iy Designation: B 49 - 98°* sprtrom he soa aks AST Sarre Copy ASIA Standard Specification for Copper Rod Drawing Stock for Electrical Purposes’ “hi end sti ner i ea the umber immed _depion ot inthe case of revision the year st revo eur ps (lees an eto change ioe te lst eis espns iy following he dsipaaion indicus the sear foil dees tte the Sear hit eeppoNa, Aspect This mda har been approved for te by eno ofthe Deptt of Deon Noo Table Ie fate wo 99.50 9 wae iy const iE fom D. 1. Seope* 1.1 This specification covers the requirements for rod draw- ing stock in diameters from 4 to 1%in. (644 to 35 mm) produced from electrolytic tough-pitch or oxygen-free coppers and ate suitable for further fabrication into electrical conduc: tors, 1.2 The values stated in inch-pound units are the standard ‘The values given in parentheses are for information only 13 The following safety hazards caveat pertains only t0 Section 13. This standard does not purport to address all ofthe safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appro- priate safety and health practices and determine the applica- bility of regulatory limitations prior to wae. 2. Referenced Documents 2.1 The following documents in the current issue of the Annual Book of ASTM Standards form a past of this specifi cation to the extent referenced herein and define materials suitable for use in rod manufactur: 2.1.1 ASTM Standards B.S Specification for High Conductivity Tough-Pitch Cop- per Refinery Shapes? B15 Specification for Blecuolytie Cathode Copper? B 170 Specification for Oxygen-Free Electrolytic Copper— Refinery Shapes? B 193 Test Method for Resistivity of Elecuical Conductor Materials* B 224 Classification of Copper? B577 Test Methods for Hydrogen Embrittement of Copper* B 846 Terminology Related to Copper and Copper Alloys? EB Test Methods of Tension Testing of Metallic Materials! B 18 Test Methods for Rockwell Hardness and Rockwell ‘Superficial Hardness of Metallic Materials* Thi specication is nde thers of ASEM Conte B.S on Copper are Copper Alloys, and the det responsibility of Sosmmatee AUSF 00 Refined Cones Crest etion sporoved March 10, 198, Pulte Jeneary 1999, Oviinaly ublstsd a B40 287. Lan previous sion B49 ®nal Bzok of ASTI Standen, Vol 2.9, nnn Book af ASTI Stade, Vol 020 “Arnucl Book of ASTM Stenderds, Val W301 A Summary of Changes section appears E20 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications E53 Test Methods for Chemical Analysis of Copper® E478 Test Methods for Chemical Analysis of Copper Alloys® 2.1.2 Other Document NBS Handbook 100—Copper Wire Tables? 3. Terminology 3.1 For definitions of general terms relating to copper and copper alloys refer to Terminology B 846. 4. Ordering Information 4.1 Orders for rod under this specification shall include the following information: 4.1.1 ASTM designation and year of issue, 4.1.2 Quantity of each size, 4.1.3 Type and requirements of copper (Sections 5 through 10), 4.1.4 Finish (Sections 9 and 10), 4.1.5 Package with or without joints (see 5.3), 4.1.6 Rod diameter (see 9.2), 4.1.7 Inspection (Section 15}, 4.18 Package size (see 19.1), and 4.1.9 Special packege marking as agreed upon between the ‘manufacturer and the purchaser (Section 19), 4.2 The following requirements are optional and should be specified in the contract or purchase order when required. 42.1 Centfication (Section 17) and 4.2.2 Test Report (Section 18), 5. Material and Manufacture 5.1 The rod shall be fabricated from copper of such quality ‘and purity that the finished product shall have the properties ‘and characteristics prescribed in this specification. Nore 1—The following specifications define materia saitable for us: Specification B 5, or Specification B 115, or Specification B 170 Copper of special qualities, forms, or types. as agreed 5 Annual Book of ASTM Swvdrds, Vol O02 ‘Amat Rook of ASTM Snundord, Wal 0808 "fava rn the National Tesh Incrmation Serv Ra, Splagield VA 22161, 5085 Port Royat the end of this standard.@ Bas ‘upon between the manufacturer and the purchaser and that will, conform to the requirements prescribed in this specification may also be used, 5.3 The rod coils shall be furnished in continuous lengths with or without joints, as ordered. 6. Chemical Composition 6.1 Each cod type shall conform to the chemical composi- tion requirements prescribed in Table 1 for the type of copper ordered (Section 4), 62 By agreement between the manufacturer and the pur- chaser, the addition of silver up to an average of 30 troy o2 per short ton of copper (0.10 %) will be considered within the specification, copper including silver in the chemical analysis, With no individual silver analysis to exceed 35 troy oz per short ton (0.12 %). In the case of oxygen-free silver-bearing coppers, the designation OFS (oxygen-free, silver-bearing) will be used as shown in Classification B 224 and will include the UNS numbers C10400, C10500, and C10700 as defined by the agreed silver content ‘633 Silver-bearing tough-pitch copper corresponds 10 the designation STP (ilver-bearing tough-pitch) as shown in Classification B 224 and to coppers having UNS numbers €11300, CL1400, C11500, and C1600. 64 Oxygen Content—Oxygen-free copper as described herein is defined as a copper containing not in excess of 0.0010 % (10 ppm) oxygen and produced without the use of metallic or other deoxidizers. 7. Physical Property Requirements TA Elecirical Resisrivity—Resistivity of the copper in the annealed condition (See Note X11) shall not exceed the following values at 20°C: TABLE 1 Chemical Composition* ‘UNS Number Ciro cvotco —_cuoaa 01000 coppor type ETP® GFE OF Gi Copper.min 9860%" oaG%F gaan? gag0K" ine! Sir ine Sher ppm pom bpm Pom ets, max 2 ? Selena 2 3 Biemah me to to Group al mex ‘sie max 5 5 Fi mee 5 2 sae mae 5 5 on. ne wo 0 New max © ig Sat max rn) ‘iver, ax as Ceygen 400-059 Smex 10 max Maram alowabie 65 carn, ax ‘ Phosparus, max 3 2re, max ; Manganese. mex ds rom @ V8 Grade 1 copper or aquivalont Fem 8170 Grace | capper oF ean ‘Fem 8170 Grade 2 Spper oF savant by eforonoe, Soe {2.12 and 181 See 13.1% ‘not nang oxen, Type of Copper Resistivity, max, at 20°C Annealed, 0+ gin 0.15176 (101.00 % IACS min) 0.15328 (100.00 LACS min) UNS €10100 only All others 8, Mechanical Property Requirements 8.1 Tensile Tests—Rod finished by hot working or anneal- ing shail have a minimum elongation of 30% in 10 in. (250 mm). (Note X1.2 and Test Methods E 8.) 8.2 Torsion Tests—If torsion tests are requested, refer to Note X1.3. 8.3. Embrinlement (Bend) Tes: 83.1 A test to reflect propensity towards hydrogen em- brittiement shall be performed only on oxygen-free copper, 8.3.2 The specimen shall be tested in accordance with 13.6 and Specification B 170, 8.3.3 The specimen, prepared and tested from the OFE (oxygen-free electwonic) copper (UNS-C10100) listed in Table 1, shall withstand without breaking into two pieces, a minimurn (of ten (10) reverse bends. 8.3.4 The specimen, prepared and tested from the OF (oxygen-free) copper (UNS-C10200) listed in Table 1, shall withstand, without breaking imo two pieces, a minimum of eight (8) reverse bends, 84 Annealabitity—Annealability is not a requirement of this specification. However, a discussion will be found in Notes X1.4-X1.6. 9. Other Requirements 9.1 Surface Oxide—The surtace oxide film thickness shall be determined in accordance with 13.5. 9.1.2 Total thickness of the copper oxide film on cleaned copper rod or angesled shaved rod or cold-finished rod shail rnot exceed 1000 A (10-7 m), 9.1.3 The residual oxide film thickness on as-shaved rod does not need to be specified. 9.14 A surface oxide requirement is not necessary for tod ordered uncleaned. 9.2 Diameter—The diaeneter of the rod at any point shall not vary from that specified by more than the amounts prescribed in Table 2, 10. Workmanship, Finish, and Appearance 10.1 The rod shall be free of defects, but blemishes of @ nature that do not interfere with the intended application are acceptable, 11, Sampling 11.1 This procedure shall be used in case of dispute between the manufacturer and the purchaser, TABLE 2 Permissible Variations in Diameter Nominal Diameto, fr Pormiosbe Vatson, ie ea) Foe (05m) ‘010 (025) (Ove (64) fo An. 18 me) 2005 (2038), (Over % (18) 201.0, 25 mm el 20020 (#051) ‘Over 1.0 125) to 436 in (5 mmm} in 210.090 (+0.78),& Bag 11.2 One sample shall be taken from each 200 000-16 (90 000-kg) lot for resistivity, elongation, surface oxide, em- brittement (bend) test, and chemical analysis, 11.3 When a cast refinery shape has been chemically analyzed and converted into rod without remelting, further chemical analysis shall not be required. 12, Number of Tests and Retests 121 Tests: 12.1.1 Chemical Analysis—Chemical composition shall be determined as per the element mean of the results from atleast two replicate analyses of the ssmple(s) 12.1.2 Other Tests. 1212.1 Electrical Resistivity, Elongation, and Surface (Oxide—Results shall be reported as the average obtained from fat least two test specimens, each taken from @ separate test piece where possible. 12.122 Hydrogen Embrintement Test and Microscopical Examination—All specimens tested must meet the require- ments of the specification, 12.2 Retests 12.2.1 When requested by the manufacturer or suppl retest shall be permitted when results of tests obtained by the purchaser fail to conform to the requirements of the product, specification. 12.2.2 The retest shall be as directed in the product speci- fication for the initial test except the number of test specimens shall be twice that normally required for the specified test 12.2.3 All test specimens shall conform to the product specification requirement(s) in retest. Failure to conform shall be cause for rejection 13, Test Methods 13.1 Chemical Analysis: 1B.L.I In case of dispute, determine copper content of the coppers other than UNS-C10100 and UNS-C11040 in Table 1 in accordance with Test Method E53. 13.1.2. Analytical method for determining impurity levels of coppers listed in Table | shall be in accordance with Specifi cation B 115, 13.1.3 Calculate copper content of UNS-C10100 and UNS- C11040 types by subtracting from 100% the total impurity concentration determined. The impurity total for U is defined as the sum of sulfur, silver, lead, arsenic, antimony, iron, niekel, zinc, phosphorus, selenium, tellurium, manganese, cadmium, and oxygen present in the sample, The impurity total for UNS-C1100 is defined as the sum of sulfur, silver. lead, tin, bismuth, arsenic, antimony, iron, nickel, selenium, tellorium, and oxygen present in the sample. 13.14 The test methods annex of Specification B 170 should be referenced for the oxygen-free coppers. Test Method E478 should be referenced for the determination of silver- bearing alloys permitted under this specification. 13.1.5 Oxygen content is determined on cleaned copper samples using a suitable laboratory apparatus or a commercial instrument designed specifically for this purpose. An ASTM ‘method has not been developed. 13.2 Blongation—Determine the elongation as the perma- nent increase in length, caused by breaking of the rod in recower | | Sauces) Paine aie sa ae ern FIG. 1 Schematic tlustration Showing Eletrotyic Redution ‘Test Method tension, measured between gage marks placed originally 10 in (250 mm) apart upon the test specimen (Note X1.2). The fracture shall be between gage marks and not closer than 1 in 25 mm to either gage mark 133 Blecirical Resisviy 133.1 Ache option of the manufacturer, electrical resistiv- ity may be determined in accontance with 13.32 oF 133.3 However, in case of dispute, 133.2 shall apply. 13.3.2 Make resistance measurements (Note X13) on speci- 1mens of the rod after cleaning and processing down 10 & diameter of approximately 0.080 in, (2.0 mm) and annealing at approximately 932°F (500°C) for 30 min. Other equivalent annealing methods may De used. Test specimens provessed to 4 diameter other than 0.080 in. may be used if agreed upon beween the manufacturer and the purchaser 13.33 Resistance measurements may be determined on specimens of the rod alter cleaning, but without further processing and anneating. However, in the event of failure of 4 rod specimen to conform to the criteria of 7.1, 2 retest is permitted using the procedure of 13.32 13.34 Determine the electrical resistivity in accordance with Test Method B 193 except that when the option of 13.3.3, is elected, the plus and minus tolerance for the cross-sectional tea as specified in Test Method B 193 shall not apply 134 Diameter—Measure the diameter of the rod with & suitable measuring device, micrometer, caliper or other, read- ing at least to the nearest 0.001 in, (0.02 mm). 135 Surface Oxide 135.1 Determine the thickness and type of unreduced oxide films remaining on the surface of rod after cleaning by an electrolytic eduction method, This testis performed by reduc- ing the surface oxide(s) to copper in an electrolytic coll® As shown by the schematic diagram in Fig. 1, the fest sample i, ‘made cathodic with respect to an anode, which shall be made from a platinum wire or an equivalent inert electrode. Supply current from a d-e power supply or a coulometer. Although 10 "Fora description of simi, yt allemative sanded poocedar to denne ‘arts on coupons expo oevitnmentl as, ee "Mrng Esk ‘mera Tes by Caulomacc Redaction of Metis Coe Samples fours! of ‘ening ne Evan, 1989. 9p. 357-367, ASTM. Ais eter fo “The Role of Surtace Orde an ty Messiramen inthe Capper Wire Int.” Wie Joo March 1977, 59. 50-37@ Bas tmilligmpere (mA) isa typical value of current, itis best to have ‘equipment capable of operating in the range of | to 20mA. The electrolyte shall be 2 0.1M solution of sodium carbonate and shall cover at least 4 in, (101.6 mm) of the test sample. Before resting, clean each rod sample of oil or grease using acetone or an equivalent solvent. 13.5.2 Each of the oxides found on copper, namely cuprous and cupric, are reduced sequentially to copper at different reduction potentials, and the voltages are to be recorded against time during the entire test. When the individual reactions between the oxides and hydrogen ions are complete, gaseous hydrogen is evolved and may be seen visually at the surface of the copper rod sample. 13.5.3 A typical curve of voltage versus time is presented in Fig. 2. Cuprous oxide is reduced initially. When this reaction is ‘complete, reduction of the cupric oxide occurs at a higher voltage. 13.54 Calculate thickness of each oxide present as follow: rt Sd Fn o where: T= oxide thickness, em: 1 = current, A; lime of reaction, s: ‘molecular weight of the oxide, g; surface area of immersed sample, em?: oxide density (6.0 gem? for CuO and 6.4 gem? for Cu0y; = Faraday constant, 96 500 C; and n= hydrogen equivalent (2), 13.6 Hydrogen Embrittlement Susceptibility: 13.6.1 Draw the specimen of oxygenfree copper rod into 1 M s a F As sussies seGin'To FORMS vours Tie FOR CUO TIME SCALE —> FIG. 2. Typical Vollage-Time Curve for the Reduction of Copper Oxide Films mm) diameter wire. Then anneal it in an ‘atmosphere containing aot less than 10 % of hydrogen for 30 min at 1560 + 45°F (850 * 25°C) and cool quickly in the ‘same atmosphere, or without undue exposure to air, quench into water. Make sure that each specimen undergoes the bend test in accordance with 13.6.2 13.62 Lightly clamp the specimen (13.6.1) between jaws ‘with edges having a radius of 0.200 in, (5.1 mm). Then bend it by hand over one edge of the jaws through an angle of 90° and retum it to its original position. This constitutes a second bend, ‘Make each successive bend in the opposite direction from the previous bend (see Test Methods B 577), 14. Significance of Numerical Limits 14.1 Calculated values shall be rounded to the nearest unit in the last right hand significant digit used in expressing the limiting value in accordance with the rounding-off method in Practice E29. 15. Inspection 15.1 All inspections ancl tests shall be made at the place of ‘manufacture unless otherwise agreed upon between the manu- facwurer and the purchaser at the time of purchase. The manufacturer shall afford the inspector representing the pur- cchaser all reasonable facilites to satisfy him that the material being furnished is in accordance with this specification 16, Rejection and Rehearing 16.1 Rejection: 16.1.1 Product that fails to conform to the requirements of the product specification may be rejected. 16.1.2 Rejection shall be reported to the manuf ssopplier, promptly and in writing. 16.1.3 In case of disagreement or dissatisfaction with the results of the test upon which rejection was based, the ‘manufacturer or supplier may make claim for 2 rehearing. 16.2 Rehearing—As.a result of product rejection, the manu- facturer or supplier may make claim for retest © be conducted by the manufacturer or supplier and the purchaser. Samples of the rejected product shall be taken in accordance with the product specification and tested by both parties as directed in the product specification, or alternatively upon agreement by both parties. an independent laboratory may be selected for the tests using the test methods prescribed in the product specifi- cation, 17. Certification 17.1 When specified in the contract or purchase order, the purchaser shall be furnished certification that samples repre senting each lot have been either tested or inspected as directed in this specification and the requirements have been met. 18. Test Report 18.1 When specified in the contract or purchase order, a report of test results shall be furnished, 19, Packaging and Package Marking 19.1 Package size shall be agreed upon between the manu= facturer and the purchaser and shall be stated in the order.Bao 19.2 The rod shall be packaged and protected against damage from normal handling and shipping as is consistent ‘with good commercial practice 19.3 Individual coils without joims and with a net mass seater than 3.000 Ib (1400 kg) shall be marked or otherwise :dentified with the following: 19.3.1 Coil production number, 19.3.2 Net weight, and 19.3.3 Manufacturer's name, brand, or trademark. 19.4 Marking for coils other than described in 19.3 shall be ‘agreed upon between the manufacturer and the purchaser. 20, Keywords 20.1 copper redraw rod; electrical conductors; oxygen-free copper; tough-pitch copper SUMMARY OF CHANGES ‘Committee B-S has identified the location of selected changes to this standard since the last issue (B49 — 92) that may impact the use of this standaed. (2) The Referenced Documents section has been updated. (2) The following sections have been acided: Terminology; Significance of Numerical Limits; Test Report, Rejection, and Rehearing; Number of Tests and Retests; Keywords. (Nonmandatory Information) X, EXPLANATORY INFORMATION Nore X1.1—Relationships that may be useful in connection with the values of electrical resistivity resribed in tis specification are showin Table 3, Resistivity units are based on the Intemational Anvealed Copper Standards (IACS) adopted by [EC in 1913, whichis U/S8 1+ mm*/m at 20°C for 100 % condicvity, The value of 2017 241 = wm/m andthe value of 0.15328 01+ pm" at 20°C ate, respectively, the international equivalent of volurae and weight resistivity of annealed copper equal (0 five signsticant figures) to 100° conduetvty. The late term means thet a copper wire Im in length and weighing 1 g would havea resistance of 10.153 28 0. This isequivalent to a esistvty Wadd of 875.20 9 mie which signifies the resistance of a copper wire | mile in length weighing IB. 118 also equivalne, for example, co 1.7241 Cem of length of @ ‘copper bar {eit in eoss section. A complete discusion of tis subject is contained in NBS Handbook 109. The ase of five significa Figures in ‘expressing resistivity dees not imply the need for grester accuracy of measurement than that specified in Test Method B 193. The use of five Significant figures is equired for reasonably accurte reversible conve sin from one set of resistivity nits to another. The equivalent resistivity values in Table 3 were derived from the fundamental TEC value (188 0 < mim*/m) computed to Seven significant figures and then rounded to five signitican igs. ‘Nore X12—In general, tested values of elongation are reduced with increased speed of the moving head ofthe testing machine in the tension testing of copper wite and ra, In the case of tests on soft or annesled ‘copper rod, however the effects of speed of esting are not pronounced. TABLE Equivalent Resistivity Velues* Condacivey at 60°F (OO), ACS 70000 Taio Ome 37520 060.53 a-gm swe a te176 foe mit soars so. ra ‘owas ‘gor7070 atin dere gera07 cm ira 37070 “The equivalent assy values for 00% JAC (ah Sapper were Sah computes tom Bye fundamental IE valve (58 f= nin) eg eanvesin factors each accurate oalleas seven agian axes {es of oft od made at speeds no greater than 12 in min (300 mavinin, the values obtained for elongation are no affected to any practical extent (Gee Test Methods), [Nove X1.3—Torsion tests are widely used by producers and users. Because ofthe uncerain corelation with performance, and te sbjectve aspect of iterpretation, these tests should enly be used a an indicator of in-house process contd. Therefore, no standardized tet is recommended Nore X1.4—Annealabiiy by Hardness Tets—A ro sample of sit. able length shal be eut from each end ofa coil ot. The aroceived sample shall be cold rolled toa lt setion, 30 that the thickness is equal to 30 ofthe oxiginal ro diameter. No edge rolling is required. The Maoned copper sail be heated at 327 = 2°F (275 = 1°C) fr 1S min in a constant temperature bath and quenched immediately into water at ambient temperature. Other temperatures and times may be vsed by special agreement between the manufacturer and purchater, Hardness shall be measured along the center Tine of the annealed. specimen using the Rockwell F scale, in accordance with Test Method E 18. [Nora XL$—Annealability by Torsion (Spiral Elongation —The spiral clongaton fst deszribed lerewith is used only for testing high conduc tivity copper that is sampled atthe rod stage and does not des the ualty of copper wire selected at later sages of commercial processing. Copper wire 35 intially given a low tmporature anneal under tight controlled conditions, subsequently wound ito a epra helical configu tation) under tensile foad, and then sretched! axially by a weight of specified mass. The change int lenght measured aller the weight is removed, and ibe spiral has relaxed, is considered 3s 9 messne of softes. Rod Treament—A rod sample of suitable length shall be cut feo the end ofa colt, and if necessary, reduced to a diameter of either 0.25 in. +0020 0.010 (635 mm +050 ~0.25) or 0.315 = 0.015 in. (6.00 = 0,40 min) by cold drawing. This sample shall either be annested or not annealed according 10 the following circumssances: @ Nonaealing treatment wil be performed ithe coppers processed according Io a specific manufacturing Schedule (6) The sample shall be subjected 19 an annealing treatment if is Uesred to compare samples produced vi different manufaetuting routes, ‘Under these citcumstances, the red sample shal be annealed under norms@ B49 atmosphere for 1h at 700°C + 20 (1286 to 1328°F) and then quenched imo wster or a due (10% wy) sulfuric acid solution et ambient temperature. Copper oxide scale shall be removed in 10 % vv volume Pet volume, sulfuric acid bath and thoroughly washed fo remove loose scale or adhoring copper dst. Preparation of Wire for Spiral Elongation Test—~The tod sample shall, bbe drawn into a 2.00-nm (0.080 in. + 0.01) diameter wige in a Series of passes, each of which shall edoce the cros-sectional area of the conductor by 20 1025 & Particular care should be ten t avoid excessive heating ofthe copper ‘daring drawing. For example, the wire shal either be allowed t0 coo! for Sin between passes or quenched to ambient lmmpeature after each pas, {mn addition, draseng speed should not exceed 60 m/min (200 f¥min), and the drawn Wire shall be wound into a coil having a minimum diameter of 200 mm. fer drawing. a coil of the wire shall he formed ty winding the ‘conductor around a mandrel having a minimum diameter of 200 nm (7.87 in}. The copper col shall then be eemoved from the mandrel, heated for 2 hat 392= (°F (200 05°C), in a constant femporatuce bath, and ‘cooled ieumediaely to ambient temperature “Temperate ofthe copper wire must be Kept nic and measured ‘ite azcaraely. Since good temperature contre is extremely important. thermocouples stould be placed at suategic loeations toughout the annealing device. It is recommended that am B-mmiameter day tod sample be formed into a 200-mm-iameter ring and placed inthe constant ‘temperature bath atthe sane position normally occupied by the test wire Using thermocouple embeded inthe ro to 2 depth equ 9 the radi, femperature should reach the annealing temperature within = S-min period, ‘est Procedures~A \400-mmlong test sample is cut from the an- realed coil of wire, Using an indelible marking tool, a 1000-mm ange length is marked oser the midlength of the copper wite. One end ofthe test sample is firmly secured tothe end ofa polished mandeel whose axis |s horizontal und which has a diameter of 20 = 01 mem, A 2.240-kg foad Js sespended fow the fee end of the wire, thereby inducing sires of 7 MPa (1000 ps). The wire shall be wound into a spiral by rotating the ‘mandrel ats speed of approximately 50 fin, taking special care that ‘each tara of the spiral touches the preceding one, that the turn are nat presed ito place, that handling is Kept to minimum, and thatthe wie js wound in the same diretion thi i was previously cae. Although the length between gage marks onthe spiral is approximately 28 mm, this stance shall be measured to the nearest J rm and recorded 2 the intial value “” ‘The spizal of wire shall hen he removed from the mance, carefully fastened atone end, and loaded axially at the other (wee) end with the same 2240 kg weight 2s that used in the aforementioned coil winding operation ‘The weight shall be supported inilly ih a platform an loaded onto ‘he spiral uniformly end smoothly by citer of two methods, namely: (a) lowering the platform supporting the Weight or (8) rising te upper end ofthe spiral at arate such that the steiching ofthe spiral does not exceed 20 mun ‘After | min of free suspension, che weight is manually removed ia very careful manner andthe clongtted spirals allowed elas by plating iton stable for an additional period of ! min, Note that the load i no to be removed by either raising the platform or lowering the upper end ofthe spiral. The extended length of the spiral between guge marks shall be measured to the nearest | snd called “1,” The spiral elongation value. in millimetres, is eaeuleted asthe diference I, — ly ‘This same procedure shal be repeated on two addtional spirals of wite fom the same col, and the average value obtained from thice separate spirals shall be referred co as the “Spiral Elongation Number” Nore X1.6—Anncalabii (General}Alhoush five different basic types of est methods have been reported in the iteature for measuring the annealabilty of wirebar or rod, numerous variations and permubations ‘exist. For @ more thorough description of these tes, refer 0 the Journal (of Testing and Evaluation” Inasnich a hardness and torsional ras ments are frequently used, detailed procedures ate contained in Notes X14 and X15. Softening values for low temperature annealing copper and for other types of copper rods, if requested, shall be decided spon between the producer and the user. * it Bland B2 Tsk Group. "The Ansty Testing of Copper” Jounal of Teutng ond Bvotuaen, Vol 1 No I, ASTM, 1973, ANNEX Mandatory Information AL. SAMPLING PLAN Al.1 This procedure shall be used in case of dispute between the manufacturer and the purchaser. Al.2 One sample shall be taken from each 200 000b (90 000-kg) lot for resistivity, tensile elongation, annealabilty, surface oxide, embritdement (bend) test, and chemical analysis AL.3 When a cast refinery shape has been chemically analyzed and converted into rod without remelting, further chemical analysis shall not be required The amonean Soci for Testing and Matar thee no posion repecting the acy of eny owen rit assoriea in connacton ‘itn any tem marwoned in ths sander. Users of hs standard are exressy aaed ha dtrmngbon oe VaNy of Oy Soe Datet ris. end the ask of ingerent of such is, are entry ther oun rapes, ‘This standards subject revision at any ine by te responibe lecnical commits and must De rexiowed every fe years and {Yootrersed eer eeporovad or wntrawn, Your comments ae led ater rovson oe tandat orf adorn asaae ‘and seu be adresse fo ASTM Hesdguariors. Your corners wil rcalve carl consiseaton sta mootng othe sponse tecrica commie, which you may abana. ou tel ha our cormants ave Mo eceved @ fa Moar ou shoud Woke your ‘ows kronm fhe ASTM Gonmtce on Sunes, 100 Bar Hara Bre, West Conshohocken, Pa 13228