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Metals and Materials International (2020) 26:719–738

https://doi.org/10.1007/s12540-019-00454-5

Overview of Small Punch Test


S. Arunkumar1 

Received: 15 July 2019 / Accepted: 4 September 2019 / Published online: 21 September 2019
© The Korean Institute of Metals and Materials 2019

Abstract
Small Punch Test (SPT) is an evolving small specimen test technique which has the potential to extract the mechanical prop-
erties from small volume specimens. This test method is used to determine the in situ mechanical properties of components
in service for measuring the structural integrity and residual life. The pre-requisite for using this test is to establish correla-
tions between SPT and conventional tests in priori. A number of correlations have been developed between traditional tests
and SPT results for determining mechanical properties. The validity of these correlations have to be examined, as these are
developed from a specified set of materials and testing conditions. To evaluate SPT and the developed correlations, it is
crucial to understand the fundamentals of this test method, the different regimes of deformation experienced by the specimen
and its sensitivity for various testing parameters. The attempt of this work is to relook the SPT as a whole and its potential
to measure the different mechanical properties. This work lists the various SPT configurations, materials used in literature
and the correlations developed. In addition, the influence of test parameters on SPT response, the viability of empirical or
analytical relations used to extract mechanical properties and the general issues in SPT is discussed.

Keywords  Small punch test · Tensile properties · Creep · Fracture

1 Introduction materials. This technique was primarily developed for inves-


tigating the post-irradiation effects in nuclear power plants
Mechanical property data of structural materials is vital [1–6]. Later, SPT was extended to find the mechanical prop-
for the material development, integrity and remaining life erties of materials like tensile, creep, fatigue, fracture etc.
assessment. In this regard, Small Specimen Test Techniques [7–9]. Recently, finite element method and neural networks
(SSTT) are preferred over conventional tests for two rea- are used for determining tensile properties through SPT. The
sons: (1) when limited volume of material is available and results of SPT are not direct, that is, the raw data of SPT
(2) when it is difficult to handle material in large volume, needs to be processed using empirical or analytical relations
for example, if the material is radioactive. SSTT is more established between SPT and conventional full scale tests
promising for integrity and remaining life estimation of in- [10, 11]. Several researchers have developed many correla-
service components, as these are easy to conduct and nearly tions which is presented in the later sections. For SPT results
non-destructive in nature. Of the available SSTT, Small to be repeatable and consistent, the viability of these corre-
Punch Test (SPT) is predominantly used for determining lations needs to be assessed. To do this, an in-depth under-
the mechanical properties of thin samples. The specimen standing of SPT and the developed correlations is essential.
size required for extracting the properties is similar to the In this regard, this work is taken up to give a brief overview
one needed for Transmission Electron Microscopy (TEM) of the principle of SPT, its sensitivity to test parameters, and
i.e. ~ 3 mm in diameter [1]. Due to such small size, SPT the mechanical properties estimated from the correlations
is applied for in-service components, and estimation of developed by various researchers.
local material properties, of weldment, functionally, graded

* S. Arunkumar
arunkumars@am.amrita.edu
1
Department of Mechanical Engineering, Amrita Vishwa
Vidyapeetham, Amritapuri, India

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Fig. 1  Schematic of SPT setups


a Test fixture of MDBT b Test
fixture of SPT [12]

2 Principle of SPT

Small Punch Test (SPT) is a modified Miniature Disk Bend


Test (MDBT), developed by Manahan M P [1], at MIT in
1981. The primary difference between MDBT and SPT is
the degree of constraint imposed on the specimens. In the
case of MDBT, the sample is simply supported while in
SPT, the sample is clamped between the two dies (Fig. 1).
Thus, MDBT may be used conveniently for brittle mate-
rials and SPT for ductile materials. In case of MDBT, it
is recommended to select such aspect ratio of specimen
where plate buckling does not occur.
In small punch test, a thin specimen, firmly clamped
between the two circular dies, is stretched till failure with
a hemispherical head punch. The punch tip is machined Fig. 2  Schematic of punch geometry a hemispherical head, b ball-
to a hemispherical shape (which is recommended in CEN punch head [87]
Workshop Agreement and used by numerous authors) [6,
13–18]. Alternatively, a hard spherical ball placed at the
tip of flat or concave—head-punch is forced through the This is accomplished by placing a rod right below the speci-
specimen, as shown in Fig. 2 [19, 20]. Either of these men, which is connected to LVDT. Since, the force applied
punch configurations are invariably used in SPT. The on this rod is very small, compliance correction for this rod
advantage of the latter configuration is that, the ball can is not necessary [21]. The typical SPT load–displacement
be replaced by a new one after few trials thereby avoiding response shown in Fig. 3 may be interpreted as follows [22,
the wear of ball and ensuring reproducible results [17]. 23]:
The punch is pushed through the specimen at a constant
displacement rate. A load cell situated above the punch head Zone I Linear elastic—The whole specimen experi-
measures the load applied to the specimen. The displace- ences linear-elastic bending deformation which
ment of the specimen is obtained by a clip gage mounted to is administered by Elastic modulus and Poisson’s
the fixture using knife edges or from the cross-head displace- ratio
ment. The recorded displacement has to be corrected for Zone II Plastic bending—The nature of deformation
compliance. This compliance correction can be eliminated changes to plastic from elastic in this stage. The
by measuring directly the displacement of the specimen. material’s response leaves from linearity with
a slope change due to yielding. This stage is

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Fig. 3  Characteristic load–displacement curve of SPT [22]

administered by K, strength coefficient, and n, a distinct load–displacement curve for a given material has
strain hardening exponent to be obtained from SPT. In the light of the above, a Euro-
Zone III Membrane stretching—The specimen is further pean code of Practice for SPT was first published in 2006
stretched due to biaxial stress. As a consequence describing the test apparatus, procedure, specimen prepara-
of this and due to strain hardening, the slope of tion and recommendations for estimating the tensile, creep
the load–displacement curve increases and fracture properties. Later this was revised in 2007 [27,
Zone IV Plastic instability—Due to continued stretching, 28]. It is also reported in the literature that, SPT response
the material thins and damage initiates with void is affected by the test parameters. Hence, it is necessary to
nucleation and coalescence. The thickness of the understand the influencing parameters on the SPT response
specimen decreases significantly in this stage to arrive at unique load–displacement curve. The following
Zone V Fracture zone—The crack grows in circumferen- section gives a brief idea about this.
tial direction leading to specimen failure. This is
reflected by the drop in the load of load–displace-
ment curve 3 Analysis of SPT Parameters

This load–displacement curve is then translated to obtain Various authors have succeeded in extracting the mechani-
the mechanical properties. The various mechanical prop- cal properties through SPT for different test parameters i.e.
erties like, elastic modulus, yield strength, ultimate tensile for different materials, specimen shapes and thickness, test
strength, creep, fatigue and fracture properties can be esti- speed, ball diameter etc. In addition, from the literature it
mated through the correlations established between SPT and is found that, the SPT response is influenced by these test
conventional full scale test results and a reasonable agree- parameters [32–34]. It is therefore imperative to understand
ment was observed between the two [10, 24–31]. Thus, a the effect of these parameters. A summary of different
pre-requisite for using this test technique is to have these test parameters and materials used by many researchers is
correlations in priori. In addition, for the estimated proper- reported in Table 1.
ties to be repeatable and reliable, it is necessary to make sure
the uniqueness of the load–displacement response. That is,

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Table 1  Selected small punch test configuration reported in the literature


722

Reference Materials tested Specimen details Test speed, Clamping Receiving hole Fillet radius of Punch configuration, mm
mm/min condition diameter, mm receiving die,

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Shape Size, mm Thickness, mm mm Ball diameter Hemispherical
tip diameter

Manahan et al. SS 316 (20% CW), Circular ϕ3 0.25 0.25 Not specified Not specified 0.3 – 1.02
[1] (MDBT) 302SS
Mao and Taka- Alloy steels: PCA, Circular ϕ3 0.25 0.2 Not specified 1.5 Not specified 1.0 –
hashi [24] SUS316, HT-60,
A533B, HT-9
Mao et al. [88] JIC—HT9 (12Cr– Square 10 × 10 0.5 0.2 Not specified Not specified Not specified 2.4 –
1Mo), A533B,
A508, KIC—SiC,
­Y2O3, ­ZrO2
Kameda and Ferritic and austenitic Square and 10 × 10 and 0.25 for circu- 1.2–1.98 for Not specified 3.4 or 4 for Not specified 2.4 for square –
Mao [23] steels, and Cu–Be circular ϕ3 lar and 0.25 both circular square speci- and 1.0 for
alloys and 0.5 for and square men, 1.5 circular
square for circular
specimen
Eto et al. [25] Neutron irradiated Square and 10 × 10 and 0.25 for circu- 0.5 0.5–1.0 N-m 4 for square 0.2 2.4 for square –
ferritic steels— circular ϕ3 lar and 0.25 specimen, and 1.0 for
F-82, F82H, HT-9, and 0.5 for 1.5 for circu- circular
2.25Cr–1Mo square lar specimen
Xu and Zhao 20% CW 316 SS, D9, Circular ϕ3 0.3 0.06 to 600 Not specified 2.4 Not specified – –
[89] Zr–4
Cheon and SA503—pressure Square 10 × 10 0.5 0.5 Not specified 4.0 Not specified 2.4 –
Kim [90] vessel steel, 12Cr—
turbine rotor steel
Fleury and Ha Pressure vessel Square 10 × 10 0.5 0.25 Not specified Not specified Not specified 2.4 –
(part I and steels—1Cr–
part II) [26, 0.5Mo, 2.25Cr–
91] 1Mo, 12Cr–1Mo,
AISI-403
Lee et al. [92] SA106 grade B, Rectangular 10 × 4 0.5 0.5 Not specified Not Specified 0.6 2.4 –
ASTM A533 grade
B
Ruan et al. [89] Eurofer97 steel Circular ϕ3 0.25 Not specified Not specified Not Specified Not Specified 1.0 –
Hussain et al. Not Specified Square, rec- 10 × 10, 0.5 for 0.2–0.25 Not specified 4.0 0.2 – 1.115, 1.633,
[93] tangular and 10 × 2.4 ϕ 3 square and and 2.309
Circular rectangular
and 0.25 for
circular
Lee and Kim ER309L stainless Square and 10 × 10, ϕ 3 0.5 for square 0.2 Not specified 1.6 for circular Not specified 1.0 for circular –
[94] steel, SA508 Cl-3 circular and 0.28 for and 4 for and 2.4 for
RPV steel plat circular square square
Metals and Materials International (2020) 26:719–738
Table 1  (continued)
Reference Materials tested Specimen details Test speed, Clamping Receiving hole Fillet radius of Punch configuration, mm
mm/min condition diameter, mm receiving die,
Shape Size, mm Thickness, mm mm Ball diameter Hemispherical
tip diameter

Eskner and 1Cr–0.5Mo low alloy Circular ϕ 5 and ϕ 3 0.05–0.35 0.06 and 0.3 Not specified 2.8 and 1.5 Not specified 1.0 and 0.5 –
Sandstrom steel, 18Cr–9Ni
[95] austenitic steel
Finarelli et al. Austenitic SS316L Circular ϕ3 0.25 Not specified Not specified 1.5 0.2 – 1.0
[96] (SA and 20%CW),
Low activation
martensitic steel
Budzakoska 6061 (Al–1 Mg– Circular ϕ 10 0.5 – 1.2
et al. [53] 0.6Si)
Contreras et al. Miroalloyed ferritic– Square 10 × 10 0.5 0.2 Not specified 4.0 Not specified – 2.5
Metals and Materials International (2020) 26:719–738

[97] pearlitic structural


steel AE460
Peñuelas et al. Not specified Square 10 × 10 0.5 0.2 Not specified 4.0 0.5 – 2.5
[98]
Isselin and Austenitic stainless Circular ϕ3 0.25 0.05 Not specified 1.5 0 1.0 –
Shoji [99] steels 304L (SA,
WR sensitized)
316L (SA, CW,
WR)348 WR
Cuesta et al. Not specified Square 10 × 10 0.5 0.2 Not specified 4.0 0.5 – 2.4
[100]
Zhao and TC4 titanium alloy Circular ϕ 10 0.6 0.036 Not specified 2.0 0.5 – 2.0
Zhang [101]
Garcia et al. High strength steels, Square 10 × 10 0.5 0.2 Not specified 4 0.2 chamfer – 2.4
[102] structural steels, edge
stainless steels,
aluminum alloy
Rasche et al. Pressure vessel Circular ϕ8 0.5 0.4 Not specified 4 0.25 – 2.5
[22] steel:22NiMoCr37,
laser beam welded
steel EMZ 355
Siegl et al. [47] Steels Circular ϕ8 0.5 0.4 15 kN optimal Not specified Not specified Not specified Not specified
clamping
force

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723

Table 1  (continued)
724

Reference Materials tested Specimen details Test speed, Clamping Receiving hole Fillet radius of Punch configuration, mm
mm/min condition diameter, mm receiving die,

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Shape Size, mm Thickness, mm mm Ball diameter Hemispherical
tip diameter

Prakash and SS304, Cu, Brass Square 10 × 10 0.3 0.5 Cu—12– Not specified Not specified 2.5 –
Arunkumar 15 N m
[32] Brass—14–
17 N m
SS306—25–
30 N m
Hong et al. Austenitic stainless Square 10 × 10 0.5 0.12 Not specified Not specified Not specified 2.4 mm –
[103] steel welds (alumnina
ball above
HRC 65)
Bruchhausen Not specified Circular ϕ8 0.5 Not specified Not specified 4 0.2 × 45 deg – 2.4
et al. [17] chamfer
Andres and P22 steel Circular ϕ8 0.5 0.3 Not specified 4 Not specified 2.5 –
Dymacek
[72]
Mareno et al. AISI 304L stainless Circular ϕ 10 0.4, 0.5, 0.6 0.1 Not specified 10 0.5 2.5 ­(Si3Ni4 –
[21] steel ceramic ball)
Altstadt et al.ferritic-martensitic Circular Not specified 0.25, 0.5 0.5 Not specified 4 and 1.75 0.2 × 45 deg – 2.5 and 1.0
[54] Cr-steels (P91, chamfer
P92, Eurofer97)
and bainitic RPV
(22NiMoCr37,
15Kh2MFA)
Dymacek et al. Fe–Al–based alloy Circular ϕ8 0.5 Not specified Not specified 4 Not specified 2.5 –
[73]
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3.1 Specimen Shape was proposed. There are two ways of normalization. In


the first type, the initial stiffness, yield load, peak load is
The commonly used specimens for SPT have circular, plotted against thickness normalized with initial sample
square and rectangular shapes with different sizes. The thickness respectively, and a power-law scaling relation-
size ranges for circular, square and rectangular are 3–8 mm ship was derived [42]. In the second case, the load–dis-
in diameter and 0.05–0.5 mm in thickness, 10 × 10 mm and placement curve is normalized to 0.5 mm thick using the
0.25–0.5 mm thickness and 10 × 4 mm and 0.25–0.5 mm specific expression given in [43]. However, the validity of
thickness respectively. The European “Code of Practice” normalization outside the materials used and test configu-
CWA 15627:2006 recommends disc shaped specimen of ration must be verified.
diameter 8 mm, and 0.5 mm thick [35, 36]. Numerical
simulation revealed that, the SPT response of flat circu- 3.3 Test Speed
lar (8 mm diameter and 0.45 mm thick) and rectangular
(6.55 × 11 mm, 0.45 mm thick) were nearly same. Limited There are four basic ways of loading the SPT specimen.
works on SPT using curved samples are also reported in First, the punch is pushed at a constant displacement rate
literature [37, 38]. When the extraction of flat sample is (CDR) and the force is measured. This is analogous to tra-
near to impossible due to significantly large curvature, ditional tensile tests. Second, the punch is pushed at con-
curved specimens are used. The SPT results indicated stant force (CF) and time dependence of displacement is
that the maximum force in curved specimen is attained measured, which is similar to traditional creep tests. Third,
for lower displacements in comparison to flat specimen, the specimen is given a constant displacement, followed by
which could be due to the curvature of the specimen. In a holding time, which allows the relaxation of forces. In
an interesting work by Cuesta et al., [39] the level of con- this case, force versus time response is recorded from this
finement of SPT specimen was varied by modifying the test [44]. Fourth, the punch is pushed cyclically by applying
shape of the specimen from conventional square to dog- cyclic loads which is similar to traditional fatigue loads [32,
bone shape with the same thickness. As the web width of 45]. For extracting the static properties, the first three mode
specimen was decreased, the ductility and maximum load of loading is used and the fourth one for assessing the fatigue
reduced. This observation needs to be verified for other and behavior. In CDR test, the typical test speed range is
materials also. Thus, the specimen shape and degree of 0.2–0.5 mm/min. The rationale for selecting such small test
confinement significantly affects the SPT response. As a speeds is to ensure quasi-static punch loading [46]. How-
consequence, for curved and dog-bone specimens, either ever, its influence on the response of SPT is not adequately
the existing correlations (actually developed from flat deliberated in literature. But, for the case of MDBT, punch
specimens) needs to be modified or new ones have to be velocity effects at room temperature is sparingly discussed
developed. This necessitates the adequate investigation on by Manhan [1]. For the case of cyclic SPT, the frequency of
the influence of specimen shapes on the response of SPT loading was around 1 Hz was used. The reason for choosing
and on the different deformation regimes. such a range was, the hysteretic energy was nearly stable
indicating negligible heat and anelastic effects. This ensures
that nearly all of the input work is used in the deforming the
3.2 Specimen Thickness specimen [32].

It is found that, the thickness of the specimen affects the 3.4 Ball Diameter
deformation regimes of the load–displacement curve
significantly. For example, a thin specimen shows a less Both hemispherical ball (1.0–2.5  mm in diameter) and
prominent linear elastic portion, lower maximum load, hemispherical punch tip (1.02–2.5 mm in diameter) have
and lower ductility when compared with a relatively thick been used in SPT. The punch configuration may not have its
specimen. These variations observed in the load–displace- effect on the load–displacement curve, as only the bottom-
ment curve considerably influence the estimated proper- hemisphere of spherical ball or hemispherical head punch
ties. Thin samples undergo more elastic bending while (for a given diameter) will be forced through the specimen.
thick samples allow significant plastic indentation and Nevertheless, the ball diameter has a significant effect on the
bending. Also, it is difficult to machine too thin samples response of SPT. As the ball diameter increases, the peak
and scooping of excess material than the necessary may load increases [22, 40]. It is reported that, for punch tip
impair the integrity of in-service component. Hence, it is diameters smaller than 1.7 mm, the yield and ultimate ten-
necessary to suggest a range of thickness within which sile strengths showed significant scatter [41]. The legitimacy
unique SPT response can be obtained [22, 40, 41]. In of this finding needs to be tested for other materials also.
order to address this problem, normalization technique

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Table 2  List of SPT yield strength correlations


Reference Yield strength relation Method

Mao and Takahashi [24] σy = 360Py/t2o Two tangent method


Xu and Zhao [89] σy = 0.477Py/t2o
Cheon and Kim [90] σy = Py/0.39 for 0.5 mm thick specimen, Offset method, ­to/100
σy = Py/0.083 for 0.25 mm thick specimen
Fleury and Ha [91] σy = 4.512 ­Py/4πrato, ­ra is the radius of contact area
between punch tip and specimen
Ruan et al. [18] σy = (413 ± 68)Py/to2 + (149 ± 108), 80 ≤ T ≤ 293 K
Lee and Kim [94] σy = 0.231Py/ to2 + 68.1 Offset method, ­to/20 for circular and ­to/15 for square
Eskner and Sandstrom [95] Plate bending theory Offset method, 0.5 μm offset from the tangent of the
initial linear slope
Finarelli et al. [96] σy = αPy/to2 , α = 0.36–0.41 Two tangent method
Contreras et al. [97] σy = 0.268Py/to2 + 207, − 60 ≤ T ≤ 50 °C Offset method, t/10
Isselin and Shoji [98] σy =  βEe  , β = 378,115, ­Ee is elastic energy ­(R2 = 0.95) Energy method

Garcia et al. [102] σy = γPy/ to2, Offset method, t/10


­ 2 = 0.922
γ = 0.346 for the tested materials with R

3.5 Clamping Force that, for different elastic modulus, the load–displacement


curve remained nearly same [22]. As the yield strength of
The clamping force between the specimen and die, prevents the materials increased, the initial linear portion (zone I)
the slipping of the specimen. This is another important remained same, but the loads in the rest of zones increased
parameter which affects the load–displacement curve. The with increase in yield strength. Thus, the findings from
clamping force must be strong enough to prevent slipping these experiments or simulations (like the proposed cor-
and small enough to cause no irreversible deformation in relations), could not be extrapolated outside the materials
specimen. Two of the research groups viz., Eto et al. [25] used for testing. As a consequence, a pool of correlations
and Siegl et al. [47] have employed a specified amount of is developed between the results of SPT and conventional
clamping force in SPT. But, no justification is provided for full-scale test (Table 2 and Table 3).
selecting such a range. The experiments of Prakash and The other parameters like fillet radius of the receiving
Arunkumar [32] showed that the clamping force affected die or the chamfer angle and receiving hole-diameter varied
the deformation behavior of the specimen. As the clamping from author to author. The influence of these parameters
force was increased, the peak load increased and at small and coefficient of friction (between punch and specimen) on
displacements higher loads are reached. Specimen thinning the load–displacement curve was obtained from numerical
in the clamped region was observed for excessive clamping simulations [22, 40]. But, the satisfactory explanation for
force. A range of clamping force was suggested for the tested observed response is not discussed amply. The list of small
materials within which the load–displacement curves were punch test configuration employed by selected authors is
nearly unique. A similar work was reported by Siegl et al. reported in Table 1.
[48]. However, for a deeper understanding further experi- The different mechanical properties that can be extracted
ments or numerical simulations are needed for explaining through SPT employing the correlations is described in the
the observed behavior. following sections.

3.6 Material
4 Tensile Properties
In all these tests different class of materials (steels-ferri-
tic, austenitic, irradiated and non-irradiated, non-ferrous 4.1 Ductility
alloys) were used for conducting SPT. It may be observed
that, the load–displacement response of SPT was not iden- Ductility is a measure of the capability of the material to
tical for the above combinations of test parameters. How- plastically deform without failure. In MDBT, the displace-
ever, the typical load–displacement response remained ment of the specimen prior to failure is the measure of duc-
the same displaying different regimes of deformation as tility. A good agreement was found between the ductility
shown in Fig. 2. The finite element simulations revealed values (for 13 different materials) estimated from MDBT

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Table 3  List of SPT ultimate Reference Ultimate tensile strength relation


tensile strength correlations
Mao and Takahashi [24] σuts = 130(Pmax/t2o) − 320, ­Pmax or ­Fm is the maximum load.
Xu and Zhao [89] σuts = nnK, K is strength coefficient, n is strain hardening exponent
Ruan et al. [18] σuts = (77 ± 15)Pmax/t2o + (218 ± 101), 133 ≤ T ≤ 293 K
Lee and Kim [94] σuts = 0.071Pmax/t2o + 60.03
Contreras et al. [97] σuts = 0.051Pmax/t2o + 269, − 60 ≤ T ≤ 50 °C
Garcia et al. [102] σuts = 0.277Pmax/(dmaxto), ­R2 = 0.94, ­dmax displacement corresponding to ­Pmax
Hong et al. [103] σuts = 2.15 ­Pmax + 228
Altstadt et al. [54] Rm= βm Fi/t2o, βm=0.183 for the tested materials with ­R2 = 0.870,

of the load–displacement curve (Fig. 4) obtained from SPT


is used for estimating elastic modulus of the material.
An equation relating elastic modulus and slope of ini-
tial portion was proposed by Giddings et  al. [51] while
investigating the SPT response of Polymethylmethacrylate
(PMMA) bone cement used in joint replacements and is
given as follows:
E = AS (2)
where E is the elastic modulus, S is the initial stiffness
or slope of initial linear portion and A is the constant of
proportionality which depends on Poisson’s ratio and fric-
Fig. 4  Typical load–displacement curve of SPT indicating slope of tional characteristics of the specimen. The value of A (for
initial linear portion
PMMA is 14.6) again, is unique for each material and testing
conditions.
and conventional tensile test [49]. An equation relating the A modified relation was proposed by Prakash et al. [32]
displacement of the specimen at failure (as indicated by a from experimental observations. The ratio of slope of the
drop in load in the disk bend test) to the strain for structural initial linear portion of load–displacement curve to the initial
materials of size 3 mm diameter and 0.3 mm thick was pro- thickness of the specimen is found to be proportional to the
posed by Hamilton and Huang [50] is given below. elastic modulus of material. This is given by the following
equation as:
t𝛿
𝜖= (1) (3)
( )
rd2 + 𝛿 2 E = k S∕to
where, E is the elastic modulus in MPa, S is the slope of
where, ‘t’ and ‘rd’ are the thickness and radius of the disk initial linear portion, to is the initial thickness of the material,
and ‘δ’ and ‘ 𝜖 ’ are the deflection and ductility respectively. and k is the proportionality constant. In this case, the value
The strain at fracture is a measure of ductility which is simi- of the k is determined using the tensile elastic modulus of
lar to total elongation in tensile test. Satisfactory correla- the material. In addition, k is unique for each material and
tion between the ductility estimated from disk bend test and obtained under optimized clamping conditions within which
tensile tests indicated that, the criterion used in this test for the load–displacement curve of SPT is nearly distinct. It is
determining ductility is acceptable. However, for highly duc- reported that, the value of k for copper, brass and SS304
tile materials small punch test is to be used for estimating the are 17.47 N/mm, 16.80 N/mm, 20.35 N/mm respectively.
ductility. Thus, the legitimacy of applying the strain equation The modulus of elasticity estimated from SPT when com-
obtained from disk bend test to small punch test needs to pared with tensile elastic modulus, the deviation was under
be verified since the constrain on the specimen is different. 0.5%. A similar relation proposed by Cuesta et al. [39] is
as follows:
4.2 Elastic Modulus
E = 𝜆(S∕t) (4)
There are two ways of calculating the elastic modulus where λ is a constant obtained using elastic modulus of ten-
through SPT. In the first method, the linear elastic portion sile test.

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Fig. 5  SPT loading and unloading curves [52] Fig. 6  Schematic of yield load estimation a Offset method b Two-
tangent method

An improved equation similar to the above was proposed


by Chica et al. [52], which is given as, stress method” employed in tensile test for estimating
the yield strength On the other hand, in the two-tangent
(5)
( )
E = 𝜆 Sunl ∕t
method, the load corresponding to the point of intersec-
where λ is the correlation factor, Sunl is the slope of unload- tion of the tangents to the initial linear portion and plastic
ing cycle and t is the specimen thickness. The correlation bending portion of load–displacement curve is used. This
factor is related only to geometrical data of the test and is akin to a sharp transition point (from elastic to plastic
independent of the material plastic properties. Thus, setups deformation) exhibited by an ideal material.
with similar geometry will have same correlation factor. The The yield load estimated from either of these methods is
rationale behind using slope of the unloading cycle (Fig. 5) then empirically correlated to the yield strength the mate-
is that, the unloading cycle is purely elastic and zone I is rial. The constants of this empirical relation are obtained
found to be a mixture of two deformation regimes: plastic by using the yield stress determined from tensile test. A
indentation of punch and elastic bending of the specimen number of such relations have been proposed by various
[30]. As a consequence, the combination of plastic and elas- researchers (Table 2). A good agreement was seen between
tic rigidities leads to lower net rigidity. Hence, the slope the yield strength estimated from SPT with conventional
of initial portion is not a suitable parameter to be related tensile test, but only for the materials used in the testing.
with elastic modulus. However, when the specimen was The applicability of these relations for all materials is ques-
loaded and unloaded, no plastic deformation observed dur- tionable as the values of constants may vary from material
ing unloading. The unloading cycle is thus, purely elastic to material and testing conditions. It may be observed from
and is independent of Poisson’s ratio of the material. Based Table 2 that different offset distances have been employed
on these arguments, the elastic modulus of two carbon steels, by different researchers like 0.5 μm, ­to/100, ­to/20, ­to/15, and
aluminum alloy, copper alloy and magnesium alloy was esti- ­to/10 in determining the yield load. Thus, the magnitude of
mated and compared with the tensile elastic modulus. The offset distance of the line is not defined yet. These offset
deviations were under 3% respectively except for magnesium distances are chosen such that the yield strength determined
alloy, which was 6%. from SPT lies close that of tensile yield strength. This might
result in a large scatter in the estimated yield strength. In
4.3 Yield Strength an attempt to draw parallel between the load–displacement
curve of SPT and the tensile stress–strain curve to determine
The transition from the linear elastic portion to plastic bend- the yield load, the differences in the stress situation in either
ing portion of the load–displacement response is used for of these methods are overlooked. In case of tensile test, the
estimating the yield strength (σy) of the material. To ensure entire volume of material in gage section experiences elastic
consistency and repeatability in the measured yield strength or plastic deformation. Hence, a clear cut transition may be
two methods namely offset method and two-tangent method observed in the stress–strain curve as the material departs
are used (Fig. 6). from elastic to plastic deformation. While in SPT, the stress
In the offset method, the load at which the line drawn situations are different from that of tensile test. As the sam-
parallel to the initial linear portion of load–displacement ple is stretched during testing, the variation in the stress
response, offset at a specified distance say t­ o/10 or t­ o/100, distribution is quite complex since some portion of sample
is considered as yield load, ­Py. This is analogous to “proof undergoes yielding while the rest could be in elastic state.

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a punch displacement of 1.29 times the specimen thickness


­(Fi) or 1.1 times the specimen thickness, if the deflection is
measured from the bottom surface the specimen, is used to
estimate the UTS (Fig. 7). The force F ­ i is chosen since at
this force, the onset of plastic-instability is found to occur.
This was corroborated from experiments and simulation by
monitoring thickness reduction versus punch displacement.
Later, the UTS was estimated from SPT using the correlation
[54] given in Table 3. It was found that, it is better to cor-
relate the force, ­Fi to UTS, than the maximum force ­(Fm), as
the use of ­Fm leads to the overestimation of UTS.

Fig. 7  Typical SPT load–displacement response showing point of


instability at ­(vi, ­Fi) maximum force, ­Fm [54] 5 Fracture Toughness

The fracture toughness (ductile fracture toughness, ­JIC and


Therefore, it is difficult to find that point in the load–dis- brittle fracture toughness, ­KIC) is estimated using fracture
placement curve where the entire thickness of the sample strain, ϵf as these two are related inherently (Fig. 8a). From
is subjected to yielding. Although the offset or two-tangent Fig. 8b it may be observed that; the fracture strain is inde-
method ensures repeatability, the accuracy of the data is pendent of the specimen thickness [1]. With increase in frac-
debatable. With a view to alleviate these problems, energy ture strain, the fracture toughness increases. In the existing
approach was proposed where the elastic deformation energy methods, the ductile fracture toughness is empirically related
(area under the load–displacement curve of SPT up to yield to equivalent fracture stain and brittle fracture toughness to
load) is related to yield strength of the material. Satisfactory fracture stress (Table 4). These correlations again are mate-
agreement was found between the yield strengths estimated rial dependent as the constants in these relations vary from
from energetic approach and tensile test for a set of selected material to material. It can be seen from Table 4 that, the
steels in comparison to offset and two-tangent methods. This constants in the expressions of equivalent fracture strain and
finding is again limited to the materials used for testing. Its fracture toughness are not the same. While estimating these
validity for other materials needs to be verified. constants from experiments it is assumed the specimen frac-
tures at the peak load, which in reality, it is not so. For purely
4.4 Ultimate Tensile Strength ductile or brittle materials, the correlations mentioned in the
Table 4 can be used to determine the fracture toughness. To
The ultimate tensile strength (UTS) is estimated from the ascertain the ductility or brittleness of a material from SPT,
maximum load (­ Fm) obtained from the load–displacement Mao et al. [55], proposed to consider the δnon/δ* ratio, where
response (Fig. 7). It is assumed that the specimen necks and δnon is the non-linear deflection including plastic bending
fractures exactly at the maximum load point similar to that and membrane stretching zones and δ* is the fracture deflec-
occurs in a conventional tension test. However, the speci- tion (Fig. 9). If the ratio δnon/δ* is greater than 0.6 the mate-
men may also thin and crack well before the maximum load rial is ductile, while if δnon/δ* is less than 0.2, it is brittle.
is reached during SPT. Researchers have used endoscopes, It is uncertain about the ductile or brittle nature, if the ratio
acoustic emission instruments to find out the onset of crack δnon/δ* is between 0.2 and 0.6.
initiation [53]. Despite the success in capturing the exact Attempts have been made to determine the fracture
crack initiation point with such sophisticated facilities, a properties from SPT using pre-cracked specimens, owing
careful investigation on relating small punch test response to the uncertainties raised by using specimens without the
with conventional tension test is necessary in reducing the pre-crack and the empirical correlations [56]. A fracture
observed uncertainties and large scatter in the quantified mechanics approach based toughness evaluation from SPT
properties. Several empirical and semi-analytical correla- was conducted by Ju et al. [57]. In this approach, a sharp
tions have been proposed for calculating the UTS as given central notch was introduced in the SPT specimen. By using
in Table 3. The error in the estimated UTS from SPT is sig- acoustic emission, the crack initiation point was determined.
nificantly large when compared with the tension test results. The load corresponding to crack initiation was obtained
This might be due to the tendency to draw parallel between from SPT load–displacement curve. The toughness was
the conventional tension test and SPT. One of the plausible then evaluated using plate bending theory. A good correla-
solution to this problem is reported by Altstadt et al. [54]. tion was observed between the fracture toughness evaluated
Rather than using maximum load, the load corresponding to from SPT and ASTM E1921 for SA 508-3 material in the

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Fig. 8  a Variation of ductile fracture toughness with fracture strain [28], b effect of specimen thickness on fracture toughness [26]

Table 4  List of correlations between fracture toughness and equivalent fracture strain


Reference Fracture strain Fracture toughness

Bayoumi and Bassim [28] – JIC = 49ϵ2f  − 8.6 for linear elastic behavior and
JIC = 310ϵf for elastic plastic behavior
2
Mao and Takahashi [16] ϵf = 0.09(δf/t0) , for 0.25 mm and 0.5 mm thick specimen JIC = 345ϵf -113
Mao et al. [88, 104] ϵf = 0.15 (δf/t0)3/2 JIC = 280ϵf − 50,
KIC = 0.07(σf(sp))2/3, fracture stress, σf(sp) = 130Pmax/t2o-320
1.72
Kameda and Mao [23] ϵf = 0.12 (δf/t0) , ϵf > 0.05 for both circular and square JIC = 345ϵf -113, ϵf > 0.4
specimens
Finarelli et al. [96] ϵf = β(δf/t0)2, –
β = 0.254 for the materials tested
Budzakoska et al. [53] ϵf = β(δf/t0)n, JIC = 82ϵf − 23
β = 0.2 ± 0.1 and n = 1±0.6 for the materials tested
Garcia et al. [102] – JIC = 1695ϵf − 1320, ­R2 = 0.8932
Ju et al. [57] –
� �√
P (1+𝜐) b2
Kc = 32 i𝜋h2 ln bc + 4c a
2
  , ­Pi is load at crack initia-
tion, h is plate thickness, b and c are contact radius and
lower die radius respectively, and a is half crack length

lower shelf region (77 K). Similar works [58, 55, 59, 60] 6 Creep Properties
reported that the use of pre-cracked specimens in SPT gives
toughness values consistent with the ASTM standard results. The structural integrity and reliability of components serv-
Recently Cuesta et al. [61] have analyzed the effect of con- ing at high temperatures depends on their creep properties.
finement on the fracture behavior of pre-cracked dog-bone Creep is the time-dependent plastic deformation of mate-
SPT specimen for the same thickness. The results provided rials under constant load above homologous temperature
an idea of variation of fracture properties with respect to the [62]. An important creep property is the time to rupture.
confinement level. The dependence of this parameter with stress and tempera-
ture differs with creep mechanisms. There are two types of
creep mechanism: Diffusion creep and Dislocation creep.
Since diffusion creep occurs at low stresses and tempera-
tures close to melting point, it is of less significance from
the engineering point of view. The dislocation creep occurs
at intermediary and high stresses and around homologous

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Fig. 9  a Relation between


fracture stress and fracture
toughness, b Illustration of non-
linear deflection and fracture
deflection [88]

temperature. The deformation is due to dislocation motion work is needed to validate the same. The comparison of time
or slip. In this mechanism the time to rupture varies non- to fracture versus stress obtained from uniaxial creep and
linearly with stress, which sets up power law creep (Arrhe- SPC tests agreed well with each other (Fig. 10).
nius law and Norton law). Since the laboratory creep tests Another method to convert SPC load to an equivalent stress
lasts for shorter durations (around 1000 h) in comparison was proposed by Izaki et al. [31]. By plotting uniaxial creep
to the duration of in-service components subjected to creep stress and SPC load versus Larson–Miller Parameter (LMP)
(more than 100,000 h), extrapolation techniques are used separately, the SPC load can be converted to equivalent uni-
to estimate the creep property. The most commonly used axial stress for a given LMP. By such conversion (Materials:
extrapolation methods are Larson–Miller, Manson–Haferd, 2.25Cr–1Mo steel boiler pipe—virgin, pre-crept and aged
Orr–Sherby–Dorn, Monkman–Grant. samples), a good correlation was observed between uniaxial
A number of researchers have attempted to obtain infor- creep and SPT creep test results, as shown in Fig. 11.
mation about creep deformation of different materials from By modifying the Chakrabarty’s membrane stretch model,
Small Punch Creep (SPC) tests. To begin with Ule et al. the European Code of Practice related SP load and equivalent
[30], compared the small punch creep results with conven- stress of uniaxial creep test through a constant known as ‘small
tional creep test for 14 MoV 6 3 and X20 CrMoV 12 1 steels. punch creep correction factor, ksp.
By developing an equation similar to Dorn type, where the
F r1.2 h0
stress term was substituted by small punch load, the time to = 3.33ksp (6)
fracture was estimated. The activation energies calculated 𝜎 (0.5D)0.2
using the same equation was lower (nearly up to 25%) in where ­h0 is the initial specimen thickness, r is the radius of
comparison to that determined from conventional creep test. punch and D is the receiving hole diameter. This correc-
In addition, the round robin exercise of these experiments tion factor is dependent on material (particularly on yield
illustrated the repeatability of results (namely, time to frac- strength) and temperature, thus limiting its utility [64–67].
ture and deflection vs time characteristics) obtained from Starting the experiments with ksp = 1, a better value of the
SPT. A similar work was performed by Dobes et al. [63], ksp is found through subsequent SPC test by comparing
for mechanically alloyed Al–C–O alloys. The difference in with uniaxial creep results. A number of SPC experiments
this work is that, the load was divided by a constant, which employing European Code of Practice demonstrated the
was determined statistically, to find the stress. The ratio of capability of SPT in extracting creep properties [68–71]. In
force in SPT and stress in conventional creep test was found addition, the creep life was estimated using Monkman–Grant
to be proportional for the same duration and depended on the relationship and Larson–Miller parameter. The results indi-
ductility of the material. In order to reduce the dispersion in cated that, the small punch creep test has the potential for
the results, a modified ratio was proposed. However, further

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Fig. 10  Time to fracture versus stress and force a in AlC1 (1 wt% carbon), b in AlC2 (2 wt% carbon) [63]

applied load and material deformation behavior. A good cor-


relation between the creep stress–strain rate data estimated
from SPT and conventional tests was obtained. However, the
validity of this correlation needs to be verified for different
testing conditions.
Hou et al. [77], noticed that the central deflection ver-
sus rupture time was akin to conventional creep curves dis-
playing three stages, viz., primary (decreasing creep rate),
secondary (constant rate) and tertiary (increasing rate) as
shown in Fig. 12. Upon proceeding to estimate the creep
properties of 1.25Cr0.5Mo pearlitic steel from SPC test,
the results were consistent with the conventional one. Thus,
claimed that, SPC test has the potential to be used as non-
destructive test to evaluate the creep properties of in-service
components.
The observed differences in the creep properties estimated
between uniaxial creep and SPC tests could be attributed to
two reasons. First, due to the complex nature of small punch
deformation, interpretation of SPT creep results in compari-
son to uniaxial creep test is difficult. In case of SPT, the
Fig. 11  Comparison between the small punch creep and uniaxial data specimen undergoes local deformation whereas in conven-
[31] tional test, the specimen is subjected to overall deformation.
Despite the fact that, the displacement–time record of SPT
evaluating creep properties and life prediction through the looks similar to conventional creep curve, it may not portray
use of this constant [72–75]. directly the primary, secondary and tertiary characteristics
A further attempt by Yang et al. [76], lead to the devel- as claimed by Hou et al. [77]. Hence, Hyde et al. [78], pro-
opment of a relation between deflection and creep strain posed a new reference based stress approach to interpret the
through which creep strain rate can be evaluated (A similar SPT creep data through finite element simulation.
finding was made by Dymacek et al. [73]). From the finite Second, the influence of SPT parameters on the creep
element simulation, it was found that, the deflection and response the specimen. Zhou et al. [79], investigated the
creep strain relation was nearly independent of temperature, effect of small punch parameters on the rupture time, central

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Fig. 12  Deflection versus time of SPC test a influence of Load on SPC, b influence of temperature on SPC [77]

deflection, ball diameter, creep damage, specimen thickness, stretching as opposed to tensile loading in conventional
temperature etc. through numerical simulation on SUS304 creep tests. Also, due to short duration of the test, it is dif-
and Cr5Mo materials. It was observed that, specimen thick- ficult to capture the information of microstructural changes
ness, load level, ball diameter, temperature and ambience occurring in the service components. Most importantly, the
influence the damage rate and rupture time of SPC specimen interpretation of the SPC creep data is not so easy due to
very strongly. Specimen diameter had little effect on the cen- complex nature of loading [82].
tre stress and damage, since there was extraordinarily severe
damage localization phenomenon in the SPC specimen and
the severest damage was always in the centre part of speci- 7 Fatigue Data
men. Since many factors influence significantly on the SPC
test results, experimental devices with high precision are Designing components subjected to fluctuating stresses
needed to ensure repeatability and accuracy. and inspection of the same during its service life to ensure
SPC test can also be extended to anisotropic materials to safety and reliability is very important, since fatigue fail-
extract the creep properties. Blagoeva et al. [80] and Zhao ure occur at stress levels much less than ultimate tensile
et al. [81], respectively evaluated the creep properties of strength, sometimes, without warning. Structural integrity
different segments of P91 and P92 steel weldment by SPC assessment of such in-service components to estimate the
test. The creep properties of base metal (BM), weldment remaining life using conventional tests require bulk speci-
(WM), fine grain heat affected zone (FGHAZ), adjacent to men and takes longer time. Extraction of such bulk speci-
base metal and coarse grain heat affected zone (CGHAZ) are mens from in-service components may impair its integrity.
estimated through experiments and simulation. In the case of Hence, non-destructive evaluation techniques, which are
anisotropic materials, the correlation between the SPC load simple and easy to conduct, becoming attractive in the pre-
and the stress (either by experiments or simulation), varies sent days. Of all the small specimen test techniques SPT
for different segments of the weldment. It was found from is one the reliable test method to assess the fatigue data.
the experiments that, the correlation between the SPC load Research in the direction of determining fatigue data using
and stress depended on the yield strength of the material. SPT is very much limited. To begin with, Villarga et al. [45],
As a consequence, the corresponding relationships between investigated the fatigue behavior of virgin and aged Ultra-
the applied load and stress needs to be determined for BM, High Molecular Weight Polyethylene (UHWMPE) using the
WM, CGHAZ and FGHAZ separately. A close relationship hysteresis energy. The monotonic response of SPT of virgin
was observed between conventional creep and SPC results and aged specimens showed significant difference in terms
of different segments of weldment. of load–displacement indicating the sensitivity of SPT. The
From the above discussion, it is clear about the poten- same set of specimens were subjected to cyclic SPT. The
tial of SPC in obtaining the creep properties. Despite the peak load and the hysteresis energy versus cycles to failure
benefits of SPC test over conventional creep ones, it suffers respectively was monitored (Fig. 13). A unique relation was
from few limitations. With respect to the type of loading seen and on fitting the power law for the data the fatigue
experienced by the specimen, it is bending and membrane information can be obtained.

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734 Metals and Materials International (2020) 26:719–738

Fig. 13  Fatigue response in terms of a peak load and cycles to failure, b hysteresis energy and cycles to failure [45]

The same idea was then extended to metallic materials by leave residual stresses, despite using advanced machining
Prakash et al. [32, 33]. The difference in this work is that, processes. This could motivate to extract a number of sam-
the fatigue damage was quantified using a damage param- ples from different locations. In the process, a large amount
eter. The remaining life of virgin and damaged SS304 mate- of data is accumulated. Since the results of SPT are not
rial using SPT was investigated by Tasdighi et al. [83]. The direct and its interpretation is difficult, it is necessary to
monotonic SPT results showed that, with increased fatigue relate the conventional and SPT results by empirical and
damage, the maximum punch load reduced. With this max- analytical relations. When such correlations are used, the
imum punch load, the change in ultimate tensile strength values of the ‘constant(s)’ vary from material to material.
could be estimated for damaged specimens using available This was evident from the various correlations proposed by
relations in literature. In order to predict the remaining a number of authors for determining the mechanical proper-
life of the damaged specimens, Palmgren–Miner rule was ties. Also, different correlations were proposed for extracting
invoked. The remaining fatigue life was thus determined and the same mechanical property through SPT. In addition, SPT
on verification through SPT confirmed a good agreement response is sensitive to various test parameters as discussed
(with maximum deviation being 18%) with actual loading. in Sect. 3. This necessitates the optimization of test param-
Lewis et al. [84] and Lancaster et al. [85, 86], carried out eters to obtain nearly unique SPT response at least for a class
series of small punch fatigue tests on Ti-6Al-4 V variants of materials.
(cast, forged and Hot-Isostatic-Pressed) material to charac- The two grounds on which the present SPT research
terize the fatigue behavior. Each of these variants were then community working on is: i) improve or develop new cor-
subjected to cyclic SPT and the response of maximum force relations by analyzing the deformation regimes of specimen
versus number of cycles was recorded. The SPT response of in conventional test and SPT and ii) develop an optimized
maximum force versus number cycles were distinct for the testing conditions or testing standard for SPT to ensure that
tested variants, indicating the capability of SPT in assessing the results are repeatable and reliable. The next question is,
the fatigue behavior. “which of the above two problems to be addressed first?”
Merely by improving or proposing new correlations based
on the understanding of mechanics of problem may not yield
8 General Issues and Challenges results consistent with conventional one. It is first necessary
to obtain unique SPT response i.e. unique load–displace-
It is demonstrated by various researchers in the above sec- ment curve for one material or a class of materials. This is
tions that SPT is capable of measuring various mechanical achieved by thoroughly investigating the sensitivity of SPT
properties and can sense the property change or degradation to various test parameters. Thus, without standardizing the
in a material. However, the reported results and findings SPT procedure in terms of specimen size and shape, meth-
comes with several caveats. To begin with, the selected sam- ods of specimen preparation, test fixture, rate of loading,
ple size may not represent the bulk material. This could be and method of data collection and analysis, a large scatter
due to the variation in defect densities in the bulk material in the estimated properties is bound occur. Also, the validity
and the secondary manufacturing process employed could of the correlations developed and the estimated properties

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Metals and Materials International (2020) 26:719–738 735

remain questionable. Hence, a consensus among the devel- means of ultrasonic impact treatment. Results Phys. 7, 1412–
oped correlations need to be arrived. These are the few chal- 1421 (2017)
5. S.-H. Chi, J.-H. Hong, I.-S. Kim, Evaluation of irradiation effects
lenges that needs to be addressed rigorously to fully exploit of 16 MeV proton-irradiated 12Cr–1MoV steel by small punch
the potential of SPT. It is good to see that few standards (SP) tests. Scr. Metall. Mater. 30(12), 1521–1525 (2000)
for SPT is available. For example, ASTM standard (ASTM 6. C. Rodríguez, E. Cárdenas, F.J. Belzunce, C. Betegón, Fracture
F2183-02, ASTM F2977-13 for tensile SP particularly for characterization of steels by means of the small punch test. Exp.
Mech. 53(3), 385–392 (2013)
polymeric materials), Japanese standard (for SPC) and the 7. M. Abendroth, M. Kuna, Determination of deformation and fail-
recent one, European code of Practice, which is evolving. ure properties of ductile materials by means of the small punch
test and neural networks. Comput. Mater. Sci. 28(3–4), 633–644
(2003)
8. E. Altstadt, H.E. Ge, V. Kuksenko, M. Serrano, M. Houska, M.
9 Summary Lasan, M. Bruchhausen, J.-M. Lapetite, Y. Dai, Critical evalua-
tion of the small punch test as a screening procedure for mechani-
At the outset, SPT is a potential technique for measuring the cal properties. J. Nucl. Mater. 472, 186–195 (2016)
mechanical properties from small volume samples extracted 9. M. Abendroth, S. Soltysiak, Assessment of Material Properties
by means of Small Punch Test, in Recent Trends in Fracture and
from in-service components. Various correlations have been Damage Mechanics, ed. by G. Hütter, L. Zybell (Springer, New
developed between SPT and conventional test results to York, 2016), pp. 127–157
determine a range of mechanical properties. However, the 10. K. Li, J. Peng, C. Zhou, Construction of whole stress-strain curve
suitability of these correlations beyond the materials tested by small punch test and inverse finite element. Results Phys. 11,
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and testing conditions needs to be verified. In addition, the 11. C.S. Catherine, J. Messier, P. Christophe, S. Rosinski, J.
state of stress in SPT is different from the conventional tests. Foulds, EPRI-CEA Finite Element Simulation Benchmark and
This makes the development of improved correlations more Inverse Method for the Estimation of Elastic Plastic Behav-
challenging. It is also found that the SPT is more sensitive ior Small Specimen Test Techniques, ASTM STP 1418, vol. 4
(ASTM International, West Conshohocken, 2002), pp. 350–370
to geometry of test set up. Hence, there is a need to arrive 12. S. Arunkumar, R.V. Prakash, Estimation of tensile properties
at the optimum geometry of test set up for which the SPT of pressure vessel steel through automated ball indentation
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