Ujjain Engineering College, Ujjain (MP) 456010 Scheme of Examination as per AICTE model curriculum 2018 Bachelor of Technology (B.Tech.) W.EF. JULY, 2018 ‘Semester - V (FIFTH)\ CHEMICAL ENGG. ee Contact Fours per [____ Distribution of Marke sm] | ce | comer Se aan t[t| P [ceeaits| ese | mst | aar| ese |taar| M75) 1 cvsaot | as Tansfer-1 afafa] s | | 2 | 2 | 2 | 2 | 10 2 cavsa0z | chemical Reaction ngineerne | 3 2[2] 5 | 7 | 20 { 20 | 20 | 20 | 250 races Equipment Design 3 al 2 3 gen | oe afafo{ « | | 2 | w 20 4 cavsa08 | Petroleum Technology afafo{ « | | »| « zo | 120 5 cavsasx | (oto cremialeneineeing| 3 o[2| « | 7 | 20 | 20 20 | 120 ¢ gue | orem fo [ol] « 2 |» | © 7 215306 | comprenensveassesinen | o[o]o] 0 xo | 30 Fou fosf ape] z | a0] 100] oo | oo | 60 | 750 [open Eta [xMi5351 [Bio Chemical Engineering] ‘Semester - VI (SIXTH) CHEMICAL ENGG. | Tanta Fours per [station of Marks ; | ele ee cours Te = Teony—~ | praca], "3! & a t|t |e [creaits| ese | mst | qar| ese |taar |“ 1 comss01 | Transport Phenomena sfofo{ s | | 2 0 2] [own | areseewmmen fafapo| « |m[~] «| |» | a ad 3 cues | crenicarocasconvs [af af2| = | | 20] 20 | a0 | m | 0 4 aneaoe | Moss raster afof2] s | | 2| 2] 3 | 2 | 10 5 | [owen | Cemmanarrawen [sof a[ = [m| =| w| = | | ‘ 216305 | chemical Process smulation-] 0] 0[ 2] 0 xo | 30 | « 7 (06306 | compehensvensesmen [ofa o| 0 x0 | 30 : Treas iefe |e [oe om | |e [ve [oe [a Internship two weok after sixth sementer [Open BSC Basi Science Course ESC Engineeing Sconce Couse |HSMC Humans & Social Sciences ining Management Courses [en16351_ [industrial Pollution Abatement ESE ust oar Loar End Semester Examination Mi Semester test (Quizzes Assignment & Regularity Lab work Quizzes Assignment & Regulatiy (JOO) Shot on vivo S Al Triple CarHEMICAL ENGINEERING COURSE CONTENTS ] Max. Min. Pee bea as Cle nari Marks Anes es 70 22 Course Objectives: The purpose of this course is to introduce the undergraduate students with the most important Separation equipment in the process industry, and provide proper understanding of unit operations. Unit Fundamentals of Mass Transfer: Introduction and classification of Mass transfer operations, Choice of separation method. Mass transfer coefficients: Individual and film coefficients, Overall mass transfer coefficient, Determination of mass transfer co-efficient. Interphase mass transfer. Analogies in transfer processes. Mass transfer theories: film, penetration and surface renewal theor Unit Diffusion Phenomena: Fick’s law of diffusion, Steady state molecular diffusion in fluids under Stagnant and laminar flow conditions, Diffusion coefficient: measurement and prediction, Diffusion in solids and its applications, Unit Tit Distillation: Vapour liquid equilibria: Boiling point diagram, Raoult’s law, Relative volatility. Azeotropes: minimum and maximum boiling mixtures. Enthalpy concentration diagrams for binary systems. Methods of distillation: Flash, Differential and Steam Distillation; Azeotropic and Extractive Distillation; Unit IV Continuous Multistage Distillation: Multistage tray towers. Analysis of bi towers using graphical methods of McCabe-Thiele and Ponchon-Savar reflux and optimum reflux ratio, open steam, multiple feed and side sir Calculations, Plate, point and overall efficiency in distillation columns, Column internals. Loading, flooding, coning etc. phenomenon in columns, Unit V ry distillation in tray ‘minimum reflux, total ream. Multi component Introduction, Types of tower packing’s, Contact between liquid and gas, Pressure drop and limiting flow rates, Material balances, Limiting gas-liquid ratio, Rate of absorption, Caleulation of tower height and number of transfer units (Concept of HTU and NTU), Alternate forms of transfer coefficients, Absorption in plate columns, Absorption with chemical reaction List of Experiment {To study the flooding and loading of packed columns using different types of packing, 2. To study different types of plates and packing, 3. To prepare the vapor 4. Determination of *- liquid equilibrium and Boiling point diagram for a binary liquid mixture. relative volatility ofa given system of acetic acid water. ‘Sper AICTE model curriesoe ee(ae) CON ete aio een] erent)on of fluid solid tribution Rate equati | Poe A eurement and analysis of Kinetic talytic reactions surface area and mechanism ofcatal ti nim nt models, Pr n = Watson & Poinule law nori-catal tic sol tough ash layer controls, Chemical catalytic reactions, Hot data, kinetics of catalyst deactivation, Modes fr uid - solid 10 mechanisms, Diffusion through gs film contos,Difusion through reaction controls, fluidized bed reactors with and without elutria List of Experiments: ciate by sodium 1. To determine velocity rate constant of the iydrolysis of ea ne 5 by 2. To study the rate constant of hydrolysis of an ester-catalyzed by aci er sulphate and 5. Determine the rate constant and order of reaction between Potassium per sulphi Potassium iodide. energy and 4. To study temperature dependency of rate constant, evaluation of activation energy verification of Arthenious law hydroxide. 5. To study a consecutive reaction system( hydraulic model) &. To study a parallel reaction system ( hydraulic model) 7. Study of non-catalytic homogeneous saponification reaction in CSTR & To study a non-catalytic homogeneous reaction in a plug flow reactor. 9. To study the residence time distribution 10. Behavior of a back mix reactor, 11. To study the RTD behavior of a tubular reactor. 2. To study the RTD behavior of a packed bed reactor. 13; To study the behavior ofa continuous flow reactor system-three reactor in series. '4. To study the kinetics of thermal decomposition of caleium carbonate, J} Study of non-catalytic saponification reaction in a tubular flow reactor. Note: Each student should perform at least eight experiments out of the above list. Course Outcomes: + Develop rate laws for homogeneous reactions + Design of ideal reactors for single and complex reactions { Develop skis to choose the right reactor among single, multiple, recycle reactor ete schemes, * Design of non-isothermal reactors and the heat exchange equipment required Suggested Readings: J. 1M. Smith CHEMICAL ENGINEERING KINETICS ~ 3" Ed, Me Graw Hit * KG; Denbigh & K.G. Tumer— CHEMICAL REACTION THEORY AN INTRODUCTION ~ 2" Fd, United Press and ELBS 1972 pre sopPet & GV Jeffery’s — CHEMICAL KINETICS AND REACTOR ENGINEERING Prentice Hall 1972 4 0 Levenspiel ~ CHEMICAL REACTION ENGG, - 2" Ea. Willey Easter, Singapore. Caushen Watson & Ragatz — CHEMICAL PROCESS PRINCIPLES PART III = (Kinetics & Catalysis) 2 Ed, Asian Publishing House Bombay. & Poslet, H.S.— ELEMENTS OF CHEMICAL REACTION ENGINEERING ~2™ Fa. Prentice Hall of India Pvt. Ltd. New Delhi, -1999 {yon — Yor e As per AICTE model curriculumAE TUU a -) CoB Thea To design pr “IBM Process equipment, vessels with associated cooling/heating equipment ies of Materials: Stress- Strain relationshi ain relationships of elastic materials subjected to tensile, Elastic and plastic ete oa stie materials subjected to tensile, compressive and shear forces, supported, td cola tion, General design considerations; Design of shell, bottom plates elf } and column supported roofs, wind girder, nozzles and other acessories Unit ee Unfired Pressure Vessel: [Pressure vessel codes, classification of pressure vessels, Design of eylindrical and spheriea shells eral pressures; Selection and design of flat plat, tore-spherical, ellipsoidal compensations of openings. High pressure Vessels: Stress analysis of thick and conical closures, Walled cylindrical shell, Design of monobloc and multilayer vessels, Unit 11 Tall Vertical & Horizontal Vessels: Pressure, dead weight, wind, earthquake and eccentric loads and induced stresses; combined siresses, Shell design of skirt supported vessels. Vessel supports; Design of skirt, ug, and saddle supports, Unit 1V Bolted Flanges: Types of Flanges, and selection, Gaskets, Design of non- standard flanges, specifications of standard flanges. Fabrication of Equipment; major fabrication steps: welding, non-destructive tests of welded joints, inspection and testing, vessel lining, materials used in fabrication of some selected chemical industries. Course outcomes: After the course student should able to: ‘+ Knowledge of basies of process equipment design and important parameters requires Design of internal and external pressure vessels Design of tall and horizontal vessels and its supports Knowledge of equipment fabrication and testing methods Suggested Readings: 1. Brownell, N.E and Young, H.E; Process Equipment Design; John Wiley. 2. Bhattacharya, B.C; Introduction of Chemical Equipment Design; CBS Publishers, Delhi. 3. Perry RH; Hand book of Chemical Engineers; Me Graw Hill Pub. Page 5 4s per AICTE model curriculum \ ak a4. 1S.: 2825-1969 Code For Unfired Pr suire Vessels. z fertical and Mild 5. LS. 803-1962, Code of Practice for Design, Fabrication and Erection of Vertical and Mik Steel Cylindrical Welded Oi! Storage Tanks, &. Joshi, M.V.; Process Equi ipment Design, suit Pao 7. Ludwig EE; Applied Pro, and Petrochemical Plants; Gulf Publishing Design in Chemical mt__B.Tech V Semester CHEMICAL ENGINEERING COURSE CONTENTS ees | Petroleum Technology [i]t] v | € I ae t{[4| 7 Duration [3 Hours Baye Course objectives: Studying this subject the students will leam about the extraction and production of oil and gas to meet energy needs, as well a refining of crude oil fora wide spectrum ‘of useful products such as petrochemicals, Chemicals, Plastics. Unit-l Origin of Petroleum: Origin and occurrence of petroleum crude, petroleum, classification and physical properties of petroleum. Ev petroleum products, future refining trends. Unit -11 tillation of Crude Crude oil Distillation Process, Pretreatment of erude, atmospheric and vacuum distillation process. Secondary conversion processes: Catalytic reforming, catalytic eracking and deep catalytic cracking Unit 111 Heavy Residue Up gradation: Hydro cracking, Hydro treating, visbreaking and delayed coking alkylation, isomerisation, dehydrogenation processes, polymerization. Unit -1V Lubricating Oil, Grease and Bitumen: Dewaning and deoiling, deasphalting, lube hydro-finishing, bitumen air blowing, Sweetening and Desulphurization. Hydro-desulphurisation of petroleum products. Unit-V Solvent Extraction: Solvent furfural process, refinery gas utilization: LPG, propylene and hydrogen recovery, Reformulated Gasoline: Present and future requirements, status of petroleum refining in India. Composition of faluation of crude oil and Course Outcomes: # Introduction with the petroleum refinery worldwide. Develop knowledge of different refining processes. Develop knowledge of safety and pollution control in the re To find the suitable refining technology for maximizing the gasoli Suggested Readings: 1. Nelson W.L. - PETROLEUM REFINERY ENGINEERING - 4th ed. McGraw Hill .(1987) 2. Hobson G.D.et al MODERN PETROLEUM TECHNOLOGY - Part & 11 9th ed. 1986 John Willy & Sons. , ee Qo — eS ‘hs per AICTE model curriculum yeNEERING. B.Tech V Semester CHEMICAL ENGINEERII | COURSE CONTENTS ut Salen ieelae Max. | Min Biochemical Engineering Sa ih ark Marks ie ae ca = Gia. ae zee | a Course objectiy this subject the sindents wil ea about the enzymes and Production of bioreactors and biofuel S {0 meet energy needs, as well as refining of crude oil for a wide Spectrum of usefil produ s Introduction to Bio-Processes Aspects of microbiology, cell theory structure of microbial cell Russilication of microorganism Essent eh Chemicals of life lipids, Sugars and Polysaccharides, RNA and DNA, Amino acids ara Proteins, Unit 1 io-Proc nicroor ils. Biochemical Kinetics, Simple xl tegulation of enzymatic activity, *SaZyine reactions in heterogeneous syne Sterilization, filtration Unit IL I vation, mathemati batch growth, products symthesie Kinetics, overall kinetics and therm death ki spores Unit 1v Genetic Engineering: Application of genetic engineering, agitation an of oxygen transfer rate id acration, Determination © determination of Kea and Kl-a Unit V aling of mass transfer equipment Design of Bioreactor: Classification and characterization of differem.biore proce Ms Feaciors, tubular, CSTR and towne Factors. Aerobie and an ManuigciS8" ad operation of typice ‘aerobic and anaerobic ‘S€-8. antibiotics aleohol/wine ete migasetamine and study the effectivenes oe Various technigu ‘microorganisms. 3. To study the kinetics of etha ‘To determine the kinetic 3 To idemity bacterial species usin 6. To determine the biochemical on 7. To determine the chemical oxy ‘AS er AICTE model cumeulom Yi NengBiTech V Semester CHEMICAL ENGINE COURSE CONTENTS T | Chemical process plant Ib r| P | c simulation -1 | Hk at Duration | 3 Hours ofo| Opera 's on following Software's © ChemCad Part +1 * Pro-simulator Part -1 Course Outcomes: Students are able to acquire different learning outcomes + Use Be * Do system analysis to understand the system behavior. + Simulate different control action on given control system. Understand the DCS system used in chemical industries. >) 1 AICTE model curriculum ERING. Max. Marks 60 | Min. | Marks 30 instrumentation simulation software for chemical process and control simulation. ‘er understanding of basic concepts as well as complex processes and controls