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GAS & VAPOR DOSING SYSTEMS GAS & VAPOR DOSING SYSTEMS
GAS & VAPOR DOSING SYSTEMS PRESSURE CONTROL IN STATIC ATMOSPHERES PRESSURE CONTROL IN FLOWING ATMOSPHERES
. .
Generation of controlled reaction atmospheres can become quite FlexiDOSE STATIC devices are pressure controllers for gases, Three different versions of the FlexiDOSE STATIC devices for FlexiDOSE FLOW devices are gas and vapor flow dosing systems p two mass flow controllers (MFC, V1, V2) for dosing a gas or
complex and troublesome when high accuracy is required. subcritical and supercritical fluids and vapors. The pressure in different pressures and/or measuring fluids consist of the main with dynamic pressure controllers. A flow of pure reaction gas, mixing gases and dosing into the balance/reactor (more gas
Rubotherm FlexiDOSE instruments are sophisticated, automated the connected reactor is exactly controlled by functional units: gas mixture or gas and vapor mixture with controlled composition lines can be added optionally)
turn-key gas and vapor dosing devices for challenging applications. p allowing the reaction atmosphere to flow into the reactor p one or more pressure sensor(s) with different measuring ranges is generated. It flows continuously through the connected reactor. p up to two pressure sensors (P1, P2) with different measuring
FlexiDOSE instruments are universal gas and vapor dosing devices (pressure increase) or p dosing valves (DVx) for controlling pressure increase or decrease The pressure of the flowing atmosphere in the reactor is exactly ranges
and pressure controllers: modular design, flexible and customizable p allowing the atmosphere in the reactor to flow out p basic configuration with selection between two reaction gas controlled by means of a dynamic backpressure controller in the p up to two pressure controlling valves (DV) in the gas flow
high pressure gas and vapor dosing systems. The systems are (pressure decrease) supply lines outlet flow. The following standard configurations of FlexiDOSE coming out of the balance/reactor with different pressure
designed for operation with Rubotherm’s magnetic suspension until the pre-defined set point pressure is reached. FLOW devices for different pressures and/or measuring fluids controlling ranges
balances as well as external reactors, for instance high pressure consist of the main functional units:
autoclaves, calorimeters, furnaces, etc. Unique features of the
FlexiDOSE systems are: The following standard configurations of FlexiDOSE STATIC devices are available:
p Highest Accuracy in Pressure Control Flexi DOSE STATIC G Flexi DOSE FLOW G
Providing atmospheres with minimal pressure fluctuations in a For measurements in static gas atmospheres in the pressure range For measurements in flowing gas or gas mixture atmospheres in
wide pressure range. up to 150 bar (HP). the pressure ranges up to 1 bar (LP), 50 bar (MP), 150 bar (HP), or
p Accurate Vapor Dosing In the basic configuration with selection between two reaction 300 bar (HPII).
Generation of vapors from liquids and precise control of vapor gas supply lines, optionally gas switch for permanent connection
pressure, composition, and humidity. of five reaction gas supply lines. Even the pressure of vapors may
p Volumetric Dosing and Mixing be controlled by this device. The controlling range for vapors is
For exact volumetric metering of reaction atmospheres and for limited to approx. 50% of the dew point pressure at ambient
producing exactly defined gas and vapor mixtures. temperature (e. g. 30 bar for CO2 ).
The FlexiDOSE devices are available in two basic configurations with
FlexiDOSE instruments are automatically operated by software different pressure control ranges from vacuum to 700 bar: Flexi DOSE STATIC SC
control. Their standard gas connections allow easy combination For measurements in static gas and subcritical fluid atmospheres Flexi DOSE FLOW G&V LP
and i ntegration with existing autoclaves or reactors. FlexiDOSE STATIC for gas or vapor pressure control in in the pressure ranges up to 150 bar (HP), 350 bar (HPII), or 700 bar For humidifying a gas or a gas mixture at ambient pressure the
widest range (HPIII). flow dosing system is equipped with a humidifier. The gas flow
Typical applications are: Accurate pressure control is not trivial when liquefied gases are bubbles through the liquid and is saturated with vapor. Humidity
p Measuring of selective reactions (absorption and adsorption / FlexiDOSE FLOW for gas and vapor flow control, mixing, involved: CO2, NH3, propane, or butane are available as liquefied control is achieved by mixing this saturated gas flow with a
catalysis) by mixture generation, volumetric metering, and and wide range pressure control gases in cylinders only with limited pressure. Dosing fluids with second dry gas flow. Humidity is measured with an accurate
composition analysis such thermodynamic properties at pressures above their dew dew point mirror and thus, independently from the used liquid /
p Vapor generation, dosing, and pressure control for evaluating For dosing condensable atmospheres like vapors or sub-critical point leads to condensation in the tubes or icing of the valves. vapor. Condensation of vapor is avoided by a heater that heats
wetting and drying processes fluids heated versions of the FlexiDOSE systems are available. This problem is solved by heating of the entire dosing system above the gas saturator, all tubes, valves and sensors which are in
p Monitoring high pressure gas or supercritical fluid solubility / Please refer to the following pages for details about the available the critical or c ondensation temperature. Therefore FlexiDOSE contact with the vapor.
extraction by pressure control in autoclaves configurations of the FlexiDOSE systems. STATIC SC dosing systems are heated to ensure supercritical tem
p Heat of reaction measurement by gas dosing and pressure perature conditions and allow accurate high pressure control of
control for calorimeters FlexiDOSE instruments are the ideal combination for our Magnetic subcritical fluids. For reaching high pressures with these fluids a
p Membrane permeability and selectivity measurements by Suspension Balance to feed it with gases and/or vapors. Both syringe pump or compressor to supply liquefied gas above cylinder
gas mixing and trans-membrane pressure control devices together form a strong and flexible scientific measuring pressure is required.
system. Flexi DOSE FLOW G&V
For vapor dosing at high pressures of 50 bar (MP) or 150 bar (HP)
Flexi DOSE STATIC G&V the FlexiDOSE FLOW G&V is equipped with a steam generator.
For measurements in static gas or vapor atmospheres in the The gas coming from the mass flow controllers can be mixed with
pressure ranges up to 2 bar (LP) or 50 bar (MP). a flow of vapor/steam. The vapor is generated by compressing
Vapors of ambient temperature liquids (H2O, toluene, b
enzene, …) and dosing a controlled flow of liquid (H2O, naphtha, toluene, …)
are generated in three vapor pressure cells (VPC). The liquids in the by means of a HPLC pump. This liquid flow is evaporated under
VPC are heated to a controlled temperature. This generates vapor pressure in a vaporizer. Humidity control is achieved by controlling
with the boiling p
ressure at heating temperature. the ratio of liquid flow and gas flows. Condensation of vapor is
By heating up to 150°C high vapor pressures can be reached in the avoided by a heater that heats all tubes which are in contact with
GAS & VAPOR DOSING SYSTEMS PRESSURE CONTROL IN STATIC ATMOSPHERES PRESSURE CONTROL IN FLOWING ATMOSPHERES
. .
Generation of controlled reaction atmospheres can become quite FlexiDOSE STATIC devices are pressure controllers for gases, Three different versions of the FlexiDOSE STATIC devices for FlexiDOSE FLOW devices are gas and vapor flow dosing systems p two mass flow controllers (MFC, V1, V2) for dosing a gas or
complex and troublesome when high accuracy is required. subcritical and supercritical fluids and vapors. The pressure in different pressures and/or measuring fluids consist of the main with dynamic pressure controllers. A flow of pure reaction gas, mixing gases and dosing into the balance/reactor (more gas
Rubotherm FlexiDOSE instruments are sophisticated, automated the connected reactor is exactly controlled by functional units: gas mixture or gas and vapor mixture with controlled composition lines can be added optionally)
turn-key gas and vapor dosing devices for challenging applications. p allowing the reaction atmosphere to flow into the reactor p one or more pressure sensor(s) with different measuring ranges is generated. It flows continuously through the connected reactor. p up to two pressure sensors (P1, P2) with different measuring
FlexiDOSE instruments are universal gas and vapor dosing devices (pressure increase) or p dosing valves (DVx) for controlling pressure increase or decrease The pressure of the flowing atmosphere in the reactor is exactly ranges
and pressure controllers: modular design, flexible and customizable p allowing the atmosphere in the reactor to flow out p basic configuration with selection between two reaction gas controlled by means of a dynamic backpressure controller in the p up to two pressure controlling valves (DV) in the gas flow
high pressure gas and vapor dosing systems. The systems are (pressure decrease) supply lines outlet flow. The following standard configurations of FlexiDOSE coming out of the balance/reactor with different pressure
designed for operation with Rubotherm’s magnetic suspension until the pre-defined set point pressure is reached. FLOW devices for different pressures and/or measuring fluids controlling ranges
balances as well as external reactors, for instance high pressure consist of the main functional units:
autoclaves, calorimeters, furnaces, etc. Unique features of the
FlexiDOSE systems are: The following standard configurations of FlexiDOSE STATIC devices are available:
p Highest Accuracy in Pressure Control Flexi DOSE STATIC G Flexi DOSE FLOW G
Providing atmospheres with minimal pressure fluctuations in a For measurements in static gas atmospheres in the pressure range For measurements in flowing gas or gas mixture atmospheres in
wide pressure range. up to 150 bar (HP). the pressure ranges up to 1 bar (LP), 50 bar (MP), 150 bar (HP), or
p Accurate Vapor Dosing In the basic configuration with selection between two reaction 300 bar (HPII).
Generation of vapors from liquids and precise control of vapor gas supply lines, optionally gas switch for permanent connection
pressure, composition, and humidity. of five reaction gas supply lines. Even the pressure of vapors may
p Volumetric Dosing and Mixing be controlled by this device. The controlling range for vapors is
For exact volumetric metering of reaction atmospheres and for limited to approx. 50% of the dew point pressure at ambient
producing exactly defined gas and vapor mixtures. temperature (e. g. 30 bar for CO2 ).
The FlexiDOSE devices are available in two basic configurations with
FlexiDOSE instruments are automatically operated by software different pressure control ranges from vacuum to 700 bar: Flexi DOSE STATIC SC
control. Their standard gas connections allow easy combination For measurements in static gas and subcritical fluid atmospheres Flexi DOSE FLOW G&V LP
and i ntegration with existing autoclaves or reactors. FlexiDOSE STATIC for gas or vapor pressure control in in the pressure ranges up to 150 bar (HP), 350 bar (HPII), or 700 bar For humidifying a gas or a gas mixture at ambient pressure the
widest range (HPIII). flow dosing system is equipped with a humidifier. The gas flow
Typical applications are: Accurate pressure control is not trivial when liquefied gases are bubbles through the liquid and is saturated with vapor. Humidity
p Measuring of selective reactions (absorption and adsorption / FlexiDOSE FLOW for gas and vapor flow control, mixing, involved: CO2, NH3, propane, or butane are available as liquefied control is achieved by mixing this saturated gas flow with a
catalysis) by mixture generation, volumetric metering, and and wide range pressure control gases in cylinders only with limited pressure. Dosing fluids with second dry gas flow. Humidity is measured with an accurate
composition analysis such thermodynamic properties at pressures above their dew dew point mirror and thus, independently from the used liquid /
p Vapor generation, dosing, and pressure control for evaluating For dosing condensable atmospheres like vapors or sub-critical point leads to condensation in the tubes or icing of the valves. vapor. Condensation of vapor is avoided by a heater that heats
wetting and drying processes fluids heated versions of the FlexiDOSE systems are available. This problem is solved by heating of the entire dosing system above the gas saturator, all tubes, valves and sensors which are in
p Monitoring high pressure gas or supercritical fluid solubility / Please refer to the following pages for details about the available the critical or c ondensation temperature. Therefore FlexiDOSE contact with the vapor.
extraction by pressure control in autoclaves configurations of the FlexiDOSE systems. STATIC SC dosing systems are heated to ensure supercritical tem
p Heat of reaction measurement by gas dosing and pressure perature conditions and allow accurate high pressure control of
control for calorimeters FlexiDOSE instruments are the ideal combination for our Magnetic subcritical fluids. For reaching high pressures with these fluids a
p Membrane permeability and selectivity measurements by Suspension Balance to feed it with gases and/or vapors. Both syringe pump or compressor to supply liquefied gas above cylinder
gas mixing and trans-membrane pressure control devices together form a strong and flexible scientific measuring pressure is required.
system. Flexi DOSE FLOW G&V
For vapor dosing at high pressures of 50 bar (MP) or 150 bar (HP)
Flexi DOSE STATIC G&V the FlexiDOSE FLOW G&V is equipped with a steam generator.
For measurements in static gas or vapor atmospheres in the The gas coming from the mass flow controllers can be mixed with
pressure ranges up to 2 bar (LP) or 50 bar (MP). a flow of vapor/steam. The vapor is generated by compressing
Vapors of ambient temperature liquids (H2O, toluene, b
enzene, …) and dosing a controlled flow of liquid (H2O, naphtha, toluene, …)
are generated in three vapor pressure cells (VPC). The liquids in the by means of a HPLC pump. This liquid flow is evaporated under
VPC are heated to a controlled temperature. This generates vapor pressure in a vaporizer. Humidity control is achieved by controlling
with the boiling p
ressure at heating temperature. the ratio of liquid flow and gas flows. Condensation of vapor is
By heating up to 150°C high vapor pressures can be reached in the avoided by a heater that heats all tubes which are in contact with
GAS & VAPOR DOSING SYSTEMS PRESSURE CONTROL IN STATIC ATMOSPHERES PRESSURE CONTROL IN FLOWING ATMOSPHERES
. .
Generation of controlled reaction atmospheres can become quite FlexiDOSE STATIC devices are pressure controllers for gases, Three different versions of the FlexiDOSE STATIC devices for FlexiDOSE FLOW devices are gas and vapor flow dosing systems p two mass flow controllers (MFC, V1, V2) for dosing a gas or
complex and troublesome when high accuracy is required. subcritical and supercritical fluids and vapors. The pressure in different pressures and/or measuring fluids consist of the main with dynamic pressure controllers. A flow of pure reaction gas, mixing gases and dosing into the balance/reactor (more gas
Rubotherm FlexiDOSE instruments are sophisticated, automated the connected reactor is exactly controlled by functional units: gas mixture or gas and vapor mixture with controlled composition lines can be added optionally)
turn-key gas and vapor dosing devices for challenging applications. p allowing the reaction atmosphere to flow into the reactor p one or more pressure sensor(s) with different measuring ranges is generated. It flows continuously through the connected reactor. p up to two pressure sensors (P1, P2) with different measuring
FlexiDOSE instruments are universal gas and vapor dosing devices (pressure increase) or p dosing valves (DVx) for controlling pressure increase or decrease The pressure of the flowing atmosphere in the reactor is exactly ranges
and pressure controllers: modular design, flexible and customizable p allowing the atmosphere in the reactor to flow out p basic configuration with selection between two reaction gas controlled by means of a dynamic backpressure controller in the p up to two pressure controlling valves (DV) in the gas flow
high pressure gas and vapor dosing systems. The systems are (pressure decrease) supply lines outlet flow. The following standard configurations of FlexiDOSE coming out of the balance/reactor with different pressure
designed for operation with Rubotherm’s magnetic suspension until the pre-defined set point pressure is reached. FLOW devices for different pressures and/or measuring fluids controlling ranges
balances as well as external reactors, for instance high pressure consist of the main functional units:
autoclaves, calorimeters, furnaces, etc. Unique features of the
FlexiDOSE systems are: The following standard configurations of FlexiDOSE STATIC devices are available:
p Highest Accuracy in Pressure Control Flexi DOSE STATIC G Flexi DOSE FLOW G
Providing atmospheres with minimal pressure fluctuations in a For measurements in static gas atmospheres in the pressure range For measurements in flowing gas or gas mixture atmospheres in
wide pressure range. up to 150 bar (HP). the pressure ranges up to 1 bar (LP), 50 bar (MP), 150 bar (HP), or
p Accurate Vapor Dosing In the basic configuration with selection between two reaction 300 bar (HPII).
Generation of vapors from liquids and precise control of vapor gas supply lines, optionally gas switch for permanent connection
pressure, composition, and humidity. of five reaction gas supply lines. Even the pressure of vapors may
p Volumetric Dosing and Mixing be controlled by this device. The controlling range for vapors is
For exact volumetric metering of reaction atmospheres and for limited to approx. 50% of the dew point pressure at ambient
producing exactly defined gas and vapor mixtures. temperature (e. g. 30 bar for CO2 ).
The FlexiDOSE devices are available in two basic configurations with
FlexiDOSE instruments are automatically operated by software different pressure control ranges from vacuum to 700 bar: Flexi DOSE STATIC SC
control. Their standard gas connections allow easy combination For measurements in static gas and subcritical fluid atmospheres Flexi DOSE FLOW G&V LP
and i ntegration with existing autoclaves or reactors. FlexiDOSE STATIC for gas or vapor pressure control in in the pressure ranges up to 150 bar (HP), 350 bar (HPII), or 700 bar For humidifying a gas or a gas mixture at ambient pressure the
widest range (HPIII). flow dosing system is equipped with a humidifier. The gas flow
Typical applications are: Accurate pressure control is not trivial when liquefied gases are bubbles through the liquid and is saturated with vapor. Humidity
p Measuring of selective reactions (absorption and adsorption / FlexiDOSE FLOW for gas and vapor flow control, mixing, involved: CO2, NH3, propane, or butane are available as liquefied control is achieved by mixing this saturated gas flow with a
catalysis) by mixture generation, volumetric metering, and and wide range pressure control gases in cylinders only with limited pressure. Dosing fluids with second dry gas flow. Humidity is measured with an accurate
composition analysis such thermodynamic properties at pressures above their dew dew point mirror and thus, independently from the used liquid /
p Vapor generation, dosing, and pressure control for evaluating For dosing condensable atmospheres like vapors or sub-critical point leads to condensation in the tubes or icing of the valves. vapor. Condensation of vapor is avoided by a heater that heats
wetting and drying processes fluids heated versions of the FlexiDOSE systems are available. This problem is solved by heating of the entire dosing system above the gas saturator, all tubes, valves and sensors which are in
p Monitoring high pressure gas or supercritical fluid solubility / Please refer to the following pages for details about the available the critical or c ondensation temperature. Therefore FlexiDOSE contact with the vapor.
extraction by pressure control in autoclaves configurations of the FlexiDOSE systems. STATIC SC dosing systems are heated to ensure supercritical tem
p Heat of reaction measurement by gas dosing and pressure perature conditions and allow accurate high pressure control of
control for calorimeters FlexiDOSE instruments are the ideal combination for our Magnetic subcritical fluids. For reaching high pressures with these fluids a
p Membrane permeability and selectivity measurements by Suspension Balance to feed it with gases and/or vapors. Both syringe pump or compressor to supply liquefied gas above cylinder
gas mixing and trans-membrane pressure control devices together form a strong and flexible scientific measuring pressure is required.
system. Flexi DOSE FLOW G&V
For vapor dosing at high pressures of 50 bar (MP) or 150 bar (HP)
Flexi DOSE STATIC G&V the FlexiDOSE FLOW G&V is equipped with a steam generator.
For measurements in static gas or vapor atmospheres in the The gas coming from the mass flow controllers can be mixed with
pressure ranges up to 2 bar (LP) or 50 bar (MP). a flow of vapor/steam. The vapor is generated by compressing
Vapors of ambient temperature liquids (H2O, toluene, b
enzene, …) and dosing a controlled flow of liquid (H2O, naphtha, toluene, …)
are generated in three vapor pressure cells (VPC). The liquids in the by means of a HPLC pump. This liquid flow is evaporated under
VPC are heated to a controlled temperature. This generates vapor pressure in a vaporizer. Humidity control is achieved by controlling
with the boiling p
ressure at heating temperature. the ratio of liquid flow and gas flows. Condensation of vapor is
By heating up to 150°C high vapor pressures can be reached in the avoided by a heater that heats all tubes which are in contact with
GENERATION & MEASUREMENT IN MIXED GAS ATMOSPHERES SOFTWARE CONTROL & AUTOMATION
Technical data are subject to change without prior notice in line with continuous product improvement.
Data treatment is per-
GENERATION & MEASUREMENT IN MIXED GAS ATMOSPHERES SOFTWARE CONTROL & AUTOMATION
Technical data are subject to change without prior notice in line with continuous product improvement.
Data treatment is per-