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https://doi.org/10.1007/s12540-019-00454-5
Received: 15 July 2019 / Accepted: 4 September 2019 / Published online: 21 September 2019
© The Korean Institute of Metals and Materials 2019
Abstract
Small Punch Test (SPT) is an evolving small specimen test technique which has the potential to extract the mechanical prop-
erties from small volume specimens. This test method is used to determine the in situ mechanical properties of components
in service for measuring the structural integrity and residual life. The pre-requisite for using this test is to establish correla-
tions between SPT and conventional tests in priori. A number of correlations have been developed between traditional tests
and SPT results for determining mechanical properties. The validity of these correlations have to be examined, as these are
developed from a specified set of materials and testing conditions. To evaluate SPT and the developed correlations, it is
crucial to understand the fundamentals of this test method, the different regimes of deformation experienced by the specimen
and its sensitivity for various testing parameters. The attempt of this work is to relook the SPT as a whole and its potential
to measure the different mechanical properties. This work lists the various SPT configurations, materials used in literature
and the correlations developed. In addition, the influence of test parameters on SPT response, the viability of empirical or
analytical relations used to extract mechanical properties and the general issues in SPT is discussed.
* S. Arunkumar
arunkumars@am.amrita.edu
1
Department of Mechanical Engineering, Amrita Vishwa
Vidyapeetham, Amritapuri, India
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720 Metals and Materials International (2020) 26:719–738
2 Principle of SPT
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administered by K, strength coefficient, and n, a distinct load–displacement curve for a given material has
strain hardening exponent to be obtained from SPT. In the light of the above, a Euro-
Zone III Membrane stretching—The specimen is further pean code of Practice for SPT was first published in 2006
stretched due to biaxial stress. As a consequence describing the test apparatus, procedure, specimen prepara-
of this and due to strain hardening, the slope of tion and recommendations for estimating the tensile, creep
the load–displacement curve increases and fracture properties. Later this was revised in 2007 [27,
Zone IV Plastic instability—Due to continued stretching, 28]. It is also reported in the literature that, SPT response
the material thins and damage initiates with void is affected by the test parameters. Hence, it is necessary to
nucleation and coalescence. The thickness of the understand the influencing parameters on the SPT response
specimen decreases significantly in this stage to arrive at unique load–displacement curve. The following
Zone V Fracture zone—The crack grows in circumferen- section gives a brief idea about this.
tial direction leading to specimen failure. This is
reflected by the drop in the load of load–displace-
ment curve 3 Analysis of SPT Parameters
This load–displacement curve is then translated to obtain Various authors have succeeded in extracting the mechani-
the mechanical properties. The various mechanical prop- cal properties through SPT for different test parameters i.e.
erties like, elastic modulus, yield strength, ultimate tensile for different materials, specimen shapes and thickness, test
strength, creep, fatigue and fracture properties can be esti- speed, ball diameter etc. In addition, from the literature it
mated through the correlations established between SPT and is found that, the SPT response is influenced by these test
conventional full scale test results and a reasonable agree- parameters [32–34]. It is therefore imperative to understand
ment was observed between the two [10, 24–31]. Thus, a the effect of these parameters. A summary of different
pre-requisite for using this test technique is to have these test parameters and materials used by many researchers is
correlations in priori. In addition, for the estimated proper- reported in Table 1.
ties to be repeatable and reliable, it is necessary to make sure
the uniqueness of the load–displacement response. That is,
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Reference Materials tested Specimen details Test speed, Clamping Receiving hole Fillet radius of Punch configuration, mm
mm/min condition diameter, mm receiving die,
13
Shape Size, mm Thickness, mm mm Ball diameter Hemispherical
tip diameter
Manahan et al. SS 316 (20% CW), Circular ϕ3 0.25 0.25 Not specified Not specified 0.3 – 1.02
[1] (MDBT) 302SS
Mao and Taka- Alloy steels: PCA, Circular ϕ3 0.25 0.2 Not specified 1.5 Not specified 1.0 –
hashi [24] SUS316, HT-60,
A533B, HT-9
Mao et al. [88] JIC—HT9 (12Cr– Square 10 × 10 0.5 0.2 Not specified Not specified Not specified 2.4 –
1Mo), A533B,
A508, KIC—SiC,
Y2O3, ZrO2
Kameda and Ferritic and austenitic Square and 10 × 10 and 0.25 for circu- 1.2–1.98 for Not specified 3.4 or 4 for Not specified 2.4 for square –
Mao [23] steels, and Cu–Be circular ϕ3 lar and 0.25 both circular square speci- and 1.0 for
alloys and 0.5 for and square men, 1.5 circular
square for circular
specimen
Eto et al. [25] Neutron irradiated Square and 10 × 10 and 0.25 for circu- 0.5 0.5–1.0 N-m 4 for square 0.2 2.4 for square –
ferritic steels— circular ϕ3 lar and 0.25 specimen, and 1.0 for
F-82, F82H, HT-9, and 0.5 for 1.5 for circu- circular
2.25Cr–1Mo square lar specimen
Xu and Zhao 20% CW 316 SS, D9, Circular ϕ3 0.3 0.06 to 600 Not specified 2.4 Not specified – –
[89] Zr–4
Cheon and SA503—pressure Square 10 × 10 0.5 0.5 Not specified 4.0 Not specified 2.4 –
Kim [90] vessel steel, 12Cr—
turbine rotor steel
Fleury and Ha Pressure vessel Square 10 × 10 0.5 0.25 Not specified Not specified Not specified 2.4 –
(part I and steels—1Cr–
part II) [26, 0.5Mo, 2.25Cr–
91] 1Mo, 12Cr–1Mo,
AISI-403
Lee et al. [92] SA106 grade B, Rectangular 10 × 4 0.5 0.5 Not specified Not Specified 0.6 2.4 –
ASTM A533 grade
B
Ruan et al. [89] Eurofer97 steel Circular ϕ3 0.25 Not specified Not specified Not Specified Not Specified 1.0 –
Hussain et al. Not Specified Square, rec- 10 × 10, 0.5 for 0.2–0.25 Not specified 4.0 0.2 – 1.115, 1.633,
[93] tangular and 10 × 2.4 ϕ 3 square and and 2.309
Circular rectangular
and 0.25 for
circular
Lee and Kim ER309L stainless Square and 10 × 10, ϕ 3 0.5 for square 0.2 Not specified 1.6 for circular Not specified 1.0 for circular –
[94] steel, SA508 Cl-3 circular and 0.28 for and 4 for and 2.4 for
RPV steel plat circular square square
Metals and Materials International (2020) 26:719–738
Table 1 (continued)
Reference Materials tested Specimen details Test speed, Clamping Receiving hole Fillet radius of Punch configuration, mm
mm/min condition diameter, mm receiving die,
Shape Size, mm Thickness, mm mm Ball diameter Hemispherical
tip diameter
Eskner and 1Cr–0.5Mo low alloy Circular ϕ 5 and ϕ 3 0.05–0.35 0.06 and 0.3 Not specified 2.8 and 1.5 Not specified 1.0 and 0.5 –
Sandstrom steel, 18Cr–9Ni
[95] austenitic steel
Finarelli et al. Austenitic SS316L Circular ϕ3 0.25 Not specified Not specified 1.5 0.2 – 1.0
[96] (SA and 20%CW),
Low activation
martensitic steel
Budzakoska 6061 (Al–1 Mg– Circular ϕ 10 0.5 – 1.2
et al. [53] 0.6Si)
Contreras et al. Miroalloyed ferritic– Square 10 × 10 0.5 0.2 Not specified 4.0 Not specified – 2.5
Metals and Materials International (2020) 26:719–738
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723
Table 1 (continued)
724
Reference Materials tested Specimen details Test speed, Clamping Receiving hole Fillet radius of Punch configuration, mm
mm/min condition diameter, mm receiving die,
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Shape Size, mm Thickness, mm mm Ball diameter Hemispherical
tip diameter
Prakash and SS304, Cu, Brass Square 10 × 10 0.3 0.5 Cu—12– Not specified Not specified 2.5 –
Arunkumar 15 N m
[32] Brass—14–
17 N m
SS306—25–
30 N m
Hong et al. Austenitic stainless Square 10 × 10 0.5 0.12 Not specified Not specified Not specified 2.4 mm –
[103] steel welds (alumnina
ball above
HRC 65)
Bruchhausen Not specified Circular ϕ8 0.5 Not specified Not specified 4 0.2 × 45 deg – 2.4
et al. [17] chamfer
Andres and P22 steel Circular ϕ8 0.5 0.3 Not specified 4 Not specified 2.5 –
Dymacek
[72]
Mareno et al. AISI 304L stainless Circular ϕ 10 0.4, 0.5, 0.6 0.1 Not specified 10 0.5 2.5 (Si3Ni4 –
[21] steel ceramic ball)
Altstadt et al.ferritic-martensitic Circular Not specified 0.25, 0.5 0.5 Not specified 4 and 1.75 0.2 × 45 deg – 2.5 and 1.0
[54] Cr-steels (P91, chamfer
P92, Eurofer97)
and bainitic RPV
(22NiMoCr37,
15Kh2MFA)
Dymacek et al. Fe–Al–based alloy Circular ϕ8 0.5 Not specified Not specified 4 Not specified 2.5 –
[73]
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It is found that, the thickness of the specimen affects the 3.4 Ball Diameter
deformation regimes of the load–displacement curve
significantly. For example, a thin specimen shows a less Both hemispherical ball (1.0–2.5 mm in diameter) and
prominent linear elastic portion, lower maximum load, hemispherical punch tip (1.02–2.5 mm in diameter) have
and lower ductility when compared with a relatively thick been used in SPT. The punch configuration may not have its
specimen. These variations observed in the load–displace- effect on the load–displacement curve, as only the bottom-
ment curve considerably influence the estimated proper- hemisphere of spherical ball or hemispherical head punch
ties. Thin samples undergo more elastic bending while (for a given diameter) will be forced through the specimen.
thick samples allow significant plastic indentation and Nevertheless, the ball diameter has a significant effect on the
bending. Also, it is difficult to machine too thin samples response of SPT. As the ball diameter increases, the peak
and scooping of excess material than the necessary may load increases [22, 40]. It is reported that, for punch tip
impair the integrity of in-service component. Hence, it is diameters smaller than 1.7 mm, the yield and ultimate ten-
necessary to suggest a range of thickness within which sile strengths showed significant scatter [41]. The legitimacy
unique SPT response can be obtained [22, 40, 41]. In of this finding needs to be tested for other materials also.
order to address this problem, normalization technique
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3.6 Material
4 Tensile Properties
In all these tests different class of materials (steels-ferri-
tic, austenitic, irradiated and non-irradiated, non-ferrous 4.1 Ductility
alloys) were used for conducting SPT. It may be observed
that, the load–displacement response of SPT was not iden- Ductility is a measure of the capability of the material to
tical for the above combinations of test parameters. How- plastically deform without failure. In MDBT, the displace-
ever, the typical load–displacement response remained ment of the specimen prior to failure is the measure of duc-
the same displaying different regimes of deformation as tility. A good agreement was found between the ductility
shown in Fig. 2. The finite element simulations revealed values (for 13 different materials) estimated from MDBT
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Fig. 5 SPT loading and unloading curves [52] Fig. 6 Schematic of yield load estimation a Offset method b Two-
tangent method
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Fig. 8 a Variation of ductile fracture toughness with fracture strain [28], b effect of specimen thickness on fracture toughness [26]
Bayoumi and Bassim [28] – JIC = 49ϵ2f − 8.6 for linear elastic behavior and
JIC = 310ϵf for elastic plastic behavior
2
Mao and Takahashi [16] ϵf = 0.09(δf/t0) , for 0.25 mm and 0.5 mm thick specimen JIC = 345ϵf -113
Mao et al. [88, 104] ϵf = 0.15 (δf/t0)3/2 JIC = 280ϵf − 50,
KIC = 0.07(σf(sp))2/3, fracture stress, σf(sp) = 130Pmax/t2o-320
1.72
Kameda and Mao [23] ϵf = 0.12 (δf/t0) , ϵf > 0.05 for both circular and square JIC = 345ϵf -113, ϵf > 0.4
specimens
Finarelli et al. [96] ϵf = β(δf/t0)2, –
β = 0.254 for the materials tested
Budzakoska et al. [53] ϵf = β(δf/t0)n, JIC = 82ϵf − 23
β = 0.2 ± 0.1 and n = 1±0.6 for the materials tested
Garcia et al. [102] – JIC = 1695ϵf − 1320, R2 = 0.8932
Ju et al. [57] –
� �√
P (1+𝜐) b2
Kc = 32 i𝜋h2 ln bc + 4c a
2
, Pi is load at crack initia-
tion, h is plate thickness, b and c are contact radius and
lower die radius respectively, and a is half crack length
lower shelf region (77 K). Similar works [58, 55, 59, 60] 6 Creep Properties
reported that the use of pre-cracked specimens in SPT gives
toughness values consistent with the ASTM standard results. The structural integrity and reliability of components serv-
Recently Cuesta et al. [61] have analyzed the effect of con- ing at high temperatures depends on their creep properties.
finement on the fracture behavior of pre-cracked dog-bone Creep is the time-dependent plastic deformation of mate-
SPT specimen for the same thickness. The results provided rials under constant load above homologous temperature
an idea of variation of fracture properties with respect to the [62]. An important creep property is the time to rupture.
confinement level. The dependence of this parameter with stress and tempera-
ture differs with creep mechanisms. There are two types of
creep mechanism: Diffusion creep and Dislocation creep.
Since diffusion creep occurs at low stresses and tempera-
tures close to melting point, it is of less significance from
the engineering point of view. The dislocation creep occurs
at intermediary and high stresses and around homologous
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temperature. The deformation is due to dislocation motion work is needed to validate the same. The comparison of time
or slip. In this mechanism the time to rupture varies non- to fracture versus stress obtained from uniaxial creep and
linearly with stress, which sets up power law creep (Arrhe- SPC tests agreed well with each other (Fig. 10).
nius law and Norton law). Since the laboratory creep tests Another method to convert SPC load to an equivalent stress
lasts for shorter durations (around 1000 h) in comparison was proposed by Izaki et al. [31]. By plotting uniaxial creep
to the duration of in-service components subjected to creep stress and SPC load versus Larson–Miller Parameter (LMP)
(more than 100,000 h), extrapolation techniques are used separately, the SPC load can be converted to equivalent uni-
to estimate the creep property. The most commonly used axial stress for a given LMP. By such conversion (Materials:
extrapolation methods are Larson–Miller, Manson–Haferd, 2.25Cr–1Mo steel boiler pipe—virgin, pre-crept and aged
Orr–Sherby–Dorn, Monkman–Grant. samples), a good correlation was observed between uniaxial
A number of researchers have attempted to obtain infor- creep and SPT creep test results, as shown in Fig. 11.
mation about creep deformation of different materials from By modifying the Chakrabarty’s membrane stretch model,
Small Punch Creep (SPC) tests. To begin with Ule et al. the European Code of Practice related SP load and equivalent
[30], compared the small punch creep results with conven- stress of uniaxial creep test through a constant known as ‘small
tional creep test for 14 MoV 6 3 and X20 CrMoV 12 1 steels. punch creep correction factor, ksp.
By developing an equation similar to Dorn type, where the
F r1.2 h0
stress term was substituted by small punch load, the time to = 3.33ksp (6)
fracture was estimated. The activation energies calculated 𝜎 (0.5D)0.2
using the same equation was lower (nearly up to 25%) in where h0 is the initial specimen thickness, r is the radius of
comparison to that determined from conventional creep test. punch and D is the receiving hole diameter. This correc-
In addition, the round robin exercise of these experiments tion factor is dependent on material (particularly on yield
illustrated the repeatability of results (namely, time to frac- strength) and temperature, thus limiting its utility [64–67].
ture and deflection vs time characteristics) obtained from Starting the experiments with ksp = 1, a better value of the
SPT. A similar work was performed by Dobes et al. [63], ksp is found through subsequent SPC test by comparing
for mechanically alloyed Al–C–O alloys. The difference in with uniaxial creep results. A number of SPC experiments
this work is that, the load was divided by a constant, which employing European Code of Practice demonstrated the
was determined statistically, to find the stress. The ratio of capability of SPT in extracting creep properties [68–71]. In
force in SPT and stress in conventional creep test was found addition, the creep life was estimated using Monkman–Grant
to be proportional for the same duration and depended on the relationship and Larson–Miller parameter. The results indi-
ductility of the material. In order to reduce the dispersion in cated that, the small punch creep test has the potential for
the results, a modified ratio was proposed. However, further
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Fig. 10 Time to fracture versus stress and force a in AlC1 (1 wt% carbon), b in AlC2 (2 wt% carbon) [63]
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Fig. 12 Deflection versus time of SPC test a influence of Load on SPC, b influence of temperature on SPC [77]
deflection, ball diameter, creep damage, specimen thickness, stretching as opposed to tensile loading in conventional
temperature etc. through numerical simulation on SUS304 creep tests. Also, due to short duration of the test, it is dif-
and Cr5Mo materials. It was observed that, specimen thick- ficult to capture the information of microstructural changes
ness, load level, ball diameter, temperature and ambience occurring in the service components. Most importantly, the
influence the damage rate and rupture time of SPC specimen interpretation of the SPC creep data is not so easy due to
very strongly. Specimen diameter had little effect on the cen- complex nature of loading [82].
tre stress and damage, since there was extraordinarily severe
damage localization phenomenon in the SPC specimen and
the severest damage was always in the centre part of speci- 7 Fatigue Data
men. Since many factors influence significantly on the SPC
test results, experimental devices with high precision are Designing components subjected to fluctuating stresses
needed to ensure repeatability and accuracy. and inspection of the same during its service life to ensure
SPC test can also be extended to anisotropic materials to safety and reliability is very important, since fatigue fail-
extract the creep properties. Blagoeva et al. [80] and Zhao ure occur at stress levels much less than ultimate tensile
et al. [81], respectively evaluated the creep properties of strength, sometimes, without warning. Structural integrity
different segments of P91 and P92 steel weldment by SPC assessment of such in-service components to estimate the
test. The creep properties of base metal (BM), weldment remaining life using conventional tests require bulk speci-
(WM), fine grain heat affected zone (FGHAZ), adjacent to men and takes longer time. Extraction of such bulk speci-
base metal and coarse grain heat affected zone (CGHAZ) are mens from in-service components may impair its integrity.
estimated through experiments and simulation. In the case of Hence, non-destructive evaluation techniques, which are
anisotropic materials, the correlation between the SPC load simple and easy to conduct, becoming attractive in the pre-
and the stress (either by experiments or simulation), varies sent days. Of all the small specimen test techniques SPT
for different segments of the weldment. It was found from is one the reliable test method to assess the fatigue data.
the experiments that, the correlation between the SPC load Research in the direction of determining fatigue data using
and stress depended on the yield strength of the material. SPT is very much limited. To begin with, Villarga et al. [45],
As a consequence, the corresponding relationships between investigated the fatigue behavior of virgin and aged Ultra-
the applied load and stress needs to be determined for BM, High Molecular Weight Polyethylene (UHWMPE) using the
WM, CGHAZ and FGHAZ separately. A close relationship hysteresis energy. The monotonic response of SPT of virgin
was observed between conventional creep and SPC results and aged specimens showed significant difference in terms
of different segments of weldment. of load–displacement indicating the sensitivity of SPT. The
From the above discussion, it is clear about the poten- same set of specimens were subjected to cyclic SPT. The
tial of SPC in obtaining the creep properties. Despite the peak load and the hysteresis energy versus cycles to failure
benefits of SPC test over conventional creep ones, it suffers respectively was monitored (Fig. 13). A unique relation was
from few limitations. With respect to the type of loading seen and on fitting the power law for the data the fatigue
experienced by the specimen, it is bending and membrane information can be obtained.
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Fig. 13 Fatigue response in terms of a peak load and cycles to failure, b hysteresis energy and cycles to failure [45]
The same idea was then extended to metallic materials by leave residual stresses, despite using advanced machining
Prakash et al. [32, 33]. The difference in this work is that, processes. This could motivate to extract a number of sam-
the fatigue damage was quantified using a damage param- ples from different locations. In the process, a large amount
eter. The remaining life of virgin and damaged SS304 mate- of data is accumulated. Since the results of SPT are not
rial using SPT was investigated by Tasdighi et al. [83]. The direct and its interpretation is difficult, it is necessary to
monotonic SPT results showed that, with increased fatigue relate the conventional and SPT results by empirical and
damage, the maximum punch load reduced. With this max- analytical relations. When such correlations are used, the
imum punch load, the change in ultimate tensile strength values of the ‘constant(s)’ vary from material to material.
could be estimated for damaged specimens using available This was evident from the various correlations proposed by
relations in literature. In order to predict the remaining a number of authors for determining the mechanical proper-
life of the damaged specimens, Palmgren–Miner rule was ties. Also, different correlations were proposed for extracting
invoked. The remaining fatigue life was thus determined and the same mechanical property through SPT. In addition, SPT
on verification through SPT confirmed a good agreement response is sensitive to various test parameters as discussed
(with maximum deviation being 18%) with actual loading. in Sect. 3. This necessitates the optimization of test param-
Lewis et al. [84] and Lancaster et al. [85, 86], carried out eters to obtain nearly unique SPT response at least for a class
series of small punch fatigue tests on Ti-6Al-4 V variants of materials.
(cast, forged and Hot-Isostatic-Pressed) material to charac- The two grounds on which the present SPT research
terize the fatigue behavior. Each of these variants were then community working on is: i) improve or develop new cor-
subjected to cyclic SPT and the response of maximum force relations by analyzing the deformation regimes of specimen
versus number of cycles was recorded. The SPT response of in conventional test and SPT and ii) develop an optimized
maximum force versus number cycles were distinct for the testing conditions or testing standard for SPT to ensure that
tested variants, indicating the capability of SPT in assessing the results are repeatable and reliable. The next question is,
the fatigue behavior. “which of the above two problems to be addressed first?”
Merely by improving or proposing new correlations based
on the understanding of mechanics of problem may not yield
8 General Issues and Challenges results consistent with conventional one. It is first necessary
to obtain unique SPT response i.e. unique load–displace-
It is demonstrated by various researchers in the above sec- ment curve for one material or a class of materials. This is
tions that SPT is capable of measuring various mechanical achieved by thoroughly investigating the sensitivity of SPT
properties and can sense the property change or degradation to various test parameters. Thus, without standardizing the
in a material. However, the reported results and findings SPT procedure in terms of specimen size and shape, meth-
comes with several caveats. To begin with, the selected sam- ods of specimen preparation, test fixture, rate of loading,
ple size may not represent the bulk material. This could be and method of data collection and analysis, a large scatter
due to the variation in defect densities in the bulk material in the estimated properties is bound occur. Also, the validity
and the secondary manufacturing process employed could of the correlations developed and the estimated properties
13
Metals and Materials International (2020) 26:719–738 735
remain questionable. Hence, a consensus among the devel- means of ultrasonic impact treatment. Results Phys. 7, 1412–
oped correlations need to be arrived. These are the few chal- 1421 (2017)
5. S.-H. Chi, J.-H. Hong, I.-S. Kim, Evaluation of irradiation effects
lenges that needs to be addressed rigorously to fully exploit of 16 MeV proton-irradiated 12Cr–1MoV steel by small punch
the potential of SPT. It is good to see that few standards (SP) tests. Scr. Metall. Mater. 30(12), 1521–1525 (2000)
for SPT is available. For example, ASTM standard (ASTM 6. C. Rodríguez, E. Cárdenas, F.J. Belzunce, C. Betegón, Fracture
F2183-02, ASTM F2977-13 for tensile SP particularly for characterization of steels by means of the small punch test. Exp.
Mech. 53(3), 385–392 (2013)
polymeric materials), Japanese standard (for SPC) and the 7. M. Abendroth, M. Kuna, Determination of deformation and fail-
recent one, European code of Practice, which is evolving. ure properties of ductile materials by means of the small punch
test and neural networks. Comput. Mater. Sci. 28(3–4), 633–644
(2003)
8. E. Altstadt, H.E. Ge, V. Kuksenko, M. Serrano, M. Houska, M.
9 Summary Lasan, M. Bruchhausen, J.-M. Lapetite, Y. Dai, Critical evalua-
tion of the small punch test as a screening procedure for mechani-
At the outset, SPT is a potential technique for measuring the cal properties. J. Nucl. Mater. 472, 186–195 (2016)
mechanical properties from small volume samples extracted 9. M. Abendroth, S. Soltysiak, Assessment of Material Properties
by means of Small Punch Test, in Recent Trends in Fracture and
from in-service components. Various correlations have been Damage Mechanics, ed. by G. Hütter, L. Zybell (Springer, New
developed between SPT and conventional test results to York, 2016), pp. 127–157
determine a range of mechanical properties. However, the 10. K. Li, J. Peng, C. Zhou, Construction of whole stress-strain curve
suitability of these correlations beyond the materials tested by small punch test and inverse finite element. Results Phys. 11,
440–448 (2018)
and testing conditions needs to be verified. In addition, the 11. C.S. Catherine, J. Messier, P. Christophe, S. Rosinski, J.
state of stress in SPT is different from the conventional tests. Foulds, EPRI-CEA Finite Element Simulation Benchmark and
This makes the development of improved correlations more Inverse Method for the Estimation of Elastic Plastic Behav-
challenging. It is also found that the SPT is more sensitive ior Small Specimen Test Techniques, ASTM STP 1418, vol. 4
(ASTM International, West Conshohocken, 2002), pp. 350–370
to geometry of test set up. Hence, there is a need to arrive 12. S. Arunkumar, R.V. Prakash, Estimation of tensile properties
at the optimum geometry of test set up for which the SPT of pressure vessel steel through automated ball indentation
response remains nearly unique. This is to ensure consist- and small punch test. Trans. Indian Inst. Met. 69, 1245–1256
ency and reliability of estimated properties from SPT. Finite (2016)
13. Small Punch Test Method for Metallic Materials, CEN work-
element technique plays an important role in this process. shop agreement, CWA 15627:2007 E
Using this tool, one can gain an insight into the test method 14. I. Cuesta, C. Rodríguez, T. García, J. Alegre, Effect of confine-
and deformation of specimen. Thus, minute details captured ment level on mechanical behaviour using the small punch test.
from numerical methods helps to develop a reliable SPT Eng. Fail. Anal. 58, 206–211 (2015)
15. K. Turba, R.C. Hurst, P. Hähner, Anisotropic mechanical
technique. Presently, no international standards have been properties of the MA956 ODS steel characterized by the
fully developed for SPT. In order for exchanging material small punch testing technique. J. Nucl. Mater. 428(1–3), 76–81
property data across different professional societies, stand- (2012)
ardization of SPT is essential. There are few standards for 16. S. Rasche, S. Strobl, M. Kuna, R. Bermejo, T. Lube, Determina-
tion of strength and fracture toughness of small ceramic discs
SPT like ASTM, Japanese standards and the evolving one, using the small punch test and the ball-on-three-balls test. Proc.
European standardization on SP testing, which is used by the Mater. Sci. 3, 961–966 (2014)
groups that have agreed upon the same. 17. M. Bruchhausen, S. Holmström, I. Simonovski, T. Austin, J.-M.
Lapetite, S. Ripplinger, R. de Haan, Recent developments in
small punch testing: tensile properties and DBTT. Theor. Appl.
Fract. Mech. 86, Part A, 2–10 (2016)
References 18. Y. Ruan, P. Spätig, M. Victoria, Assessment of mechanical prop-
erties of the martensitic steel EUROFER97 by means of punch
1. M.P. Manahan, A.S. Argon, O.K. Harling, The development tests. J. Nucl. Mater. 307, Part 1, 236–239 (2002)
of miniaturized disk bend test for the determination of post- 19. G.E. Lucas, The development of small specimen mechanical test
irradiation mechanical properties. J. Nucl. Mater. 103 & 104, techniques. J. Nucl. Mater. 117(C), 327–339 (1983)
1545–1550 (1981) 20. S. Haroush, E. Priel, D. Moreno, A. Busiba, I. Silverman, A.
2. Y. Peng, L. Cai, H. Chen, C. Bao, A new method based on energy Turgeman, R. Shneck, Y. Gelbstein, Evaluation of the mechanical
principle to predict uniaxial stress–strain relations of ductile properties of SS-316L thin foils by small punch testing and finite
materials by small punch testing. Int. J. Mech. Sci. 138–139, element analysis. Mater. Des. 83, 75–84 (2015)
244–249 (2018) 21. M.F. Moreno, G. Bertolino, A. Yawny, The significance of
3. D. Andrés, T. García, S. Cicero, R. Lacalle, J.A. Álvarez, A. specimen displacement definition on the mechanical properties
Martín-Meizoso, J. Aldazabal, A. Bannister, A. Klimpel, Char- derived from small punch test. Mater. Des. 95, 623–631 (2016)
acterization of heat affected zones produced by thermal cutting 22. S. Rasche, M. Kuna, Improved small punch testing and parameter
processes by means of Small Punch tests. Mater. Charact. 119, identification of ductile to brittle materials. Int. J. Press. Vessels
55–64 (2016) Pip. 125, 23–34 (2015)
4. X. Yang, X. Wang, X. Ling, D. Wang, Enhanced mechanical
behaviors of gradient nano-grained austenite stainless steel by
13
736 Metals and Materials International (2020) 26:719–738
23. J. Kameda, X. Mao, Small-Punch and TEM-disc testing tech- 42. S.M. Kurtz, M. Herr, A.A. Edidin, The effect of specimen thick-
niques and their application to characterization of radiation dam- ness on the mechanical behavior of UHMWPE characterized
age. J. Mater. Sci. 27, 983–989 (1992) by the small punch test, in Crosslinked and Thermally Treated
24. X. Mao, H. Takahashi, Development of a further-miniaturized Ultra High Molecular Weight Polyethylene for Joint Replace-
specimen of 3 mm diameter for tem disk (Ф 3 mm) small punch ments, ASTM STP 1445, ed. by S. M. Kurtz, R. Gsell, and J.
tests. J. Nucl. Mater. 150, 42–52 (1987) Martell (ASTM International, West Conshohocken, PA, 2003)
25. M. Eto, H. Takahashi, T. Misawa, M. Suzuki, Y. Nishiyama, pp. 192–205
K. Fukaya, S. Jitsukawa, Development of a miniaturized bulge 43. R. Lacalle, J. Álvarez, F. Guitérrez-Solana, Analysis of key fac-
test (small punch test) for post-irradiation mechanical property tors for the interpretation of small punch test results. Fatigue
evaluation. ASTM STP 1204, 241–255 (1993) Fract. Eng. Mater. Struct. 31, 841–849 (2008)
26. E. Fleury, J.S. Ha, Small punch tests on steels for steam power 44. P. Dymáček, Recent developments in small punch testing: appli-
plant (II). KSME Int. J. 12(5), 827–835 (1998) cations at elevated temperatures. Theor. Appl. Fract. Mech.
27. S. Jitsukawa, Development of a miniaturized bulge test (small 86(1), 25–33 (2016)
punch test) for post-irradiation mechanical property evaluation. 45. M.L. Villarraga, A.A. Edidin, M. Herr, S.M. Kurtz, Multiaxial
ASTM STP 1204, 241–255 (1993) fatigue behavior of oxidized and unoxidized UHMWPE during
28. M.R. Bayoumi, M.N. Bassim, Study of the relationship between cyclic small punch testing at body temperature. J. ASTM Int.
fracture toughness (JIc) and bulge ductility. Int. J. Fract. 23, 1(1), Paper ID 11218 (2004)
71–79 (1983) 46. M. Abendroth, M. Kuna, Identification of ductile damage and
29. J.M. Baik, J. Kameda, O. Buck, Development of small punch fracture parameters from the small punch test using neural net-
tests for ductile–brittle transition temperature measurement of works. Eng. Fract. Mech. 73(6), 710–725 (2006)
temper embrittled Ni–Cr steels. ASTM STP 888, 92–111 (1986) 47. J. Siegl, P. Haušild, A. Janča, R. Kopřiva, Fractographic aspects
30. B. Ule, T. Sustar, F. Dobes, K. Milicka, V. Bicego, S. Tettamanti, of small punch test results. Proc. Mater. Sci. 3, 912–917 (2014)
K. Maile, C. Schwarzkopf, M.P. Whelan, R.H. Kozlowski, J. 48. J. Siegl, P. Hausild, A. Janca, R. Kopriva, M. Kytka, Characteri-
Klaput, Small punch test method assessment for the determina- zation of mechanical properties by small punch test. Key Eng.
tion of the residual creep life of service exposed components: Mater. 606, 15–18 (2014)
outcomes from an interlaboratory exercise. Nucl. Eng. Des. 192, 49. M. Dooley, G.E. Lucas, J.W. Sheckherd, Small scale ductility
1–11 (1999) tests. J. Nucl. Mater. 103 & 104, 1533–1538 (1981)
31. T. Izaki, T. Kobayashi, J. Kusumoto, A. Kanaya, A creep life 50. M.L. Hamilton, F.H. Huang, Use of the disk bend test to assess
assessment method for boiler pipes using small punch creep the irradiation performance of structural alloys, in The Use of
test. Int. J. Press. Vessels Pip. 86, 637–642 (2009) Small-Scale Specimens for Testing Irradiated Material, ASTM
32. R.V. Prakash, S. Arunkumar, Evaluation of damage in mate- STP 888, ed. by W.R. Corwin, G.E. Lucas (American Society
rials due to fatigue cycling through static and cyclic small for Testing and Materials, Philadelphia, 1986), pp. 5–16
punch testing, in Small Specimen Test Techniques, ed. by M.A. 51. V.L. Giddings, S.M. Kurtz, C.W. Jewett, J.R. Foulds, A.A. Edi-
Sokolov, E. Lucon (West Conshohocken, ASTM International, din, A small punch test technique for characterizing the elastic
2014), pp. 168–186 modulus and fracture behavior of PMMA bone used in total
33. Prakash R V, Arunkumar S. Evaluation of fatigue data through joint replacement. Biomaterials 22, 1875–1881 (2001)
miniature specimen test techniques, in ASME Pressure Ves- 52. J.F. Chica, P.M.B. Díez, M.P. Calzada, Improved correlation
sels and Piping Conference, Volume 1A: Codes and Standards: for elastic modulus prediction of metallic materials in the small
V01AT01A059 (2015) punch test. Int. J. Mech. Sci. 134, 112–122 (2017)
34. R.V. Prakash, S. Arunkumar, Influence of friction on the 53. E. Budzakoska, D.G. Carr, P.A. Stathers, H. Li, R.P. Harrison,
response of small punch test. Trans. Indian Inst. Met. 69(2), A.K. Hellier, W.Y. Yeung, Predicting the J integral fracture
617–622 (2016) toughness of Al 6061 using the small punch test. Fatigue Fract.
35. CEN. CWA 15627: small punch test method for metallic mate- Eng. Mater. Struct. 30, 796–807 (2007)
rials. Technical reports (CEN, Brussels, 2006) 54. E. Altstadt, M. Houska, I. Simonovski, M. Bruchhausen, S.
36. European Committee for Standardization, Small punch test Holmstrom, R. Lacalle, On the estimation of ultimate tensile
method for metallic materials, CEN workshop agreement, stress from small punch testing. Int. J. Mech. Sci. 136, 1–19
CWA 15627:2007 E (2007) (2017)
37. K.K. Dwivedi, K.K. Pathak, M. Panday, A.H. Yegneshwaran, 55. J.M. Alegre, R. Lacalle, I.I. Cuesta, J.A. Alvarez, Different
E. Ramadasan, Influence of material properties on small punch methodologies to obtain the fracture properties of metallic
test using curved specimens. Arch. Appl. Sci. Res. 2(6), 211– materials using pre-notched small punch test specimens. Theor.
218 (2010) Appl. Fract. Mech. 86, 11–18 (2016)
38. I. Simonovski, S. Holmström, M. Bruchhausen, Small punch 56. T.D. Shikalgar, B.K. Dutta, J. Chattopadhyay, Assessment of
tensile testing of curved specimens: finite element analysis and fracture resistance data using p-SPT specimens. Theoret. Appl.
experiment. Int. J. Mech. Sci. 120, 204–213 (2017) Fract. Mech. 98, 167–177 (2018)
39. I.I. Cuesta, C. Rodríguez, T.E. García, J.M. Alegre, Effect of 57. J.B. Ju, J. Jang, D. Kwon, Evaluation of Fracture toughness by
confinement level on mechanical behaviour using the small small-punch testing techniques using sharp notched specimens.
punch test. Eng. Fail. Anal. 58(1), 206–211 (2015) Int. J. Press. Vessels Pip. 80, 221–228 (2003)
40. K.K. Pathak, K.K. Dwivedi, M. Shukla, E. Ramadasan, Influ- 58. E. Cardenas, F.J. Belzunce, D. Rodriguez, I. Penuelas, C. Bet-
ence of key test parameters on SPT results. Indian J. Eng. egon, Application of the small punch test to determine the
Mater. Sci. 16, 385–389 (2009) fracture toughness of metallic materials. Fatigue Fract. Eng.
41. C. Kannan, S. Bhattacharya, D.K. Sehgal, R.K. Pandey, Effect Mater. Struct. 00, 1–10 (2011)
of specimen thickness and punch diameter in evaluation of small 59. T.E. Garcia, C. Rodriguez, F.J. Belzunce, I.I. Cuesta, Devel-
punch test parameters toward characterization of mechanical opment of a new methodology for estimating the CTOD of
properties of Cr–Mo steels. J. Test. Eval. 42(6), 1–9 (2014). https structural steels using the small punch test. Eng. Failure Anal.
://doi.org/10.1520/jte20130299. ISSN 0090-3973 50, 88–99 (2015)
13
Metals and Materials International (2020) 26:719–738 737
60. J.M. Alegre, I.I. Cuesta, H.L. Barbachano, Determination of 79. Z. Zhou, Y. Zheng, X. Ling, R. Hu, J. Zhou, A study on influ-
the fracture properties of metallic materials using pre-cracked ence factors of small punch creep test by experimental investiga-
small punch tests. Fatigue Fract. Engng. Mater. Struct. 38, tion and finite element analysis. Mater. Sci. Eng., A 527(10–11),
104–112 (2014) 2784–2789 (2010)
61. I.I. Cuesta, A. Willig, A. Díaz, E. Martínez-Pañeda, J.M. 80. D.T. Blagoeva, R.C. Hurst, Application of the CEN (European
Alegre, Pre-notched dog bone small punch specimens for the Committee for Standardization) small punch creep testing code
estimation of fracture properties. Eng. Fail. Anal. 96, 236–240 of practice to a representative repair welded P91 pipe. Mater. Sci.
(2019) Eng., A 510–511, 219–223 (2009)
62. F. Abe, Development of creep-resistant steels and alloys for use 81. L. Zhao, H. Jing, L. Xu, Y. Han, J. Xiu, Y. Qiao, Evaluating of
in power plants, in Structural Alloys for Power Plants, ed. by S. creep property of distinct zones in P92 steel welded joint by
Shirzadi, S. Jackson (Woodhead Publishing Series in Energy, small punch creep test. Mater. Des. 47, 677–686 (2013)
Woodhead Publishing, Cambridge, 2014), pp. 250–293 82. M.D. Mathew, J. Ganesh Kumar, V. Ganesan, small punch creep
63. F. Dobeš, K. Milička, Comparison of conventional and small studies for optimization of nitrogen content in 316LN SS for
punch creep tests of mechanically alloyed Al–C–O alloys. enhanced creep resistance. Met. & Mat. Trans. A 45A, 731–737
Mater. Charact. 59(7), 961–964 (2008) (2014)
64. M. Bruchhausen, E. Altstadt, T. Austin, P. Dymacek, S. Holm- 83. E. Tasdighi, H. Nobakhti, N. Soltani, Application of small punch
ström, S. Jeffs, R. Lacalle, R. Lancaster, K. Matocha, J. Pet- test in predicting the axial fatigue life of 304 stainless steel
zova, European standard on small punch testing of metallic sheets. Exp. Tech., 1–9 (2015)
materials. Ubiquity Proc. 1(S1), 11 (2018) 84. D.T.S. Lewis, R.J. Lancaster, S.P. Jeffs, H.W. Illsley, S.J. Davies,
65. T.H. Hyde, W. Sun, J.A. Williams, Requirements for and use G.J. Baxter, Characterising the fatigue performance of additive
of miniature test specimens to provide mechanical and creep materials using the small punch test. Mater. Sci. Eng., A 754,
properties of materials: a review. Int. Mater. Rev. 52(4), 213– 719–727 (2019)
255 (2007) 85. R.J. Lancaster, S.P. Jeffs, H.W. Illsley, C. Argyrakis, R.C. Hurst,
66. J.P. Rouse, F. Cortellino, W. Sun, T.H. Hyde, J. Shingledecker, G.J. Baxter, Development of a novel methodology to study
Small punch creep testing: review on modelling and data inter- fatigue properties using the small punch test. Mater. Sci. Eng.,
pretation. Mater. Sci. Technol. 29(11), 1328–1345 (2013) A 748, 21–29 (2019)
67. K. Matocha, R. Hurst, Small punch testing—the transition from 86. R.J. Lancaster, H. Illsley, R.C. Hurst, S.P. Jeffs, G.J. Baxter, A
a code of practice to a European testing standard. Key Eng. novel approach to small punch fatigue testing. Key Eng. Mater.
Mater. 734, 3–22 (2017) 734, 61–69 (2017)
68. Y. Li, R. Sturm, Determination of creep properties from small 87. R.J. Lancaster, S.P. Jeffs, Small Punch Creep (INTECH Open
punch test, in Proceedings of PVP2008,2008 ASME Pressure Science, London, 2018), pp. 151–172
Vessels and Piping Division Conference, July 27–31, 2008, Chi- 88. X. Mao, M. Saito, H. Takahashi, Small punch test to predict
cago, IL, USA ductile fracture toughness JIC, and brittle fracture toughness,
69. R.J. Lancaster, W.J. Harrison, G. Norton, An analysis of small KIC. Scr. Metall. Mater. 25, 2481–2485 (1991)
punch creep behavior in the γ titanium aluminide Ti–45Al–2Mn– 89. Y. Xu, Z. Zhao, A Modified miniature disk test for determin-
2Nb. Mater. Sci. Eng., A 626, 263–274 (2015) ing material mechanical properties. J. Test. Eval. JTEVA 23(4),
70. S.P. Jeffs, R.J. Lancaster, Elevated temperature creep deforma- 300–306 (1995)
tion of a single crystal superalloy through the small punch creep 90. J. Cheon, I. Kim, Initial deformation during small punch testing.
method. Mater. Sci. Eng., A 626, 330–337 (2015) J. Test. Eval. 24(4), 255–262 (1996)
71. S. Holmström, Y. Li, P. Dymacek, E. Vacchieri, S.P. Jeffs, R.J. 91. E. Fleury, J.S. Ha, Small punch test to estimate the mechanical
Lancaster, D. Omacht, Z. Kubon, E. Anelli, J. Rantala, A. Tonti, properties of steel for steam power plant I: mechanical strength.
S. Komazaki, Naveena, M. Bruchhausen, R.C. Hurst, P. Hähner, Int. J. Pres. Vessels. Piping 75, 699–706 (1998)
M. Richardson, D. Andres, Creep strength and minimum strain 92. W.K. Lee, D.R. Metzger, A. Donner, O.E. Lepik, The use of a
rate estimation from small punch creep tests. Mater. Sci. Eng.: small punch test procedure to determine mechanical properties,
A 731, 161–172 (2018) in Small Specimen Test Techniques, ASTM STP 1329, ed. by W.R.
72. D. Andrés, R. Lacalle, J.A. Álvarez, Creep property evaluation Corwin, S.T. Rosinski, E. van Walle (American Society for Test-
of light alloys by means of the small punch test: creep master ing and Materials, West Conshohocken, 1998)
curves. Mater. Des. 96, 122–130 (2016) 93. A. Husain, D.K. Sehgal, R.K. Pandey, Design of a simple, ver-
73. P. Dymáček, F. Dobeš, Y. Jirásková, N. Pizúrová, M. Friák, Ten- satile, small-specimen punch test setup for determination of the
sile, creep and fracture testing of prospective Fe–Al-based alloys mechanical behavior of materials. Exp. Tech. 26, 33–38 (2002)
using miniature specimens. Theor. Appl. Fract. Mech. 99, 18–26 94. J.S. Lee, I.S. Kim, Evaluation of mechanical properties of RPV
(2019) clad by small punch tests. J. Korean Nucl. Soc. 34, 574–585
74. C. Wen, T. Xu, K. Guan, Correlation factor study of small punch (2002)
creep test and its life prediction. Materials 9(10), 796 (2016) 95. M. Eskner, R. Sandstrom, Mechanical property evaluation using
75. S. Yang, Y. Zheng, Y. Duan, X. Ling, Creep characteristics and the small punch test. J. Test. Eval. 31(4), 1–8 (2004)
deformation analysis of service-exposed material using small 96. D. Finarelli, M. Roedig, M. Carsughi, Small punch tests on auste-
punch creep test. Eng. Fract. Mech. 195, 242–252 (2018) nitic and martensitic steels irradiated in a spallation environment
76. Z. Yang, Z. Wang, Relationship between strain and central deflec- with 530 MeV protons. J. Nucl. Mater. 328(2–3), 146–150 (2004)
tion in small punch creep specimens. Int. J. Press. Vessels Pip. 97. M.A. Contreras, C. Rodriguez, F.J. Belzunce, C. Betegon, Use of
80, 397–404 (2003) small punch test to determine the ductile-to-brittle transition tem-
77. F. Hou, H. Xu, Y. Wang, L. Zhang, Determination of creep prop- perature of structural steels. Fatigue Fract. Eng. Mater. Struct.
erty of 1.25Cr0.5Mo pearlitic steels by small punch test. Eng. 31, 727–737 (2008)
Fail. Anal. 28, 215–221 (2013) 98. I. Peñuelas, I.I. Cuesta, C. Betegón, C. Rodríguez, F.J. Belzunce,
78. T.H. Hyde, M. Stoyanov, W. Sun, C.J. Hyde, On the interpreta- Inverse determination of the elastoplastic and damage param-
tion of results from small punch creep tests. J. Strain Anal. Eng. eters on small punch tests. Fatigue Fract. Eng. Mater. Struct. 32,
Des. 45(3), 141–164 (2010) 872–885 (2009)
13
738 Metals and Materials International (2020) 26:719–738
99. J. Isselin, T. Shoji, Yield strength evaluation by small-punch test. 104. X. Mao, H. Takahashi, T. Kodaira, Estimation of mechanical
J. Test. Eval. 37(6), Paper ID 101657 (2009) properties of irradiated nuclear pressure vessel steel by use of
100. I.I. Cuesta, J.M. Alegre, R. Lacalle, Determination of the Gur- subsized CT specimen and small punch specimen. Scr. Metall.
son–Tvergaard damage model parameters for simulating small 25, 2487–2490 (1991)
punch tests. Fatigue Fract. Eng. Mater. Struct. 33, 703–713
(2010) Publisher’s Note Springer Nature remains neutral with regard to
101. X. Zhao, J. Zhang, Small punch test of U-shaped notch of TC4 jurisdictional claims in published maps and institutional affiliations.
titanium alloy and its numerical simulation. J. Mater. Eng. Per-
form. 22, 3182 (2013)
102. T.E. García, C. Rodríguez, F.J. Belzunce, C. Suárez, Estimation
of the mechanical properties of metallic materials by means of
the small punch test. J. Alloy. Compd. 582, 708–717 (2014)
103. S.H. Hong, M.-G. Seo, C.H. Jang, K.-S. Lee, Evaluation of the
effects of thermal aging of austenitic stainless steel welds using
small punch test. Proc. Eng. 130, 1010–1018 (2015)
13