Dr. Specht Express: Analytical Report AR-21-XP-008880-02

Eurofins Dr.
Specht Express GmbH

Am Neuländer Gewerbepark 2
Dr. Specht Express DE-21079 Hamburg
GERMANY
Tel: +49 40881448 500

Fax:
specht-express@eurofins.de
Eurofins Dr. Specht Express GmbH · Am Neuländer Gewerbepark 2 · DE-21079 Hamburg
www.eurofins.de
Person in charge: Mr. S. Ring

TSI Life Science Advance, S.A.
attn. Report
Ultrapark 2. Edificio Flex, Oficina 2,
Lagunilla, Heredia
COSTA RICA
Hamburg, 10.05.2021
{249FC5AB-13BD-4535-9E5A-A26787F847FD}
Analytical report AR-21-XP-008880-02

This report replaces report number: AR-21-XP-008880-01
Sample Code 208-2021-00008324 ÌAR-21-XP-ÇÂxpÈ-02WÎ
Reception date time: 25.02.2021

Sample name: milk powder
Marking: "PIL Andina S.A.
Muestra: Leche entera instantánea en polvo, medium heat.
Origen Santa Cruz
Lote: SC 039. VENC: 08 FEB 2022
Muestreo: Las muestras se toman de los almacenes de leche
en polvo (Pil Andina S.A. –
Planta Santa Cruz)."
Client sample code: 2021PO1168-1
Origin: Bolivia
Organic: No
Original client: PIL Andina S.A.
Sampling date: 18.02.2021
Amount: 2400 g
Start analysis: 26.02.2021
End analysis: 10.05.2021
Pesticides Result MRL RL Unit
SP101 Organochlorine Pesticides and Pyrethroids (GC-ECD)

Method: ASU L 00.00-34:2010-09, DFG-S19, GC-ECD
Subcontracted to Eurofins Dr. Specht Laboratorien GmbH, Hamburg, which is accredited for this test.
Screened pesticides Not Detected
SP104 Organophosphorus Pesticides (GC-FPD)

Page 1/11
All information regarding the sample (except those recorded on site or at sample registration by Eurofins) have been
provided by the client. This information can have an impact on the validity of the analytical results and the result assessment.
The results of examination refer exclusively to the checked samples.

Any publication of this report requires written permission. An excerpt publication is not allowed.
General Manager: Marco Miebach
HRB 141396 AG Hamburg
UniCredit Bank AG 7000003300
(BLZ 207 300 17)
IBAN DE59 2073 0017 7000 0033 00
BIC-/SWIFT-Code HYVEDEMME17
DE307567456
Our General Terms & Conditions, available upon request and online at http://www.eurofins.de/lebensmittel/kontakt/avb.aspx, shall apply.
Analytical report: AR-21-XP-008880-02
Sample Code: 208-2021-00008324
Dr. Specht Express
Dr. Specht Express
Pesticides Result MRL RL Unit
Method: ASU L 00.00-34:2010-09, DFG-S19, GC-FPD

Subcontracted to Eurofins Dr. Specht Laboratorien GmbH, Hamburg, which is accredited for this test.
Screened pesticides Not Detected
Heavy Metals Result MRL RL Unit
JCHRA Lead (Pb) in honey, rice (syrup), milk products, sugar

Method: DIN EN 15763:2010 (2010-04), mod., CON-PV 01274 (2017-12), ICP-MS/MS
(Modification: incl. ICP-MS/MS, extension of the analysis parameters, extension of the application scope to feed,
tobacco and tobacco products)
Subcontracted to Eurofins WEJ Contaminants GmbH, Hamburg, which is accredited for this test.
Lead (Pb) 5 1 µg/kg
Veterinary Medicinal Drugs Result Unit
JCAM5 Aminoglycosides
Method: §64 LFGB L 06.00-62, mod., CON-PV 01324 (2020-01), LC-MS/MS
Amikacin <100 * µg/kg
Apramycin <100 * µg/kg
Gentamycine <100 * µg/kg
Hygromycin B <100 * µg/kg
Kanamycine <100 * µg/kg
Neomycin <100 * µg/kg
Paromomycin <100 * µg/kg
Spectinomycin <100 * µg/kg
Tobramycin <100 * µg/kg
JC0A2 Amphenicols
Method: Internal Method, CON-PV 01211 (2019-11), LC-MS/MS
Chloramphenicol (CAP) <0 .3 * µg/kg
Florfenicol <10 * µg/kg
Florfenicol amine <50 * µg/kg
Thiamphenicol <10 * µg/kg
JCBA1 beta-Agonists
Bromobuterol <0 .1 * µg/kg
Chlorbrombuterol <0 .1 * µg/kg
Cimaterol <0 .5 * µg/kg
Page 2/11

(BLZ 207 300 17)
IBAN DE59 2073 0017 7000 0033 00
DE307567456
Sample Code: 208-2021-00008324
Dr. Specht Express
Dr. Specht Express
Cimbuterol <0 .5 * µg/kg

Clenbuterol <0 .1 * µg/kg
Clencyclohexerol <1 * µg/kg
Clenpenterol <0 .5 * µg/kg
Clenproperol <0 .5 * µg/kg
Fenoterol <5 * µg/kg
Hydroxymethylclenbuterol <0 .1 * µg/kg
Isoxsuprine <0 .5 * µg/kg
Mabuterol <0 .1 * µg/kg
Mapenterol <0 .1 * µg/kg
Orciprenalin <10 * µg/kg
Ractopamine <1 * µg/kg
Ritodrine <0 .5 * µg/kg
Salbutamol <5 * µg/kg
Salmeterol <5 * µg/kg
Terbutalin <10 * µg/kg
Tulobuterol <0 .1 * µg/kg
Zilpaterol <5 * µg/kg
JCBL3 beta-Lactams
Amoxicillin <40 * µg/kg
Ampicillin <40 * µg/kg
Cloxacillin <20 * µg/kg
Dicloxacillin <20 * µg/kg
Methicillin <20 * µg/kg
Nafcilline <20 * µg/kg
Oxacillin <20 * µg/kg
Penicillin G <10 * µg/kg
Penicillin V <10 * µg/kg
Cefapirin <50 * µg/kg
Cefazolin <50 * µg/kg
Cefoperazon <50 * µg/kg
Ceftiofur <50 * µg/kg
Cefalexin <150 * µg/kg
Cefquinome <40 * µg/kg
Cephalonium <50 * µg/kg
JCES2 Estrogens
Page 3/11

(BLZ 207 300 17)
IBAN DE59 2073 0017 7000 0033 00
DE307567456
Sample Code: 208-2021-00008324
Dr. Specht Express
Dr. Specht Express
17ß-Estradiol <1 * µg/kg

17a-Estradiol <1 * µg/kg
Estrone <1 * µg/kg
Estriol <1 * µg/kg
Hexestrol <1 * µg/kg
Dienestrol <1 * µg/kg
Ethinyl-Estradiole <1 * µg/kg
Diethylstilbestrol <1 * µg/kg
Zeranol <1 * µg/kg
Beta-zearalanol <1 * µg/kg
JCCC4 Coccidiostats
Diclazuril <2 ** µg/kg
Lasalocid <1 * µg/kg
Maduramycin <2 ** µg/kg
Monensin <2 ** µg/kg
Narasin <2 ** µg/kg
Nicarbazin calculated as DNC <2 * µg/kg
Robenidine <4 * µg/kg
Salinomycin <2 ** µg/kg
JCCS1 Corticosteroids
Dexamethasone <0 .5 * µg/kg
Betamethasone <0 .5 * µg/kg
Flumethasone <0 .5 * µg/kg
Prednisolone <2 * µg/kg
6-alpha-methylprednisolone <5 * µg/kg
Triamcinolone acetonide (Corticoid) <5 * µg/kg
JCMA5 Macrolides
Clindamycin <100 * µg/kg
Erythromycin <100 * µg/kg
Josamycin <100 * µg/kg
Lincomycin <100 * µg/kg
Roxithromycin <100 * µg/kg
Spiramycin <100 * µg/kg
Page 4/11

(BLZ 207 300 17)
IBAN DE59 2073 0017 7000 0033 00
DE307567456
Sample Code: 208-2021-00008324
Dr. Specht Express
Dr. Specht Express
Tiamulin <100 * µg/kg

Tilmicosin <100 * µg/kg
Tulathromycin <100 * µg/kg
Tylosin <100 * µg/kg
JCNF4 Nitrofuran metabolites

AHD (1-Aminohydantoin) <0 .5 ** µg/kg
AMOZ (3-Amino-5-morpholinomethyl-2-oxazol) <0 .5 * µg/kg
AOZ (3-Amino-2-oxazolidinone) <0 .5 * µg/kg
SEM (Semicarbazide) <0 .5 ** µg/kg
JCSM4 Streptomycin
Method: §64 LFGB L 06.00-62, mod., CON-PV 01324 (2020-01), LC-MS/MS
Dihydro-streptomycin <100 * µg/kg
Streptomycin <100 * µg/kg
JCSU4 Sulfonamides
Sulfabenzamide <100 * µg/kg
Sulfacetamide <100 * µg/kg
Sulfachloropyridazine <100 * µg/kg
Sulfaclozine (Sulfachlorpyrazine) <100 * µg/kg
Sulfadiazine <100 * µg/kg
Sulfadimethoxine <100 * µg/kg
Sulfadoxine <100 * µg/kg
Sulfaguanidine <100 * µg/kg
Sulfamerazine <100 * µg/kg
Sulfameter <100 * µg/kg
Sulfadimidine (Sulfamethazine) <100 * µg/kg
Sulfamethizole <100 * µg/kg
Sulfamethoxazole <100 * µg/kg
Sulfamethoxypyridazine <100 * µg/kg
Sulfamonomethoxine <100 * µg/kg
Sulfanilamide <100 * µg/kg
Sulfaphenazole <100 * µg/kg
Sulfapyridine <100 * µg/kg
Sulfaquinoxaline <100 * µg/kg
Sulfathiazole <100 * µg/kg
Page 5/11

(BLZ 207 300 17)
IBAN DE59 2073 0017 7000 0033 00
DE307567456
Sample Code: 208-2021-00008324
Dr. Specht Express
Dr. Specht Express
Sulfisomidine <100 * µg/kg

Sulfisoxazole <100 * µg/kg
Trimethoprim <100 * µg/kg
Ormethoprim <100 * µg/kg
Dapsone <100 * µg/kg
JCTC1 Tetracyclines
Chlortetracycline <50 * µg/kg
Doxycycline <50 * µg/kg
Oxytetracycline <50 * µg/kg
Tetracycline <50 * µg/kg
JCSE1 Tranquilizer
Acepromazine <5 * µg/kg
Azaperol <5 * µg/kg
Azaperon <5 * µg/kg
Carazolol <5 * µg/kg
Chlorpromazine <5 * µg/kg
Haloperidol <5 * µg/kg
Ketamine <5 * µg/kg
Propionyl-promazine <5 * µg/kg
Xylazine <5 * µg/kg
JCBC1 Polypeptide antibiotics Bacitracin/Colistin

Bacitracin <20 ** µg/kg
Colistine <75 * µg/kg
Polymyxin B <100 * µg/kg
JCMC3 Malachite green/antiparasitic dyes

Malachite green <10 * µg/kg
Leucomalachite green <10 * µg/kg
Crystal violet (C.I. 42555) <10 * µg/kg
Leucocrystal violet <10 * µg/kg
Brilliant green <10 * µg/kg
Methylene blue <100 * µg/kg
Page 6/11

(BLZ 207 300 17)
IBAN DE59 2073 0017 7000 0033 00
DE307567456
Sample Code: 208-2021-00008324
Dr. Specht Express
Dr. Specht Express
Basic Blue 7 (C.I. 42595) <10 * µg/kg
J1050 Phosphorus (P)

Method: EN ISO 11885 (2009-09), mod., CON-PV 00006 (2020-01), ICP-OES
(Modification: extension of the scope of application to food, feed, tobacco and tobacco products after pressure
digestion)
Phosphorus (P) 7700 mg/kg
MRL = Maximum Residue Level RL = Reporting Limit

* = below indicated quantification level
** = Below indicated detection level
Page 7/11

(BLZ 207 300 17)
IBAN DE59 2073 0017 7000 0033 00
DE307567456
Sample Code: 208-2021-00008324
Dr. Specht Express
Dr. Specht Express
List of analysed substances:

Reporting Limit Reporting Limit

Substance Substance
mg/kg mg/kg
Aclonifen 0.01 Acrinathrin 0.01
Aldrin 0.002 Benfluralin 0.002
Bifenox 0.02 Bifenthrin 0.01
Binapacryl 0.01 Bromocyclen 0.01
Bromoxynil-octanoate 0.01 Butralin 0.02
Chlordane, cis- 0.002 Chlordane, oxy- 0.002
Chlordane, trans- 0.002 Chlorfenapyr 0.005
Chlorfenprop-methyl 0.01 Chlorfenson 0.01
Chloroneb 0.02 Chlorothalonil 0.01
Chlorthal-dimethyl 0.002 Cyfluthrin 0.01
Cyhalothrin, lambda-(incl. Cyhalothrin, 0.01 Cypermethrin 0.01
gamma-)
Cypermethrin, alpha- 0.01 DDD, o,p- 0.002
DDD, p,p'- 0.002 DDE, o,p- 0.002
DDE, p,p'- 0.002 DDT, o,p'- 0.002
DDT, p,p'- 0.002 Deltamethrin 0.01
Diallate 0.1 Dibromobenzophenone, p,p- 0.01
Dichlobenil 0.005 Dichlone 0.02
Dichlorobenzophenone, o,p- 0.01 Dichlorobenzophenone, p,p- 0.01
Dicloran 0.002 Dicofol, o,p- 0.01
Dicofol, p,p- 0.01 Dieldrin 0.002
Dienochlor 0.01 Dinitramine 0.005
Dinobuton 0.01 Dinocap 0.1
Endosulfan sulphate 0.004 Endosulfan, alpha- 0.002
Endosulfan, beta- 0.002 Endrin 0.003
Endrin ketone 0.01 Esfenvalerate 0.01
Ethalfluralin 0.005 Etridiazole 0.01
Fenfluthrin 0.01 Fenpropathrin 0.01
Fenson 0.01 Fenvalerate (RR-/SS-Isomers) 0.01
Fenvalerate (RS-/SR-Isomers) 0.01 Flubenzimine 0.005
Fluchloralin 0.005 Flucythrinate 0.01
Flumetralin 0.005 Fluorodifen 0.01
Fluoroimide 0.02 Fluvalinate (sum of isomers) 0.01
Genite 0.01 Halfenprox 0.01
HCH, alpha- 0.002 HCH, beta- 0.004
HCH, delta- 0.002 HCH, epsilon- 0.002
Heptachlor 0.002 Heptachlor epoxide, cis- 0.002
Heptachlor epoxide, trans- 0.002 Hexachlorobenzene (HCB) 0.002
Page 8/11

(BLZ 207 300 17)
IBAN DE59 2073 0017 7000 0033 00
DE307567456
Sample Code: 208-2021-00008324
Dr. Specht Express
Dr. Specht Express

Substance Substance
mg/kg mg/kg
Ioxynil-octanoate 0.01 Isobenzan 0.002
Isodrin 0.002 Isopropalin 0.005
Lindane (gamma-HCH) 0.002 Methoxychlor 0.01
Mirex 0.002 Nitrapyrin 0.01
Nitrofen 0.003 Nonachlor, cis- 0.002
Nonachlor, trans- 0.002 Octachlorstyrene 0.01
Oxyfluorfen 0.005 Pendimethalin 0.005
Pentachloranisole 0.002 Pentachloroaniline 0.002
Pentachlorobenzene 0.005 Pentachlorothioanisole 0.002
Permethrin 0.01 Plifenate 0.01
Polychloroterpene (Camphechlor) 0.05 Profluralin 0.002
Quintozene 0.002 S 421 0.005
Tecnazene 0.002 Tefluthrin 0.01
Tetradifon 0.005 Tetrasul 0.01
Tralomethrin 0.02 Transfluthrin 0.01
Triallate 0.01 Trichloronat 0.005
Trifluralin 0.002

Substance Substance
mg/kg mg/kg
Acephate 0.01 Amidithion 0.01
Azinphos-ethyl 0.02 Azinphos-methyl 0.02
Bomyl 0.01 Bromfenvinphos 0.01
Bromophos-ethyl 0.01 Bromophos-methyl 0.01
Butamifos 0.01 Cadusafos 0.01
Carbophenothion 0.01 Carbophenothion-methyl 0.01
Chlorfenvinphos 0.01 Chlormephos 0.01
Chlorpyrifos (-ethyl) 0.01 Chlorpyrifos-methyl 0.01
Chlorthion 0.01 Chlorthiophos 0.01
Coumaphos 0.02 Crufomate 0.01
Cyanofenphos 0.01 Cyanophos 0.01
Demeton-S-methyl 0.01 Demeton-S-methyl-sulfone 0.01
Diazinon 0.01 Dicapthon 0.01
Dichlofenthion 0.01 Dichlorvos 0.01
Dicrotophos 0.01 Dimefox 0.01
Dimethoate 0.01 Dimethylvinphos 0.01
Dioxabenzofos 0.01 Dioxathion 0.01
Page 9/11

(BLZ 207 300 17)
IBAN DE59 2073 0017 7000 0033 00
DE307567456
Sample Code: 208-2021-00008324
Dr. Specht Express
Dr. Specht Express

Substance Substance
mg/kg mg/kg
Disulfoton 0.01 Disulfoton-sulfon 0.01
Ditalimfos 0.01 Edifenphos 0.01
EPN 0.01 Ethion 0.01
Ethoprophos 0.01 Etrimfos 0.01
Famophos 0.01 Fenamiphos 0.01
Fenchlorphos 0.01 Fenitrothion 0.01
Fensulfothion 0.01 Fensulfothion-oxon-sulfone 0.03
Fenthion 0.01 Fenthion-oxon-sulfone 0.02
Fenthion-sulfone 0.02 Fenthion-sulfoxide 0.01
Fonofos 0.01 Formothion 0.01
Fosthiazate 0.01 Fosthietan 0.01
Heptenophos 0.01 Iodofenphos 0.01
Iprobenfos 0.01 Isocarbofos 0.01
Isofenphos 0.01 Isofenphos-methyl 0.01
Isoxathion 0.02 Leptophos 0.02
Malaoxon 0.01 Malathion 0.01
Mecarbam 0.01 Mephosfolan 0.01
Methacrifos 0.01 Methamidophos 0.01
Methidathion 0.01 Mevinphos 0.01
Monocrotophos 0.01 Morphothion 0.02
N-Desethyl-pirimiphos-methyl 0.01 Omethoate 0.01
Oxydemeton-methyl 0.02 Paraoxon-ethyl 0.01
Paraoxon-methyl 0.01 Parathion 0.01
Parathion-methyl 0.01 Phenkapton 0.02
Phenthoate 0.01 Phorate 0.01
Phorate-sulfone 0.01 Phorate-sulfoxide 0.01
Phosalone 0.02 Phosfolan 0.01
Phosmet 0.02 Phosphamidon 0.01
Pirimiphos-ethyl 0.01 Pirimiphos-methyl 0.01
Profenofos 0.01 Propaphos 0.01
Propetamphos 0.01 Prothiofos 0.01
Prothoate 0.01 Pyraclofos 0.02
Pyrazophos 0.02 Pyridaphenthion 0.01
Pyrimitate 0.01 Quinalphos 0.01
Quintiofos 0.01 Sulfotep 0.01
Sulprofos 0.02 TEPP 0.01
Terbufos 0.01 Tetrachlorvinphos 0.01
Thiometon 0.01 Thionazin 0.01
Tolclofos-methyl 0.01 Triamiphos 0.02
Triazophos 0.01 Trichlorfon 0.03
Page 10/11

(BLZ 207 300 17)
IBAN DE59 2073 0017 7000 0033 00
DE307567456
Sample Code: 208-2021-00008324
Dr. Specht Express
Dr. Specht Express

Substance Substance
mg/kg mg/kg
Trichloronat 0.01 Vamidothion 0.02
Page 11/11

(BLZ 207 300 17)
IBAN DE59 2073 0017 7000 0033 00
DE307567456

Dr. Specht Express: Analytical Report AR-21-XP-008880-02

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Eurofins Dr.

Specht Express GmbH

Tel: +49 40881448 500

Person in charge: Mr. S. Ring

Analytical report AR-21-XP-008880-02

Sample Code 208-2021-00008324 ÌAR-21-XP-ÇÂxpÈ-02WÎ

Reception date time: 25.02.2021

Pesticides Result MRL RL Unit

SP101 Organochlorine Pesticides and Pyrethroids (GC-ECD)

SP104 Organophosphorus Pesticides (GC-FPD)

The results of examination refer exclusively to the checked samples.

Pesticides Result MRL RL Unit

Method: ASU L 00.00-34:2010-09, DFG-S19, GC-FPD

Heavy Metals Result MRL RL Unit

JCHRA Lead (Pb) in honey, rice (syrup), milk products, sugar

Veterinary Medicinal Drugs Result Unit

The results of examination refer exclusively to the checked samples.

Veterinary Medicinal Drugs Result Unit

Cimbuterol <0 .5 * µg/kg

The results of examination refer exclusively to the checked samples.

Veterinary Medicinal Drugs Result Unit

17ß-Estradiol <1 * µg/kg

The results of examination refer exclusively to the checked samples.

Veterinary Medicinal Drugs Result Unit

Tiamulin <100 * µg/kg

JCNF4 Nitrofuran metabolites

The results of examination refer exclusively to the checked samples.

Veterinary Medicinal Drugs Result Unit

Sulfisomidine <100 * µg/kg

JCBC1 Polypeptide antibiotics Bacitracin/Colistin

JCMC3 Malachite green/antiparasitic dyes

The results of examination refer exclusively to the checked samples.

Veterinary Medicinal Drugs Result Unit

Basic Blue 7 (C.I. 42595) <10 * µg/kg

J1050 Phosphorus (P)

MRL = Maximum Residue Level RL = Reporting Limit

The results of examination refer exclusively to the checked samples.

List of analysed substances:

Reporting Limit Reporting Limit

The results of examination refer exclusively to the checked samples.

SP101 Organochlorine Pesticides and Pyrethroids (GC-ECD)

Reporting Limit Reporting Limit

SP104 Organophosphorus Pesticides (GC-FPD)

Reporting Limit Reporting Limit

The results of examination refer exclusively to the checked samples.

SP104 Organophosphorus Pesticides (GC-FPD)

Reporting Limit Reporting Limit

The results of examination refer exclusively to the checked samples.

SP104 Organophosphorus Pesticides (GC-FPD)

Reporting Limit Reporting Limit

The results of examination refer exclusively to the checked samples.

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