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NONDESTRUCTIVE EXAMINATION
Table of Contents
Page
List of Figures
Fig. 1. Electromagnetic spectrum. ................................................................................................................. 5
Fig. 2. Production of x-radiation. .................................................................................................................... 5
Fig. 3. Typical radiographic set up. ............................................................................................................... 6
Fig. 4a. ASME Hole-type IQI. ....................................................................................................................... 8
Fig. 4b. ASME Wire-type IQI. ....................................................................................................................... 9
Fig. 5. Basic ultrasonic system. .................................................................................................................. 10
Fig. 6. Steps involved in penetrant test. (1) Applying precleaner. .............................................................. 11
Fig. 6. (2) Applying penetrant. .................................................................................................................... 12
Fig. 6. (3) Applying cleaner. ........................................................................................................................ 12
Fig. 6. (4) Applying developer. .................................................................................................................... 13
Fig. 6. (5) Examination. ............................................................................................................................... 14
Fig. 7. Visible dye system. .......................................................................................................................... 15
Fig. 8. Fluorescent penetrant system. ........................................................................................................ 16
Fig. 9. Magnetic particle examination. ........................................................................................................ 18
Fig. 10. Simplified block diagram of acoustic emission system. ................................................................ 20
List of Tables
Table 1. NDE Matrix ....................................................................................................................................... 2
Table 2. Typical Discontinuities Suitable for Liquid Penetrant Examination. ............................................... 17
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17-1 Nondestructive Examination
Page 2 FM Global Property Loss Prevention Data Sheets
1.0 SCOPE
This document addresses nondestructive examination (NDE) in general terms. For additional technical
requirements refer to Section V of the ASME Boiler and Pressure Vessel Code. Recommendations for NDE
of specific machinery, boilers, pressure vessels and piping are not provided in this document; they are
contained in object-specific data sheets.
This text describes, in general, the principles that make NDE methods effective loss prevention tools. The
intent of this document is to aid field personnel in understanding how to select and apply NDE methods and
how to interpret the results of such examinations.
Described are: radiographic testing (RT); ultrasonic testing (UT); liquid penetrant testing (PT); magnetic
particle testing (MT); eddy current testing (ET); and acoustic emissions testing (AE). Brief reference also is
made to visual examination/testing (VT).
Note: Many jurisdictions have NDE requirements which may vary somewhat from the information contained
in this document. These requirements may be mandatory.
1.1 Changes
May 2003. Revised section 3.0 ‘‘Support for Recommendations.’’ Also minor editorial changes were made
for this revision.
2.1 Introduction
Most machinery component or structure failures occur from the initiation and growth of a crack. The crack
may already be present, or may initiate due to nonmetallic inclusions, hydrogen embrittlement, stress relief
heat treatment, stress corrosion, or fatigue at a point of stress concentration. In other cases failure may be
due to accidental overload or overloading at working stresses due to thinning of material from its working
environment.
NDE is a major predictive maintenance tool when used as a part of a condition monitoring program for any
piece of equipment or process, from imperfections in weldments, to engine parts, to power presses the size
of a large building.
The techniques used in NDE find telltale signs such as tiny subsurface cracks in hard-to-reach areas; if left
undetected, such cracks can widen and propagate until failure of a machine or structural component occurs.
4.0 REFERENCES
There are no references for this document.
Gamma rays are produced by the disintegration of a radioactive atom. When the nucleus of this atom emits
an alpha or beta particle, the daughter nucleus is left in a high energy or excited state. The excess energy
is emitted as gamma radiation. Thus, gamma radiation originates in the nucleus of the atom.
In industrial radiography, the penetrating radiation source (x-ray machine or radioactive isotope) is posi-
tioned on one side of the object to be radiographed, such as rolled plate or a weld (Fig. 3). A fixed film in a
light tight, protective cassette is placed on the opposite side of the object in close contact with it. The object
is then bombarded by a beam of radiation. The object absorbs some of this radiation. Radiation that is not
absorbed by the object exposes the film emulsion in the same way that light exposes photographic film.
Development of the film produces a two-dimensional shadow image of the object.
Variations in density, thickness and composition of the object affect the degree of darkening, or density of
the film image. The degree of darkening must be within specific limits when performing radiography to the
ASME Code.
One factor that makes radiography an effective tool is its sensitivity.
Sensitivity is the ability to detect a small discontinuity. It is expressed as the percent ratio of the thickness
of the smallest detectable defect to the thickness of the specimen being examined. An image quality indica-
tor (IQI), representing a percentage of the thickness of the specimen being examined is placed on the radio-
graphic film. IQIs are essential to determining the quality of a radiographic image. Figure 4a and 4b illustrate
several of the IQIs specified in the ASME Code.
Radiography as an inspection tool, when conducted according to ASME Boiler and Pressure Vessel Code sec-
tions, is typically used to reveal internal discontinuities in welded joints. Some of the more commonly encoun-
tered discontinuities within the weld include the following:
1. Porosity: gas pockets or voids, free of solid material. Porosity appears on the radiograph as dark spots
with an essentially circular shape.
2. Slag inclusions: oxides and nonmetallic solids that are entrapped in weld metal, or between weld metal
and base metal. Slag appears on the radiograph as irregular, dark, elongated areas or lines.
3. Tungsten inclusions: metallic particles of tungsten transferred to the weld deposit by the tungsten elec-
trode used in the gas-tungsten arc welding process. Tungsten appears on the radiograph as light irregu-
lar spots.
4. Incomplete fusion: failure to fuse together adjacent layers of weld metal, or weld metal and base metal.
Incomplete fusion appears on the radiograph as regular dark lines, generally straight and often paralleling
each other.
5. Inadequate joint penetration: failure of the filler metal and the base metal, or base metal alone if no filler
is used, to fuse at the root of the weld. It generally appears on the radiograph as a straight, dark line run-
ning longitudinally through the center of the weld.
In addition to the above, cracks, undercutting and surface irregularities are also observed. The appropriate
ASME Code section should be consulted regarding acceptability criteria for the above named discontinuities.
Shear or angle ultrasonic waves are commonly used for flaw detection in welded joints of plate or piping, but
may have other equally valuable applications. Longitudinal waves are widely used for the examination of cast-
ings, billets, shafting journals, crankshafts, and pipe-to-flange weldments where the flange faces can be
used as a contact surface, as well as for the detection of laminations. Surface or Raleigh waves are more sen-
sitive to surface cracks and surface cuts or breaks. They are valuable for detecting defects that may other-
wise be overlooked by visual examination. These waves will pass rounded corners and reflect from a sharp
edge or break in the surface even at a location hidden from view. The reflection or oscilloscope pattern
obtained from good welds or sound material are the only means of appraising quality.
There are several ultrasonic thickness measuring instruments that are also useful in detecting unfused areas
of forge welds and laminations in plates and tubes.
The principles used in today’s liquid penetrant inspection are similar; however, the materials used are con-
siderably more sophisticated than the early kerosene and whitewash. These more advanced materials make
liquid penetrant testing a highly sensitive nondestructive method for locating surface discontinuities in today’s
manufactured products.
Liquid penetrant examination depends on the ability of the liquid to wet the surface of a specimen, to flow
evenly over its surface, and then to migrate into tiny cavities on the specimen’s surface. These cavities could
be the result of pores, cracks, or voids, either inherent or manufactured in the part. The ability of a liquid
to migrate into these tiny cavities is the phenomenon of capillarity. Wetting ability and capillarity illustrate the
basic principles by which a penetrant enters cavities in the surface of a test piece.
Several steps are involved in performing an accurate liquid penetrant examination (Fig. 6):
1. Preclean the part to remove contaminants such as oil, water or dirt from any cavities open to the sur-
face. Vapor degreasing and solvent cleaning are acceptable methods. Shot blasting or peening should not be
used, as these methods may result in forcing shut any surface discontinuities.
2. Apply the penetrant by dipping, spraying, or other means to ensure complete coverage. The total time dur-
ing which the penetrant is allowed to remain on the part (dwell time) is dependent on the test piece mate-
rial and the type of discontinuity sought.
3. Remove excess penetrant from the surface of the part. This leaves behind only the penetrant that has
seeped into the discontinuity. Different removal methods are used on post-emulsification, solvent-removable,
and water-washable penetrants as follows:
a) Post-emulsification penetrants require the addition of an emulsifier. This renders the penetrant water
washable. It is then removed with a water spray. The time during which the emulsifier is left on the
penetrant-covered part is critical. If left too long, the emulsifier might mix with penetrant in shallow dis-
continuities and subsequently be washed away. If not left long enough, discontinuities might be obscured
by excessive background.
b) Solvent-removable penetrants are wiped from the part’s surface with a solvent-dampened lint cloth.
The solvent is never applied directly to the part as this might remove penetrant from discontinuities. These
are less sensitive types of penetrants; however, they are the most portable. Penetrant and solvent are sup-
plied in aerosol spray cans for use in field applications.
c) Water-washable penetrants have the emulsifier built in. These types avoid the intermediate step of
emulsification time and can be water-washed immediately after the dwell time. Sensitivity is decreased,
however. The penetrant in wide, shallow discontinuities can be more easily washed out.
4. Development takes place after the excess penetrant is removed and the part is completely dried. (Hot
air dryers are used with washing techniques.) The developer has two functions: first, it acts as a blotter to help
the penetrant bleed out of a discontinuity; second, it provides a contrasting background for the color con-
trast penetrants. Dry developers are supplied as fluffy, white powder to be sprinkled over the surface or in
aerosol cans to be sprayed onto the surface.
Wet developers are supplied as particles dispersed in a liquid medium. The part is dipped in the liquid prior
to drying. After drying, only the powdery developer remains.
5. Examination is performed under white light or black light conditions, depending on whether visible dye or
fluorescent penetrants are used. Liquid penetrant examination includes both fluorescent and visible dye
(color contrast) penetrant methods. The only true difference between the two is the means by which the ulti-
mate examination of the part is made. In the fluorescent penetrant system, examination is made using a
black light operating at near-ultraviolet frequencies averaging 3650 A. In the visible dye system, the dye (usu-
ally red) is provided with a contrasting background (usually white) and the inspection is made using white
light.
The six methods, then, in order of decreasing sensitivity, are (Figs. 7 and 8):
1. Post-emulsifiable fluorescent
2. Solvent-removable fluorescent
3. Water-washable fluorescent
4. Post-emulsifiable visible dye
5. Solvent-removable visible dye
6. Water-washable visible dye
Liquid penetrant examination methods can provide indication of surface discontinuities in metals (magnetic
or nonmagnetic) and other nonporous materials. These discontinuities must be open to the surface. Some
typical discontinuities and the manufacturing process associated with them are listed in Table 2.
Some commonly used terms relating to magnetic particle testing are listed below:
Continuous method: a method wherein the indicating medium is applied while the magnetizing force is
present.
Curie point: the temperature at which ferromagnetic materials can no longer be magnetized by outside forces,
and at which they lose their residual magnetism (approximately 1200 to 1600°F [635 to 857°C] for many mag-
netic metals).
Electromagnet: a magnet created by inserting a suitable metal core within or near an electric field which is usu-
ally formed by passing electric current through a coil of insulated wire.
Ferromagnetic: a term applied to materials that can be magnetized or strongly attracted by a magnetic field.
Flux density, magnetic: the strength of a magnetic field, expressed in flux lines per unit area.
Magnetic writing: a form of non-relevant indication, sometimes caused when the surface of a magnetized
part comes in contact with another piece of ferromagnetic material.
Permeability: the ratio of flux density produced to magnetizing force (the ease with which a material can
become magnetized).
Prods: hand-held electrodes.
Residual field, magnetic: the field that remains in a piece of magnetizable material after the magnetizing
force has been removed.
Retentivity: the ability of a material to retain a portion of the magnetic field after the magnetizing force has
been removed.
Yoke: a magnet that induces a magnetic field in the area of a part that lies between its poles. Yokes may
be permanent magnets or either alternating-current or direct-current electromagnets.
The above definitions and others relating to magnetic particle inspection can be found in ASTM E269-68.
AE testing involves listening to the sounds (usually inaudible to the human ear) made by a material, struc-
ture or machine in use or under load and drawing conclusions about its condition from what was heard. The
sounds may arise from friction (such as bearing wear), crack growth, turbulence (including from leakage)
and material changes such as corrosion.
Application of the method involves placing one or more AE sensors on the surface of a stressed compo-
nent to detect high frequency sound from the material anomalies. Once sound is detected by the sensor it
is converted into an electric signal (Fig. 10) and then statistically categorized by the AE system.
Objects deform in many different ways depending primarily on the object (component), material, and applied
stress. Some of the test conditions that change the AE signal response are: material characteristics, rate
and type of stress applied, and temperature. The AE system statistical summary of the signal characteris-
tics provides insight into material deformation mechanisms and their origin. Success of AE examinations
depends on the examiner’s experience with the materials being checked, the procedure being used and
follow-up NDE.
The advantages of AE are that a whole structure may be monitored from a few locations, the structure can
be continuously monitored and alarmed while in use (without removing it from service). Microscopic changes
can be detected if sufficient energy is released and source location determination is possible using multiple
sensors.
Applications include testing pipelines and storage tanks (both above and below ground), fiberglass structures,
rotating machinery, weld monitoring, highly stressed press components and biological and chemical changes.
Figure 10 illustrates a typical AE system.
In addition to the methods discussed here, there are other nondestructive examination methods that have a
great potential for loss prevention applications. Two common ones are leak testing and visual examination-
,both of which are discussed in detail in Section V of the ASME Code. Other less conventional methods
include infrared thermography, neutron radiography, optical holography, acoustic holography, and micro-
wave inspection. For a thorough discussion of these methods, the American Society for Metals (ASM) Met-
als Handbook, Volume 11, Eighth Edition, should be consulted.
Some commonly used terms relating to acoustic emission testing are listed below:
Acoustic emission (AE): the class of phenomena whereby transient elastic waves are generated by the rapid
release of energy from localized sources within a material, or the transient waves so generated. Acoustic
emission is the recommended term for general use. Other terms that have been used in AE literature include:
1) stress wave emission, 2) micro seismic activity; and 3) emission or acoustic emission with other qualify-
ing modifiers.
Acoustic emission sensor: a detection device, generally piezoelectric, that transforms the particle motion pro-
duced by an elastic wave into an electrical signal.
Location accuracy: a value determined by comparison of the actual position of an AE source (or simulated
AE source) to the computed location.
Location source: any of several methods of evaluating AE data to determine the position on the structure
from which the AE originated. Several approaches to source location are used, including zone location, com-
puted location, and continuous location.
APPENDIX D BIBLIOGRAPHY
ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination, 1998 Edition with the 2000
addenda.
American Society for Metals (ASM) Metals Handbook, Volume 11, Eighth Edition.