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Viscotester VT01 / 02
808-0701
2-1-060-1/3 10.1993
Tel. +49(0)721 4094-444 Tel. 608 327 6777 Tel. +33(0)1 64 54 0101
Fax +49(0)721 4094-418 Fax 608 273 6827 Fax +33(0)1 64 54 0187
info@thermohaake.com infousa@thermohaake.com info@thermorheo.com
www.thermohaake.com www.thermohaake.com www.thermohaake.com
Table of Contents
General Notes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
1. Description . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
3. Measurement . . . . . . . . . . . . . . . . . . . . . . . . . 6
4. Technical Specifications . . . . . . . . . . . . 11
5. Optional Accessories . . . . . . . . . . . . . . . 13
1
General Notes
! lowing instructions!
This instruction manual describes exactly how this device is
to be used.
The following points should especially be kept in mind:
Dieselstr. 4
The following specifications should be given when product
ThermoHaake D–76227 KARLSRUHE enquiries are made:
TYP
V/Hz Unit name printed on the front of the unit and specified on
the name plate.
2
Description
1. Description
The Viscotesters VT 01 and VT 02 are simple rotational vis-
cometers, specially suited for fast comparison tests on liq-
uids.
1.1 Measuring Principle
A rotor, driven by a speed-controlled, battery-operated mo-
tor, is immersed into the liquid to be tested. The viscosity of
the liquid is measured as a resulting torque and is indicated
directly on the scale.
1.2 Drive
Speed controlled motor, battery: 6 V.
Speed of rotor: 62.5 min–1.
1.3 Measuring Ranges
Both Viscotesters have three measuring ranges each. There
is a special rotor for each measuring range. The scale indi-
cates which rotor should be used. The scale values given are
calibrated with Newtonian liquids (mineral oils).
VT01:
Scale Measuring Range Rotor
4 1.5 ... 33 mPas (cP) 4
5 15 ... 150 mPas (cP) 5
3 50 ... 330 mPas (cP) 3
VT02:
3 0.3 ... 13 dPas (P) 3
1 3 ... 150 dPas (P) 1
2 100 ... 4000 dPas (P) 2
Please note:
1 mPas (milli Pascalsecond) = 1 cP (centi Poise)
1 dPas (deci Pascalsecond) = 1 P (Poise)
1 dPas (deci Pascalsecond) = 100 mPas
3
Functional and Operating Elements
1) Battery container Four 1.5 Volt leak-proof Mignon-batteries. Insert the bat-
teries according to the drawing on the bottom of the instru-
ment.
2) Screw To open 1).
3) Socket for mains power Note: When using an external power supply, the batteries
must be removed from the instrument.
4) Main switch Move switch in direction of the arrow to start the instru-
ment.
5) Indicator With 3 scales.
5a) Scale number Corresponds to the number of the rotor used.
6) Battery-charge indicator Ready status with light emitting diode display red.
(ON/OFF indicator) If the left LED flashes, change the battery.
7) Level During measurement, the instrument must be held
horizontally.
4
Functional and Operating Elements
5
Measurement
3. Measurement
6
Measurement
7
Measurement
T(°C)
Temperature
8
Measurement
3.7 Reproducibility
Two consecutive measurements under identical measuring
conditions will not differ by more than ± 2 % of total range.
9
Information concerning the CE sign
10
Technical Specifications
4. Technical Specifications
Data on VT01:
Motor:
Rated voltage of motor: . 4.5 to 6.5 Volts
Rotor:
Rated speed of rotors: . . 62.5 min–1 ± 5%
Dimensions:
Material:
Rotor 3: . . . . . . . . . . . . . . . stainless steel
Rotors 4 and 5: . . . . . . . . anodized aluminium
Measuring Cup:
Dimensions:
11
Technical Specifications
Data on VT02:
Motor:
Rated voltage of motor: . 4.5 to 6.5 Volts
Rotor:
Rated speed of rotors: . . 62.5 min–1 ± 5%
Dimensions:
Measuring Cup:
Dimensions:
12
Optional Accessories
5. Optional Accessories
13
Terms of Rheological Measurements
Steady Rotation:
Creep/Recovery
CS measuring mode to determine the viscous and elastic properties of a
material, e.g. for the determination of the zero-viscosity or as a criterion of
shelf life.
(Thermo Haake RheoStress / RheoWave)
Stress Growth/Decay
CR measuring mode to determine the time behavior and steady state flow
curves.
(Thermo Haake ViscoTester / RotoVisco / RheoStress)
14
Terms of Rheological Measurements
Oscillating movement:
OSC: Oscillation
Measuring mode for the non-destructive determination of elastic and
viscous material properties.
Here e.g. the influence of the frequency by forced oscillating stress on the
storage and loss modules (G’ and G”) can be investigated.
The measuring data gained in the linear visco-elastic range allow conclu-
sions on other physical quantities (e.g. molecular quantities for polymers)
(Thermo Haake RheoStress / RheoWave)
Newtonian: Property of substances where the viscosity will not change under shear
rate and shear stress.
(Thermo Haake Falling Ball Viscometer, System Höppler)
Pseudoplastic: Property of substances where the viscosity will decrease under shear
rate and shear stress.
(Most common material behavior)
Dilatant: Property of substances where the viscosity will increase under shear rate
and shear stress.
Plastic: Property of non-Newtonian substances which only start flowing after being
subject to a certain force (shear stress), i.e. after a certain yield point. The
yield point strongly depends on external parameters like temperature and
change rate of the acting force. Therefore, a ”practical” yield point is
determined taking in account the environmental conditions specific for the
application.
(Measuring modes: CD, CS)
(Thermo Haake ViscoTester 550 / RotoVisco1 / RheoStress)
15
Terms of Rheological Measurements
Instrument quantities:
Md – torque
Ω – angular velocity
φ – rotation angle
ω – angular velocity ( 2⋅π⋅f )
FN – normal force
R, h, ... – dimensions of sensor
– etc.
Measuring parameter:
T – temperature
p – pressure
t – time
– etc.
Rheometrical quantities:
τ – shear stress
g – shear rate
g – deformation
N1, N2 – normal stress differences
– etc.
Rheological quantities:
Material functions:
η, η∗, η+, η– – viscosities
Ψ1, Ψ2 – normal stress functions
G – shearing modulus
G*, G’ G” – dynamic shear moduli
J – compliance
J*, J’, J” – dynamic compliances
– etc.
Material parameters:
η0 – zero viscosity
τy – yield point
Ψ10 – 1st normal stress coefficient
– etc.
16