Method 8330

EPA Method 8000 Series

Explosives

Method 8330 Explosives by HPLC

M-8330-R-SET $ 175 / set of 14 x 1 mL
Each at 0.1 mg/mL in MeOH : AcCN (1:1)
Composite Explosive Mixture
M-8330-R $ 105 / 1 x 1 mL
M-8330-R-SET-10X $ 200 / set of 14 x 1 mL 1.0 mg/mL each in MeOH : AcCN (1:1) 14 comps.
Each at 1.0 mg/mL in MeOH : AcCN (1:1)
1,3-Dinitrobenzene 3-Nitrotoluene
1,3-Dinitrobenzene (01) 3-Nitrotoluene (08) 2,4-Dinitrotoluene 4-Nitrotoluene
2,4-Dinitrotoluene (02) 4-Nitrotoluene (09) 2,6-Dinitrotoluene Tetryl
2,6-Dinitrotoluene (03) Tetryl (10) HMX TNT
HMX (04) TNT (11) RDX 1,3,5-Trinitrobenzene
RDX (05) 1,3,5-Trinitrobenzene (12) Nitrobenzene 2-Amino-4,6-dinitrotoluene
Nitrobenzene (06) 2-Amino-4,6-dinitrotoluene (13) 2-Nitrotoluene 4-Amino-2,6-dinitrotoluene
2-Nitrotoluene (07) 4-Amino-2,6-dinitrotoluene (14)

Method 8330 Explosive Mixtures

M-8330A $ 40 / 1 x 1 mL M-8330B-R $ 30 / 1 x 1 mL
0.1 mg/mL each in AcCN : MeOH (1:1) 7 comps. 0.1 mg/mL each in AcCN : MeOH (1:1) 7 comps.
M-8330A-10X $ 50 / 1 x 1 mL M-8330B-R-10X $ 45 / 1 x 1 mL
1.0 mg/mL each in AcCN : MeOH (1:1) 7 comps. 1.0 mg/mL each in AcCN : MeOH (1:1) 7 comps.

1,3-Dinitrobenzene RDX 2-Amino-4,6-dinitrotoluene 2-Nitrotoluene

2,4-Dinitrotoluene 1,3,5-Trinitrobenzene 4-Amino-2,6-dinitrotoluene 3-Nitrotoluene
HMX TNT Tetryl 4-Nitrotoluene
Nitrobenzene 2,6-Dinitrotoluene

M-8330A-R $ 45 / 1 x 1 mL M-8330B-R2 $ 30 / 1 x 1 mL
0.1 mg/mL each in AcCN : MeOH (1:1) 8 comps. 0.1 mg/mL each in AcCN : MeOH (1:1) 6 comps.
M-8330A-R-10X $ 55 / 1 x 1 mL M-8330B-R2-10X $ 40 / 1 x 1 mL
1.0 mg/mL each in AcCN : MeOH (1:1) 8 comps. 1.0 mg/mL each in AcCN : MeOH (1:1) 6 comps.

2-Amino-4,6-dinitrotoluene Nitrobenzene 4-Amino-2,6-dinitrotoluene 2-Nitrotoluene

1,3-Dinitrobenzene RDX Tetryl 3-Nitrotoluene
2,4-Dinitrotoluene 1,3,5-Trinitrobenzene 2,6-Dinitrotoluene 4-Nitrotoluene
HMX TNT

Technical Note Internal Standard

M-8330-IS $ 15 / 1 x 1 mL
AccuStandard formulated the following A & B mixes to provide M-8330-IS-PAK SAVE 20% $ 60 / 5 x 1 mL
better resolution between possible coeluting analytes. The way 1.0 mg/mL in MeOH
the chemist chooses to optimize the HPLC system dictates which
3,4-Dinitrotoluene
A & B mix is finally used: (M-8330A & M-8330B) or (M-8330A &
M-8330B-R) or (M-8330A-R & M-8330B-R2). When first
performing Method 8330 development, AccuStandard suggests Surrogate Standard
purchasing the high concentration 14 x 1 mL sets. M-8330-SS $ 15 / 1 x 1 mL
1.0 mg/mL in MeOH
M-8330B $ 25 / 1 x 1 mL
0.1 mg/mL each in AcCN : MeOH (1:1) 5 comps. 1,2-Dinitrobenzene

M-8330B-10X $ 40 / 1 x 1 mL
1.0 mg/mL each in AcCN : MeOH (1:1) 5 comps.
Standards of Interest
Tetryl 3-Nitrotoluene
2,6-Dinitrotoluene 4-Nitrotoluene For more Explosive Standards see Method 8095 page 184.
2-Nitrotoluene

To help prevent premature breakdown of thermally labile products

when in transit, we suggest you request a "Cold Pack".

No. 5057
A measuring apparatus for explosions for the
offical investigation of gun powder and
different explosives

210 Quality System is Certified to comply with the International ISO 9001 Quality Standard
 EPA Method 8000 Series Method 8330-
8440
Explosives

Method 8330 Additional Explosives by HPLC

Analyte Concentration Solvent Cat. No. Price
(mg/mL) (1 x 1 mL)
Nitroglycerin 0.1 EtOH M-8330-ADD-1 $ 20
PETN 0.1 MeOH M-8330-ADD-2 20

Method 8330-8440
Picric acid 0.1 AcCN : MeOH (1:1) M-8330-ADD-3 20
3,5-Dinitroaniline 0.1 AcCN : MeOH (1:1) M-8330-ADD-4 20
EGDN 0.1 AcCN M-8330-ADD-5 20
Nitroguanidine 0.1 MeOH M-8330-ADD-6 20
Nitromethane 0.1 MeOH M-8330-ADD-7 20
Hydrazine 0.1 MeOH M-8330-ADD-8 20
1,2-Diaminopropane 0.1 MeOH M-8330-ADD-9 20
Guanidine nitrate 0.1 MeOH M-8330-ADD-10 20
PYX(2,6-bis,bis-(picrylamino) -3,5-dinitropyridine 0.1 AcCN M-8330-ADD-11 20
2,4-Diamino-6-nitrotoluene 0.1 AcCN M-8330-ADD-12 40
2,6-Diamino-4-nitrotoluene 0.1 AcCN M-8330-ADD-13 40
1,3,5-Triamino -2,4,6-trinitrobenzene (TATB) 0.04 Dimethylformamide M-8330-ADD-14-DMF 40
2,2’,6,6’-Tetranitro-4,4’-azoxytoluene 0.1 AcCN : MeOH (1:1) M-8330-ADD-15 75
4,4’,6,6’-Tetranitro-2,2’-azoxytoluene 0.1 AcCN : MeOH (1:1) M-8330-ADD-16 75
2,2’,6,6’-Tetranitro-4,4’-azotoluene 0.1 AcCN M-8330-ADD-17 100
4,4’,6,6’-Tetranitro-2,2’-azotoluene 0.1 AcCN M-8330-ADD-19 100
2-Hydroxylamino-4,6-dinitrotoluene * 0.1 AcCN M-8330-ADD-18 115
4-Hydroxylamino-2,6-dinitrotoluene * 0.1 AcCN M-8330-ADD-20 115
2,3-Dimethyl-2,3-dinitrobutane 0.1 AcCN M-8330-ADD-21 30
Picramic acid 0.1 AcCN : MeOH (1:1) M-8330-ADD-22 30
2,4,6-Triaminotoluene trihydrochloride NEW 10 mg neat M-8330-ADD-23N 25

* 3 month stability
Technical Note
Standards of Interest
Expanded Explosives Offering - Contact us for additional requirements.
See pages 18-26 for Second Source, Third Party Certified ACES
AccuStandard’s synthesis department has added several additional
Standards.
explosive analytes for analysis by Method 8330. Please contact our
Technical Service Department at 800-442-5290 if you have
requirements for analytes not listed.

Method 8410 Semi-Volatiles by GC/FTIR Method 8440 Total Petroleum Hydrocarbon Analysis
Internal Standard Total Recoverable Petroleum Hydrocarbon Mix
M-8410-IS $ 30 / 1 x 1 mL M-8440 $ 20 / 1 x 1 mL
M-8410-IS-PAK SAVE 20% $ 120 / 5 x 1 mL M-8440-PAK SAVE 20% $ 80 / 5 x 1 mL
2.0 mg/mL each in CH2Cl2 2 comps. At stated conc. in Tetrachloroethene 3 comps.
1-Fluoronaphthalene p-Terphenyl-d14 Chlorobenzene (0.10 w/w %) Isooctane (0.15 w/w %)
n-Hexadecane (0.15 w/w %)
Standards of Interest
For Analytes see Z-014-R-SET, page 102. Silica Gel Cleanup Calibration Solution
M-8440-SGC $ 10 / 1 x 1 mL
M-8440-SGC-PAK SAVE 20% $ 40 / 5 x 1 mL
10.0 mg/mL in Tetrachloroethene

Corn Oil
Method 8430 bis(2-Chloroethyl)ether & Hydrolysis
Products
Total Petroleum Hydrocarbon Concentrate Mix
M-8430 $ 20 / 1 x 1 mL M-8440-CON $ 30 / 1 x 1 mL
1.0 mg/mL each in Water 5 comps. M-8440-CON-PAK SAVE 20% $ 120 / 5 x 1 mL
3 comps.
bis(2-Chloroethyl)ether Diethylene glycol
Chlorobenzene (10 vol %) Isooctane (15 vol %)
2-Chloroethanol Ethylene glycol
n-Hexadecane (15 vol %)
2-(2-Chloroethoxy)-ethanol

AccuStandard • Tel. 800-442-5290 / 203-786-5290 • Fax 203-786-5287 • www.accustandard.com 211