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Thermodynamic characterization of single-stage spray

dryers: Mass and energy balances for milk drying


Cleuber Raimundo da Silva, Evandro Martins, Arlan Caldas Pereira Silveira,
Moisés Simeão, Ariel Lessa Mendes, Italo Tuler Perrone, Pierre Schuck,
Antonio Fernandes de Carvahlo

To cite this version:


Cleuber Raimundo da Silva, Evandro Martins, Arlan Caldas Pereira Silveira, Moisés Simeão,
Ariel Lessa Mendes, et al.. Thermodynamic characterization of single-stage spray dryers: Mass
and energy balances for milk drying. Drying Technology, Taylor & Francis, 2017, 35 (15),
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Drying Technology
An International Journal

ISSN: 0737-3937 (Print) 1532-2300 (Online) Journal homepage: http://www.tandfonline.com/loi/ldrt20

Thermodynamic characterization of single-stage


spray dryers: Mass and energy balances for milk
drying

Cleuber Raimundo da Silva, Evandro Martins, Arlan Caldas Pereira Silveira,


Moisés Simeão, Ariel Lessa Mendes, Ítalo Tuler Perrone, Pierre Schuck &
Antônio Fernandes de Carvalho

To cite this article: Cleuber Raimundo da Silva, Evandro Martins, Arlan Caldas Pereira Silveira,
Moisés Simeão, Ariel Lessa Mendes, Ítalo Tuler Perrone, Pierre Schuck & Antônio Fernandes de
Carvalho (2017): Thermodynamic characterization of single-stage spray dryers: Mass and energy
balances for milk drying, Drying Technology, DOI: 10.1080/07373937.2016.1275675

To link to this article: http://dx.doi.org/10.1080/07373937.2016.1275675

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DRYING TECHNOLOGY
https://doi.org/10.1080/07373937.2016.1275675

none defined

Thermodynamic characterization of single-stage spray dryers: Mass


and energy balances for milk drying
Cleuber Raimundo da Silvaa, Evandro Martinsa, Arlan Caldas Pereira Silveiraa, Moisés Simeãoa,
Ariel Lessa Mendesa, Ítalo Tuler Perronea, Pierre Schuckb, and Antônio Fernandes de Carvalhoa
a
Food Science and Technology Department, Universidade Federal de Viçosa, Viçosa, MG, Brazil; bSTLO, Agrocampus Ouest, INRA,
Rennes, France

ABSTRACT ARTICLE HISTORY


Spray drying is an efficient unit operation applied in food drying that demands a high amount of Received 30 August 2016
energy compared to vacuum evaporation and membrane filtration. The objective of this work was Revised 19 December 2016
to present a mathematical model-like basis for the construction of mass and energy balances. For Accepted 19 December 2016
this purpose, two lab-scale single spray dryers in milk drying with different evaporative capacities KEYWORDS
have been used as example. The values of the absolute humidity, mass and energy losses, Energy consumption; mass
energetic specific consumption (ESC), and the efficiency of the process were obtained by and energy balances;
calculations developed in this work. The mathematical model was valid for the evaluation of mass mathematical modeling;
Downloaded by [Pierre Schuck] at 04:02 21 August 2017

and energy losses, and it allowed us to compare the efficiencies of spray dryers with different spray drying
designs. From this model, it is possible to compare different drying processes and dryers.

Introduction Although spray drying is largely applied to the


manufacturing of dried dairy products on an industrial
In 2014, the global milk production was 802 million
scale, the energy consumption of this technique is still
tons, with an increase in 3.3% compared to the
considerable (1,000–2,000 KWh t 1 removed water).[4]
production in 2013.[1] Since milk is perishable, the
Thus, the appropriate operation of spray dryer should
surplus production is designated for the fabrication of
be performed to reduce the cost of production and
dehydrated dairy products to improve its conservation
improve the quality of milk powder.[8,10–12] Sustainabil-
over time. However, in 2014, approximately 50 million
ity issues and reduction of energy costs are the next
tons of milk were designated for the production of
challenge for the dairy industry.[13,14]
whole milk powder.[1]
The final cost of the milk powder formulas is
In freeze-drying, the energy consumption is from
associated with the losses (mass and energy) that occur
5,000 to 10,000 KWh t 1 of removed water and in drum
during the drying process.[15] The mass losses are
drying is from 300 to 1,000 KWh t 1 of removed
related to the adherence of milk particles on the
water.[2–5] Although there are advantages to both tech-
internal surface of the drying tower or to transport of
niques, spray drying is still the most used in the dairy
the particles by the air flow. In this study, the
industry for milk powder production. The energetic
thermal energy losses can be estimated as the sum of
consumption of spray drying is approximately 10-fold
dissipated energy through the equipment surface and
lower than that of freeze-drying, and contrary to the
the energy not used in the conversion of water to
drum drying technique, the product does not reach high
vapor.
temperatures during water evaporation.[6,7]
The mass and energy balance is a mathematical tool
In spray drying, milk is pulverized in droplets inside
that allows the evaluation of the mass and energy losses
a drying tower where the product comes in contact with
in the process of spray dryer dehydration. In addition,
heated air. Due to an increase in the surface contact
this tool makes possible the estimation of the produc-
between the milk and air, water is evaporated quickly
tion cost, the comparison of the efficiency of different
without excessive heat treatment, during this
equipment, and the determination of the amount of
operation.[8] Thus, milk powder with low water activity
energy necessary to evaporate 1 kg of water from the
(aw ¼ 0.18–0.22) is formed without excessive losses of
product. The application of the mathematical tool in
the nutritional and sensorial characteristics of milk.[9]

CONTACT Antônio Fernandes de Carvalho afc1800@yahoo.com Food Science and Technology Department, Universidade Federal de Viçosa,
36570-000, Viçosa, MG, Brazil.
© 2017 Taylor & Francis
2 C. R. DA SILVA ET AL.

dairy industry ensures the better control of the dairy different positions of the section of straight cylindrical
powder technology.[16,17] ducts.[18]
In this paper, we present a mathematical basis for
construction of the mass and energy balance for the
milk drying process using single-stage spray dryer Validation of mathematical models and
equipment. It aims to create a protocol that will evaluation of optimal efficiency of
work as a support for industries that plan to operation of spray dryers
evaluate the production efficiency of their spray
Evaporation of water
dryers. For this, we will use as an example the milk
Water heated at 40°C was injected into SD1 or SD2
drying in two lab-scale spray dryers with different
where it was evaporated in the presence of heated inlet
evaporative capacities.
air at 165 � 5°C. The flow rate of the water was adjusted
to maintain the outlet air temperature at approximately
90 � 3°C. The process was executed with three
Materials and methods repetitions on different days.
The experiments were performed using two lab-scale
single-stage spray dryers. Table 1 summarizes the Drying of milk
principal characteristics of each equipment. Concentrated whole milk (40% dry material) at 40°C
The relative humidities and temperatures were was injected into SD1 or SD2 where it was dehydrated
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measured as presented in the scheme (Figs. 1–3) using with inlet air at 165 � 5°C. The flow rate of milk was
a thermohygrometer (Rotronic, Hydropalm). The air adjusted to maintain the outlet air temperature at
velocity measurements were performed using an approximately 95 � 3°C to SD1 and 90 � 3°C to SD2.
anemometer (Air Velocity Transducers, model TSI All experiments were performed with three repeti-
Alnor 84455) whose catheter was introduced in five tions on different days.

Table 1. Characteristics of spray dryers.


Evaporative capacity
Spray dryer Atomizer (kg water · h 1) Superficial area (m2) Model Fabricator
SD1 Pressure nozzle 1 0.51 MSD 1.0 Labmaq, Brazil
SD2 Rotating disk 20 7.54 Minor production Niro Atomizer, GEA, Germany

Figure 1. Scheme of single-stage spray dryers. SD1: Labmaq, Brazil; SD2: Niro Atomizer, GEA, Germany.
DRYING TECHNOLOGY 3
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Figure 2. Balance of mass–energy using water evaporation as reference.

Figure 3. Balance of mass–energy using milk.


4 C. R. DA SILVA ET AL.

Results and discussion and (2), Fdry,air can be written as:


Balance of mass–energy using water Fd;air ¼ Fh;air Mwa;out
evaporation as reference 1
ð3Þ
Fd;air ¼ Va;out Aout qð1 þ AHout Þ
Mass balance for water evaporation: Validation
of the mathematical model The mass of water presented in the inlet air
To create a mathematical model for the evaporation (Mwater air,in; kg h 1) is the product of Fdry,air and the absol-
process in spray dryers, the simpler condition will be ute humidity of inlet air (AHin, kg water kg dry air 1):
tested. Before promoting the drying of dairy products,
Mw;in ¼ Fd;air AHin
simple water evaporation will be performed. This means ð4Þ
1
that in the equipment inlet, water will be injected, and Mw;in ¼ AHin Va;out Aout qð1 þ AHout Þ
only vapor will be recovered in the outlet of the spray
The total water mass entering the equipment
dryers.
(Mtotal water,in; kg h 1) is calculated by addition of the
During the process of water evaporation, all water
water injected into spray dryer (Mwater, inj; kg h 1) and
entering the equipment is assumed be converted to
the amount of water carried from the inlet air
vapor, i.e., no mass loss occurs. Thus, the mass balance
(Mwater air, in; kg h 1):
under this condition has a finality to verify the accuracy
of the mathematical equations and ensure that the Mtw;in ¼ Mw;inj þ Mwa;in
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measurements with the thermohygrometer and � �


anemometer (temperature, relative humidity, and air Mtw;in ¼ Mw;inj þ AHin Va;out Aout qð1 þ AHout Þ 1
velocity) are consistent. ð5Þ
The first step of mass balance consists of calculating
In the outlet, all water mass evaporated is eliminated
the flow rate of humid air (Fhumid air; kg air h 1), which
by air in the vapor form. The total mass of evaporated
is similar in both the input and output of the equip-
water (Mtotal water,out; kg h 1) is determined by
ment. However, this parameter is preferably calculated
combination of Eqs. (1) and (2):
from the outlet data, since in some spray dryers, the
air can enter by small slots or holes close to the Mtw;out ¼ Mw;out ¼ Fd;air AHout ð6Þ
atomizer, thus resulting in underestimation of the data. 1
Fhumid air is calculated from the air velocity measured Mtw;out ¼ Va;out Aout qAHout ð1 þ AHout Þ ð7Þ
by an anemometer in the outlet (Vair,out; m h 1), The final step for mass balance (Δmass; kg h 1) is
the area of the transversal section of outlet tubing performed by subtracting the total of the water exiting
(Aout; m2), and the air density (ρ; kg m 3): the spray dryer (Mtotal water,out; Eq. 7) and the water
total mass entering the equipment (Mtotal water,in;
Fh;air ¼ Va;out Aout q ð1Þ
Eq. 5), thus:
where ρ is assumed be constant and equal to 1.0 kg m 3.
The second step consists of determining the mass of Dmass ¼ Mtw;out Mtw;in ð8Þ
water contained in the air (Mwater,air out; kg h 1). Mwater, Table 2 shows the parameters measured in the spray
air out can be estimated from the absolute humidity of dryers during water evaporation and mass balance of
the outlet air (AHout; kg water kg dry air 1) and the flow process.
rate of humid air (Eq. 2).[19] Using the mathematical treatment presented above,
1 the mass balance (Δmass ¼ 0) is according to the
Mwa;out ¼ Fh;air AHout ð1 þ AHout Þ ð2Þ
theoretical assumption for water evaporation. In other
The dry air flow rate (Fdry,air; kg h 1) is calculated by words, the mathematical model, as well as the measure-
subtraction of the flow rate of humid air and the water ments performed with the anemometer and the thermo-
mass contained in the outlet air. By combining Eqs. (1) hygrometer, was consistent with the reality of the drying

Table 2. Inlet and outlet parameters used in mass balance for water evaporation.
Inlet parameters Outlet parameters
AHin* Mwater,inj* Mtotal water,in Aout AHout* Vair,out* Mtotal water,out Δmass
Equipment ðkgwater � kgdry1 air Þ (kg h 1) (kg h 1) (m2) ðkgwater � kgdry1 air Þ (m h 1) (kg h 1) (kg h 1)
SD1 1.63 � 10 2 8.30 � 10 1 1.69 � 100 9.62 � 10 4
3.20 � 10 2
5.65 � 104 1.69 � 100 0.00
SD2 1.34 � 10 2 7.68 � 100 1.27 � 101 7.24 � 10 3
3.39 � 10 2
5.35 � 104 1.27 � 101 0.00
*Measurement performed in triplicate with standard variation inferior to 5%.
DRYING TECHNOLOGY 5

procedure. In our case, the mass balance was equal to By substitution of Eqs. (12) and (13) into Eq. (9), the
zero, but some variations can be found due to errors total energy entering the system can be understood as:
in measurements and numeric rounding.
et;in ¼ ½Ta;in ð1:01 þ 1:89AHin Þ þ 2500AHin �
ð14Þ
½Va;out Aout qð1 þ AHout Þ 1 � þ Mw;inj Cpw Tw;inj
Energy balance for water evaporation
Since the water is in a completely free state, meaning The total outlet energy (εtotal,out; kJ h 1) is deduced
that it is not linked to any substrate, the energy balance analogously to that demonstrated for εtotal,in using the
has a finality, permitting the determination of the outlet data. Therefore, εtotal,out can be written as:
minimal energy consumed by each equipment. This
et;out ¼ ea;out þ ew;out
approach allows a comparison of the energetic
performance of spray dryers with different evaporative et;out ¼ ½Ta;out ð1:01 þ 1:89AHout Þ þ 2500AHout � ð15Þ
1
capacities and designs without the interference of the ½Va;out Aout qð1 þ AHout Þ � þ Mtw;out Cpw Ta;out
properties of a food matrix. In food, the water may be
linked or partially linked to the main food components. where Mtotal water,out(kg h 1) denotes the mass of water
This water does not act as a solvent; rather, it presents in the vapor form.
resistance to mechanical strength in addition to low Substituting Eq. (6) into (15) yields:
molecular mobility and different dielectric properties et;out ¼ ½Va;out Aout qð1 þ AHout Þ 1 �
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of free water, thus making the drying process more


difficult.[20] � ½Ta;out ð1:01 þ 1:89AHout Þ þ AHout ð250 ð16Þ
In addition to mass balance, in the energy balance, þ Cpw Ta;out Þ�
the calculation can be divided into energy entering
From the inlet (εtotal,in; Eq. 14) and outlet (εtotal,out;
and leaving the spray dryer.
Eq. 16) data, it is possible to determine the energy loss
The total inlet energy (εtotal,in; kJ h 1) is calculated
(εloss; in percentage):
by the addition of energy of hot inlet air (εair,in; kJ h 1)
� �
and the energy of water entering the drying tower et;out
(εwater,in; kJ h 1): eloss ¼ 1 � 100 ð17Þ
et;in
et;in ¼ ea;in þ ew;in ð9Þ This parameter allows evaluation of the amount of
energy that is dissipated from spray dryer or simply
The energy of the hot air inlet (εair,in) is given by
wasted during drying process. Another parameter that
multiplication between the air enthalpy (Eair,in; kJ kg 1)
allows comparison of the drying efficiency of different
and flow rate of the air (from Eq. 3):
equipment is the (ESC; kJ kg 1 evaporated water),
ea;in ¼ Ea;in Fd;air ð10Þ which is defined as the amount of energy necessary to
evaporate 1 kg of water:[21]
where Eair,in is calculated from the temperature
et;in
(T°Cair,in) and the absolute humidity (AHin) of the inlet ESC ¼
air: Mtw;out
et;in ð18Þ
ESC ¼ � �
Ea;in ¼ Ta;in ð1:01 þ 1:89AHin Þ þ 2500AHin ð11Þ Va;out Aout qAHout ð1 þ AHout Þ 1
By substituting Eqs. (3) and (11) into (10), the εair,in The energetic efficiency of the process (εefficiency) can
can be rewritten as: be estimated by division of the ESC value (Eq. 17) by
the latent heat of vaporization of water (Lwater ¼
ea;in ¼ ½Ta;in ð1:01 þ 1:89AHin Þ þ 2500AHin � 2337.46 kJ kg 1):
ð12Þ
½Va;out Aout qð1 þ AHout Þ 1 �
ESC
eef ¼ ð19Þ
The second term of Eq. (9), i.e., the energy of water Lw
entering into the drying tower (εwater,in), is determined This allows an estimation of how much more
from the product of flow rate of water injected into energy was expended in relation to the theoretical value
spray dryer (Mwater,inj; kg h 1), specific heat (Cpwater ¼ (Lwater). The higher the value of εefficiency, the lower is
4.18 kJ · °C 1 · kg 1), and its temperature (T°Cwater,inj): the efficiency of drying process.
All parameters necessary to calculate the energetic
et;in ¼ Mw;inj Cpw Tw;inj ð13Þ loss (εloss), ESC, and the energetic efficiency of the
6 C. R. DA SILVA ET AL.

Table 3. Energetic balance for water evaporation.


Inlet data Outlet data
1
Equipment T°Cair,in* (°C) T°Cwater,inj* (°C) εtotal,in (kJ h ) T°Cair,out*(°C) εtotal,out (kJ h 1) εloss (%) ESC (kJ kg 1) εefficiency
SD1 1.63 � 102 4.00 � 101 1.12 � 104 9.12 � 101 9.89 � 103 12.24 6.70 � 103 2.87
SD2 1.70 � 102 4.00 � 101 7.98 � 104 8.82 � 101 7.51 � 104 8.76 5.93 � 103 2.55
*Measurement performed in triplicate with standard variation inferior to 5%.

process (εefficiency) are displayed in Tables 2 and 3 for of powder milk recovered (Mpowder; kg), its dry extract
1
SD1 and SD2. (DEpowder; kgsolid �kgconcentrated milk ), and the total time
The heat balance shows a difference between inputs of the drying process (t; h):
and outputs (εloss) of approximately 12 and 9% for � �
SD1 and SD2, respectively. This difference is related Mp TSp
Mts;out ¼ ð21Þ
to the heat loss from not insolated parts of equipment t
and probable errors of calculation and measurements.
The mass balance is calculated as the difference
Although SD2 shows a superficial area (7.54 m2) larger
between the amount of solids recovered after drying
than SD1 (0.51 m2), the noninsulated parts of each
(Mtotal solid,out; Eq. 21) and mass of solids injected into
equipment present 100 and 20%, respectively. Addition-
equipment (Mtotal solid,in; Eq. 20):
ally, SD2 shows the best value for ESC and εefficiency,
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indicating greater use of energy by this equipment. Dmass ¼ Mts;out Mts;in


The equipment (SD1 and SD2) presented high � �
Mp TSp ð22Þ
energy loss compared to industrial spray dryers, which Dmass ¼ Fmilk;inj TSm
t
present losses between 3 and 5%.[3]. In addition to the
heat isolation capacity, the size of equipment may In an ideal drying process, all solids entering into
influence the energy loss and efficiency.[21] system should be recovered after drying; however, in
milk drying, a considerable part of the powder is lost
Milk drying in the air flow or adhered to the drying tower. The mass
of milk powder lost (Mloss, in percentage) can be
In the previous section, the mathematical model and the calculated as
measurements performed using an anemometer and a � �
thermohygrometer were validated by mass balance. Mts;out
Mloss ¼ 1 � 100 ð23Þ
Furthermore, the ideal energetic operation of the spray Mts;in
dryers was evaluated using an energetic balance for
water evaporation. Substitution of Eqs. (21) and (22) into (23) yields:
In this section, the mathematical approach used for � �
1 Mp TSp
water evaporation in spray dryer will be used for Mloss ¼ � 100 ð24Þ
tFm;inj TSm
balance of mass and energy for milk drying.
Table 4 shows the inlet and outlet data necessary to
Mass balance for milk drying calculate the loss of mass for milk drying.
The total content of solids entering into drying tower The negative sign of Δmass indicates that part of the
(Mtotal solid,in; kg h 1) is given by multiplication between milk solids were lost during drying. Another relevant
the flow rate of concentrated milk (Fmilk,inj; kg h 1) and factor for mass loss is the dissipation of powder together
1
its dry extract (DEmilk, kgsolid �kgconcentrated milk ): with the outlet air, and this loss increases based on how
much finer the powder is. Lab-scale equipment
Mts;in ¼ Fm;inj TSm ð20Þ
produces finer particles than industrial equipment,
In the outlet, the amount of solids after drying and the spray dryers utilized in this experiment are
(Mtotal solid,out; kg h 1) is calculated from the amount compounds with a unique stage drying that increases

Table 4. Mass balance for milk drying.


Inlet data Outlet data
Equipment Fmilk,inj* (kg h 1) DEmilk*(kg kg 1) Mpowder* (kg) DEpowder* (kg kg 1) t* (h) Δmass (kg) Mloss (%)
SD1 1.24 � 100 3.83 � 10 1
2.92 � 10 1 9.55 � 10 1
6.67 � 10 1
0.06 12
SD2 1.83 � 101 3.83 � 10 1
1.46 � 100 9.56 � 10 1
2.73 � 10 1
1.90 26
*Measurement performed in triplicate with standard variation inferior to 5%.
DRYING TECHNOLOGY 7

Table 5. Energetic balance for milk drying.


Inlet data Outlet data
T°Cair,in* AHin* T°Cmilk,inj* εtotal,in Vair,out* AHout* T°Cair,out* εtotal,out εloss ESC
Equipment (°C) ðkgwater � kgdry1 air Þ (°C) (kJ h 1) (°C) Aout (m2) ðkgwater � kgdry1 air Þ (°C) (kJ h 1) (%) (kJ kg 1) εefficiency
SD1 1.62 � 102 1.59 � 10 2 4.0 � 101 1.11 � 104 5.65 � 104 9.62 � 10 4 3.07 � 10 2 9.76 � 101 9.68 � 103 13.89 1.52 � 104 6.55
SD2 1.70 � 102 1.36 � 10 2 3.9 � 101 9.82 � 104 6.55 � 104 7.24 � 10 3 3.80 � 10 2 8.84 � 101 9.04 � 104 10.72 9.19 � 103 3.93
*Measurement performed in triplicate with standard variation inferior to 5%.

the formation of these fine powders and consequently (T°Cair,out) subtracted from 20°C. The temperature of
their loss.[22,23] the particle during spray drying is between the outlet
air temperature and wet-bulb temperature of the
Energy balance for milk drying outlet air, which means 10–20°C below the outlet air
The energy balance for milk drying is very similar to temperature.[27,28]
that shown for water evaporation and it was previously Replacing Cppowder in Eq. (28) by its correspondent
described.[24–26] However, instead of the parameters for relation (Eq. 26) yields:
water, the data for concentrated milk will be used. Using
et;out ¼ ½Ta;out ð1:01 þ 1:89AHout Þ þ 2500AHout �
Eq. (14) as a base, the energy entering during the drying
process can be rewritten as: � ½Va;out Aout qð1 þ AHout Þ 1 � ð29Þ
Mp �
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et;in ¼ ½Ta;in ð1:01 þ 1:89AHin Þ þ 2500AHin � þ ½ð1 0:56TSp Þ4:186� Ta;out 20


ð25Þ t
½Va;out Aout qð1 þ AHout Þ 1 � þ Fm;inj Cpm Tm;inj
The energy loss (εloss), ESC for milk, and energetic
where Cpmilk corresponds to the specific heat of milk in efficiency of process (εefficiency) are also calculated for
kJ kg 1 and T°Cmilk,inj is the temperature of concen- drying milk from Eqs. (17)–(19), respectively.
trated milk in°C. Tables 4 and 5 list the parameters needed to calculate
Cpmilk is estimated by the following relation:[3] the energy balance for milk drying.
For spray dryers SD1 and SD2, the energetic losses
Cpm ¼ ð1 0:56TSm Þ4:186 ð26Þ (εloss) were approximately 1.1 and 1.2 times higher than
where Cpmilk corresponds to the specific heat of milk in the energetic losses for water evaporation (Table 3).
kJ kg 1, the equation 1 0.56 � DEmilk refers the mean- These differences between milk drying and ideal drying
specific heat of the milk solid components, which is (water evaporation) are directly related to powder mass
established as 44% of the specific heat of water (4.186) lost during the process and the larger energy necessary
and DEmilk is the dry mass of the milk. to evaporate the water from food.[20,29]
Substitution of Eq. (26) into Eq. (25) yields:

et;in ¼ ½Ta;in ð1:01 þ 1:89AHin Þ þ 2500AHin � Conclusion


1
� ½Va;out Aout qð1 þ AHout Þ � þ ½ð1 0:56TSm Þ The mathematical model was valid for evaluation of the
� 4:186�Fm;inj Tm;inj mass and energy losses, and it allowed a comparison of
ð27Þ the efficiency between spray dryers with different
designs. Using this model, it is possible to compare
The outlet energy (εout; kJ h 1) can be calculated different drying processes and dryers. Spray dryer SD2
from Eq. (15) by adapting the parameters for milk showed higher energy efficiency than SD1. Application
powder: of this protocol of calculus to industrial processes
should measure the air flow rate, area of transversal
et;out ¼ ½Ta;out ð1:01 þ 1:89AHout Þ þ 2500AHout �
section of outlet air tubing, air velocity, absolute
½Va;out Aout qð1 þ AHout Þ 1 � ð28Þ humidity of the air (inlet and outlet), temperature
Mp � (water or milk, inlet and outlet air), and mass (water
þ ½ Cpp Ta;out 20 �
t or milk, powder).
where Mpowder and Cppowder correspond to the rate of
powder production in kg h 1 and the specific heat of
the powder (kJ kg 1 · °C 1), respectively. Note that the Funding
temperature of powder in the outlet of equipment The authors thank the Brazilian agencies FAPEMIG, CNPq,
was estimated as the temperature of outlet air and CAPES for financial support.
8 C. R. DA SILVA ET AL.

ORCID industry: A comprehensive critical review. Drying


Technology 2016, 34, 1773–1790.
Antônio Fernandes de Carvalho http://orcid.org/0000- [14] O’Donnell, C.P.; McKenna, B.M.; Herlihy, N. Drying of
0002-3238-936X skim milk: Opportunities for reducted steam. Drying
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