Report Quality Biodiesel Plant (Sept, 2021)

PT LOUIS DREYFUS COMPANY LAMPUNG
DAILY ANALYSIS BIODIESEL REPORT
Date 1-Sep-21
Time
No Materials Sampling Point Parameters Unit Control Limit Average Remark
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.094 0.094 0.092 0.089 0.079 0.079 0.088
Moisture % ≤ 0.1 0.025 0.026 0.027 0.026 0.025 0.025 0.026

1 Feed (RBDPO) 180E1 inlet
IV % ≥ 47 51.75 51.51 51.66 51.63 51.45 51.52 51.59
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4034 3964 4316 4237 4386 4425 4167 4306 4127 4209 4359 4268 4233
2 1st Washed FAME 163S2 LP Methanol % 1.2 Max 0.69 0.69
Soap ppm 500 Max 150 162 143 151 146 140 149 160 127 143 139 140 146
Water ppm ≤ 3000 2424 2562 2859 2664 3000 2913 3152 3016 3170 3146 3049 2976 2911
3 2nd Washed FAME 163S20 LP Methanol % 1.2 Max 0.32 0.32
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.69 857.77 857.76 857.74
Density (15 deg C) g/l 860 -900 875.29 875.36 875.40 875.35
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.51 4.52
CFPP oC 15 Max 12.8 12.8 12.8 12.8 12.6 12.6 12.7
Cloud Point oC 18 Max 15.8 15.8 15.8 15.8 15.6 15.6 15.7
Acid Value mgKOH/g ≤ 0.40 0.056 0.067 0.064 0.062 0.064 0.065 0.065 0.063 0.053 0.056 0.058 0.055 0.061
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.7 98.7 98.7 98.7
Methanol % ≤ 0.2 0.010 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 94 90 88 91 93 94 90 89 96 92 98 92 92
Total Contaminated mg / kg ≤ 24 12 12 12 12 11 12 12
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.56 0.57 0.57 0.56 0.56 0.56 0.56
Di Glyceride % ≤ 0.2 0.07 0.06 0.05 0.06 0.05 0.05 0.06
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.01 0.01 0.02 0.01
Total Glycerol % ≤ 0.25 0.158 0.160 0.159 0.158 0.156 0.157 0.158
IV % ≥ 47 min 51.68 51.58 51.46 51.57
Moisture % 2 Max 1.26 1.52 1.29 1.41 1.91 2.16 1.59

5 Fatty Matter 166P4
FFA % 5 Min 19.89 21.80 20.63 21.17 18.47 16.29 19.71
Gly Content % 84 min 85.04 84.90 84.85 84.93
pH % Neutral 5.86 5.86 5.77 6.00 5.98 6.04 5.92
MONG % 3 max 1.82 1.85 1.78 1.82

6 Crude Glycerine 166E3
Salt % 10 max 4.23 4.20 4.22 4.25 4.14 4.19 4.21
Ash % 7 max 4.14 4.17 4.09 4.13
Water % 9.5 max 9.00 9.02 9.08 9.13 9.28 9.31 9.14
7 Recovery Methanol 160E2 Moisture ppm 1000 max 761 625 118 208 314 697 454
Analyst Eko Setyono Analyst Asariyanto Analyst : : Angga Renata
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Dose of Catalyst 1.543% | Pukul 14:30 1.546% Dose of Catalyst : 1.550% Dose of Catalyst : 1.550%
Dose of Methanol 10.70% Dose of Methanol : 10.70% Dose of Methanol : 10.70%
Source of Feeding 106 Source of Feeding : 106 Refinery Source of Feeding : 106 Refinery
Storage Tank PME H2 Storage Tank PME : H2 Storage Tank PME : H2
Date 2-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.084 0.097 0.102 0.098 0.090 0.090 0.094
Moisture % ≤ 0.1 0.026 0.026 0.026 0.026 0.027 0.025 0.026

IV % ≥ 47 51.38 50.35 50.46 50.50 50.59 50.51 50.63
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4036 3957 3855 4066 3985 4241 4316 4187 3904 4312 4102 4201 4097
Soap ppm 500 Max 129 120 114 125 127 147 138 142 162 170 184 176 145
Water ppm ≤ 3000 2461 2704 2970 2880 3216 3274 2982 2468 2377 2784 2532 2630 2773
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.71 857.74 857.70 857.72
Density (15 deg C) g/l 860 -900 875.31 875.33 875.36 875.33
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52
CFPP oC 15 Max 12.6 12.6 12.6 12.6 12.8 12.6
Cloud Point oC 18 Max 15.6 15.6 15.6 15.6 15.8 15.6
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.7 98.8 98.8 98.8
Methanol % ≤ 0.2 0.010 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 95 90 86 87 88 93 90 94 84 90 92 98 91
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.53 0.52 0.50 0.51 0.52 0.52 0.52
Di Glyceride % ≤ 0.2 0.04 0.04 0.04 0.05 0.05 0.04 0.04
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.02 0.02 0.01 0.01
Total Glycerol % ≤ 0.25 0.148 0.147 0.139 0.144 0.146 0.145 0.145
IV % ≥ 47 min 51.21 50.37 50.42 50.67
Moisture % 2 Max 1.91 1.54 1.21 1.36 2.05 1.98 1.68

FFA % 5 Min 19.28 23.25 25.95 25.72 21.84 21.86 22.98
Gly Content % 84 min 84.94 84.93 84.80 84.89
pH % Neutral 6.02 6.02 6.13 6.15 6.10 6.12 6.09
MONG % 3 max 1.78 1.74 1.71 1.74

Salt % 10 max 4.24 4.27 4.25 4.20 4.15 4.16 4.21
Ash % 7 max 4.12 4.16 4.11 4.13
Water % 9.5 max 9.16 9.11 9.17 9.13 9.38 9.08 9.17
Analyst Eko Setyono Analyst Analyst : : M YUSUF
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Dose of Catalyst 1.556% Dose of Catalyst : 1.556% Dose of Catalyst : 1.556%
Source of Feeding H3 Source of Feeding : H3 Source of Feeding : H3
Date 3-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.087 0.088 0.089 0.083 0.082 0.086 0.086
Moisture % ≤ 0.1 0.026 0.026 0.025 0.025 0.026 0.027 0.026

IV % ≥ 47 51.47 51.48 51.70 51.73 51.76 51.80 51.66
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 3871 3925 4032 3934 4026 3976 4413 4618 4528 4677 4512 4420 4244
Soap ppm 500 Max 152 133 127 138 131 140 147 148 151 155 158 160 145
Water ppm ≤ 3000 2657 2802 2792 2825 2831 2775 2556 2672 2513 2683 2512 2632 2688
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.70 857.64 857.66 857.67
Density (15 deg C) g/l 860 -900 875.30 875.24 875.30 875.28
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52
CFPP oC 15 Max 12.7 12.6 12.5 12.6 12.5 12.6 12.6
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.7 98.7 98.7 98.7
Methanol % ≤ 0.2 0.010 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 95 97 94 91 88 90 90 95 100 98 97 85 93
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.53 0.52 0.52 0.51 0.51 0.51 0.52
Di Glyceride % ≤ 0.2 0.04 0.05 0.04 0.05 0.04 0.05 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.147 0.146 0.145 0.143 0.142 0.145 0.145
IV % ≥ 47 min 51.40 51.48 51.70 51.53
Moisture % 2 Max 1.99 1.84 1.77 1.28 1.88 1.86 1.77

FFA % 5 Min 26.34 28.24 26.64 29.73 28.76 27.12 27.81
Gly Content % 84 min 84.91 84.93 84.76 84.87
pH % Neutral 5.88 5.91 6.12 6.12 6.10 6.12 6.04
MONG % 3 max 1.78 1.80 1.82 1.80

Salt % 10 max 4.30 4.26 4.25 4.25 4.28 4.15 4.25
Ash % 7 max 4.15 4.12 4.10 4.12
Water % 9.5 max 9.16 9.11 9.15 9.10 9.32 9.30 9.19
Analyst Eko Setyono Analyst Angga Analyst : : M YUSUF
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Source of Feeding 106 Source of Feeding : 106 Source of Feeding : 106
Date 4-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.088 0.084 0.087 0.087 0.089 0.088 0.087
Moisture % ≤ 0.1 0.027 0.026 0.025 0.025 0.027 0.026 0.026

IV % ≥ 47 51.66 51.57 51.58 51.32 51.42 51.46 51.50
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4413 4507 4310 4264 4079 4113 4612 4536 4640 4512 4672 4710 4447
Soap ppm 500 Max 154 164 146 152 171 155 160 158 163 150 155 154 157
Water ppm ≤ 3000 2481 2506 2976 2508 2677 2567 2765 2812 2732 2810 2613 2723 2681
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.68 857.70 857.68 857.69
Density (15 deg C) g/l 860 -900 875.33 875.40 875.33 875.35
Viscosity mm2/s 3.5 - 5.0 4.51 4.52 4.52 4.52
CFPP oC 15 Max 12.6 12.8 12.6 12.6 12.6 12.5 12.6
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.8 98.8 98.8
Methanol % ≤ 0.2 0.010 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 92 93 88 94 96 91 90 98 97 93 90 100 94
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.51 0.50 0.51 0.51 0.52 0.52 0.51
Di Glyceride % ≤ 0.2 0.05 0.05 0.05 0.05 0.05 0.04 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.145 0.141 0.145 0.145 0.147 0.144 0.145
IV % ≥ 47 min 51.58 51.52 51.32 51.47
Moisture % 2 Max 1.28 1.38 1.55 1.52 1.64 1.72 1.52

FFA % 5 Min 20.74 21.16 18.92 18.70 17.64 18.21 19.23
Gly Content % 84 min 84.87 84.88 84.92 84.89
pH % Neutral 6.10 6.03 6.00 6.14 6.14 6.10 6.09
MONG % 3 max 1.80 1.73 1.81 1.78

Salt % 10 max 4.18 4.16 4.19 4.20 4.21 4.25 4.20
Ash % 7 max 4.09 4.12 4.17 4.13
Water % 9.5 max 9.24 9.32 9.27 9.02 9.10 9.21 9.19
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Source of Feeding 106 Source of Feeding : H3 Source of Feeding : H3
Date 4-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.089 0.094 0.113 0.118 0.115 0.117 0.108
Moisture % ≤ 0.1 0.026 0.027 0.027 0.028 0.026 0.026 0.027

IV % ≥ 47 51.48 50.87 46.88 46.72 46.90 46.84 48.28
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4170 4727 4297 4374 4354 4423 4555 4491 4113 4251 4288 3861 4325
Soap ppm 500 Max 171 160 156 137 166 169 153 147 152 158 169 155 158
Water ppm ≤ 3000 2367 3023 2801 2862 2815 2937 3298 2867 2601 2739 2807 2874 2833
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.73 857.55 857.35 857.54
Density (15 deg C) g/l 860 -900 875.32 875.15 874.95 875.14
Viscosity mm2/s 3.5 - 5.0 4.52 4.51 4.51 4.51
CFPP oC 15 Max 12.6 12.8 13.4 13.6 13.8 13.8 13.3
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.7 98.7 98.7 98.7
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 93 90 92 93 90 86 89 94 91 93 96 92 92
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.51 0.52 0.52 0.54 0.55 0.53 0.53
Di Glyceride % ≤ 0.2 0.04 0.06 0.05 0.06 0.05 0.06 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.142 0.147 0.146 0.152 0.154 0.150 0.149
IV % ≥ 47 min 51.32 50.11 46.77 49.40
Moisture % 2 Max 1.28 1.37 1.28 1.76 1.84 1.79 1.55

FFA % 5 Min 25.41 26.35 26.82 26.22 21.41 21.33 24.59
Gly Content % 84 min 84.90 84.86 84.85 84.87
pH % Neutral 6.06 6.04 5.98 6.09 6.12 6.07 6.06
MONG % 3 max 1.82 1.80 1.76 1.79

Salt % 10 max 4.22 4.24 4.25 4.20 4.22 4.19 4.22
Ash % 7 max 4.10 4.14 4.14 4.13
Water % 9.5 max 9.18 9.15 9.20 9.18 9.25 9.31 9.21
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Source of Feeding 106 Source of Feeding : 106 Source of Feeding : 106
Date 6-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.116 0.115 0.118 0.117 0.118 0.115 0.117
Moisture % ≤ 0.1 0.026 0.025 0.027 0.028 0.028 0.026 0.027

IV % ≥ 47 46.81 46.80 46.88 46.83 46.85 46.81 46.83
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4186 4986 4554 4618 4254 4312 2443 4421 3897 4124 4176 4017 4166
Soap ppm 500 Max 140 208 189 193 144 150 168 170 177 55 169 165 161
Water ppm ≤ 3000 2764 2955 3529 3210 3064 3092 3252 3157 2790 2817 2902 2885 3035
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.32 857.35 857.34
Density (15 deg C) g/l 860 -900 874.92 874.90 874.91
Viscosity mm2/s 3.5 - 5.0 4.51 4.51 4.50 4.51
CFPP oC 15 Max 13.8 13.8 13.6 13.7 13.6 13.8 13.7
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.7 98.7 98.7
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 92 95 89 91 84 90 99 96 99 94 91 95 93
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.53 0.54 0.55 0.55 0.55 0.54 0.54
Di Glyceride % ≤ 0.2 0.05 0.05 0.05 0.05 0.06 0.05 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.02 0.02 0.04 0.02
Total Glycerol % ≤ 0.25 0.148 0.150 0.152 0.155 0.156 0.155 0.153
IV % ≥ 47 min 46.78 46.80 46.88 46.82
Moisture % 2 Max 1.33 1.19 1.12 1.86 1.44 1.61 1.43

FFA % 5 Min 21.74 22.80 19.61 17.04 18.27 17.64 19.52
Gly Content % 84 min 84.80 84.88 84.85 84.84
pH % Neutral 6.03 6.01 6.08 6.00 6.04 6.01 6.03
MONG % 3 max 1.76 1.80 1.81 1.79

Salt % 10 max 4.23 4.24 4.28 4.25 4.24 4.21 4.24
Ash % 7 max 4.16 4.10 4.13 4.13
Water % 9.5 max 9.28 9.10 9.22 9.14 9.21 9.29 9.21
Analyst YUSUF Analyst Angga Analyst : : Asariyanto
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Source of Feeding G1 Source of Feeding : G1 Source of Feeding : G1
Date 7-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.117 0.118 0.117 0.118 0.120 0.123 0.119
Moisture % ≤ 0.1 0.026 0.027 0.025 0.028 0.027 0.027 0.027

IV % ≥ 47 46.84 46.80 46.81 46.75 46.80 46.84 46.81
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4316 4284 4877 4610 4912 4792 4683 4507 4371 4487 4151 4391 4532
Soap ppm 500 Max 158 160 158 168 171 153 156 161 152 160 147 145 157
Water ppm ≤ 3000 2872 2811 2987 2874 2700 2684 2379 2475 2581 2617 3084 3112 2765
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.32 857.32 857.3 857.31
Density (15 deg C) g/l 860 -900 874.92 874.92 874.9 874.91
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.51 4.52
CFPP oC 15 Max 14.0 14.0 14.0 13.8 14.0 14.0 14.0
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.7 98.7 98.7 98.7
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 92 92 97 90 90 93 97 95 96 92 94 99 94
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.55 0.55 0.56 0.57 0.57 0.55 0.56
Di Glyceride % ≤ 0.2 0.06 0.06 0.06 0.06 0.06 0.05 0.06
Tri Glyceride % ≤ 0.2 0.02 0.02 0.03 0.03 0.05 0.01 0.03
Total Glycerol % ≤ 0.25 0.156 0.156 0.160 0.162 0.164 0.154 0.159
IV % ≥ 47 min 46.70 46.72 46.65 46.69
Moisture % 2 Max 1.28 1.48 1.04 1.14 1.22 1.51 1.28

FFA % 5 Min 17.68 18.10 18.14 23.78 21.67 19.82 19.87
Gly Content % 84 min 84.80 84.99 84.88 84.89
pH % Neutral 6.02 6.03 6.05 6.03 6.04 6.01 6.03
MONG % 3 max 1.78 1.74 1.79 1.77

Salt % 10 max 4.25 4.25 4.23 4.26 4.24 4.21 4.24
Ash % 7 max 4.11 4.22 4.13 4.15
Water % 9.5 max 9.31 9.27 9.05 9.14 9.20 9.29 9.21
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Date 8-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.120 0.125 0.121 0.123 0.116 0.104 0.118
Moisture % ≤ 0.1 0.025 0.025 0.027 0.026 0.027 0.027 0.026

IV % ≥ 47 46.80 46.78 46.72 46.77 46.81 50.46 47.39
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4139 4316 4412 4564 4613 4731 4163 4309 4913 4688 4421 4461 4478
Soap ppm 500 Max 178 168 153 155 161 150 169 166 185 186 188 159 168
Water ppm ≤ 3000 2689 2710 2684 2731 2688 2710 2589 2881 3422 3209 3099 3027 2870
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.40 857.38 857.39
Density (15 deg C) g/l 860 -900 875.00 875.02 875.01
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52
CFPP oC 15 Max 14.0 14.0 14.2 14.2 14.2 14.0 14.1
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.7 98.7 98.7
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 95 98 93 96 84 97 99 90 97 94 97 95 95
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.53 0.52 0.53 0.53 0.55 0.54 0.53
Di Glyceride % ≤ 0.2 0.05 0.05 0.06 0.05 0.05 0.05 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.02 0.01 0.02 0.01 0.01
Total Glycerol % ≤ 0.25 0.148 0.146 0.152 0.150 0.155 0.153 0.151
IV % ≥ 47 min 46.70 46.62 46.79 46.70
Moisture % 2 Max 1.31 1.74 1.68 2.15 1.86 1.72 1.74

FFA % 5 Min 21.21 20.28 21.68 20.86 20.55 21.13 20.95
Gly Content % 84 min 84.92 84.78 84.62 84.77
pH % Neutral 6.05 6.12 6.10 6.01 6.00 6.01 6.05
MONG % 3 max 1.78 1.82 1.83 1.81

Salt % 10 max 4.21 4.21 4.28 4.24 4.27 4.28 4.25
Ash % 7 max 4.11 4.15 4.18 4.15
Water % 9.5 max 9.19 9.02 9.25 9.32 9.37 9.11 9.21
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Source of Feeding G1 Source of Feeding : G1 Source of Feeding : H3
Date 9-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.092 0.099 0.098 0.096 0.103 0.096 0.097
Moisture % ≤ 0.1 0.026 0.026 0.025 0.027 0.026 0.026 0.026

IV % ≥ 47 51.03 51.89 51.84 51.85 52.08 51.46 51.69
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4517 4482 4359 4336 4632 4594 4613 4718 4716 4692 4417 4325 4533
Soap ppm 500 Max 160 155 142 167 160 158 160 155 181 170 175 186 164
Water ppm ≤ 3000 2948 2924 3002 2892 3084 3024 2976 2992 2838 2907 2957 2882 2952
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.46 857.44 857.84 857.58
Density (15 deg C) g/l 860 -900 875.06 875.10 875.44 875.20
Viscosity mm2/s 3.5 - 5.0 4.51 4.51 4.50 4.51
CFPP oC 15 Max 13.6 13.4 13.4 13.5 12.8 13.0 13.3
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.8 98.8 98.8
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 92 90 95 88 94 91 88 90 95 92 90 94 92
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.54 0.53 0.52 0.52 0.51 0.5 0.52
Di Glyceride % ≤ 0.2 0.05 0.05 0.05 0.06 0.05 0.03 0.05
Tri Glyceride % ≤ 0.2 0.02 0.01 0.01 0.01 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.154 0.148 0.146 0.147 0.144 0.138 0.146
IV % ≥ 47 min 50.89 51.80 51.93 51.54
Moisture % 2 Max 1.61 1.73 1.83 1.80 2.04 1.95 1.83

FFA % 5 Min 22.08 24.02 23.80 23.72 19.64 20.44 22.28
Gly Content % 84 min 84.81 84.72 84.77 84.77
pH % Neutral 6.03 6.02 6.04 6.08 6.00 6.02 6.03
MONG % 3 max 1.80 1.84 1.79 1.81

Salt % 10 max 4.26 4.22 4.21 4.28 4.24 4.25 4.24
Ash % 7 max 4.20 4.40 4.18 4.26
Water % 9.5 max 9.19 9.26 9.04 9.15 9.26 9.17 9.18
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Date 9-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.110 0.108 0.105 0.110 0.108 0.109 0.108
Moisture % ≤ 0.1 0.026 0.027 0.026 0.026 0.027 0.027 0.027

IV % ≥ 47 51.12 50.99 51.08 50.98 50.98 50.99 51.02
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4279 4388 4566 4813 3923 4017 4172 4155 4225 4069 4459 4317 4282
Soap ppm 500 Max 179 172 177 170 194 190 185 181 177 183 187 179 181
Water ppm ≤ 3000 2934 2876 2930 2512 2819 2880 2866 2792 2427 2557 2695 2582 2739
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.80 857.78 857.79
Density (15 deg C) g/l 860 -900 875.39 875.40 875.40
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.51 4.52
CFPP oC 15 Max 12.7 12.6 12.6 12.4 12.6 12.6 12.6
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.8 98.8 98.8
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 85 90 87 90 95 92 85 91 100 99 95 98 92
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.50 0.5 0.5 0.51 0.5 0.50
Di Glyceride % ≤ 0.2 0.05 0.04 0.04 0.04 0.04 0.04
Tri Glyceride % ≤ 0.2 0.01 0.01 0.02 0.01 0.02 0.01
Total Glycerol % ≤ 0.25 0.140 0.139 0.140 0.142 0.143 0.141
IV % ≥ 47 min 50.98 50.95 50.95 50.96
Moisture % 2 Max 1.18 1.82 2.15 2.20 2.09 2.05 1.92

FFA % 5 Min 25.18 21.68 24.94 22.76 20.17 22.05 22.80
Gly Content % 84 min 84.87 84.89 84.91 84.89
pH % Neutral 6.10 6.08 6.11 6.08 6.05 6.07 6.08
MONG % 3 max 1.80 1.78 1.81 1.80

Salt % 10 max 4.30 4.22 4.20 4.28 4.26 4.27 4.26
Ash % 7 max 4.15 4.18 4.14 4.16
Water % 9.5 max 9.18 9.20 9.15 9.24 9.14 9.21 9.19
Analyst ANGGA Analyst Angga Analyst : : Asariyanto
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Storage Tank PME H2 Storage Tank PME : H2,H4 Storage Tank PME : H4
Date 11-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.110 0.115 0.112 0.111 0.112 0.112 0.112
Moisture % ≤ 0.1 0.026 0.026 0.027 0.026 0.026 0.026 0.026

IV % ≥ 47 51.08 50.95 50.97 51.08 50.96 51.00 51.01
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4365 4472 4376 4411 4501 4177 4251 4362 4543 4416 4417 4308 4383
Soap ppm 500 Max 179 182 177 180 198 182 184 178 169 164 169 172 178
Water ppm ≤ 3000 3188 3112 3011 3084 3048 2832 2445 2746 3040 2983 3152 3021 2972
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.79 857.79 857.77 857.78
Density (15 deg C) g/l 860 -900 875.39 875.39 875.36 875.38
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52
CFPP oC 15 Max 12.4 12.5 12.8 12.6 12.6 12.6 12.6
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.7 98.7 98.7 98.7
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 86 92 92 97 87 90 92 90 94 95 94 91 92
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.53 0.54 0.55 0.54 0.53 0.53 0.54
Di Glyceride % ≤ 0.2 0.05 0.05 0.04 0.05 0.04 0.04 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.148 0.150 0.152 0.151 0.147 0.147 0.149
IV % ≥ 47 min 50.97 50.68 50.91 50.85
Moisture % 2 Max 2.16 2.28 1.59 2.05 2.56 1.70 2.06

FFA % 5 Min 22.70 21.76 25.32 21.03 19.33 20.59 21.79
Gly Content % 84 min 84.86 84.89 84.95 84.90
pH % Neutral 6.10 6.05 6.02 6.00 6.08 6.05 6.05
MONG % 3 max 1.82 1.80 1.82 1.81

Salt % 10 max 4.24 4.22 4.25 4.28 4.32 4.30 4.27
Ash % 7 max 4.12 4.27 4.18 4.19
Water % 9.5 max 9.20 9.32 9.04 9.02 9.05 9.22 9.14
Analyst ANGGA Analyst Angga Analyst : : Asariyanto
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Date 12-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.117 0.115 0.110 0.112 0.118 0.116 0.115
Moisture % ≤ 0.1 0.026 0.026 0.026 0.026 0.026 0.027 0.026

IV % ≥ 47 50.96 50.95 50.94 50.89 50.85 50.82 50.90
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4643 4764 4632 4533 4596 4477 4520 4486 4779 4761 4672 4718 4632
Soap ppm 500 Max 174 170 162 165 170 160 190 178 196 182 177 181 175
Water ppm ≤ 3000 3259 2773 2811 2760 3122 3012 3016 2984 3236 3188 3092 3144 3033
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.79 857.72 857.74 857.75
Density (15 deg C) g/l 860 -900 875.39 875.40 875.44 875.41
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52
CFPP oC 15 Max 12.4 12.5 12.6 12.8 12.6 12.6
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.8 98.8 98.8
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 92 97 88 90 86 92 93 92 96 95 90 92 92
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.53 0.53 0.52 0.53 0.53 0.53 0.53
Di Glyceride % ≤ 0.2 0.05 0.05 0.05 0.05 0.04 0.05 0.05
Tri Glyceride % ≤ 0.2 0.02 0.01 0.01 0.01 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.150 0.149 0.146 0.148 0.147 0.148 0.148
IV % ≥ 47 min 50.92 50.91 50.78 50.87
Moisture % 2 Max 1.28 1.44 1.36 1.48 1.53 1.49 1.43

FFA % 5 Min 20.56 21.66 21.03 22.92 20.16 21.16 21.25
Gly Content % 84 min 84.85 84.80 84.78 84.81
pH % Neutral 6.01 6.01 6.05 6.03 6.01 6.04 6.03
MONG % 3 max 1.82 1.77 1.75 1.78

Salt % 10 max 4.28 4.29 4.31 4.27 4.25 4.27 4.28
Ash % 7 max 4.18 4.15 4.18 4.17
Water % 9.5 max 9.15 9.12 9.28 9.24 9.29 9.26 9.22
Analyst Angga Analyst Analyst : : Asariyanto
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Dose of Catalyst 1.540% Dose of Catalyst : Dose of Catalyst :
Dose of Methanol 10.70% Dose of Methanol : Dose of Methanol :
Source of Feeding H3 Source of Feeding : Source of Feeding :
Storage Tank PME H4 Storage Tank PME : Storage Tank PME :
Date 12-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.118 0.115 0.114 0.116 0.114 0.117 0.116
Moisture % ≤ 0.1 0.026 0.026 0.026 0.027 0.026 0.026 0.026

IV % ≥ 47 50.90 50.88 50.94 51.05 51.08 50.95 50.97
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4764 5178 4970 5449 4695 4417 4428 4553 4439 4502 4637 4587 4718
Soap ppm 500 Max 192 187 182 210 156 167 175 171 156 164 146 152 172
Water ppm ≤ 3000 3122 2532 2568 3076 2321 2507 2506 2936 3194 3088 3308 2996 2846
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.82 857.51 857.54 857.62
Density (15 deg C) g/l 860 -900 875.42 875.11 875.14 875.22
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52
CFPP oC 15 Max 12.5 12.5 12.5 12.6 12.6 12.6 12.6
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.7 98.7 98.8 98.7
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 85 82 89 97 92 96 87 94 97 92 96 91 92
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.55 0.55 0.54 0.54 0.54 0.54 0.54
Di Glyceride % ≤ 0.2 0.06 0.06 0.04 0.05 0.04 0.06 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.155 0.155 0.150 0.151 0.150 0.152 0.152
IV % ≥ 47 min 50.85 50.89 50.94 50.89
Moisture % 2 Max 1.10 1.42 1.26 1.21 1.61 1.67 1.38

FFA % 5 Min 21.90 20.80 22.14 21.94 16.04 17.22 20.01
Gly Content % 84 min 84.93 84.72 84.82 84.82
pH % Neutral 6.03 6.05 6.02 6.04 6.03 6.05 6.04
MONG % 3 max 1.80 1.78 1.72 1.77

Salt % 10 max 4.28 4.26 4.31 4.28 4.26 4.24 4.27
Ash % 7 max 4.12 4.20 4.18 4.17
Water % 9.5 max 9.15 9.28 9.30 9.21 9.28 9.32 9.26
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Dose of Catalyst 1.540% Dose of Catalyst : Dose of Catalyst :
Dose of Methanol 10.70% Dose of Methanol : Dose of Methanol :
Source of Feeding H3 Source of Feeding : Source of Feeding :
Storage Tank PME H4 Storage Tank PME : Storage Tank PME :
Date 14-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.115 0.115 0.119 0.120 0.118 0.122 0.118
Moisture % ≤ 0.1 0.026 0.026 0.026 0.026 0.026 0.027 0.026

IV % ≥ 47 50.99 50.88 51.01 51.08 51.05 50.98 51.00
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4339 4410 4512 4610 4096 4204 3959 4175 4470 4328 4616 4587 4359
Soap ppm 500 Max 172 180 175 180 142 155 164 166 173 168 178 172 169
Water ppm ≤ 3000 3112 3040 3112 3105 2824 2535 2372 2736 2807 2776 3049 2964 2869
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.78 857.74 857.77 857.76
Density (15 deg C) g/l 860 -900 875.40 875.33 875.35 875.36
Viscosity mm2/s 3.5 - 5.0 4.51 4.51 4.51 4.51
CFPP oC 15 Max 12.6 12.6 12.6 12.6 12.6 12.6 12.6
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.7 98.7 98.7 98.7
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 89 96 97 90 88 85 90 94 95 91 93 89 91
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.53 0.53 0.52 0.52 0.52 0.53 0.53
Di Glyceride % ≤ 0.2 0.06 0.05 0.04 0.05 0.05 0.05 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.01 0.02 0.01 0.01
Total Glycerol % ≤ 0.25 0.150 0.155 0.145 0.146 0.147 0.148 0.149
IV % ≥ 47 min 50.79 50.75 50.89 50.81
Moisture % 2 Max 2.15 1.90 2.17 2.35 1.55 1.92 2.01

FFA % 5 Min 18.12 18.10 18.09 17.25 17.07 16.81 17.57
Gly Content % 84 min 84.90 84.77 84.74 84.80
pH % Neutral 6.01 6.08 6.04 6.07 6.05 6.01 6.04
MONG % 3 max 1.78 1.81 1.80 1.80

Salt % 10 max 4.25 4.20 4.27 4.30 4.27 4.24 4.26
Ash % 7 max 4.12 4.16 4.18 4.15
Water % 9.5 max 9.20 9.18 9.26 9.20 9.28 9.31 9.24
Analyst Angga Analyst Eko Analyst : : Asariyanto
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Dose of Catalyst 1.540% Dose of Catalyst : 1.540% Dose of Catalyst :
Dose of Methanol 10.70% Dose of Methanol : 10.70% Dose of Methanol :
Source of Feeding H3 Source of Feeding : H3 Source of Feeding :
Storage Tank PME H2 Storage Tank PME : H2 Storage Tank PME :
Date 15-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.120 0.120 0.122 0.118 0.113 0.108 0.117
Moisture % ≤ 0.1 0.026 0.026 0.027 0.025 0.026 0.026 0.026

IV % ≥ 47 50.92 50.90 50.96 51.56 51.53 51.45 51.22
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4502 4289 4801 4764 4470 4520 4250 4175 4708 4692 4330 4500
Soap ppm 500 Max 132 142 153 160 163 168 174 168 154 163 177 159
Water ppm ≤ 3000 2958 2505 2941 2884 2247 2562 3030 2966 3308 3276 2892 2870
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.70 857.89 857.91 857.83
Density (15 deg C) g/l 860 -900 875.42 875.48 875.51 875.47
Viscosity mm2/s 3.5 - 5.0 4.51 4.51 4.52 4.51
CFPP oC 15 Max 12.4 12.4 12.4 12.2 12.4 12.2 12.3
Acid Value mgKOH/g ≤ 0.40 0.066 0.061 0.061 0.061 0.062 0.059 0.059 0.061 0.055 0.056 0.056 0.060
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.7 98.8 98.8
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 99 81 89 98 94 91 89 93 92 96 95 92
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.53 0.54 0.53 0.53 0.53 0.53 0.53
Di Glyceride % ≤ 0.2 0.05 0.05 0.05 0.05 0.04 0.05 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.148 0.150 0.148 0.148 0.147 0.148 0.148
IV % ≥ 47 min 50.87 50.91 51.04 50.94
Moisture % 2 Max 1.25 1.29 1.59 1.35 1.29 1.46 1.37

FFA % 5 Min 18.93 19.10 17.95 20.34 21.78 19.41 19.59
Gly Content % 84 min 84.92 84.68 84.75 84.78
pH % Neutral 6.06 6.07 6.05 6.00 6.04 6.06 6.05
MONG % 3 max 1.85 1.80 1.78 1.81

Salt % 10 max 4.24 4.24 4.28 4.26 4.28 4.25 4.26
Ash % 7 max 4.11 4.14 4.16 4.14
Water % 9.5 max 9.12 9.40 9.38 9.31 9.31 9.33 9.31
Analyst Angga Analyst Eko Analyst : : Asariyanto
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Dose of Catalyst 1.540% Dose of Catalyst : 1.540% Dose of Catalyst :
Dose of Methanol 10.70% Dose of Methanol : 10.70% Dose of Methanol :
Source of Feeding H3 Source of Feeding : G1 Source of Feeding :
Storage Tank PME H2 Storage Tank PME : H2 Storage Tank PME :
Date 16-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.110 0.111 0.110 0.109 0.114 0.113 0.111
Moisture % ≤ 0.1 0.026 0.027 0.027 0.028 0.027 0.027 0.027

IV % ≥ 47 51.42 51.37 51.40 51.43 51.46 51.42 51.42
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4292 4388 4212 4476 4382 3863 3917 4414 4089 4176 4308 4229
Soap ppm 500 Max 130 135 132 138 145 175 170 153 171 167 163 153
Water ppm ≤ 3000 2707 2670 2676 2513 3039 3242 3106 3051 3092 3066 3117 2934
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.96 857.93 857.91 857.93
Density (15 deg C) g/l 860 -900 875.56 875.53 875.5 875.53
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.51 4.52
CFPP oC 15 Max 12.2 12.5 12.6 12.4 12.2 12.3 12.4
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.7 98.8 98.8
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 85 80 93 90 92 96 93 94 97 97 93 92
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.53 0.53 0.54 0.53 0.53 0.54 0.53
Di Glyceride % ≤ 0.2 0.05 0.04 0.04 0.06 0.05 0.05 0.05
Tri Glyceride % ≤ 0.2 0.02 0.02 0.02 0.03 0.02 0.02 0.02
Total Glycerol % ≤ 0.25 0.149 0.148 0.150 0.153 0.150 0.152 0.150
IV % ≥ 47 min 51.40 51.39 51.44 51.41
Moisture % 2 Max 1.20 1.32 1.26 1.76 2.14 2.16 1.64

FFA % 5 Min 13.28 13.38 17.25 16.86 14.92 13.17 14.81
Gly Content % 84 min 84.90 84.86 84.76 84.84
pH % Neutral 6.00 6.06 6.00 6.11 6.02 6.06 6.04
MONG % 3 max 1.80 1.77 1.83 1.80

Salt % 10 max 4.28 4.24 4.31 4.25 4.22 4.23 4.26
Ash % 7 max 4.12 4.15 4.16 4.14
Water % 9.5 max 9.18 9.15 9.22 9.14 9.25 9.21 9.19
Analyst Angga Analyst Eko / 18:00 Trouble separator Analyst : : Asariyanto
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Source of Feeding 10.70% Source of Feeding : G1 Source of Feeding : G1
Date 17-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.116 0.117 0.115 0.110 0.112 0.114
Moisture % ≤ 0.1 0.026 0.026 0.026 0.027 0.026 0.026

IV % ≥ 47 51.40 51.48 51.50 51.22 51.28 51.38
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4322 4670 4222 5158 4984 4747 4728 4460 4573 4572 4378 4619
Soap ppm 500 Max 158 160 180 198 184 118 126 148 157 162 152 158
Water ppm ≤ 3000 2519 2813 2858 2882 2912 3084 3004 3354 3191 2908 2894 2947
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.97 857.92 857.9 857.93
Density (15 deg C) g/l 860 -900 875.56 875.52 875.5 875.53
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52
CFPP oC 15 Max 12.4 12.4 12.6 12.4 12.4 12.4
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.8 98.8
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 90 92 97 93 98 95 93 98 96 91 93 94
Total Contaminated mg / kg ≤ 24 12 12 12 12 12 12
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.55 0.54 0.54 0.54 0.54 0.54
Di Glyceride % ≤ 0.2 0.06 0.05 0.05 0.04 0.05 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.02 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.155 0.151 0.152 0.150 0.151 0.152
IV % ≥ 47 min 51.38 51.40 51.24 51.34
Moisture % 2 Max 1.58 1.91 2.04 1.87 1.77 1.83

FFA % 5 Min 20.09 18.90 21.65 22.04 21.43 20.82
Gly Content % 84 min 85.02 84.76 84.89
pH % Neutral 6.08 6.07 6.04 6.01 6.03 6.05
MONG % 3 max 1.84 1.86 1.85

Salt % 10 max 4.24 4.23 4.16 4.20 4.23 4.21
Ash % 7 max 1.84 4.14 2.99
Water % 9.5 max 9.02 9.12 9.26 9.24 9.28 9.18
7 Recovery Methanol 160E2 Moisture ppm 1000 max 505 516 154 348 378 380
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Date 18-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.118 0.120 0.119 0.116 0.118 0.117 0.118
Moisture % ≤ 0.1 0.027 0.027 0.027 0.027 0.026 0.026 0.027

IV % ≥ 47 51.34 51.25 51.30 51.24 51.21 51.25 51.27
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4852 4881 4950 5288 5017 4822 4938 4872 4877 4764 4769 4697 4894
Soap ppm 500 Max 183 187 177 195 179 170 164 175 189 178 166 162 177
Water ppm ≤ 3000 2461 2694 2606 2933 2595 2713 2808 2894 2638 2784 2672 2844 2720
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.94 857.96 857.93 857.94
Density (15 deg C) g/l 860 -900 875.54 875.56 875.53 875.54
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52
CFPP oC 15 Max 12.4 12.6 12.6 12.4 12.4 12.6 12.5
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.7 98.7 98.7 98.7
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 95 90 86 91 87 92 92 94 95 97 91 93 92
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.55 0.55 0.55 0.55 0.56 0.56 0.55
Di Glyceride % ≤ 0.2 0.05 0.07 0.06 0.05 0.05 0.05 0.06
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.02 0.01 0.02 0.01
Total Glycerol % ≤ 0.25 0.154 0.157 0.156 0.155 0.156 0.157 0.156
IV % ≥ 47 min 51.30 51.28 51.20 51.26
Moisture % 2 Max 1.57 1.46 1.52 1.87 1.81 1.92 1.69

FFA % 5 Min 21.90 20.75 18.70 16.72 17.23 16.54 18.64
Gly Content % 84 min 84.78 84.83 84.76 84.79
pH % Neutral 6.00 6.01 6.04 6.05 6.02 6.02 6.02
MONG % 3 max 1.82 1.80 1.83 1.82

Salt % 10 max 4.30 4.32 4.29 4.26 4.24 4.27 4.28
Ash % 7 max 4.15 4.15 4.14 4.15
Water % 9.5 max 9.25 9.21 9.22 9.26 9.27 9.30 9.25
Analyst Eko Analyst Analyst : : Asariyanto
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Date 19-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.110 0.114 0.115 0.110 0.114 0.116 0.113
Moisture % ≤ 0.1 0.027 0.026 0.026 0.026 0.026 0.026 0.026

IV % ≥ 47 51.48 51.77 51.62 51.66 51.70 51.72 51.66
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4827 4612 4787 4527 4706 4680 4738 4838 4812 5012 4913 5070 4794
Soap ppm 500 Max 175 166 156 169 181 176 180 176 180 194 180 186 177
Water ppm ≤ 3000 2633 2517 3102 3054 3147 3076 2977 3011 3010 3124 2977 2758 2949
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.98 857.96 857.9 857.95
Density (15 deg C) g/l 860 -900 875.58 875.56 875.55 875.56
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52
CFPP oC 15 Max 12.4 12.4 12.6 12.4 12.4 12.6 12.5
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.6 98.6 98.8 98.7
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 90 95 91 94 90 92 90 97 98 92 90 90 92
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.57 0.57 0.57 0.55 0.54 0.54 0.56
Di Glyceride % ≤ 0.2 0.05 0.05 0.07 0.04 0.04 0.05 0.05
Tri Glyceride % ≤ 0.2 0.02 0.01 0.01 0.01 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.160 0.159 0.162 0.152 0.150 0.151 0.156
IV % ≥ 47 min 51.40 51.66 51.65 51.57
Moisture % 2 Max 1.76 2.35 2.29 2.19 1.94 1.90 2.07

FFA % 5 Min 18.46 15.61 19.11 20.12 21.10 20.17 19.10
Gly Content % 84 min 84.70 84.80 84.96 84.82
pH % Neutral 6.00 6.04 6.00 6.01 6.05 6.02 6.02
MONG % 3 max 1.83 1.82 1.72 1.79

Salt % 10 max 4.30 4.26 4.34 4.35 4.32 4.29 4.31
Ash % 7 max 4.19 4.20 4.22 4.20
Water % 9.5 max 9.28 9.32 9.18 9.15 9.10 9.18 9.20
7 Recovery Methanol 160E2 Moisture ppm 1000 max 612 416 1.92 347 350 4.23 289
Analyst Eko Analyst Eko Analyst : : Angga & Yusuf
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Dose of Catalyst 1.54% / pkl 11:00 1.546% Dose of Catalyst : 1.566% Dose of Catalyst : 1.566%
Date 20-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.114 0.116 0.114 0.115 0.116 0.112 0.115
Moisture % ≤ 0.1 0.026 0.026 0.027 0.027 0.026 0.027 0.027

IV % ≥ 47 51.65 51.74 51.70 51.72 51.70 51.77 51.71
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4533 4208 4472 4515 4154 4261 4287 4316 4144 4472 4260 4312 4328
Soap ppm 500 Max 153 144 170 165 150 158 177 170 168 160 172 180 164
Water ppm ≤ 3000 2432 2526 3043 2908 3236 3086 3198 3082 2947 2876 2838 2910 2924
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.91 857.95 857.96 857.94
Density (15 deg C) g/l 860 -900 875.51 875.55 875.56 875.54
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52
CFPP oC 15 Max 12.4 12.2 12.2 12.0 12.0 12.2
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.8 98.8 98.8
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 92 89 87 90 97 93 96 93 95 90 86 89 91
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.50 0.49 0.5 0.5 0.5 0.51 0.50
Di Glyceride % ≤ 0.2 0.04 0.06 0.05 0.06 0.06 0.06 0.06
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.139 0.137 0.141 0.142 0.142 0.144 0.141
IV % ≥ 47 min 51.64 51.62 51.55 51.60
Moisture % 2 Max 1.49 1.25 1.42 1.47 1.04 1.10 1.30

FFA % 5 Min 21.36 24.65 24.42 22.81 20.92 21.12 22.55
Gly Content % 84 min 84.84 84.73 85.02 84.86
pH % Neutral 6.00 6.01 6.00 6.02 6.05 6.02 6.02
MONG % 3 max 1.78 1.81 1.79 1.79

Salt % 10 max 4.27 4.28 4.26 4.22 4.23 4.28 4.26
Ash % 7 max 4.15 4.22 4.14 4.17
Water % 9.5 max 9.23 9.20 9.29 9.26 9.05 9.12 9.19
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Dose of Catalyst 1.54% / pkl 11:00 1.546% Dose of Catalyst : 1.566% Dose of Catalyst : 1.560%
Date 21-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.110 0.111 0.112 0.110 0.115 0.114 0.112
Moisture % ≤ 0.1 0.026 0.026 0.027 0.026 0.025 0.026 0.026

IV % ≥ 47 51.70 51.69 51.64 51.60 51.70 51.71 51.67
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4486 4417 4625 4734 4763 4668 4807 4841 4075 4124 4314 4470 4527
Soap ppm 500 Max 158 144 147 135 144 139 148 152 160 163 160 168 152
Water ppm ≤ 3000 2560 2608 2882 2634 2791 2824 2844 2796 2912 2874 2760 2773 2772
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.98 857.97 857.97 857.97
Density (15 deg C) g/l 860 -900 875.58 875.56 875.56 875.57
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52
CFPP oC 15 Max 12.2 12.6 12.8 12.6 13.0 12.8 12.7
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.8 98.8 98.8
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 92 90 87 89 93 91 94 97 105 97 100 110 95
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.51 0.51 0.51 0.5 0.51 0.51 0.51
Di Glyceride % ≤ 0.2 0.06 0.05 0.06 0.05 0.05 0.05 0.05
Tri Glyceride % ≤ 0.2 0.02 0.01 0.01 0.02 0.01 0.02 0.02
Total Glycerol % ≤ 0.25 0.144 0.143 0.144 0.142 0.143 0.144 0.143
IV % ≥ 47 min 51.67 51.59 51.63 51.63
Moisture % 2 Max 1.13 1.28 1.41 1.58 1.02 1.12 1.26

FFA % 5 Min 20.17 21.02 18.84 18.71 17.11 17.24 18.85
Gly Content % 84 min 84.80 84.70 84.92 84.81
pH % Neutral 6.07 6.05 6.02 6.04 6.05 6.04 6.05
MONG % 3 max 1.86 1.84 1.72 1.81

Salt % 10 max 4.27 4.28 4.25 4.23 4.21 4.21 4.24
Ash % 7 max 4.16 4.17 4.11 4.15
Water % 9.5 max 9.18 9.24 9.29 9.32 9.25 9.30 9.26
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Dose of Catalyst 1.566 % / pkl 09:00 1.560% Dose of Catalyst : 1.556% Dose of Catalyst : 1.566%
Date 22-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.112 0.109 0.114 0.111 0.110 0.111 0.111
Moisture % ≤ 0.1 0.026 0.027 0.027 0.027 0.026 0.026 0.027

IV % ≥ 47 51.78 51.60 51.61 51.64 51.60 51.72 51.66
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 3885 4278 4037 3964 4732 4801 4766 4826 4948 4970 4816 4860 4574
Soap ppm 500 Max 167 172 160 157 165 161 158 164 156 160 162 155 161
Water ppm ≤ 3000 2738 2415 279 2685 3106 3148 3092 2976 2629 2738 2880 2713 2617
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.96 857.92 857.9 857.93
Density (15 deg C) g/l 860 -900 875.56 875.52 875.55 875.54
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52
CFPP oC 15 Max 12.8 12.6 12.4 12.8 12.6 12.6 12.6
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.8 98.8 98.8
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 89 91 94 92 95 97 96 93 88 90 98 92 93
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.51 0.51 0.5 0.51 0.51 0.52 0.51
Di Glyceride % ≤ 0.2 0.05 0.05 0.04 0.06 0.05 0.05 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.144 0.144 0.139 0.145 0.144 0.145 0.144
IV % ≥ 47 min 51.72 51.57 51.55 51.61
Moisture % 2 Max 1.25 1.21 1.38 1.51 1.04 1.14 1.26

FFA % 5 Min 16.49 17.45 18.11 17.24 23.14 22.32 19.13
Gly Content % 84 min 84.93 84.66 84.80 84.80
pH % Neutral 6.05 6.02 6.00 6.03 6.01 6.05 6.03
MONG % 3 max 1.77 1.84 1.71 1.77

Salt % 10 max 4.38 4.32 4.27 4.24 4.46 4.32 4.33
Ash % 7 max 4.18 4.18 4.30 4.22
Water % 9.5 max 9.12 9.16 9.32 9.30 9.19 9.26 9.23
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
Date 23-Sep-21
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1 0.113 0.112 0.113
Moisture % ≤ 0.1 0.026 0.027 0.027

IV % ≥ 47 51.78 51.62 51.70
flowrate mT/H 42 Max 42 42 42 42 42
Water ppm ≤ 5000 4036 4217 4487 4426 4292
Soap ppm 500 Max 172 180 163 167 171
Water ppm ≤ 3000 2416 2586 2654 2575 2558
Soap ppm 15 Max 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 858.10 858.10
Density (15 deg C) g/l 860 -900 875.69 875.69
Viscosity mm2/s 3.5 - 5.0 4.52 4.52
CFPP oC 15 Max 12.8 12.8 12.8
Cloud Point oC 18 Max 15.8 15.8 15.8
Acid Value mgKOH/g ≤ 0.40 0.048 0.049 0.063 0.060 0.055
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.8 98.8
Methanol % ≤ 0.2 0.01 0.010

4 Fame 163E3B
Water mg / kg ≤ 200 90 88 86 90 89
Total Contaminated mg / kg ≤ 24 12 12 12
Flash Point oC ≥ 120 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.52 0.52 0.52
Di Glyceride % ≤ 0.2 0.05 0.04 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01
Total Glycerol % ≤ 0.25 0.146 0.145 0.146
IV % ≥ 47 min 51.70 51.70
Moisture % 2 Max 1.24 1.55 1.40

FFA % 5 Min 17.91 15.30 16.61
Gly Content % 84 min 84.76 84.76
pH % Neutral 6.02 6.00 6.01
MONG % 3 max 1.76 1.76

Salt % 10 max 4.44 4.34 4.39
Ash % 7 max 4.20 4.20
Water % 9.5 max 9.28 9.32 9.30
7 Recovery Methanol 160E2 Moisture ppm 1000 max 200 912 556
Time 08:00 - 16:00 Time : 16:00 - 20:00 Time : 24:00-08:00
August
No Materials Sampling Point Parameters Unit Control Limit
1 2 3 4 5 6 7 8 9
FFA % ≤ 0.1 0.088 0.094 0.086 0.087 0.108 0.117 0.119 0.118 0.097
Moisture % ≤ 0.1 0.026 0.026 0.026 0.026 0.027 0.027 0.027 0.026 0.026
IV % ≥ 47 51.59 50.63 51.66 51.50 48.282 46.830 46.807 47.39 51.69
flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42
Water ppm ≤ 5000 4233 4097 4244 4447 4325 4166 4532 4478 4533
2 1st Washed FAME 163S2 LP Methanol % 1.2 Max 0.69 0.62 0.69 0.62 0.62 0.62 0.60 0.64 0.62
Soap ppm 500 Max 146 145 145 157 158 161 157 168 164
Water ppm ≤ 3000 2911 2773 2688 2681 2832.583 3035 2765 2870 2952
3 2nd Washed FAME 163S20 LP Methanol % 1.2 Max 0.32 0.30 0.29 0.31 0.320 0.31 0.29 0.31 0.31
Soap ppm 15 Max 3 3 3 3 3 3 3 3 3

Density (40 deg C) g/l 850 - 890 857.74 857.72 857.67 857.69 857.54 857.34 857.31 857.39 857.58
Density (15 deg C) g/l 860 -900 875.35 875.33 875.28 875.35 875.14 874.91 874.91 875.01 875.20
Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52 4.51 4.51 4.52 4.52 4.51
CFPP oC 15 Max 12.7 12.6 12.6 12.6 13.33 13.72 13.97 14.1 13.3
Cloud Point oC 18 Max 15.7 15.6 15.6 15.6 16.367 16.72 16.97 17.1 16.3
Acid Value mgKOH/g ≤ 0.40 0.061 0.053 0.051 0.053 0.051 0.061 0.056 0.067 0.053
Sediment Vol. % ≤ 0.05 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Ester % ≥96.5 98.7 98.8 98.7 98.8 98.7 98.7 98.7 98.7 98.8
Methanol % ≤ 0.2 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010 0.010
4 Fame 163E3B
Water mg / kg ≤ 200 92 91 93 94 92 93 94 95 92
Total Contaminated mg / kg ≤ 24 12 12 12 12 12 12 12 12 12
Flash Point oC ≥ 120 170.5 170.5 170.5 170.5 170.5 170.5 170.5 170.5 170.5
Free Glyceride % ≤ 0.02 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005
Mono Glyceride % ≤ 0.55 0.56 0.52 0.52 0.51 0.528 0.543 0.56 0.53 0.52
Di Glyceride % ≤ 0.2 0.06 0.04 0.05 0.05 0.053 0.052 0.058 0.05 0.05
Tri Glyceride % ≤ 0.2 0.01 0.01 0.01 0.01 0.010 0.018 0.027 0.01 0.01
Total Glycerol % ≤ 0.25 0.158 0.145 0.145 0.145 0.149 0.153 0.159 0.151 0.146
IV % ≥ 47 min 51.57 50.67 51.53 51.47 49.400 46.819 46.690 46.70 51.54
Moisture % 2 Max 1.59 1.68 1.77 1.52 1.553 1.425 1.278 1.74 1.83
FFA % 5 Min 19.71 22.98 27.81 19.23 24.590 19.517 19.865 20.95 22.28
Gly Content % 84 min 84.93 84.89 84.87 84.89 84.87 84.84 84.89 84.77 84.77
pH % Neutral 5.92 6.09 6.04 6.09 6.060 6.028 6.030 6.05 6.03
MONG % 3 max 1.82 1.74 1.80 1.78 1.79 1.79 1.77 1.81 1.81
Salt % 10 max 4.21 4.21 4.25 4.20 4.22 4.24 4.24 4.25 4.24
Ash % 7 max 4.13 4.13 4.12 4.13 4.13 4.13 4.15 4.15 4.26
Water % 9.50 max 9.14 9.17 9.19 9.19 9.21 9.21 9.21 9.21 9.18
7 Recovery Methanol 160E2 Moisture ppm 1000 454 633 418 757 220 548 505 622 738
Dosing (%)
Date Time Flowrate (tph) Source of Feeding Final PME Tank
Catalyst Methanol
September 23, 2021 12:00 42 H5 H2 1.547% 10.7%
Sampling Point Parameter

Feed MC (%) FFA (%) IV (g-I2/100g)
180E1 0.027 0.112 51.62
MC (ppm) Soap (ppm)
163S2LP 4487 163
163S20LP 2654 3 8:00
AV
Ws (%) MC (ppm) Mg (%) Dg (%) Tg (%) Fg (%) Total Gly (%) CFPP
PME 163E3B (mg-KOH/g)
0.063 0.01 86 0.52 0.05 0.01 0.005 0.146 12.8 Total Glu 0.146 200
NaCl MC
pH
Glycerine 166E3 NaCl (% ) MC (%)
6.00 4.34 9.32
MC (%) FFA (%)

FATTY 166 P4
1.55 15.30
MC (ppm)
MeOH 160E2
912
Note : Outspec
MC (%) Ph Err:522 0 0 0
Glycerine Tank
9.47 6.06 Too Good
Target Quality
MC CG (%) AV MC PME Mg Dg Tg Fg Total Gly
9.5 Max 0.4 Max 200 ppm Max 0.55 % Max 0.20 % Max 0.20 % Max 0.020 % Max 0.250 % Max
Dosing (%)
Date Time Flowrate (tph) Source of Feeding Final PME Tank
Catalyst Methanol
August 12, 2021 4:00 42 G1 H4 1.510% 10.7%
Sampling Point Parameter

AV 20:00
MC (ppm) Ws (%)
(mg-KOH/g) Mg (%) Dg (%) Tg (%) Fg (%) Total Gly (%)
PME 163E3B
94 0.058 0.01 0.51 0.04 0.01 0.005 0.142
MC (%)
Glycerine 166E3 Note : Outspec
9.42 Too Good
Target Quality
MC CG (%) AV MC PME Mg Dg Tg Fg Total Gly
9.5 Max 0.4 Max 200 ppm Max 0.55 % Max 0.20 % Max 0.20 % Max 0.020 % Max 0.250 % Max
Date :
Time
08.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 02.00 04.00 06.00
FFA % ≤ 0.1
Moisture % ≤ 0.1
IV % ≥ 47
flowrate mT/H 42 Max
Water ppm ≤ 5000
2 1st Washed FAME 163S2 LP Methanol % 1.2 Max
Soap ppm 500 Max
Water ppm ≤ 3000
3 2nd Washed FAME 163S20 LP Methanol % 1.2 Max
Soap ppm 15 Max

Density (40 deg C) g/l 850 - 890
Density (15 deg C) g/l 860 -900
Viscosity mm2/s 3.5 - 5.0
CFPP oC 15 Max
Cloud Point oC 18 Max
Acid Value mgKOH/g ≤ 0.40
Sediment Vol. % ≤ 0.05
Ester % ≥96.5
Methanol % ≤ 0.2
4 Fame 163E3B
Water mg / kg ≤ 200
Total Contaminated mg / kg ≤ 24
Flash Point oC ≥ 120
Free Glyceride % ≤ 0.02
Mono Glyceride % ≤ 0.55
Di Glyceride % ≤ 0.2
Tri Glyceride % ≤ 0.2
Total Glycerol % ≤ 0.25
IV % ≥ 47 min
Moisture % 2 Max
FFA % 5 Min
Gly Content % 84 min
pH % Neutral
MONG % 3 max
Salt % 10 max
Ash % 7 max
Water % 9.5 max
7 Recovery Methanol 160E2 Moisture ppm 1000 max

Analyst : Analyst : : Analyst :
Time : 08:00 - 16:00 Time : 16:00 - 24:00 Time : 24:00 - 08:00
Dose of Catalyst : Dose of Catalyst : Dose of Catalyst :
Dose of Methanol : Dose of Methanol : Dose of Methanol :
Source of Feeding : Source of Feeding : Source of Feeding :
Storage Tank PME : Storage Tank PME : Storage Tank PME :
ID Sample : RBDPO ID Sample : BPO
Date : Febuary 05, 21 Date : Febuary 05, 21
Dosing BE : 1.0% Refinol X Dosing BE : 1.0% Refinol X
Refinol M : 0.05% Refinol M : 0.05%
ID Sample : RBDPO ID Sample : BPO

ID Sample : CPO ID Sample : CPO

Date Time Sample
20:00 163P5
20:00 163P13
20:00 S20
9-Apr-21
20:00 S2LP
4:00 S20
4:00 S2LP
Date Time Sample

Dozing Catalyst % IV Feed IV Product
16:00 PME Proses 1.9 56.55
17:00 PME Proses 1.9
7-Jul-21
18:00 PME Proses 1.9
20:00 PME Proses 1.9 58.05 58.3
Parameters
Mg Dg Tg Fg Tot Gly MeOH
0.43 0.03 0.01 0.005 0.120
0.49 0.06 0.01 0.005 0.140
0.25
0.57
0.24
0.59
Parameters
CP °C CFPP °C MG % SMG % SMG mg/kg
12 0.35 0.1562 1562
12 0.36 0.1607 1607
12 0.37 0.1651 1651
10 0.38 0.1525 1525
Date : 20-Nov-20
Time Update : 8:00
Flow (mT/h) : 42.0
Source of Feeding : H5
Storage Tank PME : H2
Dose of Catalyst (%) : 1.583
Dose of Methanol (%) : 10.70
Parameters
Sampling Point
MC (ppm) Soap (ppm) FFA (%) IV (g-I2/100g) WS (%) Mg (%) Dg (%) Tg (%) Fg (%) EC CFPP NaCl (% ) NaCl (% )
180E1 (Feed) 0.024 0.083
163S2LP (Crude PME)
163S20LP (Crude PME)
163E3B (Final PME)
166E3 (Crude Glycerin)
166P4 (Fatty Matter)
160E2 (Methanol)
: Outspec
Target Quality
AV MC CG MC PME Mg Dg Tg Fg Total Gly CFPP
0.4 Max 9.80 Max 200 ppm Max 0.55 % Max 0.20 % Max 0.20 % Max 0.020 % Max 0.250 % Max 15 Max
total gly 0.00000

Report Quality Biodiesel Plant (Sept, 2021)

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Report Quality Biodiesel Plant (Sept, 2021)

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PT LOUIS DREYFUS COMPANY LAMPUNG

DAILY ANALYSIS BIODIESEL REPORT

Moisture % ≤ 0.1 0.025 0.026 0.027 0.026 0.025 0.025 0.026

flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42

2 1st Washed FAME 163S2 LP Methanol % 1.2 Max 0.69 0.69

3 2nd Washed FAME 163S20 LP Methanol % 1.2 Max 0.32 0.32

Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.51 4.52

CFPP oC 15 Max 12.8 12.8 12.8 12.8 12.6 12.6 12.7

Ester % ≥96.5 98.7 98.7 98.7 98.7

Methanol % ≤ 0.2 0.010 0.010

Flash Point oC ≥ 120 170.5 170.5 170.5 170.5

Di Glyceride % ≤ 0.2 0.07 0.06 0.05 0.06 0.05 0.05 0.06

IV % ≥ 47 min 51.68 51.58 51.46 51.57

Moisture % 2 Max 1.26 1.52 1.29 1.41 1.91 2.16 1.59

Gly Content % 84 min 85.04 84.90 84.85 84.93

pH % Neutral 5.86 5.86 5.77 6.00 5.98 6.04 5.92

MONG % 3 max 1.82 1.85 1.78 1.82

Ash % 7 max 4.14 4.17 4.09 4.13

DAILY ANALYSIS BIODIESEL REPORT

Moisture % ≤ 0.1 0.026 0.026 0.026 0.026 0.027 0.025 0.026

flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42

2 1st Washed FAME 163S2 LP Methanol % 1.2 Max 0.62 0.62

3 2nd Washed FAME 163S20 LP Methanol % 1.2 Max 0.30 0.30

Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52

CFPP oC 15 Max 12.6 12.6 12.6 12.6 12.8 12.6

Cloud Point oC 18 Max 15.6 15.6 15.6 15.6 15.8 15.6

Ester % ≥96.5 98.7 98.8 98.8 98.8

Methanol % ≤ 0.2 0.010 0.010

Flash Point oC ≥ 120 170.5 170.5 170.5 170.5

Di Glyceride % ≤ 0.2 0.04 0.04 0.04 0.05 0.05 0.04 0.04

IV % ≥ 47 min 51.21 50.37 50.42 50.67

Moisture % 2 Max 1.91 1.54 1.21 1.36 2.05 1.98 1.68

Gly Content % 84 min 84.94 84.93 84.80 84.89

pH % Neutral 6.02 6.02 6.13 6.15 6.10 6.12 6.09

MONG % 3 max 1.78 1.74 1.71 1.74

Ash % 7 max 4.12 4.16 4.11 4.13

DAILY ANALYSIS BIODIESEL REPORT

Moisture % ≤ 0.1 0.026 0.026 0.025 0.025 0.026 0.027 0.026

flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42

2 1st Washed FAME 163S2 LP Methanol % 1.2 Max 0.69 0.69

3 2nd Washed FAME 163S20 LP Methanol % 1.2 Max 0.29 0.29

Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Viscosity mm2/s 3.5 - 5.0 4.52 4.52 4.52 4.52

CFPP oC 15 Max 12.7 12.6 12.5 12.6 12.5 12.6 12.6

Ester % ≥96.5 98.7 98.7 98.7 98.7

Methanol % ≤ 0.2 0.010 0.010

Flash Point oC ≥ 120 170.5 170.5 170.5 170.5

Di Glyceride % ≤ 0.2 0.04 0.05 0.04 0.05 0.04 0.05 0.05

IV % ≥ 47 min 51.40 51.48 51.70 51.53

Moisture % 2 Max 1.99 1.84 1.77 1.28 1.88 1.86 1.77

Gly Content % 84 min 84.91 84.93 84.76 84.87

pH % Neutral 5.88 5.91 6.12 6.12 6.10 6.12 6.04

MONG % 3 max 1.78 1.80 1.82 1.80

Ash % 7 max 4.15 4.12 4.10 4.12

DAILY ANALYSIS BIODIESEL REPORT

Moisture % ≤ 0.1 0.027 0.026 0.025 0.025 0.027 0.026 0.026

flowrate mT/H 42 Max 42 42 42 42 42 42 42 42 42 42 42 42 42

2 1st Washed FAME 163S2 LP Methanol % 1.2 Max 0.62 0.62

3 2nd Washed FAME 163S20 LP Methanol % 1.2 Max 0.31 0.31

Soap ppm 15 Max 3 3 3 3 3 3 3 3 3 3 3 3 3

Viscosity mm2/s 3.5 - 5.0 4.51 4.52 4.52 4.52