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1, February 2015 : 18 - 28
ABSTRACT
This study investigates the effectiveness of magnetic concentration techniques for the beneficiation of borehole
samples of Arasuko - West Sumatera iron ore. It is a low-grade type of ore sample (±35% Fe) with high silica
and calcium content (±36%). Based on the fact, that there are appreciable differences in magnetic susceptibility
between the desired iron minerals and the gangue minerals, hence, it was suggested that multi-stages magnetic
separation may be useful to concentrate this type of ore. Because of the fine dissemination of the iron minerals
and the most abundant gangue mineral, the particles size of ore was set at 80% passing 150 meshes. Rougher
tests of magnetic separation produced concentrates with iron content of about 58.2% Fe; the tailing of rougher
stage was then scavenged using higher magnetic intensity. Further, the rough and scavenged concentrates
were mixed and fed into a cleaner stage with low magnetic intensity. Results indicate that the final iron concen-
trate assaying of 68.1% Fe at a recovery of about 80% is achieved and reckoned as an iron premium-grade
concentrate.
SARI
Penelitian dilakukan untuk mempelajari keefektifan teknik pemisahan magnetik untuk meningkatkan kadar
percontoh inti bor bijih besi kualitas rendah asal Arasuko – Sumatera Barat. Percontoh bijih tersebut berkadar
rendah yaitu ±35% Fe, mengandung pengotor silika dan kalsium yang tinggi yaitu ±36%. Berdasarkan kenyataan,
perbedaan kerentanan magnetik antara mineral besi dan mineral bukan besi cukup besar, sehingga pengonsen-
trasian cara magnetik bertingkat efektif dilakukan terhadap percontoh bijih tersebut. Percontoh bijih dihaluskan
hingga 80% lolos 150 mesh, dilanjutkan dengan uji pemisahan mineral magnetik tingkat penyesah yang dapat
menghasilkan konsentrat dengan kadar Fe 58,2%. Ampas dari proses penyesah dibilas secara magnetik pada
intensitas magnet lebih tinggi, selanjutnya konsentrat bilasan dicampur dengan konsentrat penyesah untuk
dibersihkan lagi secara magnetik pada intensitas magnet yang rendah. Hasil penelitian menunjukkan bahwa
kadar Fe pada konsentrat akhir 68,1% dengan perolehan sekitar 80% yang termasuk konsentrat besi kadar
premium.
18 Received : 03 November 2014, first revision : 22 December 2014, second revision : 26 January 2015, accepted : February 2015
Beneficiation of Borehole Iron Ore Samples Through ... Nuryadi Saleh and Ngurah Ardha
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Indonesian Mining Journal Vol. 18, No. 1, February 2015 : 18 - 28
tion degree analysis. Chemical analysis used AAS in Figure 2. The tests results were then evaluated
method while mineralogical and liberation degree based on chemical and mineralogical interpreta-
analysis used optical microscopic method. Both tion. Calculation of magnetic separation results in
of ground samples were mixed into a composite a closed-circuit with recycling of the cleaner tail
sample with mixing ratio of MS/LMS = 0.6/0.4 into the initial feed is also discussed.
(w/w); The composite sample was mixed with wa-
ter within 30% solid, and was then tested through
a wet multi-stages magnetic separator (feed rate RESULTS AND DISCUSSION
of 25 kg/hour) with adjustable magnetic intensity.
During the separation tests, a typical “SLon” Chemical Composition of Ore Raw Material
vertically pulsating high gradient magnetic sepa-
rator was used as depicted in Figure 1. Rougher Both of ore samples i.e. magnetic (MS = magnetic
magnetic and cleaner magnetic separations have sample) and less magnetic (LMS = less magnetic
applied magnetic intensity of 2,000 gauss (0.2 sample) have been chemically analyzed to know
Tesla) and 1,000 gauss (0.1 Tesla), respectively. the grade of the main elements as shown in Table
The tail of rougher stage was fed into a 1st scav- 1. MS samples were obtained from the depth in
enger magnetic separator with applied magnetic between 35 m to 45 m, while LMS samples were
intensity of 2,000 gauss (0.2 Tesla), and then the obtained from the depth in between 21.5 m to 59
tail of 1st scavenger magnetic separator was fed m. The ore samples were ground to reach a size
into a 2nd scavenger magnetic separator with of 80% - 150 mesh (100 µm). Furthermore, after
applied magnetic intensity of 4,300 gauss (0.43 analyzing the chemical content, it is known that
Tesla). The magnetic intensities were applied in each sample of MS contains Fe about 36 to 57%
different strength for different separation steps with silica content around 5 to 13%, on the other
that are based on the difference of magnetic hand, each sample of LMS contains Fe about 20
properties between the ore minerals, i.e., ferro- to 37% with high silica content.
magnetic, paramagnetic and diamagnetic (Wills,
2007). Steps of the multi-stages magnetic separa- Based on the principle of mining operation, where
tor was conducted in an open circuit as depicted in the one area of the ore deposits should have
Figure 1. A typical of “SLon” vertically pulsating high gradient magnetic separator (Outotec, 2013)
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Beneficiation of Borehole Iron Ore Samples Through ... Nuryadi Saleh and Ngurah Ardha
Composite sample
of iron ore bearing
minerals
tail.Ro
Rougher
separator
0.2 Tesla 1st Scavenger
tail.Scav1
separator
0.2 Tesla
Conc.Ro
Recycl.tail.Clean
separator
0.43 Tesla
Conc.Scav2
Cleaner
Final tail
tail.Clean separator
0.1 Tesla
Final concentrate
a uniform ore grade, thus, the two drilling core Mineral Composition of Ore Raw Material
samples were mixed with mixing ratio of MS/LMS
= 0.6/0.4(w/w) to obtain a composite sample hav- The ground samples of MS and LMS as well as its
ing calculated grade of Fe around 35%. However, composite were also analyzed mineralogically by
the actual grade of the composite sample obtained counting through optical microscopic image. The
from chemical analysis contains 36.56% Fetotal, result as shown in Table 2, clarify that magnetite
20.82% CaO, 15.14% SiO2, 1.49% S, 6.5% Al2O3, is the predominant minerals with small amount of
1.32% TiO2, 0.8% MnO2 and P2O5 is nil (Table 1). native iron. On the other hand, significant amount
The grade of the composite sample used in this of sulphide metallic minerals of bornite is found
study is likely similar to the grade of low-grade especially in the LMS ore sample. Gangue miner-
iron ore in Egypt studied by Al-Wakeel and Abdel- als (non-metallic minerals) content of about 40%
Rahman, 2005, as well as Ahmed et al, 2012. may consist of quartz and calcium oxide, which
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Indonesian Mining Journal Vol. 18, No. 1, February 2015 : 18 - 28
clearly realizes that the present ore samples re- 93% for MS sample, and also relatively similar is
ceived are low-grade iron mineral type. found for LMS sample, where its magnetite libera-
tion degree is more than 92%. As the fact of high
Degree of Liberation liberation degree for magnetite mineral in these
ores, hence, the process of magnetic separation
Magnetite as the predominant mineral found in would be subjected to be successful.
the present iron ore sample was counted for its
degree of liberation. Table 3 presents that within Referring to all data with respect to chemical
particle sizes of passing 150 mesh (100 µm), the analysis, mineralogical analysis and liberation
liberation degree of magnetite is found more than degree analysis of magnetite would be compared
MS (Magnetic Samples)
No.
Core depth Weight, g Fe total,% CaO, % SiO2, % S, % Al2O3, % TiO2, % MnO2, % P2O5, %
1 35-40M 8.600 41.8 23.79 10.27 0.80 4.91 0.50 1.58 0
2 40-41M 6.000 41 23.79 11.98 0.80 4.16 0.50 1.27 0
3 40-45M 5.800 39.6 23.79 12.62 0.90 5.67 0.84 1.42 0
4 41-42M 6.600 57.6 7.7 5.78 0 3.40 0.17 0.32 0
5 42-43M 5.600 56.5 8.81 5.35 1 5.29 0.50 0.32 0
6 43-44M 5.800 46 18.47 10.27 0 4.16 0.50 0.95 0
7 33-35M 8.400 36.8 25.89 13.48 1.60 6.05 1.34 1.27 0
8 40-45M 9.200 38.9 23.37 13.69 0.90 4.53 0.84 1.27 0
TOTAL (MS) 56.000 44.03 20.09 10.72 0.79 4.79 0.68 1.09 0
A composite Sample
No. Composite Weight, g Fe total,% CaO, % SiO2, % S, % Al2O3, % TiO2, % MnO2, % P2O5, %
(0.6/0.4)
1 MS+LMS 94.500 36.56 20.82 15.14 1.49 6.5 1.32 0.8 0
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Beneficiation of Borehole Iron Ore Samples Through ... Nuryadi Saleh and Ngurah Ardha
Table 3. Liberation degree of magnetite within ore 400 µm found interlocked with magnetite of size
size of P80, -150 mesh 100 µm as shown in Photomicrograph 2. Further,
Photomicrograph 3 shows magnetite and bornite
No. Samples Liberation Degree (%) of size about 40 – 50 µm are bound to spread in-
1. MS 93.45 side of a gangue mineral particle of size 200 µm.
The characteristic of LMS drilling core sample,
2. LMS 92.73
as presented by Photomicrograph 4, is found a
liberated magnetite and bornite of size around
50 – 100 µm. While from Photomicrograph 5 is
with some Photomicrographs of MS and LMS pol- found magnetite of size about 100 µm interlocks
ished samples as revealed in Photomicrographs with a particle of gangue mineral of size 150 µm.
1 to 5. The Photomicrograph 1 presents a drilling Therefore, from all Photomicrographs confirm
core for MS ore sample, which shows free mag- that magnetite mineral might be appreciable to be
netite minerals at particle sizes around 100 to 200 separated through a low-magnetic intensity sepa-
µm. For the similar ground MS ore sample also rator at sizes finer than 150 mesh (100 µm).
presents a particle of gangue mineral of size about
M
GM
M
Photomicrograph1. Sample MS, free magnetite (M) Photomicrograph 2. Sample MS, magnetite (M)
interlock in gangue mineral (GM)
GM
B
M M
B
Photomicrograph 3. Sample MS, magnetite (M) and Photomicrograph 4. Sample LMS, free magnetite
bornite (B) interlock in gangue (M) and bornite (B)
mineral (GM)
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Indonesian Mining Journal Vol. 18, No. 1, February 2015 : 18 - 28
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Beneficiation of Borehole Iron Ore Samples Through ... Nuryadi Saleh and Ngurah Ardha
B
M
M
Photomicrograph 6. Rougher concentrate contains Photomicrograph 7. Rougher tails contains free small
predominantly magnetite (M) amount of magnetite (M) and
bornite (B)
magnetic separation, therefore, the final iron 1st scavenger and 2nd scavenger. Multi-stages
concentrate is obtained containing 68.1% Fetotal separation and recycling of intermediate tail were
with recovery of 81% (Table 5). Other metallic used to maximize the iron concentration and its
non-magnetic components (i.e., bornite and pyrite recovery (Karmazin et al, 2002). The tail of the
at rougher concentrate as presented in Table 4) cleaning stage is recycled into initial feed, while
are distributed in small amount, except for gangue the concentrate of rougher and 1st scavenger as
minerals which may be due to fines interlocking well as 2nd scavenger are mixed together to feed
with the magnetic particles. However, based on into the cleaner stage. The weight of overall feed
iron content with assumption of limited grade of becomes 105.99%, while the weight of final tail
non-ferrous metals, so the concentrate obtained obtained from the tailing of the 2nd scavenger
is considerably as a premium-grade. likely increases from originally 53.41% (as batch
test) to 55.41% (as recycled calculation). The iron
Based on the flowsheet of the process as depicted content loosed into the final tail increases from
in Figure 2 and a series of experimental data, so originally 8.13% Fe (as batch test) to 12.13% Fe
that, calculation of the materials balance within the (as recycled calculation). The phenomenon of
closed-circuit of multi-stage magnetic separation loosed iron into the final tail may be due to the
process is solved to understand the reliability of locked magnetite with gangue minerals, and also
the process, if it would be applied in plant scale there may present some iron based limonite and
in the future. The calculated data of closed-circuit pyrite loosed into final tail. Therefore, in order to
process is presented in Table 6. The flow of the increase the recovery of iron minerals, it might
materials is calculated through 4 (four) steps be important to regrind of the rougher tails prior
of magnetic separation, i.e., rougher, cleaner, to be fed into the scavenging stages (Karmazin
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Indonesian Mining Journal Vol. 18, No. 1, February 2015 : 18 - 28
et al, 2002). Whatever the cause is, the data ob- (0.76%wt) with size less than 100 µm (see Pho-
tained from calculated material balance present tomicrograph 8) and having grade about 12.13%
final concentrate of iron ore treated in multi-stage Fe is still loosed into the final tails (see Table
magnetic separators, that have had high grade 6). According to Al-Wakeel and Abdel-Rahman,
(68.1%Fe) with a recovery around 80 %. This 2005, who stated that fine fraction requires high
typical concentrate is considered as a premium- magnetic intensity, so that in the present tests of
grade iron concentrate, which is suitable for blast multi-stages magnetic separation, which apply
furnace operation (Al-Wakeel and Abdel-Rahman, magnetic intensity within 0.1 to 0.43 Tesla may
2005). Moreover, concentration ratio of the sepa- be inadequate yet for attracting the fine magne-
ration process is found 100/40.6 or 2.46, thus, it is tite particles. From the photomicrograph 8 to 11,
supposed to produce 1 ton iron concentrate with fine magnetite minerals are looked interlock with
grade of 68% Fe requires 2.46 tons of iron ore gangue minerals and also it is shown some iron
with grade around 35% Fe. minerals based limonite and pyrite or chalcopy-
rite. Those minerals contain iron causing high
Characteristic of Final Tail grade of iron presents in the final tail. Pyrite and
chalcopyrite as well as limonite present in free
Final tail rejected from 2nd scavenging stage of particles condition. In general, however, final tail is
magnetic separator using high magnetic intensity predominated by less-magnetic sulphide minerals
of 4,300 gauss (0.43 Tesla) contains such minerals as well as non-magnetic gangue mineral such as
as shown in Table 7 and in the Photomicrographs pyrite, bornite, chalcopyrite and gangue minerals
8 to 11. Small amount of fine magnetite particle of quartz and calcium oxide.
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Beneficiation of Borehole Iron Ore Samples Through ... Nuryadi Saleh and Ngurah Ardha
M
L
GM
Photomicrograph 8. final tail, magnetite (M),100µm, Photomicrograph 9. final tail, free limonite (L),
interlocks with gangue mineral ±50µm.
(GM)
P C
Photomicrograph 10. final tail, free pyrite (P), ±100µm Photomicrograph 11. final tail, free chalcopyrite (C),
±40µm
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