button use. Always protect the instrument from condi- 3.2.2)
Start an action (e.g. measurement) tions that could damage the mechanical, optical • Set the language (see section 3.2.3)
and electrical components. Please note the fol- • Set the date and time (see section 3.2.4)
Start zero lowing in particular: • Run the self-test (see section 3.2.5)
Start zero adjustment for a method • The temperature and humidity during opera-
tion and storage must be within the limits
Apply specified in the "Technical Data" section (see NOTE
2
2 the Operating Manual) For our Operating Manual please visit: 2
The instrument must never be exposed to www.sigmaaldrich.com/spectroquant
Save the following: For more information about the technical videos
• Extreme dust, humidity and moisture please visit:
• Intense light and heat www.sigmaaldrich.com/photometry
Stop • Fumes that are corrosive or contain high con-
centrations of solvents
In addition take care of the following:
• For measuring, the instrument must be placed
3.2.1 Connecting the Power Supply
Close
on a flat surface Power is supplied through the power adapter
• Spilled liquid or other material should be re- provided. The power adapter supplies the spec-
Logout moved immediately (see the Operating trophotometer with the required voltage and
3 User logout Manual) type of current (24 V DC). 3
• If a cell has broken in the cell holder, the cell
Search method holder should be cleaned immediately (see the CAUTION
Operating Manual) The line voltage at the user location must fulfil
• The cover should always be closed when the the specifications stated on the power adapter
Search/results list spectrophotometer is not in use (the specifications are also indicated in the Op-
Search function, search criterion: method name, method number or item number • When the spectrophotometer is being trans- erating Manual). Only ever use the 24 V power
ported, the cell compartment must be empty adapter provided. Please note that damage
Filter cancellation button
caused by using a different power adapter than
Cancel all set filter options
the one supplied voids all warranty claims.
Edit
4 For editing parameters 4
Create method
Print
Print to pdf (USB device) or printer
Export button
All selected results are exported to an external memory device as .csv file
Import button
5 Updates/Methods are imported from an external memory device into the instru- 5
ment
Delete
The selected items are deleted
1 3.2.2 First Power-on 3.2.3 Language Setup 3.2.4 Date, Time and Country-specific
1
After switching on the spectrophotometer for the The software supports several languages. When Settings
first time you are automatically guided through you switch on the spectrophotometer for the During initial setup, having set the language op-
the language, date and time setup procedures. first time, a list of language options is automati- tion you are a utomatically guided through the
cally displayed after the boot procedure. date and time setup procedure.
1
1
2 1
2
5 5
1
8 5
10
9
2 2
7
1
5. Tap on the Time format button 5 . The nu-
meric key panel 6 pops up. Now you can
Switching on
enter the time. 2
1. Remove all cells and close the cell compart- 1. Press the ON/OFF button 1 . The spectro-
6. Tap on OK 7 to confirm.
ment cover. photometer gives an audible signal (beep)
7. Tap on the Arrow button 8 to choose the
2. Start the self-test with the Start button 1 . and starts booting for approximately 2 min-
country-specific basic time setting. The time
3. The spectrophotometer performs the self- utes. You will see the following display: 4. Start the self-test with the Start button 2 .
format can be set and displayed for EU and
US. test. 5. The spectrophotometer performs the self-
8. Tap on the Arrow button 9 to choose the test.
3
3 decimal separator "."/"," used in your coun- Self-test 3
try. The self-test covers: Self-test
9. Tap on the Save button 10 to confirm. • Checks on memory, processor, internal inter- The self-test covers:
faces, filter and lamp • Checks on memory, processor, internal inter-
• A calibration of the wavelength faces, filter and lamp
• A calibration of the wavelength
When the self-test has ended, the display shows
the main menu. When the self-test has ended, the display shows
the main menu.
5 5
1 1
4.2 System Setup
Energy-saving mode – display Switching off General instrument setup is carried
Press the ON/OFF button 4 to switch the spectro- out in the "System" menu.
photometer off.
4
2 2
Buttons Description
Information
This submenu displays the following information about the device:
Software/method versions, device class, lamp counter and serial number
NOTE
The instrument has an Auto-Power-Off function, Interface
The spectrophotometer automatically switches which switches it automatically off after a user- This submenu displays the following settings options and standard settings:
off the backlight of the display 3 when no but- defined time. This function is not active out of
Audible signals – ON, Backlight – 100 %, Print to pdf – ON
3 ton has been tapped within a period of 10 min- the box, but you can turn it on in "System (In- 3
utes. The backlight is switched on again with the strument settings)". Region
next tap. This submenu displays the following settings options and standard settings:
The button functions are activated only following Language, date, time and country zone EU/US, decimal separator – "."/"," (dot or comma)
a further tap.
Quality
This submenu displays the following settings options and standard settings:
NOTE Quick zero – OFF, AQA1 and AQA2 lock – OFF, Zero Adjustment expiry – ON (interval:
You can set a user-defined time for this function 7 days), Use expired reagents – OFF, Service reminder – ON
(please see the Operating Manual for detailed in-
Automation (Setup 4)
structions). This submenu displays the following settings options and standard settings:
4
4 Energy saving mode – ON (10 minutes), Auto Power off – OFF, Auto log off – OFF,
Auto store – ON, Auto print – OFF, Sample ID popup – OFF 4
User management
This submenu displays the following settings options and standard settings:
Activation of user management and administrator settings, User login required – OFF
Service
This submenu displays the following settings options:
Various service functions such as backup, restore, export of log or system data and
import of methods
Update
This submenu displays the option for performing software and method updates
5 5
5
7
1
1 5.1 Certificates
1
Measuring with rectangular cells with open Measuring with rectangular cells with open
lid: lid:
Insert rectangular cells (10, 20, 50 mm) Insert 100 mm rectangular cells (Prove 600)
2 2
10
3 3
11
adjusted or repaired by specialist personnel Empty cells 16 mm ∅ (1 pack = 25 pcs) with screw cap 1.14724.0001
authorized by the manufacturer. Noncompliance
Zero Cell (1 pack = 1 pc) 1.73503.0001
invalidates any warranty claims.
Rectangular cell 100 mm 1.74011.0001
Keep the original packing including the inner Prove Connect to LIMS Unlimited License Y110860001
packing to protect the instrument against hard
shocks if it has to be shipped. Note that damage
caused by improper transport voids all warranty
claims.
4 4
5
5 5
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Distributed by EMD Millipore Corporation, 400 Summit Drive, Burlington MA 01803, USA
Sigma-Aldrich Canada Co. or Millipore (Canada) Ltd., 2149 Winston Park, Dr. Oakville, Ontario, L6H 6J8
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Detailed information on trademarks is available via publicly accessible resources.
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