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Article history: The gyroid has been identified as a cellular topology suitable for engineering applications and, particularly in its
Received 27 July 2020 solid-network form, for biomedical applications. Its solid-surface form has received less attention but offers ad-
Received in revised form 21 August 2020 ditional benefits of a continuous surface that partitions space and provides large surface area for heat transfer
Accepted 23 August 2020
or cell attachment. Through numerical methods it is shown for the first time that under uniaxial loading the
Available online 26 August 2020
solid-surface gyroid distributes loads predominantly within helical substructures. Furthermore, by adjusting
Keywords:
the thickness of the load carrying helical regions, the mechanical response can be tuned in different directions.
Triply periodic minimal surfaces This novel discovery enables more efficient use of material distribution while taking advantage of the unique
Compression properties of the solid-surface gyroid.
Finite element analysis © 2020 Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://
Functional grading creativecommons.org/licenses/by-nc-nd/4.0/).
Relative stiffness
1. Introduction (TPMS) which was neither self-intersecting nor contained any straight
lines [1]. The gyroid has been recognised in biological and crystallo-
The gyroid was described by Schoen in 1970, as a surface topology graphic structures [2,3]; as photonic crystal structures in butterfly
which obeys the requirements of a triply periodic minimal surface wing scales [4], and mitochondria membranes on retinal cones in spe-
cies of tree shrews [5].
⁎ Corresponding author at: RMIT Centre for Additive Manufaturing, RMIT University,
Due to its smooth repeating surface with locally minimum area
Melbourne, Australia. which divides space into two distinct regions, the gyroid offers opportu-
E-mail address: martin.leary@rmit.edu.au (M. Leary). nities for efficiency in engineering applications. However, due to its
https://doi.org/10.1016/j.matdes.2020.109096
0264-1275/© 2020 Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
D. Downing, A. Jones, M. Brandt et al. Materials and Design 197 (2021) 109096
complex shape - difficult to produce with traditional manufacturing bending-dominated, displaying stiffness indices between 1.6 and 2.4;
methods - it did not receive much attention as a load bearing depending on respective orientation of the unit cell to the load [21].
engineering structure. Prior to the flexibility provided by additive On the other hand, the solid-surface gyroid stiffness response has
manufacturing (AM), foams represented some of the earliest been reported as closer to stretch-dominated with n ≈ 1.4 [13], al-
engineered forms of cellular structures. Attention to the gyroid grew though only primary loading directions 〈001〉 were presented. At the
with the emergence of industrial AM processes which could replicate same time, the conductivity of the solid-surface gyroid was described
its form in advanced engineering materials [6,7]. Compared to the as isotropic, however only the three primary directions were evaluated.
random pore architecture produced by non-AM methods, the controlled The repeatability of the solid-surface gyroid structure, and the ease
pore size of a stereolithographic produced gyroid demonstrated a with which its volume fraction can be managed with local thickness
10-fold increase in permeability [8]. Structures based on the gyroid has enabled the gyroid to be exploited as a building block for radio-
and other TPMS can now be found in aerospace, automotive and bio- graphic dosage phantoms, providing indistinguishable readings in
medical applications [9,10].The material efficiency of the gyroid pro- Hounsfeld units (a measure of radiodensity) between orientations as
vides structural performance benefits for light-weighting and stiffness opposed to alternate slit based phantoms [22]. The three-dimensional
modification as well as large surface area for heat transfer or biological repeating nature of the gyroid, and the symmetry of the terms in its
cell attachment [10–13]. representative level-set equations might lead to the presumption that
There are several structural forms derived from the gyroid surface the gyroid structures are isotropic in their mechanical response. How-
which are of engineering interest, including: the lattice or solid- ever, both the structure's topology and the AM process used to fabricate
network form (filling one side with material leaving the other as a them introduce directional differences. The AM process can influence
void) [14], the cellular, matrix or solid-surface form [15] (a thickened microstructural alignment and introduce orientation dependence in
surface, maintaining two distinct void regions) (Fig. 1). the mechanical response [17]. Numerical investigation of compressive
The solid-network form has received considerable attention in stiffness and strength for the solid-network form showed up to 30% var-
biomedical applications for use in patient specific implants. [17,18]. iation of strength and stiffness with load orientation [21,23]. Further-
However, the solid-surface gyroid consistently shows superior perfor- more, as commonly observed in AM parts, the as-manufactured
mance compared to the solid-network gyroid, particularly at low thickness can be dependent on build orientation; for instance, on a
volume fraction [15]. 316L stainless steel AM gyroid, the regions fabricated with surface nor-
Besides the gyroid, a variety of lattice and cellular structures are seen mal perpendicular to the build direction were undersized, while regions
in nature providing high material efficiency, such as light weight trabec- with surface normal parallel to the build direction were oversized [24].
ular and cortical bone structures, wood and honeycombs [19]. These The surface-based gyroid structures show improved fatigue perfor-
benefits are sought in engineering applications, where lattice and cellu- mance over strut based lattices [25]. Nevertheless, the surface gyroids
lar structures have been employed to efficiently attenuate the mechan- tend to suffer from crack initiation from lack-of-fusion micro-pores
ical, thermal and electrical response of their parent material. A useful under the surface and from increased surface roughness [26]. Process
metric is the ratio of the density of the cellular structure, ρ, to the den- parameters were more effective at enhancing fatigue performance on
sity of its parent material, ρs, known as the relative density or volume thicker walled structures (50–60% macro-porosity) than on thin walled
fraction. In relation to the properties of the solid material, these struc- structures (80–90% macro-porosity) [27]. As-built and stress relieved
tures tend to respond to an increase in their relative density with a Ti6Al4V gyroids tend to show brittle fracture at relative low cycle num-
power law behaviour [20]. A physical property of the cellular structure, ber, while hot isostatic pressing can extend fatigue life [26].
P, can be related to the property of the solid material, Ps, through Eq. (1). Significant variation in mechanical strength and stiffness between
The power index, n, and the constant, C, can be determined experimen- loading directions can also be introduced through design; with func-
tally. The value of n is dependent on the nature of the cellular structure tionally graduated changes in relative density or cell size along the prin-
(open-celled, closed-cell etc.) and the topology. cipal directions [28]. Compression loading along the direction of
n gradient change can produce a controlled layer-by-layer crushing be-
P ρ haviour while maintaining a shear band crushing when loaded perpen-
¼C ð1Þ
Ps ρs dicular to the gradient direction [23].
To further investigate the mechanical behaviour of gyroid structures,
In the case of mechanical properties such as stiffness and strength, many researchers have used numerical modelling methods. These
lattice structures tend to be categorised by their topology into methods have been used to identify stress distribution, and to extend
bending-dominated and stretch-dominated structures. Gibson and experimental findings by investigating the effect of selected design pa-
Ashby identify foams as bending-dominated structures. The solid- rameters [16]. The structural performance of the gyroid compares well
network gyroid's uniaxial compression response is predominantly with other TPMS structures [29]. Under compression loading, the
Fig. 1. Gyroid forms: triply periodic minimal surface (a); solid-network or lattice form (b), solid-surface, solid-sheet, matrix or cellular form (c) [16].
D. Downing, A. Jones, M. Brandt et al. Materials and Design 197 (2021) 109096
2
distribution of high stress throughout the unit cell has been identified as 2π 2π 2π 2π 2π 2π 2
sin x cos y þ sin y cos z þ sin z cos x ≤h
a sign of effective load transfer through the structure [29]. Often numer- a a a a a a
ical results are evaluated with Gibson and Ashby's power relationship ð4Þ
(Eq. (1)), highlighting the strong dependence on relative density.
2
This research uses numerical methods to examine the compression 2π 2π 2π 2π 2π 2π 2
sin x cos y þ sin y cos z þ sin z cos x ≥h
response of the gyroid structure. Through analysis of high stress regions a a a a a a
within the solid-surface gyroid, previously unknown, orientation de- ð5Þ
pendent load carrying substructures are identified. Furthermore, the
paper provides a novel method for locally tuning the thickness of For the gyroid represented by implicit function G(x, y, z) as given by
these substructures to provide bulk anisotropic stiffness and strength Eq. (2), the local surface normal direction, n, is defined by combining the
properties which lead to superior performance through increased mate- partial derivatives of G, as shown in Eq. (6)-Eq. (9).
rial efficiency.
∂G 2π 2π 2π 2π 2π 2π
2. Methods ¼ cos x cos y − sin x sin z ð6Þ
∂x a a a a a a
Fig. 2. Voxel model of 3Z3Z3 gyroid. Nodes identified with kinematic coupling to controlled boundary conditions. Inset shows fine mesh scale.
3
D. Downing, A. Jones, M. Brandt et al. Materials and Design 197 (2021) 109096
σ
ε pl ¼ ln ð1 þ eÞ− ð11Þ 3. Results
E
Compression properties for the bulk material were obtained through The following subsections describe the high stress regions observed
simulation of a solid cube under the same boundary conditions as the in the voxel model, relate these regions to the local surface normal and
gyroid model (Fig. 2). These bulk material compression properties apply the findings to the shell model to explore tuneable performance
(Table 1) were then used to determine relative stiffness and strength. and material efficiency.
Fig. 4. Spiral or helix structure load path within solid-surface gyroid, observed in a finite element voxel mesh from alternate view directions.
4
D. Downing, A. Jones, M. Brandt et al. Materials and Design 197 (2021) 109096
Fig. 5. Helical substructures for gyroid surfaces aligned with the principal directions; x-direction [100] (a), y-direction [010] (b), and z-direction [001] (c). View from [010].
Fig. 6. Comparison of surface alignment to loading direction [001] and stress magnitude. Focussing on results from the central unit cell in a 3Z3Z3 solid-surface gyroid structure under
compressive loading. Surface alignment with load direction is indicated by the dot product b b (a), von Mises stress on voxel mesh (b), chart of element stress versus inclination-load dot
vn
product (c). Stresses are largest in regions where the surface normal is approximately perpendicular to the load direction (b b≈0), and decrease as the surface normal becomes aligned
vn
with the load direction (vbnb ≈1).
5
D. Downing, A. Jones, M. Brandt et al. Materials and Design 197 (2021) 109096
Uniform Thickness 0.025 Z - Helix 0.05 3.1. Structure within a 3D voxel model
X - Helix 0.05 Y - Helix 0.05
XYZ - Helix 0.05 Uniform Thickness 0.05 A 3Z3Z3 gyroid structure was simulated using a solid voxel finite
80 element mesh. The model was loaded by compressing two opposite
Engineering Stress (MPa)
faces, through the linear elastic region, past the yield point, and beyond
60 the compression strength. At a displacement within the linear elastic re-
gion of the response, the elements with von Mises stress greater than
40 half the materials yield stress were identified (Fig. 4). The majority of
these elements lie within several isolated regions, each of these regions
appear as a spiral or helix between the compressed faces.
20
Loading along any one of the three principal axes of the gyroid struc-
ture (eg. [001], [010], [100]) induces stresses predominantly within he-
0
0 0.02 0.04 0.06 0.08 lical substructures aligned with that loading direction. These helical
Engineering Strain (mm/mm) regions, aligned to loading along the principal axis, are evenly spaced
in a square grid and adjacent helices alternate in handedness (or chiral-
Fig. 7. Chart showing stress-strain response of a 3Z3Z3 gyroid nominal uniform thickness
ity). These substructures appear to provide the most direct load path
(0.025 unit length), and the effect of increased thickness (0.05 unit length) applied to the through the structure.
helices associated with the three principal axes (X, Y and Z).
(a)
Uniform (0.025U) Dual-Thick Dist. Thick Dist. Thick
Thickness (U)
Rao 1.0 Rao 2.52 Rao 2.5 Rao 5.0
(b)
Fig. 8. Reinforcing effect of redistributing material to the helical substructures. Normalised compression strength and stiffness at fixed relative density of 0.077 (a). Thickness distribution
contours for select thickness ratios (b). Distributed thickness based on stress-inclination relationship shows significantly greater improvement than the sharp transition of the dual-
thickness distribution across a ± 10° helical band.
6
D. Downing, A. Jones, M. Brandt et al. Materials and Design 197 (2021) 109096
Fig. 9. Gyroid substructures aligned with loading direction. Identifying alternating helices in square grid arrangement along primary axis [001] direction (a), Identifying alternating helices
in hexagonal grid arrangement along body diagonal [111] direction (b), and an intermediate connected structure along [110] direction (c). Structures are viewed along loading direction in
each case.
3.2. Load carrying sub-structures 3.3. Exploration of helix reinforcing effects using shell models
The regions of the gyroid surface which are parallel with the load are To explore the effects of thickening the helical subregions, the
expected to be more efficient at carrying the load. These regions can be modelling shifts to shell elements, where thickness variation can be
identified in the shell model. Shell elements are selected and grouped explored efficiently. Three sets of helices were identified by shell ele-
based on their alignment with the load direction. The selection is ments near perpendicular (80° ≤ α ≤ 100°) to the principal X, Y and Z di-
achieved by determining the angle, α, of the shells unit normal, n b , rela- rections. Compression loading is applied in the Z-direction. For a 3Z3Z3
tive to the load direction, b
v (Eq. (12)). Shell elements with normal ap- celled gyroid structure, with nominal thickness of 0.025 unit length, the
proximately perpendicular to the loading direction are expected to effect of doubling the thickness of the helical substructures for each of
dominate the stiffness response. the principal axes are displayed in Fig. 7. Doubling the thickness on
the Z-aligned helix, increases the peak load by approximately 25% com-
bn
α ¼ arccos v b ð12Þ pared to the original. The same increase on the X- and Y-aligned helices
increase the peak under compression loading aligned with the Z-axis by
Fig. 5 shows the shell elements that have been selected within the approximately 5%. Doubling the thickness of the helical regions for all
range 80° ≤ α ≤ 100° from each of the principal X, Y and Z directions, three directions in the same model increased the peak load by 37%.
for a gyroid defined by Eq. (2). These substructures appear as helices The reinforcing effect of the helices was also explored at a constant
similar to those identified by large von Mises stress in the voxel model. relative density. Balancing increased material at the load aligned helices
The stress distribution from the solid voxel model was extracted with material removed from the remaining structure highlights possible
along with the coordinates of the voxel centroid. The normal vector efficiency gains. Concentrating material within the helical band (de-
(n) for these voxels was then calculated based on the surface gradient fined by 80° ≤ α ≤ 100°), showed stiffness and strength improving to ap-
(Eq. (9)). The alignment with the loading direction is then found by proximately 6% and 10.5% respectively at a thickness ratio of 2.5. Further
increase in thickness ratio beyond 2.5 caused a reduction in perfor-
the dot product between the unit loading direction (bv) and the unit nor-
mance Fig. 8. The gains made by reinforcing the helices appears to be
mal vector (n b).
counteracted by reduced support from surrounding geometry and per-
Comparison of stress with surface inclination was made by isolating
haps stress concentrating effects caused by the increasing step change
the central unit cell within the 3Z3Z3 voxel model in order to reduce
in thickness at the edges of the helices.
boundary effects. The results, displayed in Fig. 6, clearly show higher
In addition to specifying distributions with two distinct thickness
local von Mises stress for the surfaces with normal perpendicular to
regions (Dual-thick), a continuous thickness distribution (Dist-thick),
the load direction, and lower local von Mises stress for surfaces with
based on the stress-inclination relation determined from the voxel
normal parallel to the load direction. Furthermore, the stress measured
model (Eq. (13)), was applied with increasing max/min thickness
at the helix is up to six times that measured elsewhere in the structure.
ratio. These results show a 22% increase in strength and 18% in-
The correlation between surface inclination and stress results are
crease in stiffness from the nominal uniform thickness and across
considered with a best fit curve based on a cosine relationship on the
a larger range of thickness ratio. A summary of these data appear
scalar product of surface normal and load direction vectors (Eq. (13)).
in Table 2.
This analysis was completed for a stress state within the linear-elastic
region corresponding to an effective strain of 0.005 and effective stress
of 27.2 MPa. 3.4. Alternative loading directions
StressVM b b ¼ A cos πb
v n b þB
v n
ð13Þ As the loading direction shifts from the principal X-, Y- and
A ¼ 258:6, B ¼ 361:6, R2 ¼ 0:8402, RMSE ¼ 69:24 Z-directions the substructures (defined by the shell elements normal
to the loading direction) take alternative forms, in particular:
Table 1
Experimental tensile properties and simulated bulk compression properties.
Experimental Tensile Test (from [33] 30\um PBF) Simulated Compression Test of Solid Cube (Relative Density = 1)
Elastic Modulus (E) 113,800 MPa Modulus (0.5% strain) 124,190 MPa
Ultimate Strength (true stress) 1,200 MPa Max Compressive Strength (engineering stress, first peak) 1,287 MPa
7
D. Downing, A. Jones, M. Brandt et al. Materials and Design 197 (2021) 109096
• The [001] loading direction (and other principal axes [100], [010]) has alternative directions will likely shed light on the orientation specific
a square arrangement of the spirals, with adjacent spirals rotating in differences in the structures response.
the opposite direction (Fig. 9a). The association of helices with the gyroid are not entirely new.
• The [111] loading direction (and other body diagonals [111],̅ [111], ̅ Previously, the solid-network gyroid has been approximated by
̅
[111]) has a hexagon arrangement of spirals with adjacent spirals ro- intersecting helices aligned with the three orthogonal principal di-
tating in opposite directions (Fig. 9b). rections (X,Y,Z). The intention, to simplify modelling the complex
• The [110] loading direction has an intermediate connected structure gyroid topology defined by the level set (Eq. (3)) [6]. There was no
(Fig. 9c). speculation of alternative substructure arrangements. By compari-
son, the current paper identifies different helical structures to
those of the solid-network model simplification. Here the helices
If the loading orientation is shifted continuously between the pri- are understood as load paths in the solid-surface gyroid, they alter-
mary axis and body diagonal the helices distort, join into a larger con- nate in chirality and their arrangement are particular to specific
nected structures and split again to a form a new set of helices aligned loading directions.
to different primary axis or body diagonal. The identification of the substructures representing the
Simulation of voxel models for the three cases identified in Fig. 9 re- dominant load path could also inform material location in multi-
produce the same substructures as the most highly stressed regions. The material additive manufacturing applications. The material provid-
simulations also indicate that the stiffness and strength along these al- ing the structural resistance would be concentrated at the load
ternate directions are different from those in the primary X, Y and Z di- path substructure and a second material could conform to the gyroid
rections. These results highlight that the solid-surface gyroid structure shape, providing, for instance, a fluid interface that takes advantage
is not isotropic in response to loading from alternative directions. of the gyroids superior permeability [8].
Fig. 8 showed limitations to improving efficiency by shifting material
4. Discussion from the bulk of the gyroid solid-surface to concentrate at the helical
substructures in two distinct thicknesses, while maintaining a fixed
In this research, it was shown that under macroscopic uniaxial load- mass. The overall structure weakens as the thickened helix receives
ing, the solid-surface gyroid distributes loads predominantly through less support from surrounding material. Advantages may come from
substructures which are load orientation dependent. These substruc- retaining thickness at other linking substructures to provide supporting
tures manifest as arrangements of helices for the loading directions as- interconnections between the main load carrying substructures rather
sociated with the principal axes and the cubic body diagonals. than isolating them.
Furthermore, by adjusting the thickness of the load carrying regions, The substructures, identified in this research for load path align-
the response can be tuned in specific directions. ment, could also be considered for build orientation manufacturability.
The compression response of the solid-network gyroid structure is The AM process allows flexibility to fabricate the complex cellular struc-
also orientation dependent [23]. Using numerical methods, the relative tures, but also has inherent behaviours which introduce non-uniformity
stiffness was observed to range between 0.0057 at [001] and 0.008 at to the fabricated part. Local geometry influences the thermal response,
[111], with the 〈110〉 family of directions providing an intermediate which in turn influences the surface. Inclined geometries are often pro-
stiffness. Across a volume fraction range of 5–15% the stiffness variation duced with increased thickness compared to geometries more aligned
between the three selected directions at the same volume fraction was with the build direction. The method used to identify the dominant
consistently measured at approximately 30%. By comparison, the solid- load carrying sub-structures can also identify regions that align pre-
surface gyroid examined here at lower relative density of 7.7%, showed dominantly with the build direction in AM, regions expected to be fab-
relative stiffness of 0.022 along the [001] loading direction, which in- ricated with tighter tolerances. Regions with surface inclined to the
creased by approximately 20% at the same relative density through build direction and tending to accumulate additional material could
the use of the locally distributed thickness. Further investigation of the also be identified by adjusting the selected angle range (Eq. (12)). The
substructures associated with loading the surface-based gyroid along geometry could then be tuned to accommodate the expected variation
Table 2
Relative Density, Stiffness and Strength of simulated gyroid structures as compared to the compression simulation of the bulk material properties. (U represents unit cell length).
Description Unit Cell Repetitions Helix/Web Thickness Element Size Relative Density Relative Stiffness Relative Strength
Solid voxel model 3Z3Z3 0.05 U nominal 0.03125 (1/32)U 0.155 0.043 0.050
Shell uniform 0.05 U thickness 3Z3Z3 0.05 U 0.024 U 0.155 0.044 0.050
Shell uniform 0.05 U thickness 3Z3Z3 0.05 U 0.048 U 0.155 0.044 0.051
Shell uniform 0.05 U thickness 3Z3Z3 0.05 U 0.096 U 0.156 0.044 0.052
Shell uniform 0.025 U thickness 3Z3Z3 0.025 U 0.024 U 0.0773 0.0204 0.0227
Shell Z-helix, Dual-thick 2.0 3Z3Z3 0.05 U / 0.025 U 0.024 U 0.0863 0.0243 0.0286
Shell X-helix, Dual-thick 2.0 3Z3Z3 0.05 U / 0.025 U 0.024 U 0.0863 0.0218 0.0240
Shell Y-helix, Dual-thick 2.0 3Z3Z3 0.05 U / 0.025 U 0.024 U 0.0863 0.0219 0.0238
Shell XYZ-helices, Dual-thick 2.0 3Z3Z3 0.05 U / 0.025 U 0.024 U 0.1016 0.0271 0.0312
Shell Z-helix, Dual-thick 1.45 3Z3Z3 0.03454 U / 0.02375 U 0.024 U 0.0773 0.0212 0.0243
Shell Z-helix, Dual-thick 1.96 3Z3Z3 0.04409 U / 0.0225 U 0.024 U 0.0773 0.0216 0.0249
Shell Z-helix, Dual-thick 2.52 3Z3Z3 0.05363 U / 0.02125 U 0.024 U 0.0773 0.0216 0.0251
Shell Z-helix, Dual-thick 3.16 3Z3Z3 0.06317 U / 0.02 U 0.024 U 0.0773 0.0214 0.0250
Shell Z-helix,Dual-thick 3.88 3Z3Z3 0.07271 U / 0.01875 U 0.024 U 0.0773 0.0210 0.0245
Shell Z-helix, Dual-thick 4.70 3Z3Z3 0.08825 U / 0.0175 U 0.024 U 0.0773 0.0204 0.0234
Shell Z-helix, Dist-thick 1.5 3Z3Z3 0.0304 U / 0.0203 U 0.024 U 0.0773 0.0220 0.0253
Shell Z-helix, Dist-thick 2.0 3Z3Z3 0.0341 U / 0.0170 U 0.024 U 0.0773 0.0228 0.0265
Shell Z-helix, Dist-thick 2.5 3Z3Z3 0.0368 U / 0.0147 U 0.024 U 0.0773 0.0233 0.0271
Shell Z-helix, Dist-thick 3.0 3Z3Z3 0.0388 U / 0.0129 U 0.024 U 0.0773 0.0237 0.0274
Shell Z-helix, Dist-thick 3.5 3Z3Z3 0.0404 U / 0.00115 U 0.024 U 0.0773 0.0239 0.0275
Shell Z-helix, Dist-thick 4.0 3Z3Z3 0.0417 U / 0.0104 U 0.024 U 0.0773 0.0240 0.0277
Shell Z-helix, Dist-thick 4.5 3Z3Z3 0.0427 U / 0.0095 U 0.024 U 0.0773 0.0241 0.0278
Shell Z-helix, Dist-thick 5.0 3Z3Z3 0.0436 U / 0.0087 U 0.024 U 0.0773 0.0242 0.0278
8
D. Downing, A. Jones, M. Brandt et al. Materials and Design 197 (2021) 109096
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D. Downing, A. Jones, M. Brandt et al. Materials and Design 197 (2021) 109096
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