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J. Inst. Eng. India Ser.

C
https://doi.org/10.1007/s40032-022-00895-9

CASE STUDY

Influence of Nano‑Clay and Strain Rate on the In‑Plane


Compression Response of Nano‑Clay/AA3003 Honeycomb
Sandwich Panels
P. V. Prasanth1 · M. Edwin Sahaya Raj2 · R. S. Jayaram3 · S. Senthil Murugan4 

Received: 3 June 2022 / Accepted: 4 October 2022


© The Institution of Engineers (India) 2022

Abstract  Sandwich panels (SPs) are promising materi- Introduction


als for aerospace, transportation, naval, and civil construc-
tion applications because of their excellent acoustic damp- Sandwich panels are known for their low specific gravity,
ening qualities, high specific strength, and stiffness. As excellent bending strength, and stiffness. Such panels are
far as sandwich panel failure is concerned, face and core employed in a variety of areas like aeronautical, automo-
debonding in the SPs are the worst of the lot. Hybrid com- bile, and marine transportation. The core of such panels is
posites with glass-fibre face sheets and aluminium honey- usually constructed of low-density materials (aluminium
comb sandwich structures were studied in this work for their or Nomex honeycomb, metal, or polymer foam) [1–3].
interfacial bonding and compressive strength. SPs’s in-plane Some of the factors which affect the mechanical qualities
compression properties were also studied in relation to the of sandwich panels are the top and bottom face sheets, the
strain rates. Further investigation was conducted about the centre core, adhesives used to join them together, and even
possibility and the effect of integrating nano-clay into glass- their geometrical dimensions [4]. The face sheets provide
fibre face sheets (FSs) and aluminium honeycomb cores. the panel bending strength and stiffness, and their primary
As a result, the honeycomb core fillet, resin and nano-clay role is to transmit shear forces between them. The sandwich
at the interface form a composite. To improve the in- and structure’s response and failure under varied load circum-
out-plane properties, the authors added the nano-clay to the stances are controlled by the core material [5]. The core is
FS. The in-plane failure load of sandwich panels was greatly usually made of foam or balsa wood, or it is constructed
influenced by increasing nano-clay concentration, but the using corrugated, truss, or honeycomb structures. The face
loading rate had no impact. sheet is supported in one direction by the corrugated core,
while the honeycomb core offers two-way support [6]. Alu-
Keywords  Strain rate · Honeycomb · AA3003 · minium, plastics, and composite materials like Nomex are
Composite · Sandwich panels the most often utilised honeycomb manufacturing materials
[7]. Numerous investigations on the mechanical behaviour
of sandwich panels made of various face sheets and core
* P. V. Prasanth
materials have been conducted [8, 9].Wei et al. developed
findprasanth@gmail.com three-dimensional failure mechanism maps by examining the
1
Department of Mechanical Engineering, Noorul Islam Centre
in-plane compressive characteristics of sandwich panels and
for Higher Education, Kumarakoil, Tamilnadu 629180, India optimised their load-weight efficiency [10]. Load dispersion,
2
Department of Automobile Engineering, Noorul Islam Centre
face-core adhesion, and material characteristics all have a
for Higher Education, Kumarakoil, Tamilnadu 629180, India role in the application of stresses and subsequent damage
3
Department of Mechanical Engineering, Amrita
types [11]. Honeycomb sandwich topologies, according to
College of Engineering and Technology, Erachakulam, [12], exhibit various mechanical properties depending on the
Tamilnadu 629901, India size, density, material, and thickness of the cells [13–15]. A
4
Department of Mechanical Engineering, Rajalakshmi three-point bending test was used to analyse failure mecha-
Engineering College, Chennai, Tamilnadu 602105, India nisms such as core shear and crushing and face wrinkling

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J. Inst. Eng. India Ser. C

and debonding in composite sandwich panels using natural is possible to maintain polyester resin nano-clay concentra-
and synthetic fibre reinforcements. Zhou et al. [14] con- tions as low as 0, 2, and 4% weight. When the top face sheet
sidered the skin thickness and core density of honeycomb was attached to the core using two layers of glass-woven
sandwiches to learn more about their mechanical charac- fabric, a honeycomb core, and polyester resin, the bottom
teristics and failure mechanisms under bending loads. The face sheet was generated [19]. It took 24 h for the sand-
researchers found that interfacial debonding are a common wich composites to harden once the lamination technique
source of damage starting in sandwich structures and that was completed. A glass–fibre/polyester matrix facing sheet
this decreases the stiffness and strength of the structure sig- was used to construct the sandwich specimen SP. Specimens
nificantly. “The risk of delamination between the composite (sandwich panel with nano-clay) like SPN2 and SPN4 were
face sheets and honeycomb core due to local surface contact, made by adding the nano-clay of 2 and 4 wt.%, respectively,
low energy impact, or unintentional high load has a substan- on the polyester resin in face sheet materials.
tial influence on the long-term performance of honeycomb
core sandwich systems”. Z-pinning, stitching, and embed-
ding are some of the interfacial toughening procedures that Results and Discussion
have been proposed [15, 16] to link the core to the face sheet.
There are still issues with bonding strength and interfacial Influence of Nano-clay in In-plane Compression Properties
toughness despite the advances made by the technologies of Sandwich Panels: Under in-plane compressive load, face
listed above. As a result of Z-pinning and sewing during sheets carry the majority of the load, while the core serves
the recurrent stitching process, sandwich structures may to stabilise and prevent face sheets from the buckling. Fig-
lose structural integrity [17]. The mechanical, thermal, and ure 1(a) shows the load–deflection curve from an in-plane
flame retardant characteristics of polymer composites are all compression test. All of the panels’ load–deflection curves
improved when nano-clay is added. As a result of the high are linear until they reach a failure load, at which point they
surface-to-volume ratios of nano-clays in polymers, they are begin to drop owing to failure. The nano-clay included
dispersed at a nanoscale size scale. Using both experimental panels, i.e. the SPN2 and SPN4 panels, have a higher fail-
and computational methods, Shahverdi et al. [18] investi- ure load than the SP without nano-clay. It is the addition
gated the post-clasping characterisation of actually great/ of nano-clay to the resin fillet in the sandwich panel that
flawed honeycomb centre sandwich panels with graphene gives it a higher failure load capacity than SP [12].With
platelet built-up face sheets. Graphene platelet dispersion and without nano-clay, the failure modes of sandwich panels
in the facings was expected to improve the post-clasping are different. Panels containing nano-clay failed owing to
problem. There has also been no investigation towards alu- global buckling, a phenomenon characterised by bending
minium honeycomb–glass-fibre sandwich composites with and compression damage caused by face core that did not
nano-clay grids in-plane. Sandwich panels made of alu- debond. The interfacial strength of SPN2 and SPN4 pan-
minium honeycomb and glass-fibre are constructed using els was improved by nano-clay. The SP had a load-bearing
a polyester grid containing nano-clay. It is explored how capacity of 5,172 N, whereas NSP2 and NSP4 possessed
in-plane compression and the strain rate of polyester resin capabilities of 8,764 N and 9461 N, respectively.
containing nano-clay affect sandwich laminates. Influence of Strain Rate in In-plane Compression Proper-
ties of Sandwich Panels: There were three strain rates used
in the in-plane compression test: one millimetre per minute,
Materials and Methods ten millimetres per minute, and one hundred millimetres per
minute. Compression testing of SP panels yielded the curve
A composite panel is fabricated with two layers of fibre- shown in Fig. 1(b) for in-plane load versus deflection. It is
glass-woven fabric with an areal density of 600 g/m2 and known that the compressive behaviour of SP panels is influ-
nano-clay/polyester resin face sheets. Methylene ethyl enced by the strain rate. When the strain rate is increased
ketone peroxide (MEK) was employed as a catalyst, while from 1 mm/min to 10 mm/min and 100 mm/min, in-plane
cobalt naphthenate was utilised as an accelerator. AA3003 compressive strength increases by 8.04% and 18.4% respec-
aluminium alloy of height 10 mm is used as the core mate- tively. Research on foam-filled sandwich panels also came
rial. Owing to its excellent strength, ductility, and corro- to the same conclusion [20]. High loading rates occur over
sion resistance, AA3003 is utilised. The AA3003 proper- a short period, which tends to favour the elastic properties
ties such as density, young’s modulus, Poisson’s ratio, and of materials. Elasticity is related to load-bearing capacity
yield strength are 2680 kg/m3, 69 GPa, 0.3, and 116 MPa, and is represented by attributes like strength and stiffness.
respectively. Figure 1(c) and (d) shows that strain rate has an impact on
In this investigation, Cloisite Na + nano-clay was used. the SPN2 and SPN4 panels, respectively. For SPN panels,
Using layup methods, sandwich laminates are hand-made. It a higher strain rate has a stronger favourable impact on

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J. Inst. Eng. India Ser. C

Fig.  1  a-d: a In-plane compression load–deflection curves of SP, load–deflection curves of SPN2 sandwich panels, d in-plane com-
SPN2 and SPN4 sandwich panels, b in-plane compression load– pression load–deflection curves of SPN4 sandwich panels
deflection curves of SP sandwich panels, c in-plane compression

in-plane compressive characteristics than for SP panels, as sandwich laminates. The SPN4 panel’s in-plane compres-
can be shown in Table 1. From one to ten millimetres per sive characteristics were improved by raising the nano-
second, the SPN2 board’s in-plane compressive strength clay concentration from 2 to 4 weight percentage. The
increased by 5.6% and 11.3%, respectively, after increasing impact of strain rates on the in-plane properties of SP and
the strain rate. Strength in-plane for the SPN4 panel was SPN sandwich panels was investigated, and the results
increased by 4.6% and 10.12%, respectively. revealed that the strain rate had a minor impact on the in-
plane properties. The flexural properties of SPN4 panels
increased as the strain rate was raised more than SPN2
Conclusions and SP panels. As a result, SPN panels with nano-clay are
superior to SP panels for constructing composite structural
The compressive properties of SP and SPN panels components.
were found to be greatly improved by adding nano-clay
to glass–fibre face sheets and aluminium honeycomb

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J. Inst. Eng. India Ser. C

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