Nama : Erisha Putri Diketahui

NPM : 1815041025 P 1 atm

Xw 0.05
Xd 0.95

Xf 0.6
F 450
D 275
B 175

Ditanya
a. Nmin c. n for R/Rmin=1.3 and the optima
b. Rmin

Plot garis Kesetimbangan plot garis 45 derajat

Xa Ya x y
1 1 0 0 1.2
0.78 0.9 0.2 0.2
0.581 0.777 0.4 0.4
0.411 0.632 0.6 0.6 1 q line
0.258 0.456 0.8 0.8
0.13 0.261 1 1
0 0
0.8
a. Mencari Nmin
Nmin= 6.7
y'
0.6

b. Mencari R min 0.4

Vf/F = D/F 0,611

q= Lf/F (F-Vf)/F 0.2

q = 0.388889

X'
0 Xw
q/q-1 -0.636363636 0 0.2 0.4 0.6
arctgn -32

slope operating line

x' 0.465
y' 0.684 1.2

Rm= Xd-y'/Xd-x'= Rm/Rm+1= 0.548454

Rm 1.214612 1
c. Mencari R 1.3

0.8
 1

R1.3= 1.578995434
0.8
Slope of operating line for rectifying section for rectifying section
R/R+1= 0.612252125 P
N= 13.2
0.6

Enriching Operation line

Yn+1= 0.612252 Xn + 0.36836 0.4
plot garis
Yn+1 Xn
0.686732 0.52 0.2
0.705099 0.55
0.735712 0.6
0.766324 0.65 Xw
0
0.796937 0.7 0 0.2 0.4 0.6
0.82755 0.75
0.858162 0.8
0.888775 0.85
0.919387 0.9
0.95 0.95

y= 0.981818
Garis qline = 0.981818 -0.636364 Xn
x y
0.6 0.6
0.46 0.689091

Garis Operasi Stripping Garis Enriching

x y x y
0.05 0.05 0.95 0.95
0.46 0.636364 0.46 0.636364
 D/F 0.611111

Rmin=1.3 and the optimal location of feed stage

q line

garis kesetimbangan
Horizontal line
q line

X' Xf Xd
2 0.4 0.6 0.8 1 1.2
 P
Column G
Column D
q line kesetimbangan
diagonal line
q line

Xf Xd

2 0.4 0.6 0.8 1 1.2

Nama : Erisha Putri
NPM : 1815041025

heptane ethyl benzene heptane (H)

TB {oC) 136.2 98.5 ethyl benzene (EB)
Cp (cal/mol K) 51.9 43.4
7575 8600 Tref= 0 16000
Δhsol= 0
t (oC) XH yH λH λEB
136.2 0 0 1 14000
129.5 0.08 0.233 1.23 1
122.9 0.185 0.428 1.19 1.02
119.7 0.251 0.514 1.14 1.03 12000
116 0.335 0.608 1.12 1.05
110.8 0.487 0.729 1.06 1.09
106.2 0.651 0.834 1.03 1.15
10000
103 0.788 0.904 1 1.22
100.2 0.914 0.963 1 1.27
98.5 1 1 1
8000
Cari h,λ,H dengan rumus : H
h=XH*CpH(t-tref)+XEB*CpEB(T-TREF)+ΔHsol
6000
λmix =XH*λH +XEB*λEB
H = h + λmix
4000
t (oC) XH XEB h λmix H
136.2 0 1 5911.08 8600 14511.08
129.5 0.08 0.92 5708.36 8518 14226.36
122.9 0.185 0.815 5527.12 8410.375 13937.495 2000
119.7 0.251 0.749 5450.36 8342.725 13793.085
116 0.335 0.665 5364.71 8256.625 13621.335
110.8 0.487 0.513 5267.377 8100.825 13368.202 0
0
106.2 0.651 0.349 5196.738 7932.725 13129.463
103 0.788 0.212 5160.094 7792.3 12952.394
100.2 0.914 0.086 5127.134 7663.15 12790.284
98.5 1 0 5112.15 7575 12687.15
 16000

Vapor
14000

12000

10000

2 fasa
8000
H

6000

4000

Liquid
2000

0
0 0.2 0.4 0.6 0.8 1 1.2

X
X
 sauturated vapor
saturated liquid

1 1.2
 Diketahui
xf 0.5 berat
Tf 23.4 C
F 5 ton/jam
xd 0.95 berat
xw 0.01 berat
Tresidu 37.8 C
R 1.5Rm

2. Menentukan destilat dan laju bottom produk/destilat 4. plate teoritis minimum

Neraca massa
F= D+W W= 2.39361702 1.2
5= D+W
1
neraca massa komponen
F.Xf= Dxd+W.Xw 0.8
2.5= 0.95D+0.01W
2.5= 0.95D+0.01(5-D) 0.6
2.45 0.94 D
0.4
D= 2.606383 ton/jam
0.2
3. Tentukan reflux ratio minimum
refluks ratio minimum L/V=1
0
q=Lf/F=(F-Vf)/F 0 0.2 0.4 0.6 0
q= 0.478723
q line= -0.918367 didapat 5 stages

membuat garis kesetimbangan membuat garis diagonal

x y x y 6. Overall efficiency 50%, p
0 0 0 0
0.02 0.134 0.1 0.1 EO =
0.04 0.23 0.2 0.2
0.06 0.304 0.3 0.3 N ideal = N - (reboiler) 1
0.08 0.365 0.4 0.4
0.1 0.418 0.5 0.5 N actual = N/EO
0.15 0.517 0.6 0.6
0.2 0.579 0.7 0.7
0.3 0.665 0.8 0.8
0.4 0.729 0.9 0.9
0.5 0.779 1 1
0.6 0.825
0.7 0.87 log Ne/Ns =
0.8 0.915
 0.9 0.958
0.95 0.979 Ne/Ns
1 1 N ideal =
Ns =

sehingga, feed masuk pada p

garis q digambarkan dengan menggambarkan garis dari xf dengan slope sebesar 0.478723
R= 1,5 x Rm 7.Refux Ratio Internal tiap k
R= 1.114286
Ri = L/(L+D)
Ri =
0.527027027 xn+ 0.449324
8.Kadar Liquids ketika masu
q line Garis Operasi Stripping Garis Enriching
x y x y x y F.xf = W.xw
0.5 0.5 0.01 0.01 0.95 0.95 2.5
0.3 0.607432 0.32 0.60743243 0.32 0.607432 xw=

minimum reflux ratio Rm 9. beban kondesor dan reboil

KONDENSER
menghitung energi umpan

Rm/(Rm+1) = 0.42623 y'= 0.69 Komponen

0.57377 x'= 0.34 Methanol
Rm = 0.742857 Air (H2O)
Total

1.2

1 garis
kese-
timban- Menghitung energi distilat
0.8 gan
y' diagonal
Komponen
Methanol
0.6 q line Air (H2O)
Total
0.4 operasi
stripping

0.2 Enriching
x' line
Menghitung energi bottom
0
0 0.2 0.4 0.6 0.8 1 1.2
Komponen
Methanol
5. Jumlah Plate pada kondisi operasi Air (H2O)
Dari gambar grafik di atas, di dapat nilai Nmin sebanyak = 9,5 Total

1. Sketsa
 10.Jika efisiensi murphree

EM=(yn-yn+1)/(yn*-yn+1
EM = 0,6

Efisiensi totalnya adalah

Eo= Log [1+EM(Mv/L-1)
Condensor Eo= Log [1+EM(Mv/L-1)
Eo=
Eo=

Rectrifying
Reflux Destilate
xd = 0,95
FEED Preheater
F = 5 ton/jam
xF = 0,5
T = 23,4 C

Stripping

xw = 0,01
Bottom
Reboiler
 garis
kese-
timban-
gan

diagonal

0.4 0.6 0.8 1 1.2

Overall efficiency 50%, platte keberapa feed masuk?

0.5

ideal = N - (reboiler) 1
8.5
actual = N/EO
17

0,206 log 0.918367

0.206 -0.036984
 -0.007619
0.98261
8.5
8.650427

hingga, feed masuk pada plate ke 8

Refux Ratio Internal tiap kolom

0.657343

Kadar Liquids ketika masuk reboiler

2,393617. xw
1.044444 (berat)

beban kondesor dan reboiler

ONDENSER REBOILER
enghitung energi umpan menghitung energi bottom

kmol/jam Cp/Dt DH (m.cp.dt) Komponen kmol/jam Cp/Dt

85.61 2.53 47.817 Methanol 85.61 2.53
131.338 41,855 791059.5 Air (H2O) 131.338 41,855
41857.53 791107 Total 41857.53

jadi delta H umpan 791107 kj/jam jadi delta H bottom =

enghitung energi distilat

kmol/jam Cp/Dt DH (m.cp.dt) Menghitung beban reboiler
85.61 2.53 16.192 DH In=DH out
131.338 41,855 267872 Dh umpan +DH reboiler = DH bottom + DH disti
41857.53 267888
DH reboiler= (DH bottom + DH distilat + DH
jadi delta H distilat= 267888 kj/jam DH reboiler= 775191.44934

enghitung energi bottom jadi beban reboiler :

kmol/jam Cp/Dt DH (m.cp.dt)
85.61 2.53 -16.192
131.338 41,855 -267872
41857.53 -267888

jadi delta H bottom= -267888 kj/jam

 jadi beban condenserDhumpan+DH distilat + DH bottom
791107 kj/jam

.Jika efisiensi murphree 60%, berapakah efisiensi total?

M=(yn-yn+1)/(yn*-yn+1)

isiensi totalnya adalah

o= Log [1+EM(Mv/L-1)]/(Log (m V/L) Equation 11.5-4 geankoplis
o= Log [1+EM(Mv/L-1)]/(Log (m V/L)
1.6
0.20412

Cooler
 DH (m.cp.dt)
0.95634
1566298
1566299

1566299 kj/jam

er = DH bottom + DH distilat+DH condensor

bottom + DH distilat + DH condensor)-DH umpan

kj/jam

775191 kj/jam