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  • Quantitative Analysis of A Brass Alloy Using CF-LIBS and A Laser Ablation Time-Of-Flight Mass Spectrometer

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    This document summarizes a study that used laser-induced breakdown spectroscopy (LIBS), energy dispersive x-ray spectroscopy (EDX), and laser ablation time-of-flight mass spectrometry (LA-TOF-MS) to perform a quantitative analysis of a brass alloy. The techniques were used to determine the plasma temperature, electron number density, and elemental composition of the alloy. The results found the plasma temperature was 10,000 ± 1,000 K, electron number density was 2.0 ± 0.5 × 1017 cm-3, and the composition was 62% copper and 38% zinc, consistent with certification.

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    This document summarizes a study that used laser-induced breakdown spectroscopy (LIBS), energy dispersive x-ray spectroscopy (EDX), and laser ablation time-of-flight mass spectrometry (LA-TOF-MS) to perform a quantitative analysis of a brass alloy. The techniques were used to determine the plasma temperature, electron number density, and elemental composition of the alloy. The results found the plasma temperature was 10,000 ± 1,000 K, electron number density was 2.0 ± 0.5 × 1017 cm-3, and the composition was 62% copper and 38% zinc, consistent with certification.

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    11 views1 page

    Quantitative Analysis of A Brass Alloy Using CF-LIBS and A Laser Ablation Time-Of-Flight Mass Spectrometer

    Uploaded by

    ameet kumar
    This document summarizes a study that used laser-induced breakdown spectroscopy (LIBS), energy dispersive x-ray spectroscopy (EDX), and laser ablation time-of-flight mass spectrometry (LA-TOF-MS) to perform a quantitative analysis of a brass alloy. The techniques were used to determine the plasma temperature, electron number density, and elemental composition of the alloy. The results found the plasma temperature was 10,000 ± 1,000 K, electron number density was 2.0 ± 0.5 × 1017 cm-3, and the composition was 62% copper and 38% zinc, consistent with certification.

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    5/24/22, 9:30 PM Quantitative analysis of a brass alloy using CF-LIBS and a la..

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     Quantitative analysis of a brass alloy using CF-LIBS and a laser ablation time-of-flight mass spectrometer
    DOI
    Ahmed, Nasar (National Centre for Physics, Quaid-i-Azam University Campus, 45320 Islamabad (Pakistan)); Abdullah, M (National
    Centre for Physics, Quaid-i-Azam University Campus, 45320 Islamabad (Pakistan)); Ahmed, Rizwan (National Centre for Physics,
    Quaid-i-Azam University Campus, 45320 Islamabad (Pakistan)); Baig, M Aslam (National Centre for Physics, Quaid-i-Azam University
    Campus, 45320 Islamabad (Pakistan)); Piracha, N K (Department of Physics, John Carroll University, University Heights, OH-44118,
    (United States)), E-mail: baig@qau.edu.pk, E-mail: baig77@gmail.com  Citation
     Export

    Abstract

    [en] We present a quantitative analysis of a brass alloy using laser induced breakdown spectroscopy, energy dispersive x-ray
    spectroscopy (EDX) and laser ablation time-of-flight mass spectrometry (LA-TOF-MS). The emission lines of copper (Cu I) and zinc
    (Zn I), and the constituent elements of the brass alloy were used to calculate the plasma parameters. The plasma temperature was
    calculated from the Boltzmann plot as (10 000  ±  1000) K and the electron number density was determined as (2.0  ±  0.5)  ×  1017
    cm−3 from the Stark-broadened Cu I line as well as using the Saha–Boltzmann equation. The elemental composition was deduced
    using these techniques: the Boltzmann plot method (70% Cu and 30% Zn), internal reference self-absorption correction (63.36%
    Cu and 36.64% Zn), EDX (61.75% Cu and 38.25% Zn), and LA-TOF (62% Cu and 38% Zn), whereas, the certified composition is
    (62% Cu and 38% Zn). It was observed that the internal reference self-absorption correction method yields analytical results
    comparable to that of EDX and LA-TOF-MS. (paper)

    Primary Subject INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY (S37)

    Secondary Subject MATERIALS SCIENCE (S36)

    Source Available from http://dx.doi.org/10.1088/1555-6611/aa962b; Country of input: International Atomic Energy Agency (IAEA)

    Record Type Journal Article

    Journal Laser Physics (Online); ISSN 1555-6611; ; v. 28(1); [7 p.]

    Country of publication Russian Federation

    Descriptors (DEI)
     ABLATION, BOLTZMANN EQUATION, BRASS, COPPER, ELECTRON DENSITY, ELECTRON TEMPERATURE, ION TEMPERATURE,
    LASER BEAM MACHINING, QUANTITATIVE CHEMICAL ANALYSIS, SELF-ABSORPTION, TIME-OF-FLIGHT MASS
    SPECTROMETERS, X-RAY SPECTROSCOPY, ZINC

    Descriptors (DEC)
     ABSORPTION, ALLOYS, CHEMICAL ANALYSIS, COPPER ALLOYS, COPPER BASE ALLOYS, DIFFERENTIAL EQUATIONS,
    DYNAMIC MASS SPECTROMETERS, ELEMENTS, EQUATIONS, INTEGRO-DIFFERENTIAL EQUATIONS, KINETIC EQUATIONS,
    MACHINING, MASS SPECTROMETERS, MEASURING INSTRUMENTS, METALS, PARTIAL DIFFERENTIAL EQUATIONS,
    SORPTION, SPECTROMETERS, SPECTROSCOPY, TIME-OF-FLIGHT SPECTROMETERS, TRANSITION ELEMENT ALLOYS,
    TRANSITION ELEMENTS, ZINC ALLOYS

    Publication Year 2018

    Language English

    Reference Number 52038113

    INIS Volume 52

    INIS Issue 17

    External URL http://dx.doi.org/10.1088/1555-6611/aa962b

     
    Quantitative analysis of a brass alloy using CF-LIBS and a la..|INIS

    https://inis.iaea.org/search/search.aspx?orig_q=RN:52038113 1/1

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