REPORT OF MIGRATION OF COMPOUNDS BY THE NSF/ANSI

61-2013 “DRINKING WATER SYSTEM COMPONENTS –

HEALTH EFFECTS” REGULATION FROM PRODUCTS USED
TO BE IN CONTACT WITH WATER FOR HUMAN
CONSUMPTION

Report Code: 1704821

This report only affects the sample. You can only partially reproduce with the written
permission of the laboratory.

Date: 21/11/14 Date: 21/11/14 Date: 21/11/14

Elaborated by: Revised by: Approved by:

Jorge Agulló Carpena Julio Llorca Porcel Francisco García

Technician Head of Chromatography Technical Manager
Department

LABAQUA S.A. / C/ Dracma, 16-18 • Polígono Industrial Las Atalayas / 03114 Alicante / Tel. +34 965 106 070 /
www.labaqua.com
Report 1704821 21/11/2014
Informe complementario

INDEX

1. INTRODUCTION AND GENERAL INFORMATION. .................. 3

2. ELEMENTS OF STUDY DESCRIPTION. ....................................... 4

3. EXPERIMENTAL PROCEDURE..................................................... 5

4. RESULTS. ........................................................................................... 6

5. CONCLUSIONS. .............................................................................. 17

6. ANNEXES ......................................................................................... 18

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1. INTRODUCTION AND GENERAL INFORMATION.

The company PINTURAS VILLADA SKC, S.A. has required a migration study of a liquid
material used to be in contact with water intended for human consumption following NSF/ANSI
61-2013: Drinking Water System Components – Health Effects Regulation.
.

LABORATORY DATA:
LABAQUA S.A.
Addres:
C/ Dracma, 16-18
Polígono Industrial Las Atalayas
03114 – Alicante
España

Phone: 965 10 60 70
Fax: 965 10 60 80
info@labaqua.com

CLIENT DATA:
PINTURAS VILLADA SKC
Address:

Crtra. Villalón, 9 – 11 VILLADA

34340 - Palencia
España
Phone: 979 847 251 Fax: 979 847 263

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2. ELEMENTS OF STUDY DESCRIPTION.

Material pieces. The pieces consist in glass sheets covered with the product. The
samples have been identified as 2340963 (Sample) and 2340964 (Blank).

Application: The material has been indicated to be used in products intended to

be in contact with water for human consumption.
Commercial mane and batch: PROTECFULL SFP 108
Componente A (Base): LABP. 1370-2
Componente B (Endurecedor): LABP. 1370-3

Reception data in LABAQUA 25/09/2014

Manufactured: PINTURAS VILLADA SKC

Samples remitted by: PINTURAS VILLADA SKC

Samples prepared by: PINTURAS VILLADA SKC.

Assay pieces preparation: The sample consist in glass sheets covered with the product.
PINTURAS VILLADA SKC applied the product on the sheets according with the
manual instructions of the product:
● Pieces characteristics and dimensions:

Dimensions:
S = 1 dm2 each piece Total pieces = 14
Volume: 2 L
Ratio S/V = 7.0 dm-1

Figure 1. Image of the test piece.

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3. EXPERIMENTAL PROCEDURE.

According to customer requirements, this study is based on “NSF/ANSI 61-2013: Drinking

Water System Components – Health Effects” Regulation
When the migration water was obtained, the water sample was analyzed, indicated in the Annex
I, in order to calculate the migration rate.
According with this Regulation and with CEN/CENELEC regulations, all the European
countries are required to reach the specifications indicated.

Table 1. General information about the migration test:

Parameter Data
Total number of sheets 14 pieces
Final water volume 2L
Disinfection process Not appropriate for this test
Chlorinated water containing chlorine (Cl2)
Water assay characteristics
1ppm
Water assay and temperature Chlorinated water at 23±1ºC for 72±1h
Test deviations No deviations.
Incidences No incidences
Star data: 26/09/2014
Final data: 13/10/2014

Reagents used:
- Tap water from the laboratory.
- Assay water, chlorated water with a total chlorine content of 1ppm (Cl2).
- Chronometer ID Plan 1873, ID Calibration 25126. (Laboratory code G-154)
- Bath of water ID Calibración 42667. Laboratory code (B-131)

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Migration steps:
- Sampling, shipment and preservation. The sample was provided by the company
PINTURAS VILLADA SKC. No special preservation condition was required.
- Sample preparation. The client covered the glass sheets. According with NSF/ANSI 61-
2013: Drinking Water System Components – Health Effects Regulation only the surface
in contact with the water must be into consideration for the migration. Two sheet faces
were covered with the product.
- Static contact period. Following this Regulation the sheets were complete immersed in
one (1) liter of Chlorinated water during 14 days. Each day the test water was replaced.
- Migration assay. The sheets were immersed in 2L of Chlorinated water at 1ppm at
23±1ºC for 72±1h. At the same time, a blank without samples pieces, have been also
carried out in the same conditions than the samples.
- Analysis. The final concentration of the organic compounds was determined by means
of the analytical methods indicated in the Annex I.

4. RESULTS.

Sample codification.

The Table 2 show the number of each analysis reports.

Table 2. Sample denomination.

Code Sample name Total migration

period (hours)

Analysis date “PRODUCTO POLIURETANO 100%

2340963 72±1
26/09/2014 SOLIDOS: PROTECFULL SFP”

Analysis date “BLANCO PRODUCTO

2340964 POLIURETANO 100% SOLIDOS: 72±1
26/09/2014 PROTECFULL SFP”

Analytical results:

Annex I of the final report with analytical results is. Likewise in Annex II the results of the
Organic Compounds Analysis.
In the next Table the analytical results are showed.

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2340963
(PRODUCTO POLIURETANO 100% SOLIDOS: PROTECFULL SFP)

(m+p)-cresol < 4.0 µg/L

1,1,1,2 – Tetracloroetano < 0.5 µg/L
1,1,1 – Tricloroetano < 0.5 µg/L
1,1,2,2 – Tetracloroetano < 0.5 µg/L
1,1,2 – Tricloroetano < 0.5 µg/L
1,1 – Dicloroetano < 0.5 µg/L
1,1 - Dicloroeteno < 0.5 µg/L
1,1-Dicloropropeno < 0.5 µg/L
1,2,3-Tricloropropano < 0.5 µg/L
1,2,4-Trimetilbenceno 1.5 µg/L
1,2-Dibromo-3-cloropropano < 0.5 µg/L
1,2-Dibromoetano < 0.5 µg/L
1,2-Diclorobenceno < 0.5 µg/L
1,2-Dicloroetano < 0.5 µg/L
1,2-Dicloropropano < 0.5 µg/L
1,3,5-Trimetilbenceno < 0.5 µg/L
1,3-Diclorobenceno < 0.5 µg/L
1,3-Dicloropropano < 0.5 µg/L
1,4-Diclorobenceno < 0.5 µg/L
2,4,6-triclorofenol < 0.5 µg/L
2,4-diclorofenol < 0.5 µg/L
2,4-dimetilfenol < 1.0 µg/L
2-clorofenol < 1.0 µg/L
2-Clorotolueno < 0.5 µg/L
2-nitrofenol < 5.0 µg/L
4-Clorotolueno < 0.5 µg/L
4-cloro-3-metilfenol < 1.0 µg/L
Antimonio <2 µg/L
Arsénico <2 µg/L
Bario <2 µg/L
Barrido de compuestos orgánicos BS EN 15768 Informe adjunto --

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Benceno < 0.5 µg/L
Berilio <2 µg/L
Bromobenceno < 0.5 µg/L
Bromodiclorometano < 0.5 µg/L
Bromoformo < 0.5 µg/L
Cadmio <1 µg/L
cis-1,2-Dicloroeteno < 0.5 µg/L
cis-1,3-Dicloropropeno < 0.5 µg/L
Clorobenceno < 0.5 µg/L
Cloroformo < 0.5 µg/L
Cobre <2 µg/L
Cromo <2 µg/L
Dibromoclorometano < 0.5 µg/L
Dibromometano 6.9 µg/L
Diclorometano < 0.5 µg/L
Estireno < 0.5 µg/L
Etilbenceno 2.1 µg/L
Fenol < 1.0 µg/L
Isopropilbenceno < 0.5 µg/L
m+p-Xileno 5.5 µg/L
Mercurio < 0.20 µg/L
n-Butilbenceno < 0.5 µg/L
n-Propilbenceno < 0.5 µg/L
Naftaleno < 0.5 µg/L
o-Cresol < 2.0 µg/L
o-Xileno 2.2 µg/L
p-Isopropiltolueno < 0.5 µg/L
Pentaclorofenol < 0.05 µg/L
Plomo <2 µg/L
sec-Butilbenceno < 0.5 µg/L
Selenio <2 µg/L
Talio <2 µg/L
tert-Butilbenceno < 0.5 µg/L
Tetracloroeteno < 0.5 µg/L
Tetraclorofenol < 0.2 µg/L

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Tetracloruro de carbono < 0.5 µg/L
Tolueno 0.9 µg/L
trans-1,2-Dicloroeteno < 0.5 µg/L
trans-1,3-Dicloropropeno < 0.5 µg/L
Tricloroeteno < 0.5 µg/L
Tetraclorofenol < 0.2 µg/L

2340964
(BLANCO PRODUCTO POLIURETANO 100% SOLIDOS: PROTECFULL SFP)

(m+p)-cresol < 4.0 µg/L

1,1,1,2 – Tetracloroetano < 0.5 µg/L
1,1,1 – Tricloroetano < 0.5 µg/L
1,1,2,2 – Tetracloroetano < 0.5 µg/L
1,1,2 – Tricloroetano < 0.5 µg/L
1,1 – Dicloroetano < 0.5 µg/L
1,1 - Dicloroeteno < 0.5 µg/L
1,1-Dicloropropeno < 0.5 µg/L
1,2,3-Tricloropropano < 0.5 µg/L
1,2,4-Trimetilbenceno < 0.5 µg/L
1,2-Dibromo-3-cloropropano < 0.5 µg/L
1,2-Dibromoetano < 0.5 µg/L
1,2-Diclorobenceno < 0.5 µg/L
1,2-Dicloroetano < 0.5 µg/L
1,2-Dicloropropano 0.8 µg/L
1,3,5-Trimetilbenceno < 0.5 µg/L
1,3-Diclorobenceno < 0.5 µg/L
1,3-Dicloropropano < 0.5 µg/L
1,4-Diclorobenceno < 0.5 µg/L
2,4,6-triclorofenol < 0.5 µg/L

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2,4-diclorofenol < 0.5 µg/L
2,4-dimetilfenol < 1.0 µg/L
2-clorofenol < 1.0 µg/L
2-Clorotolueno < 0.5 µg/L
2-nitrofenol < 5.0 µg/L
4-Clorotolueno < 0.5 µg/L
4-cloro-3-metilfenol < 1.0 µg/L
Antimonio <2 µg/L
Arsénico <2 µg/L
Bario <2 µg/L
Barrido de compuestos orgánicos BS EN 15768 Informe adjunto --
Benceno < 0.5 µg/L
Berilio <2 µg/L
Bromobenceno < 0.5 µg/L
Bromodiclorometano < 0.5 µg/L
Bromoformo < 0.5 µg/L
Cadmio <1 µg/L
cis-1,2-Dicloroeteno < 0.5 µg/L
cis-1,3-Dicloropropeno < 0.5 µg/L
Clorobenceno < 0.5 µg/L
Cloroformo < 0.5 µg/L
Cobre <2 µg/L
Cromo <2 µg/L
Dibromoclorometano < 0.5 µg/L
Dibromometano 7.7 µg/L
Diclorometano < 0.5 µg/L
Estireno < 0.5 µg/L
Etilbenceno < 0.5 µg/L
Fenol < 1.0 µg/L
Isopropilbenceno < 0.5 µg/L
m+p-Xileno < 1.0 µg/L
Mercurio < 0.20 µg/L
n-Butilbenceno < 0.5 µg/L
n-Propilbenceno < 0.5 µg/L
Naftaleno < 0.5 µg/L

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o-Cresol < 2.0 µg/L
o-Xileno 2.2 µg/L
p-Isopropiltolueno < 0.5 µg/L
Pentaclorofenol < 0.05 µg/L
Plomo <2 µg/L
sec-Butilbenceno < 0.5 µg/L
Selenio <2 µg/L
Talio <2 µg/L
tert-Butilbenceno < 0.5 µg/L
Tetracloroeteno < 0.5 µg/L
Tetraclorofenol < 0.2 µg/L
Tetracloruro de carbono < 0.5 µg/L
Tolueno 0.9 µg/L
trans-1,2-Dicloroeteno < 0.5 µg/L
trans-1,3-Dicloropropeno < 0.5 µg/L
Tricloroeteno < 0.5 µg/L

The migration rate (M) was calculated with the next equation:

M = cn / (S / V · t) [mg dm-2d-1]
where:
M = Migration rate
cn = The concentration obtained (expressed as mg/L and calculated with (cn = an – bn ) where an
is the concentration obtained in the migration and bn the concentration obtained in the blank).
t = Migration period (10 days)
S/V = rate surface / volume in dm-1 (1.2dm-1)

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Migration rate calculation:

Table 2.1. Results 2340963 to 23±1 ºC.

COMPOUNDS Concentration and migration

ANALYZED rate
INCLUDED IN THE
bnT anT cnT MnT
REPORT (ANNEX I)
(m+p)-cresol < 1.90 ×10-4
< 4.0µg/L < 4.0 µg/L < 4.0 µg/L
mg/dm2 día
1,1,1,2 – < 2.38 ×10-5
Tetracloroetano < 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,1,1 – Tricloroetano < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,1,2,2 – < 2.38 ×10-5
Tetracloroetano < 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,1,2 – Tricloroetano < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,1 – Dicloroetano < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,1 - Dicloroeteno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,1-Dicloropropeno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,2,3-Tricloropropano < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,2,4-Trimetilbenceno 7.14 ×10-5
< 0,5 µg/L 1.5 µg/L 1.5 µg/L
mg/dm2 día
1,2-Dibromo-3- < 2.38 ×10-5
cloropropano < 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,2-Dibromoetano < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,2-Diclorobenceno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,2-Dicloroetano < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día

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1,2-Dicloropropano < 2.38 ×10-5
0.8 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,3,5-Trimetilbenceno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,3-Diclorobenceno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,3-Dicloropropano < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
1,4-Diclorobenceno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
2,4,6-triclorofenol < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
2,4-diclorofenol < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
2,4-dimetilfenol < 4.76 ×10-5
< 1.0 µg/L < 1.0 µg/L < 1.0 µg/L
mg/dm2 día
2-clorofenol < 4.76 ×10-5
< 1.0 µg/L < 1.0 µg/L < 1.0 µg/L
mg/dm2 día
2-Clorotolueno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
2-nitrofenol < 2.38 ×10-4
< 5.0 µg/L < 5.0 µg/L < 5.0 µg/L
mg/dm2 día
4-Clorotolueno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
4-cloro-3-metilfenol < 4.76 ×10-5
< 1.0 µg/L < 1.0 µg/L < 1.0 µg/L
mg/dm2 día
Antimonio < 9.52 ×10-5
< 2 µg/L < 2 µg/L < 2 µg/L
mg/dm2 día
Arsénico < 9.52 ×10-5
< 2 µg/L < 2 µg/L < 2 µg/L
mg/dm2 día
Bario < 9.52 ×10-5
< 2 µg/L < 2 µg/L < 2 µg/L
mg/dm2 día
Benceno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Berilio < 9.52 ×10-5
< 2 µg/L < 2 µg/L < 2 µg/L
mg/dm2 día

Bromobenceno < 2.38 ×10-5

< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día

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Bromodiclorometano < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Bromoformo < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Cadmio < 9.52 ×10-5
< 2 µg/L < 2 µg/L < 2 µg/L
mg/dm2 día
cis-1,2-Dicloroeteno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
cis-1,3-Dicloropropeno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Clorobenceno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Cloroformo < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Cobre < 9.52 ×10-5
< 2 µg/L < 2 µg/L < 2 µg/L
mg/dm2 día
Cromo < 9.52 ×10-5
< 2 µg/L < 2 µg/L < 2 µg/L
mg/dm2 día
Dibromoclorometano < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Dibromometano < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Diclorometano < 2.38 ×10-5
7.7 µg/L 6.9 µg/L < 0,5 µg/L
mg/dm2 día
Estireno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Etilbenceno 1.00 ×10-4
< 0,5 µg/L 2.1 µg/L 2.1 µg/L
mg/dm2 día
Fenol < 4.76 ×10-5
< 1.0 µg/L < 1.0 µg/L < 1.0 µg/L
mg/dm2 día
Isopropilbenceno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
m+p-Xileno 2.62 ×10-4
< 0,5 µg/L 5.5 µg/L 5.5 µg/L
mg/dm2 día
Mercurio < 9.52 ×10-6
< 0.20 µg/L < 0.20 µg/L < 0.20 µg/L
mg/dm2 día
n-Butilbenceno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día

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n-Propilbenceno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Naftaleno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
o-Cresol < 9.52 ×10-5
< 2.0 µg/L < 2.0 µg/L < 2.0 µg/L
mg/dm2 día
o-Xileno 1.05 ×10-4
< 0,5 µg/L 2.2 µg/L 2.2 µg/L
mg/dm2 día
p-Isopropiltolueno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Pentaclorofenol < 2.38 ×10-6
< 0,05 µg/L < 0,05 µg/L < 0,05 µg/L
mg/dm2 día
Plomo < 9.52 ×10-5
< 2 µg/L < 2 µg/L < 2 µg/L
mg/dm2 día
sec-Butilbenceno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Selenio < 9.52 ×10-5
< 2 µg/L < 2 µg/L < 2 µg/L
mg/dm2 día
Talio < 9.52 ×10-5
< 2 µg/L < 2 µg/L < 2 µg/L
mg/dm2 día
tert-Butilbenceno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Tetracloroeteno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Tetraclorofenol < 9.52 ×10-6
< 0.2 µg/L < 0.2 µg/L < 0.2 µg/L
mg/dm2 día
Tetracloruro de carbono < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Tolueno 4.29 ×10-5
< 0,5 µg/L 0.9 µg/L 0.9 µg/L
mg/dm2 día
trans-1,2-Dicloroeteno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
trans-1,3- < 2.38 ×10-5
Dicloropropeno < 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Tricloroeteno < 2.38 ×10-5
< 0,5 µg/L < 0,5 µg/L < 0,5 µg/L
mg/dm2 día
Barrido de compuestos 7.31 ×10-3
orgánicos BS EN 5.25µg/L 158.8 µg/L 153.55 µg/L
15768 mg/dm2 día

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5. CONCLUSIONS.

- The final liquid obtained in the migration process in the test water has been analyzed in
order to determine some compounds included in NSF/ANSI 61-2013 Regulation and
indicated in table 2.1 and calculated the migration rate.
- Different organic compounds such as Ethylbenzene, m+p–Xylene and o–Xylene were
detected in the sample coded as 2340963. These compounds are included in D1 and D4
tables in NSF/ANSI 61-2013 Regulation. In the case of Ethylbenzene, it does not
exceed the value set by that Regulation, which sets a maximum value of 0.7mg/L. in
the case of Xylenes, does not exceed the value set by that Regulation, which sets a
maximum value of 10mg/L
- In the Analysis of Organic Compounds (ANEX II), Diethyl Phthalate, Ethylbenzene and
Xylenes, were detected. These compounds are included in D1, D3 and D4 tables in
NSF/ANSI 61-2013. In the case of Diethyl Phthalate does not exceed the value set by
that Regulation, which sets a maximum value of 6mg/L. the value obtained was
0.009mg/L. Other compounds were detected in that analysis, but are not included in
NSF/ANSI 61-2013 tables and no toxicity was found for these substances.
- The product coded as 2340963 (PROTECFULL SFP 108) meets all the criteria set out
in NSF/ANSI 61-2013 Regulation.

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6. ANNEX

ANNEX I. Analysis report for samples 2323323 (Samples) and 2323324(Blanks).

ANNEX II. Screening of organic compounds.

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