SYSTEMATIC ANALYSIS oF SIMPLE SALT NO-4 —— EXPERIMENT OBSERVATION | INFERENCE | | PRELIMINARY ANALYSIS. la. Colouy of the sal colourless [soy be the absence of 1s noked Copper and Manganese tons Heat a sant) 2 Flame Lesh ic MOY be the absence of A HELE of solk is No chanackniskic Raniun , Skronbiuns , Caletuns made into paste » Flare i fear ae with cone. Ho] A ‘008 Gal, 67°, ca*) 91095 rod tg clipped JO1k and show Lo flare 3. Ash Lesh s_ May be Lhe absence of No chanackenislic MY | A thble of sclk is an Alarinium , Zine , with conc No, Megresiuns jong @*t aft Ng) Cobalk nikrade. | Solutio. 4 piney | PSPEX 19 chipped io (hard bundk be ashes | ANALYSIS FOR IDENTIFICATION OF ANION le A little of the Brisk effervescence Moy be the preaencuof | - Salk is mixed evith vith coloumless cantooneks to (Co? ) dil Hcl odorless gas cohich 3 | bunns Sime askin | | sailkey CONFIRMATORY. TEST FOR ANION (co27) [a ea Wilde of the Lina ed [Presence of Canbonake Salk. soluckions dil: Hd milky | 192 confirmed. 18 addid and tha rs miley ara ie oe whit, poucipitak Presence of Cnboeiee eee Solable to 100 confirmed. i i , basiuns Chlovide Hel solutionGROUP TeST FoR CATIONS A Toe Lhe oho} preapilale = : eee ee greup sald solution. Na,COs ty adie 33 addlecl ie ANALYSIS FOR GROUP ZERO CATIONS Wu? porgent smelling ga} Preseoce of erhich producs danse hike Funes cohin a. glass rok clipped io Sdluties NaOH vis Ammoniuns ig CoFi reed. 2 To a Lidhbe of Salt solution Nessler5 reagents aclalect . Brows precipiLate Presence of Aromoenians is onfivmed UL Resue =— TTR Gives staple Salk is Anamsoricany arbors (GH5,C0, )SYSTEMATIC ANALYSIS OF SIMPLE SALT NO-@ i EXPERIMENT OBSERVATION [tweceence PRELIMINARY ANALYSIS. : 7 1: Colour of the salk | colourless 1S noked May be the absence ‘of | Coppex anol Mar gonese igns. | i. Mn? ) 4 likble of scJk ts No chanackeniskic| rode into paste. — | Flame with conc, HC]. A 2. Flame Lesh :— Mey be the absence of Raxiun , StvornLiuns , Coleiuns ions (6.3, Sy**, co?t) glass rod 15 clippecl Wik and shown Lo flame . } 3. Ash Lesk j_ No chanackenishi¢ A liebe of selk is May be. Lhe absence of aie Aluminium , Zine : with gone. HNO Magresians fons jit zat Mi) Cobol nikrate “Solution. 5 poy PSP Is. chipped ic iE ancl 4 i umek Lo ashesANALYSIS FoR IDENTIFICATION OF ANION t SA Ubthe of the’ salt] ie chanacken 1S mixed with observatiso dil, uc] 2A Le of the ealk 15 vubbed with dil 4sQ, cued gona % & wedch glass HSkic Absence of Conbosake ion Presence of acelote jon ie CONFIRMATORY. TEST FOR ANION eg (CH,coo™ ) AUA Wikble of Lhe salk 18 mixed wilh nouknal ferric chlovids solukion and kepl By Somekime coi bboud cbisbunbance 2. A likkle of Lhe sak 18 mixed asith conc. 450, 8g and ethanol , boiled *xlune and passel| lol excess woken GROUP TEST FOR CATIONS ee a Te Bittle of Sale yd precipiteds. solution Naco, ig * addad.. 2. A LdHe of the sall. white precipiLate '8 mixed with dik Hcl ‘ Reddish browe alalieo, Pleasant Sraiky grell Presence of acetoke 409 15 rfirmsed. Presence of acelake io 16 ‘confi venecl, Absence of group zevo cohion Presence of group one cation G42 ) at ANALYSIS FOR GROUP ONE CATIONS (P42+) 2 A didtbbe of salk is breaded with acekic acill and potassians Chromake solubion 2 Ta Little of sath Sdludien pokassicans Yellow precipiboke Yellow Precipilake Presence of Jed lan lead io is. comfiveed. Presence of lead ion soluble to hot wabn andl 6 af uersach or reappeans as goldurs Sake Spergles om cobizy I RasuLr =— The giver siopl salt is Lead acetate fovea |SYSTEMATIC ANALYSIS OF SIMPLE SALT N@-3 eee EXPERIMENT OBSERVATION INFERENCE = PRELIMINARY ANALYSIS fe Colour of the salk is noked @ Flame tesh:-* A Jikkle of Lhe salk 9 made inks poste esith con uel. 9 glass} Tod is dippe: ad tai and showe bg ey Flare 3. Ash Lesh :~ A lithe of tall is healed ewith con. Hnog and coboll nikvate soludis 4 Filler pape 'S dipped ic ik. and bunek Lo ashes moixed vith dil. Hcl 2 A Whe of the salk. is stubbed. with dil i ina coodkth glaés. 13 boiled cwith Gon. 4.50, 19 boiled coith con: H,50, and p ball 15 iokyoduced. tol ike |S. A Bde of the salk Is mIxeh with bantans chloride abi , Colounless No chanacteniskic flame Blue Linked ash ANALYSIS FoR IDENTIFICATION: OF AN\O la. A iittle of the salt iS} ng chanactanishic observadieo Sect of vi No 129% | chonackoishic obseivaiep ae sof the salk| No chanackmniskic * obsewvelisn [fA tithe of the call! 5 chaniachsiolic obsewadisn Thick ehike precipiLae| Fesdlable in dil. tc) May be the absence of * Copper and Mangansas iors Gu a matt) May be the absence of Baniun, Strorbiun, Calcians ions (@it 54 eat) May be the presence oF Alamicians ion (44) N Absence of Canbonaks. | ion PAREERES of acekake iv0 Absence of chlorida loo Absence of niliche ion Presence of salphaka ionJ CONFIRMATORY TEST FOR ANION Pr of A Toa title of gal | trick white prucipilads | Presence Salphake comfismal dood. actohe soliclion is addad . 2. Te the above Th Lake Beery olf - eS ip fr eel Done Sulphate. coofivmed Ammonium acekate solution GROUP TEST FoR CATIONS A a lle of salt Solution NaC vis added 2A Tiddle of the salt male b: of gro while powcipibele eee Speci No chonackanistic observalixp Abserce of group 48 mixed wilh oll Hel eT, oo oid Q, ; salt Eis [No characteristic Absence of group #8 adldel and is geo ob.renvatios © cation % passcd though Aha solution 4: To a Bittle of sath q Soludion aromorians chloride anak excess of BramOr Ie byl xids © eoldod Presence of group whike gelatinous three cakino 3 precipibals. er) 1 ees enna ANALYSIS FOR: GROUP THREE cations (a) 31) [= = Te a Ltlh of salt [wri precipilate sduble | Presence of Soludier NaOH Ws fo excess NaoH solution Alarsiniars ion is addlack drop by dnop confirmed. “4 excess 2. Ash dash A Liddle of sald vs Presence of heated woth con! HNOg Alamiciun ios is ComPrarred. RESULT The, giver dnple sak i8 Aluminiars Sasulphae (A1,6%25 )SYSTEMATIC ANALYSIS OF siMPLE SALT No- 4 EXPERIMENT PRELIMINARY ANALYSIS 2: Coloun of the soll is nated 2. Flame tesk :— A SdH of sald us roads oko passe with Gon Cl. x glass vod 'S dspped io ik. ancl Show te Saene 3. Ash Lesk ._ A idle of sald is | heeded with con. uno OBSERVATION colourless Fale greeo Flare No chanackernatic INFERENCE May ba dhe abasnce of Coppen and Mangonase ions ut a m2 5 Moy be the presence of barium ion (Ba2+) May bo the abssnce of Alanrsiciows 5 Zinc, Mogresiane ions @i, 22+, mgt) oa wack slass SA Gelb of he sabe 3 Srooked cit Com Ha 50, Ss and cobale nikrate solution. A fitox Poypen 2 hy fo ik aod Bunk bo ashes. L ANALYSIS FoR IDENTIFICATION OF ANION _ AA Sidhle of the salt is! ne chanackenishic mixed with lil yc ebsewehien RA LAM 3k the salt is No chanackenishic vabbad cwith dil. 250, | ohaenadion 4 pangenk saoellicy gus sore Produce, darse whike fumes when a glass yok stppedd ic Arononian| bydororide is showe be the mouth of he| Arsh Aubo Presence of Absence of canbonahe ion Absence of Acebake jon Presence of Chlorice ion (eI")CONFIRMATORY TEST FOR ANION (cI7) } a A Abbe of dhe salt 4s heat with con. 4,50, diioxids A Little of the salt 43 mixed with dil. HNO, and silver cikraks Sdlution FE and pinch of Manganese greenish gas Soluble 19 Armonians hydoioxils, GROUP TEST FOR CATIONS Whike conday precipitate, -y Presence of hlovide ion 16 confiamed. Presecce of Hloride ion is confiared. 2+ Toa itll, of salt Dludien Na,co, ts added 2 A Lldle of the salt 48 mixed. with dil HCl 3. Toa Ade of the salt Solution dil ucl is addled. through the soldien iar otes Leetee lL Solution ammoniuns Chloride. crcl excess of amemosiun hydooxide | is | PS A Aide of the sol Soludier is mixecl asith| Aromoniun chlovide , OXCESS AMomon Ind hydooxicle Ammonia chlovide 9 Armenians hyclnoncle , and WmonieunD Corborake, jg Lack and 45 10 passe whide precipitods No chanactenvalic observatien Ne chanackenistic obsenvaten No chanactnishic obsewatino No chanackenistic obssnvation Whe precipitate Absence of group ze cok Abaence of guxip catiso ene Absence of group taco cotisno | Absence of group three cation | Absence of group Foun cotter Presence of qvoup five cation © Bot Sums (ca)ANALYSIS FOR GROUP Five CATIONS . Presence of Boriuns TA Side of salt us Yellow precipitake | ios } oe 2 mixed. with acdic a io cect (Cat acid and pokassians Ghomaks soludioo 2: Flame best :— p . * tale of salt ts | Pale greeo Same er ems made. fobs paske worth, confi ell fom. Hel. 4 glass ved eee ‘The giver sieple sulk 15 Boseurs chloviola (Bacl,)