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POWDER METALLURGY
Powder metallurgy (PM) is a metal working process for forming precision metal components
from metal powders. The metal powder is first pressed into product shape at room
temperature. This is followed by heating (sintering) that causes the powder particles to fuse
together without melting. Strength and other properties are imparted to the components by
sintering operations.
The most commonly used metals in P/M are iron, copper, aluminium, tin, nickel, titanium and
refractory metals.
Metal powder production techniques are used to manufacture a wide spectrum of metal
powders designed to meet the requirements of a large variety of applications. Powders of
almost all metals can be produced. Various powder production processes allow precise control
of the chemical and physical characteristics of powders and permit the development of
specific attributes for the desired applications. Powder production processes are constantly
being improved to meet the quality, cost and performance requirements of all types of
applications. Metal powders are produced by mechanical or chemical methods. The most
commonly used methods include water and gas atomization, milling, mechanical alloying,
electrolysis, and chemical reduction of oxides.
The parts produced by PM have adequate physical and mechanical properties while
completely meeting the functional performance characteristics. The cost of producing a
component of given shape and the required dimensional tolerances by PM is generally lower
than the cost of casting or making it as a wrought product, because of extremely low scrap and
the fewer processing steps. The cost advantage is the main reason for selecting PM as a
process of production for high – volume component which needs to be produced exactly to, or
close to, final dimensions. The rate of production of parts is quite high, a few hundred to
several thousand per hour. Parts can be produced which are impregnated with oil or plastic, or
infiltrated with lower melting point metal. They can be electroplated, heat treated, and
machined if necessary.
Industrial applications of PM parts are several. These include self – lubricating bearings,
porous metal filters and a wide range of engineered shapes, such as gears, cams, brackets,
sprockets, etc.
Basic steps of the Powder Metallurgy Process
The manufacturing of parts by powder metallurgy process involves the following steps:
(a) Manufacturing of metal powders
(b) Blending and mixing of powders
(c) Compacting
(d) Sintering
(e) Secondary and Finishing operations
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Chemical and electrolytic methods are used to produce high purity powders. Mechanical
milling is widely used to produce hard metals and oxides.
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Gas atomization: Here instead of water, high velocity argon, nitrogen and helium gas jets are
used.
Vacuum atomization: In this method,
when a molten metal supersaturated with a
gas under pressure is suddenly exposed into
vacuum, the gas coming from metal
solution expands, causing atomization of
the metal stream. This process gives very
high purity powder. Usually hydrogen is
used as gas.
Centrifugal atomization (disk or cup)
Centrifugal force can be used to break up the liquid as it is removed from the periphery of
spinning disk/cup. The molten metal is disintegrated into fine droplets as it falls on the
rotating disc.
Rotating consumable electrode method
Another method is that an electric arc is struck between non-rotating, non-consumable
tungsten electrode and rotating consumable electrode (metal from which power is to be
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produced).The metal droplets from the rotating consumable electrode are thrown off, are
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Iron
F e (impure iron ore)+5 CO→F e (CO )5 ↑ (gas)
F e (CO )5 → Fe +5 CO (Fine iron powder + carbon monoxide)
Carbonyls powder is spherical, fine and porous with an onion skin structure. Carbonyl powder
has high purity (99.5%) and excellent sintering properties and flow ability.
Comminution method (Mechanical pulverization by crushing and milling)
It is mechanical method of powder preparation involving breaking solid particles in
pulverizing mills (ball, vibratory, hummer). This method is generally applied for the
preparation of powders of brittle materials. Metal particles is mixed with ball mills and rotated
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or send through the rolling mill to pulverize the metal to form powder.
compressibility=
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4. Binders can be added to the mixture of the powder particles to enhance the green
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Single Action Die Compaction: Used to manufacture flat, thin parts such as washers, discs,
thin rings etc. The lower punch is stationery during the application of pressure by the motion
of the upper punch acting from the direction only on the powder placed in the cavity.
Double Action Die Compaction: The powder is compacted simultaneously from opposite
directions by both the top and bottom punches. Equal or different amounts of pressure may be
employed from each direction.
uniform density and strength. After pressing, the compact is removed from chamber. The
pressure-transmitting medium used is liquid such as water, oil mixture.
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Hot iso-static pressing (CIP) is combining the compaction and sintering processes in PM
production process. So it eliminates separate sintering.
Advantages
1. Little or no porosity
2. Better surface finish
3. Neat net shape product
4. Improvements in mechanical and physical properties, fatigue, surface finish, reliability
5. Fast delivery
6. More uniform strength
7. Less pressure requirement
Disadvantages
1. Very expensive
2. Protective environment is needed
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Mechanism of sintering
Sintering occurs by diffusion of atoms through the microstructure at high temperature. The
atoms in the materials diffuse across the boundaries of the particles, fusing the particles together
and creating one solid piece. The main driving force during the sintering process is the
reduction of energy due to the reduced surface area. Powders with a greater surface area will
have a higher driving force towards bonding. The porosity of the material decreases due to the
bridge formation among particles given by the minimization of the internal energy of the system.
Stages of Sintering
This process is carried out a constant temperature and time is varied to obtain the desirable
results. The four phases of sintering are:
1. Initial stage: Local bonding: Particles stick together and neck formation
2. Second stage: Neck growth
3. Final stage: Pores are round up then finally closed
The time, temperature and the furnace atmosphere are the three critical factors that control the
sintering process. Sintering process enhances the density of the final part by filling up the
incipient holes and increasing the area of contact among the powder particles in the compact
perform
.
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Microscopic scale the changes that occur during sintering of metallic powders.
the size of the particle is small (and its curvature is high), these effects become very large in
magnitude.
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5. Difficult to machine materials like carbide and tungsten can be made by this method
6. Wide property control is possible with the product with variation in composition and
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Cutting Tools and Dies: Cemented carbide cutting tool inserts find extensive applications in
machine shops. These are produced by PM from tungsten carbide powder mixed with cobalt
binder.
Machinery Parts: Several machinery parts including gears, bushes and bearings, sprockets,
rotors are made from metal powders mixed with sufficient graphite to give to produce the
desired carbon content.
Friction Materials: These are made by powder metallurgy. Clutch liners and Brake bands are
the example of friction materials.
Gears and Pump Rotors: Gears and pump rotor for automobile oil pumps are manufactured
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by powder metallurgy.
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Traditional machining is mostly based on removal of materials using tools that are harder than
the materials themselves. Traditional machining methods are often ineffective in machining
hard materials like ceramics and composites or machining under very tight tolerances as in
micro machined components. Nano level surface finish on complex geometries which are
impossible to achieve by any traditional methods
Need for Non-Traditional Machining
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A manufacturing system consists of machine and control system. In the past humans were the
main methods for controlling a system. More recently electricity has been used for control and
early electrical control was based on relays. These relays allow power to be switched on and
off without a mechanical switch. Depending on the type of technology used, controllers can
be divided into pneumatic, hydraulic, electrical and electronic controllers. Frequently, a
combination of different technologies is used. Microprocessors are now rapidly replacing the
mechanical cam-operated controllers and being used in general to carry out control functions.
Introduction to control devices relay- timers and counter
Relay
A relay is an electrically operated switch. Relays are switches that open and close circuits
electromechanically or electronically. Relays control one electrical circuit by opening and
closing contacts in another circuit. Relays are the primary protection as well as switching
devices in most of the control processes or equipment’s. Early electrical control systems were
composed of mainly relays and switches.
Relays are either electromechanical relays or solid-state relays. In electromechanical
relays (EMR), contacts are opened or closed by a magnetic force. With solid-state
relays (SSR), there are no contacts and switching is totally electronic.
Apply a voltage to the coil and a magnetic field is generated. This magnetic field sucks the
contacts of the relay in, causing them to make a connection. These contacts can be considered
to be a switch. Relays are ideally suited for controlling everything from lights and motors to
telecommunication, audio, and video signals. Relays come in many sizes and ratings.
Basic parts and functions of electromechanical relays include coil, armature and contacts
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Relays typically have two or three connections: Common, Normally Open, and Normally
Closed. Relays often have two ratings: AC and DC. These rating indicate how much power
can be switched through the relays.
The NO Normally relay has an opened circuit state when no current is applied to its coil so
basically it disconnects the power to the load in the inactive state. When current is applied to
its coil the generated magnetic field switches the armature and closes the contact so you can
say that it turned ON the load (fan, light bulb, etc). Normal Closed contact allows the current
to flow when the contact is still or de-energised state
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Clock
Accumulator
reset
Register
contact
Contact
output
Types of timer
It is possible to construct a relay with a built-in time delay device that causes the relay to
either switch on after a time delay, or to switch off after a time delay. These types of relays
are called time delay relays, or TDR’s. There are two basic types of time delay relay. They
are the delay-on timer, sometimes called a TON (pronounced Tee-On), and the delay off
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ON delay timer - after the input is turned on there is a delay before the output is turned on.
EN-Enable Bit: - The enable bit indicates the TOF instruction is enabled.
DN- Done Bit: - The done bit changes state whenever the accumulated value reaches the
preset value.
Off-Delay timers
After the input is turned off there will be a delay before the output is turned off.
In this case, at the instant power is applied to the relay coil, the contacts activate - that is, the
N/O contacts close, and the N/C contacts open. The time delay occurs when the relay is
switched off. After power is removed from the relay coil, the contacts stay activated until the
relay times-out.
Counters
Counters are provided as built-in elements in PLCs and allow the number of occurrences of
input signals to be counted. This might be where items have to be counted as they pass along a
conveyor belt, or the number of revolutions of a shaft, or perhaps the number of people
passing through a door. A counter is set to some pre-set number value and, when this value of
input pulses has been received, it will operate its contacts. Digital counters output in the form
of a relay contact when a pre-assigned count value is reached. A counter is a register capable
of incrementing and/or decrementing its contents
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Accumulator
reset
contact
output
written in the programs which are stored in the memory. Then it evaluates their logic
The program is written on a computer and is downloaded to the PLC via cable. It can be used
for different applications via means of changing the program. The original task of a PLC
involved the interconnection of input signals according to a specified program and, if "true",
to switch the corresponding output.
1. Variety of programs can process the multiple inputs to give multiple outputs.
2. The programs can be altered/ reprogrammed to change the output specifications.
3. There is programmable memory to store instructions and carry out control function
Due to its robust construction, exceptional functional features like sequential control, counters
and timers, ease of programming, reliable controlling capabilities and ease of hardware usage
– this PLC is used as more than a special-purpose digital computer in industries as well as in
other control-system areas.
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The basic idea behind these programmable controllers was to provide means to eliminate high
cost associated with inflexible, conventional relay controlled systems. Programmable
controllers offer a system with computer flexibility.
PLC Programming
There are six programming language available for any PLC, But the most common between
them is Ladder Programming.
Ladder programming (ladder diagram)
A very commonly used method of programming PLCs is ladder diagrams. Writing a program
is equivalent to drawing as witching circuit. Ladder logic uses symbols, instead of words, to
emulate the real world relay logic control. The left and right rails indicate the positive and
ground of a power supply. Circuits are connected as horizontal lines, i.e. the rungs of the
ladder, between these two verticals. The completed program looks like a ladder but in
actuality it represents an electrical circuit.
Components of ladder diagram and instruction
1. Two vertical line called power rails –input and output power rails
2. Horizontal lines called rungs (rung1, rung2 etc) can be any number depending upon
the complexity of problem- number of rungs, but limed by PLC capacity
3. Each rung can have more than one input, but not more than one output devices.
4. All the input devices are graphically represented in left hand side of rungs
5. All the input devises are represented as switches (temperature sensor, flow sensor etc)
6. Input region is full of combinations of NC and NO switches
7. All outputs in laden diagram is represented by circle sign (motor, lamp, solenoids etc.)
8. Run the program from left to right and down ward till ends and repeats the same cycle
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Example 2
Motor should remain in ON state after Start pushbutton is pressed and should Off When Stop
pushbutton is pressed. Checking if the motor is running normally by pressing test pushbutton.
1. Press START button lightly and X0 = ON. The Motor will keep running if no error
occurred (X3 = OFF). The action can be practiced by a latching circuit which takes
output Y0 as one of the input condition to keep the motor running even if the START
button is not pressed (See normally open contact M0.1 below X0).
2. When STOP button is pressed, X1 = ON and M0.1 = OFF. The motor will stop
running.
3. If error occur (X3 = ON), M0.1 will be OFF and the motor will stop running.
When TEST is pressed (X2 = ON), M0.1 = ON. The motor will start running if no error
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occurred (X3 = OFF). On the contrary, when TEST is released, the motor will stop running.
The testing function is performed by this process.
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Example 3
Example 4
When is switch is ON, motor and green light is ON and if motor is OFF red light will glow
Example 5
Consider the design of a Burglar Alarm for a house. This alarm will be activated if an
unauthorized person is detected by a Window Sensor or a Motion Detector. Implement
this Alarm System in PLC using Ladder Diagram programming language.
Example 6
Ladder program for automatic water filling tank
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There are two sensors are used, for standing and fallen bottles detection, one pneumatic
cylinder for pushing the fallen bottle from the conveyor.
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Example 9
Ladder logic diagram for starting the oil pump motor immediately when START is pressed.
The main motor will be started after a 10 sec delay and then the auxiliary motor after a 5 sec
delay and also stopping all motors immediately when STOP is pressed.
stops T2.
When STOP is pressed, the NC contact X1 will be activated, which makes Y0, Y1 and
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Y2 OFF. The oil pump motor, main motor and auxiliary motor will stop working.
Example 11
Enabling the indicator to be ON immediately when switch pressed and OFF after a 5 sec delay
by the switch.
X1 – Start Switch.
Y1 – Output Indicator
T1 – 5 second Timer,
When X1 = ON, Timer T1 will be ON and start counting for 5 sec and indicator will be ON
When T1 reaches its set value, closed contact T1 becomes open and indicator will be
OFF
Problem 12
Once the photoelectric sensor detects 10 products, the robotic arm will begin to pack up.
When the action is completed, the robotic arm and the counter will be reset.
X0 – Start Switch.
X1 – Low level float sensor. X1 = ON when
the liquid level reaches X1.
X2 – High level float sensor. X2 = ON when
the liquid level reaches X2.
X3 – Stop Switch.
X10 - EMERGENCY STOP button. X10 =
ON when the button is pressed.
Y0 – Liquid A Inlet
Y1 – Liquid B Inlet
Y2 – Mixture Outlet
Y3 – Agitator /Stirrer
T0 – 60 second Timer, 100 ms Time Base.
(See K60 Preset Value for Timer)
T1 – 120 second Timer, 100 ms Time Base.
X0 = ON when START is pressed. Y0 will be ON and the valve will be opened for
infusing liquid A until the level reaches the low-level float sensor.
X1 = ON when the level reaches the low-level float sensor. Y1 will be ON and
latched, and the valve will be opened for infusing liquid B until the level reaches the
high-level float sensor.
X2 = ON when the level reaches the high-level float sensor. Y3 will be ON and
activates the agitator. Also, timer T0 will start to count for 60 sec. After 60 sec, T0
will be ON, and the agitator motor Y3 will stop working. Y2 will be ON and latched,
and the mixture will drain out of the container.
When Y2 = ON, timer T1 will start to count for 120 sec. After 120 sec, T1 will be ON
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will be ON to disable all the outputs. The system will then stop running.
For a lathe, the infeed/radial axis is the x-axis, the carriage/length axis is the z-axis. There is
no need for a y-axis because the tool moves in a plane through the rotational center of the
work. In drilling and milling machines the X and Y axes are horizontal. For example, a
positive motion command in the drill moves the X axis from left to right, the Y axis from
front to back, and the Z axis toward the top. In the lathe only two axes are required to
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NC drill presses are a good example of PTP systems. The spindle must first be positioned at a
particular location on the work piece. This is done under PTP control. Then the drilling of the
hole is performed at the location, and so forth. Since no cutting is performed between holes,
there is no need for controlling the relative motion of the tool and work piece between hole
locations. Example figure above illustrate path of three drilled holes.
Straight-cut Positioning Control:
Straight-cut control systems are capable of moving the cutting tool parallel to one of the major
axes at a controlled rate suitable for machining. It is therefore appropriate for performing
milling operations to fabricate work pieces of rectangular configurations. An example of a
straight cut operation is shown in Figure. An NC machine capable of straight cut movements
is also capable of PTP movements.
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To achieve contoured motion, a series of points is provided during programming, and the
motion controller extrapolates a smooth line or curve from these points. In contouring motion
guarantees that the tool system passes through each point, using either linear or circular
interpolation.
Difference between contouring and point-to-point motion
With point-to-point systems, control is achieved over the x and y coordinates. With straight-
cut systems, control is provided for either dx/dt or dy/dt, but only one at a time. With
contouring systems, both of the rates dx/dt and dy/dt can be controlled simultaneously. This is
accomplished by breaking the curved path into very short straight-line segments that
approximate the curve.
Contouring is the most complex, the most flexible, and the most expensive type of machine
tool control. It is capable of performing both PTP and straight-cut operations. In addition, the
distinguishing feature of contouring NC systems is their capacity for simultaneous control of
more than one axis movement of the machine tool.
The choice between point-to-point or contoured motion depends on the application and
process. The smooth shapes generated by contouring are important for CNC applications such
as cutting, welding, and routing, as well as for dispensing applications where a specific path
must be followed. In point-to-point motion, the end position is designated, but the path used to
reach the end position is irrelevant.
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Linear interpolation is used when the desired move is a straight line involving two axes of
motion. The controller synchronizes the motion of both axes. Circular interpolation works
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much the same way as linear interpolation, but also requires the specification of a center point,
Advantages
For complicated components, this dimensioning is more advantageous.
Disadvantages
Positioning errors add up in incremental positioning. If error occurs at any line in the
program, all the subsequent lines will add up to the error.
It is difficult to check a program written in incremental system
Absolute System
With absolute coordinates, the origin is always in a fixed position. Each new location is
calculated from this fixed origin instead of the previous location. Even if there is an error
while reaching the current location, that error is corrected once the tool or work piece moves
to the next location
Advantages
Very easy to correct and check a program when written
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If there is any mistake in any block, only that block will be affected. The remaining of
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2. Economical.
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3. Easy to maintain.
4. Generally stable.
In encoder-based systems each pulse indicates a motion of 1 BLU (basic length unit) of axis
travel. Therefore, the number of pulses over a period represents incremental change in
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position over the period and the encoder pulse frequency is proportional to the axis velocity.
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In such a system, fed from a reference pulse interpolator the comparison is done by an up-
down counter which is fed by two sequences of pulses: reference pulses from the interpolator
27. In what ways might the final density of a P/M product be reported?
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28. What are some of the other methods that can produce high-density PIM products?
29. Why is there a density variation in compacting powders?
57. Should green compacts be brought up to the sintering temperature slowly or rapidly?
Explain the advantages and limitations of each.
Heat treating:
The main purpose is to improve wear resistance rather than strength. The process of heating
and cooling sintered parts is to improve
1. Wear Resistance
2. Grain Structure
3. Strength
The following heat treatment processes are used to the parts made by powder metallurgy:
1. Stress relieving
2. Carburising
3. Nitriding
4. Induction Hardening
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