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Methods 320A
to 320F:1976
Incorporating
Amendment No. 1
Methods of testing
Plastics —
Part 3: Mechanical properties —
IMPORTANT NOTE Before reading this method it is essential to read the foreword, general
introduction and instructions to BS 2782, issued separately.
UDC 678.5/.8:678.01+620.175.22:678–416
BS 2782-3:Methods 320A to 320F:1976
A British Standard does not purport to include all the necessary provisions of
a contract. Users of British Standards are responsible for their correct
application.
Compliance with a British Standard does not of itself confer immunity
from legal obligations.
Summary of pages
This document comprises a front cover, an inside front cover, pages i and ii,
pages 1 to 12 and a back cover.
This standard has been updated (see copyright date) and may have had
amendments incorporated. This will be indicated in the amendment table on
the inside front cover.
Contents
Page
Committees responsible Inside front cover
0 Introduction 1
1 Scope and field of application 1
2 References 1
3 Definitions 1
4 Principle 2
5 Apparatus 2
6 Test pieces 2
7 Preparation of test pieces 3
8 Conditioning 4
9 Speed of testing 4
10 Procedure 4
11 Calculation and expression of results 5
12 Test report 6
Appendix A Informatory notes 7
Figure 1 — Figure deleted 8
Figure 2 — Figure deleted 8
Figure 3 — Method 320C: Test piece 9
Figure 4 — Method 320D: Test piece 9
Figure 5 — Method 320E 10
Figure 6 — Method 320F 11
Figure 7 — Stress/strain curves 12
Table 1 — Test procedure details 8
© BSI 01-1999 i
ii blank
BS 2782-3:Methods 320A to 320F:1976
1)
In course of preparation.
© BSI 01-1999 1
BS 2782-3:Methods 320A to 320F:1976
3.5 4 Principle
off-set yield stress
The principle of the test is the subjection of test
the stress on the stress-strain curve where the curve pieces of defined groups of plastics materials to a
departs from initial linearity by a specified strain tensile force and the calculation of any of the
(see Figure 7) properties defined in clause 3, as required.
3.6
percentage elongation 5 Apparatus
the elongation produced in the gauge length of the The following apparatus is required.
test piece by a tensile stress and expressed as a 5.1 Tensile testing machine. The tensile testing
percentage of the original gauge length (distance machine shall be power driven and capable of
between the reference lines) maintaining the appropriate rate of grip separation
3.7 as specified for the appropriate test procedure. In all
percentage elongation at yield cases, a continuous indication of the force applied to
the test piece, preferably recorded autographically
the elongation produced in the gauge length of the
with a permanent indication of the maximum force,
test piece at the yield stress, expressed as a
shall be provided. The force scale shall be calibrated
percentage of the original gauge length (distance
by a suitable method to ensure that the error does
between the reference lines)
not exceed the requirements for grade A
3.8 of BS 5214-1:1975 (see A.1).
percentage elongation at break
Unless otherwise specified, the machine shall be
the elongation at break produced in the gauge provided with a type of grip which maintains or
length of the test piece expressed as a percentage of increases grip pressure as the force applied to the
the original gauge length (distance between the test piece increases. The test piece shall be held in
reference lines) (see A.9) such a manner that slip relative to the grips is
3.9 prevented as far as possible, and the clamping
elastic modulus system should not produce premature failure at the
grips.
the ratio of stress to corresponding strain below the
proportional limit, where the proportional limit is 5.2 Extensometer. When an extensometer is used, a
the greatest stress which a material is capable of continuous indication of the elongation of the gauge
supporting without any deviation from length, and, if appropriate, a permanent indication
proportionality of stress to strain (Hooke’s Law). of the maximum elongation shall be given.
The stress-strain relationship of many plastics does Preferably the elongation should be recorded
not conform to Hooke’s Law throughout the elastic autographically in the form of a force elongation
range but deviates therefrom even at stresses well curve. When an extensometer is attached to the test
below the yield stress. For such materials, the slope piece, care should be taken to ensure that any
of the tangent to the stress-strain curve at a low distortion of, or damage to, the test piece is minimal,
strain is usually taken as the elastic modulus and it is essential that no slippage occurs between
the extensometer grips and the test piece. The
3.10 instrument shall be essentially free from inertia lag
secant modulus at the specified speed of testing and shall be
in general, the ratio of stress to corresponding strain calibrated by a suitable method to ensure that the
at any given point on the stress-strain curve. error does not exceed 2 % of the actual strain.
However, for rigid materials (e.g. for Method 320E), 5.3 Micrometers. For measuring the thickness and
it is usual to define secant modulus as the ratio of width of rigid materials, a screw micrometer
stress to corresponding strain measured relative to reading to 0.01 mm or less shall be used.
a level of pre-stress applied to straighten the test
For measuring the thickness of flexible materials, a
piece. In such instances, the secant modulus shall be
dial gauge micrometer (or comparator) reading
based on the stress required to extend the gauge
to 0.01 mm or less and provided with a flat circular
length of the test piece by 0.2 % from a pre-stress of
foot that will apply a pressure of 20 ± 3 kPa shall be
approximately 10 % of the expected force
used.
at 0.002 strain (see A.8)
6 Test pieces
The test pieces for each test procedure are listed
in Table 1 and are shown with detailed dimensions
and tolerances in Figure 3 to Figure 6.
2 © BSI 01-1999
BS 2782-3:Methods 320A to 320F:1976
It should be noted that the geometry of the test 7.4 Method 320C. The dumb-bell test piece shown
pieces and clamping system dictates the pattern of in Figure 3 shall be machined to shape by means of
stress concentrations set up during the test. These a profiling system (i.e. machined from a rectangular
will be altered if the test piece size is scaled up or blank, which is clamped firmly between plates and
down. It may not be valid to compare results from traversed by a high speed router-cutter guided by a
one type of test piece with those obtained on a test shaped template).
piece of different size or shape. 7.5 Method 320D. For test pieces either injection or
A minimum of five test pieces shall be tested in each compression moulded (Figure 4), the moulding
of the required directions of testing. conditions (temperatures and pressures) shall be
Dumb-bell test pieces that do not break within the those recommended in the relevant standard for the
central parallel portion shall be discarded and material or by the material manufacturer.
further test pieces shall be tested. Allowance shall be made for the mould shrinkage for
different materials (usually catered for when the
7 Preparation of test pieces moulding tool is made).
All “flash”, if present, shall be removed from the
7.1 General. As stated in BS 2782: Foreword,
general introduction and instructions: 1975, the moulded test piece, taking care not to damage the
properties of certain types of sheet material may moulded surface.
vary in accordance with the direction of the plane of 7.6 Method 320E. The rectangular test piece shown
the sheet. In practice it is usual to cut two groups of in Figure 5(a) shall be sawn from a blank by means
test pieces with their major axes respectively of a suitable saw (e.g. a carbide or diamond tipped
parallel and perpendicular to the direction of some circular saw or a bonded carborundum wheel). A
feature of the sheet that is either visible or inferred suitable method of preparing the rectangular test
from a knowledge of the method of its manufacture. piece with end pieces attached is to cut from the
moulding or sheet under test a rectangular
The direction of testing is defined as the direction of
blank 230 mm long × 150 mm wide and to attach
the long axis of the test piece, unless otherwise
strips to it to form the end pieces as shown
stated.
in Figure 5(b). The end pieces shall be prepared
The method of preparation varies according to the from material similar to that under test. It is
type of materials being tested and the form of the convenient to use a cold setting epoxide adhesive as
test piece. the bonding agent provided that care is taken to
When test pieces are prepared by machining (i.e. for follow the instructions of the manufacturer about
Methods 320C, 320E and 320F), the speed of the relative proportions of the resin and hardener
machining depends on the material being tested and and other conditions of use. Before the adhesive is
wherever possible the speeds should be based on the applied, the surface to be bonded should be slightly
details given in the appropriate British Standard roughened with a fine grade of abrasive paper and
covering the material or on the recommendations of thoroughly cleaned with solvent. It is recommended
the manufacturer. The machining conditions used that the assembly should be allowed to stand
shall not overheat the test piece and if a coolant is overnight under pressure. Individual test pieces can
used it shall not have a deleterious effect on the then be cut from the blank by a circular saw as
material being machined. All surfaces of a test piece described above.
shall be free from visible flaws scratches or When machining a sheet material of standard
imperfections. Marks left by machining operations thickness to a particular specimen thickness, one
or, in the case of coarse laminates, loose fibre ends, face of the manufactured sheet should be left intact.
may be smoothed with fine abradents used in place
7.7 Method 320F. The dumb-bell test pieces shown
of the cutting tool on the profiling machine. In all
in Figure 6 shall be prepared from a rectangular
machining operations, precautions shall be taken
blank by means of a profiling system (or a milling
against inhalation of dust and the occurrence of skin
irritation. cutter if the small radius test piece is being
prepared).
7.2 Text deleted
In the case of hard materials such as carbon fibre
7.3 Text deleted composites, the machining operations may require
the use of diamond or tungsten carbide tipped tools.
Aluminium sheet end pieces shall be bonded to the
specimens as shown in Figure 6 by means of an
epoxide adhesive.
© BSI 01-1999 3
BS 2782-3:Methods 320A to 320F:1976
4 © BSI 01-1999
BS 2782-3:Methods 320A to 320F:1976
© BSI 01-1999 5
BS 2782-3:Methods 320A to 320F:1976
12 Test report
The test report shall include the following
particulars.
a) A complete identification of the material
tested, including type, source, manufacturer’s
code numbers, forms, principal dimensions,
previous history, etc.
b) A reference to the appropriate
British Standard method
(e.g. BS 2782:Method 320C:1976).
c) The speed of testing.
d) The conditioning and test atmosphere used.
e) The number of test pieces tested.
f) The mean value of the required tensile
properties recorded.
g) The individual test results.
h) The standard deviation of the individual test
results (if required).
6 © BSI 01-1999
BS 2782-3:Methods 320A to 320F:1976
Appendix A Informatory notes A.3 When the material has a pronounced yield and
extends a large amount beyond the yield point
A.1 Attention is drawn to the fact that different before rupture and such materials are tested up to
force measuring systems have markedly different the point of rupture at a “slow” speed that has been
characteristics. In particular, pendulum types of selected primarily to produce initial stress/strain
machine may have high friction and inertia which data, the test will become unnecessarily prolonged
significantly affect their dynamic response. and indeed, in certain circumstances, be invalid.
Inertialess transducer types of machine are The testing of some highly flexible materials may
therefore to be preferred. fall into this category.
Although tensile testing machines fitted with A.4 In cases where the yield stress is not well
electronic force measuring devices can be regarded defined by the stress/strain curve, it is necessary to
as sufficiently free of inertia for the speeds of testing define an offset yield stress. This is done by
given in this standard, this does not necessarily specifying a point on the stress/strain curve where
apply to the recorders normally used with them. the curve departs from linearity by a specified
As a guide to recorder requirements, the response percentage elongation or extension (see Figure 7).
time for full scale travel Te should be considerably A.5 Strain data at or beyond the point of yield
less than the rise time of the force Tw if the dynamic should only be reported if the yield has taken place
errors are to be comparable with the static within the gauge length.
inaccuracy. It is recommended that for grade A
machines Tw $ 10 Te and for grade B A.6 When testing test specimens whose
machines Tw $ 5 Te. cross-sectional area decreases considerably before
break, the force may decrease to some extent after
For a full scale response the relationship with the having reached a maximum value, so that the
testing speed would be maximum force and the force at break are not the
lo Ep lo Ep same.
a) grade A machine 100 V M = ------------- # --------------- A.7 If a secant modulus is used the relationship
T w 10 T e
between stress and strain need not be linear below
lo Ep lo Ep the strain at which the modulus is taken.
b) grade B machines 100 V M = ------------
-# ------------- A.8 For certain composite materials consisting of
Tw 5 Te
thermosetting resin systems reinforced with layers
where of glass fibre and manufactured by the wet lay-up
process, it may be relevant for some applications to
express the result in terms of ultimate tensile unit
VM is the testing speed (in mm/min)
strength (see C.6 of BS 4994:1973).
lo is the grip or gauge mark separation (in mm)
F max
Ep is the percentage elongation corresponding Thus u = ---------------
-
b n g
to the maximum force
where
If only a fraction d of full scale deflection is involved,
the permissible maximum testing speed is increased
u is the ultimate tensile unit strength
to Vm, which is given approximately by the
(in kN/m per kg/m2 glass)
relationship.
Fmax is the force at maximum load (in N)
l
V m » --V
d M b is the width of stressed portion of test piece
(in mm)
A.2 On some test machines, the grip attached to the
n is the number of laminate layers in test
load recording mechanism may itself move a
piece
significant distance during the test and thereby
influence the applied rate of strain. g is the mass of glass in one layer of
laminate in test piece (in kg/m2)
© BSI 01-1999 7
BS 2782-3:Methods 320A to 320F:1976
It may also be relevant to express the stiffness of Fs is the force applied to produce an initial
such materials in similar terms and the term (straightening) stress (normally 10 % of
“extensibility” is given in C.7 of BS 4994:1973 as the expected force at 0.2 % strain) (in N)
follows. and b, n and g are as defined above.
F 0.2 – F S A.9 In certain composite materials, the matrix alone
X = -------------------------------- may fracture and leave fibrous reinforcement
0.002 b n g
bridging the gap between the broken parts of the
where specimen. When this phenomenon occurs, a suitable
annotation should be made to the test report.
X the extensibility of laminate
Figure 1 — Figure deleted
(in kN/m per kg/m2 glass)
Figure 2 — Figure deleted
F0.2 is the force required to produce a strain
of 0.2 % beyond the strain imposed by the
pre-stress (in N)
8 © BSI 01-1999
BS 2782-3:Methods 320A to 320F:1976
© BSI 01-1999 9
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