This paper studied struvite precipitation from septage sludge as a form of
phosphorus recovery. The septage sludge sample was subjected to alkaline hydrolysis to increase the phosphorus recovered in the form of struvite. The total amount of phosphorus contained in the sample as phosphate increased from 17.05% to 46.88%. Struvite precipitation was conducted after alkaline hydrolysis, and the phosphorus recovery percentages ranged from 39.39% to 53.12%. Thus precipitation of struvite makes a feasible strategy for lowering wastewater's phosphate concentration. The results of the ANOVA analysis revealed that only the interactive effects of the Mg:P ratio and residence time had a significant impact on phosphorus recovery. Amorphous precipitates were assumed to have formed based on the sample's XRD diffractogram, which was supported by minor peaks. After alkaline hydrolysis, it was found from the Mg2+ and Ca2+ analyses that phosphorus recovery thru calcium phosphate was less likely. It is most likely that phosphorus was recovered as aluminum phosphates based on the d-spacing of the minor peak with a value of 4.13 obtained from the XRD study. Future works will include metal ion removal process as pre-treatment to the hydrolysed sample to eliminate or minimize the formation of other phosphate salts.