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Designation: D3230 − 13

Standard Test Method for


Salts in Crude Oil (Electrometric Method)1
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1. Scope* 3. Terminology
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FDOFLXP DQG PDJQHVLXP 2WKHU FRQGXFWLYH PDWHULDOV PD\ DOVR 4. Summary of Test Method
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safety concerns, if any, associated with its use. It is the PHDVXUHG 7KH FKORULGH VDOW FRQWHQW LV REWDLQHG E\ UHIHUHQFH
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2. Referenced Documents 5. Significance and Use



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15. Keywords

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ANNEX

(Mandatory Information)

A1. APPARATUS

A1.1 Electrometric Chloride Apparatus (Custom Manu- $ Potentiometer,  RKP WHQ WXUQ
facture) VHH )LJ $ DQG 1RWH $) $ Potentiometer,  RKP WHQ WXUQ
$ Milliammeter,  WR  P$ GF ZLWK  WR  P$ DF VFDOH
127( $²$Q HTXLYDOHQW SDUW FDQ EH VXEVWLWXWHG LQ HDFK FDVH
 RKP LQWHUQDO UHVLVWDQFH SURYLGHG WKH HOHFWULFDO FKDUDFWHULVWLFV RI WKH HQWLUH FLUFXLW UHPDLQ XQ
$ Bridge Rectifier, IXOOZDYH  $ FDSDFLW\ DW  +] FKDQJHG DQG WKH LQGXFWLYH HIIHFWV DQG VWUD\ FXUUHQWV DUH DYRLGHG
DPELHQW WHPSHUDWXUH PLQLPXP RI  359 3HDN 5HYHUVH A1.2 Test Cell Components (Custom Manufacture) VHH
9ROWDJH  )LJ $
$ AC Voltmeter, UHFWLILHU W\SH  RKP9  WR  9 $ Beaker,  P/ WDOO IRUP ZLWKRXW OLS DV GHVFULEHG
UDQJH IRU XVH LQ 7HVW 0HWKRG '
$ Variable Voltage Autotransformer , LQSXW  WR  $ Electrode Assembly, DV VKRZQ LQ )LJ $ DQG )LJ
9  +] RXWSXW  WR  9  $ FDSDFLW\ $ 7KH HOHFWURGHV PRXQWHG LQ SDUDOOHO SRVLWLRQ H[DFWO\
$ Transformer, SODWH VXSSO\  9 FHQWHU WDS  RSSRVHG DQG  6  PP DSDUW DQG HOHFWULFDOO\ VHSDUDWHG E\
+]  P$ GF FDSDFLW\ D Q\ORQ RU 7)(IOXRURFDUERQ VSDFHU
D3230 − 13
A1.3 Electrometric Chloride Apparatus (Commercial A1.4 Test Cell Components (Commercial Manufacture)
Manufacture)4
$ Beaker,  P/ WDOO IRUP ZLWKRXW OLS DV GHVFULEHG
$ 7KH DSSDUDWXV VKDOO FRQVLVW RI D FRQWURO XQLW FDSDEOH IRU XVH LQ 7HVW 0HWKRG ' LV FRPPRQO\ XVHG KRZHYHU
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WKH WHVW VROXWLRQ EHWZHHQ WKH HOHFWURGHV DW HDFK YROWDJH OHYHO $ Electrode Assembly, VKRZQ E\ H[DPSOH LQ )LJ $
VHH 1RWH   DQG )LJ $ 7KH HOHFWURGH DVVHPEO\ GLPHQVLRQDO UHTXLUH
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FIG. A1.1 250 or 540 Volt Transformer


D3230 − 13

FIG. A1.2 Test Cell

FIG. A1.3 Electrode Assembly


D3230 − 13

SUMMARY OF CHANGES

Subcommittee D02.03 has identified the location of selected changes to this standard since the last issue
(D3230 – 10) that may impact the use of this standard.

(1) Updated 8.1.

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in this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk
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