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10 1061@asceem 1943-7889 0001822
10 1061@asceem 1943-7889 0001822
Abstract: The cracking behaviors of rocks significantly affect their mechanical properties. In this paper, a digital analysis approach with
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X-ray Computed Tomography (CT) imagery is developed to investigate the cracking and mechanical behaviors of rocks. The damage ratio,
integrity, and porosity of rocks subjected to triaxial compression are firstly defined based on X-ray CT image and the pixel coordinate system.
Then, the evolution process of two-dimensional (2D) and three-dimensional (3D) cracks are studied via 2D CT images and reconstructed 3D
fracture models, respectively. Finally, the stress–strain relationship of rocks is simulated by converting the reconstructed models to the finite-
element (FE) models. The results show that the rock damage ratio, integrity, and porosity are good factors to describe the cracking behaviors,
in which the evolution process of cracks is divided into five stages including: (1) the compaction of initial fissures; (2) the initiation and
propagation of microcracks; (3) microcracks coalescence, i.e., the formation and stable propagation of macrocracks; (4) the unstable propa-
gation of macrocracks; and (5) the complete failure of rock samples. The numerical stress–strain curves are in good agreement with the
experiment data. DOI: 10.1061/(ASCE)EM.1943-7889.0001822. © 2020 American Society of Civil Engineers.
Author keywords: Digital rock X-ray computed tomography (CT) image; Damage ratio; 3D reconstruction; 2D and 3D crack evolution
process; Stress–strain relations.
Fig. 2. Experiment devices: (a) mechanical loading system; (b) mechanical control system; (c) X-ray CT scanning system; and (d) Dicom image
process system. (Images by Zhi Zhao.)
Fig. 4. Sketch maps of obtaining and cropping process of X-ray CT images: (a) sandstone sample; (b) CT slice; (c) 3D region of interest; and
(d) simplified 2D model.
computing time and memory space, which are then applied to study where I f represents the digital image; N = dimension of the re-
the evolution process of 3D cracks and simulate the stress-stain re- sampling scale of image; ∯ represents the resampling function;
lationship, as shown in Fig. 4. fbr ðx; yÞ = gray level before reconstruction; and Π denotes the
quantifying and reconstructing function.
Once all the location and amplitude values of pixels in an image
Digital Analysis Approach are discrete and constrained within a certain range, the original im-
age can be converted to digital image.
Digital X-Ray CT Image Fig. 5 shows the digitalization procedure of image. The most
advantage of digital image is that different objects have different
Usually, the obtained DICOM images from the X-ray CT scanner gray intensities, and can be distinguished from each other. Mean-
cannot be directly used for the image analysis by computers. Thus, while, the objects can be separated by threshold segmentation al-
an image digitalization preprocessing step is first applied to convert gorithm and reproduced by imagesec in image toolboxes.
the DICOM image to the common digital image (bmp) for image
analysis. A digital image is composed of a pixel matrix consisted of
a series of gray intensity values with coordinates. X-ray CT images Digital Image Processing
can be converted to digital images represented by a 2D function Considering an X-ray CT image of rocks while it is digitalized, the
of gray intensity values fðx; yÞ in the pixel coordinate system using expression of the image can be written as
image digitalization procedure. Image digitalization is the pro-
cess of resampling, quantifying, and reconstructing the coordinates fð1; 1Þ fð1; 2Þ · · · fð1; NÞ
and amplitude values of pixels in a DICOM image, which is ex-
X
N −1 X
N −1 fð2; 1Þ fð2; 2Þ · · · fð2; 1Þ
pressed as
If ¼ fðx; yÞ ¼ .. .. .. .. ð2Þ
X
N −1 X
N −1 . . . .
i¼1 j¼1
If ¼ fðx; yÞ ¼ Π ∯ ½fbr ðx; yÞN×N ð1Þ
fðN; 1Þ fðN; 2Þ · · · fðN; NÞ
i¼1 j¼1
!
X
L Definition of Pore Network Variables
σ2T ðT 1 Þ ¼ arg wi ðui − uÞ ð3Þ
i¼0
Once the digital images of rock X-ray CT images are segmented by
Eqs. (3)–(6), the digital pixel sets of crack and pore space for each
image can be obtained. On the basis of the pixel coordinate system,
where σ2T = maximum of the square deviations; L = gray scale sub- the digital pixel set for crack space and pore space can be written as
sets of gray intensity values of digital image; wi and ui = probability
and average grayscale of each grayscale subset divided by the op- PC ¼ fλðx; yÞjλðx; yÞεΩg
timal crack segmentation threshold T 1 , respectively; u = total aver-
PP ¼ fλ̄ðx; yÞjλ̄ðx; yÞεΩg ð7Þ
age grayscale; and arg represents the searching function of the
maximum.
For the determination of the crack segmentation threshold, the where PC , PP , and Ω = digital pixel sets for crack space, pores
P space, and the image, respectively.
probability wi ¼ ðGS < T i Þ=M (GS is the grayscale and M is the
Thus, the whole void space set can be represented by P ¼
level of grayscale) and average grayscale ui ¼ meanðGS < T i Þ for
PP þ PC , as shown in Fig. 7(d). According to the digital image-
the divided section are first computed. Then, the crack the crack
processing principles (phase segmentation) and the definition of
segmentation threshold T 1 is determined by solving Eq. (3). Once
porosity (pore phase ratio), the damage ratio, integrity, and porosity
the crack segmentation threshold T 1 is determined, the gray inten-
based on the digital image-processing technology can be respec-
sity values of the digital pixels representing crack are marked as
tively written as (Fang et al. 2015; Zhao et al. 2020)
NaN, and the crack space PC can be represented by the set of these
digital pixels. Then, after the crack space set PC is excluded, the P P
PC ½ΓðλÞ Γ½λðx; yÞjλðx; yÞεΩ
segmentation procedure is also implemented to segment the pores DS ¼ P ð1 − ηÞ ¼ P ð1 − ηÞ ð8Þ
ΩðΓÞ Γ½ðx; yÞjx; yεΩ
and solid objects by
where P1 and P2 = digital pixel sets before and after the sandstone
specimen is damaged.
Based on the definition of the void space, the void ratio can be
expressed by
P P
½Γðλ̄ þ λÞ Γ½ðλ̄ðx; yÞ þ λðx; yÞjðλ̄ðx; yÞ þ λðx; yÞεΩ
η¼ P ¼ P
ΩðΓÞ Γ½ðx; yÞjx; yεΩ
ð12Þ
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where DS , DI , and DP = damage ratio, integrity, and the porosity, where SD~ ðx; y; zÞ = vector data set of digital voxels; and pok =
respectively; Γ = counter of digital pixel; and η = correction factor, set of digital voxels within the nonzero kernel Hp , which is modi-
which is expressed as fied as
Fig. 7. Digital image-processing results: (a) original macroimage for intact image; (b) original microimage for intact sample; (c) segmented image for
intact sample; (d) original macroimage for damaged image; (e) original micromage for damaged sample; and (f) segmented image for damaged
sample.
where Fϑ ðDÞ ~ denotes the neighbor voxel toward the direction of where PRD denotes the collected discrete data set of 3D digital
ϑ ¼ 0, 45, 90, and 135 in each XOY, XOZ, and YOZ plane. voxel.
While a digital voxel is crossed through by a ray beam (R), and Thus, based on this modified method, the reconstructed 3D mod-
projected to the vector data field, the contribution of the single sam- els with good qualities [compared with the failed sandstone samples
pling voxel D ~ to the ray at point x, y, z can be written as in Figs. 3(b, d, and f), respectively] are obtained, from which the
Z ∞ reliable and accurate 3D data can be extracted by Eq. (17).
~ x; y − D
~ y; z − D
~ z ÞFðDÞdR
~ Figs. 8(a–c) show the 3D real models of samples C2–C4.
Ssingle ðx; y; zÞ ¼ HP ðx − D ð15Þ
−∞ Figs. 8(d–f) show the 3D microstructure models with cracks and
pores. Obviously, the 3D microstructure models with crack and
~ is a constant. Thus, along
Apparently, the integral term FðDÞ pores are almost the same as the real models and the original sam-
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with the z axis direction of the ray, Eq. (13) is modified as ples shown in Fig. 3, and display the intuitive microstructures of
Z ∞ cracks and pores in sandstone. It is easy to find that the failure mode
~
Ssingle ðx; yÞ ¼ FðDÞ ~ x; y − D
HP ðx − D ~ y ; zÞdz ¼ FðDÞ
~ Ssplat of all specimens is shear failure. The failure surfaces have slight
−∞ differences with each other, the sample C2 is failed by the approxi-
ð16Þ mate half cross-shaped cracks, and samples C3–C4 are failed by the
oblique shear crack with different angles. Therefore, the evolution
where Ssplat ðx; yÞ ¼ ∫ ∞
−∞ H P ðx; y; zÞdz = weight value of a single process of 3D cracks in microscale can be investigated by analyz-
pixel contributed to the projection ray; and x, y = given location of ing the microstructures using the ReMESH method (Attene and
sampling pixel from the center of the pixel’s image plane projection Falcidieno 2006). Moreover, this microstructure models are con-
in shadow area. verted to the FE models to simulate the stress–strain relations in
Considering a digital image of X-ray CT image with a size of microscale. Fig. 9 shows the mesh model of first digital image from
N × N, once all the digital voxels are crossed through by the ray, the sample C3. The mesh segmentation threshold is set as 0.7 for
and projected on the digital image plane (Fig. 5), the projection of pore space matrix [Fig. 9(a)], and 0.1 for solid matrix [Fig. 9(b)].
this digital image can be written as The size of each triangular patch and its maximal volume are 5 μm
Fig. 8. Reconstructed failed sandstone samples C2–C4: (a) 3D reconstructed macro-models for C2; (b) 3D reconstructed macro-models for C3;
(c) 3D reconstructed macro-models for C4; (d) 3D reconstructed micro-models for C2; (e) 3D reconstructed micro-models for C3; and
(f) 3D reconstructed micro-models for C4.
Fig. 9. 3D mesh model reconstructed from X-ray CT images of intact sandstone sample C3 with a scale of 2562 × 40 pixels: (a) 3D reconstructed
micromodel for solid objects (2562 × 40); and (b) 3D reconstructed micromodel for pore space (2562 × 40).
Fig. 10. Porosity distribution curves of sandstone samples C2–C4 and the histogram of damage ratio-void ratio-porosity of typical X-ray CT slices:
(a) porosity for sample C2; (b) porosity for sample C3; (c) porosity for sample C4; and (d) damage ratio, void ratio, and porosity from typical stage for
sample C2–C4.
and 50 μm3 for pore space and 2 μm and 10 μm3 for solid objects, process of rock are in the range of 0.41‰–8.98‰, which is a rea-
respectively. sonable error range. Meanwhile, the estimated porosity distributions
of sandstone samples C2–C4 are almost the same, which agrees well
with the experimental value of 27.256 (Table 1). Therefore, it can be
Results and Discussions concluded that the proposed digital analysis method is feasible and
reliable to investigate the damage ratio, integrity, and porosity of
porous geo-materials.
Evolution Process of 2D Cracks
Except for the porosity, the distribution of integrity or damage
Digital X-ray CT image of rocks is not only applicable to show ratio is also discussed. The statistics of the integrity from samples
the different components, but also to show the microstructures. C2–C4 subjected to the confining pressure of 10, 20, and 30 MPa
Pore network variables have significant effect on the physical and indicate that the failure process of sandstone samples shares ap-
mechanical characteristics. In this subsection, pore network varia- proximately the same characteristics, and the integrity distribution
bles of damaged sandstone samples C2–C4 are calculated by curves are corresponding with the complete failure process of sand-
Eqs. (8)–(12). In addition, the evolution process of 2D cracks is stone. Meanwhile, the evolution processes of cracks in the whole
discussed based on the integrity of intact X-ray CT images and their samples and corresponding cropped ROIs are similar to each other.
corresponding ROIs. The complete failure processes of sandstone samples C2–C4 are
Fig. 10 shows the distribution curves of porosity obtained from classified into five stages based on the integrity (Fig. 11), and are
sandstone samples C2–C4 and the histogram of damage ratio-void concluded as follows:
ratio-porosity of typical X-ray CT slices in different damage stages. 1. The first stage (I) is the compaction of initial fissures (OA). The
Figs. 10(a–c) show the porosity distribution of X-ray CT slices initial fissures in sandstone samples are compressed and closed
in the range of 22.018%–31.917% with the average value of under axial stress. No apparent damage characteristics are ob-
26.548% for the sample C2, 22.018%–31.917% with the average served. The integrity of sandstone samples almost is 1.
value of 27.348% for the sample C3, and 21.957%–32.858% with 2. The second stage (II) is the initiation and propagation of mi-
the average value of 27.032% for the sample C4, respectively. crocracks (AB). With the increase of axial stress, microcracks
Fig. 10(d) shows the histogram of damage ratio-void ratio-porosity initiate and propagate. The integrity decreases gradually. The
of the typical X-ray CT slices during the failure process of sand- tendency and descent rate of integrity from RIOs of samples
stone samples C2–C4, and the corresponding data is listed in C2–C4 are nearly the same as those from the whole samples.
Table 2. The errors of the porosity before and after the failure However, compared to the whole samples, the tendency and
Fig. 11. Integrity distribution and failure process of samples C2–C4: (a) integrity and failure process of intact sample C2; (b) integrity and failure
process of intact sample C3; (c) integrity and failure process of intact sample C4; (d) integrity and failure process of ROI for sample C2; (e) integrity
and failure process of ROI for sample C3; and (f) integrity and failure process of ROI for sample C4.
descent rate of integrity from RIOs show better agreement with 4. The fourth stage (IV) is unstable propagation of macrocracks
each other. (CD). At this stage, the macroscopic cracks gradually propagate
3. The third stage (II) is microcracks coalescence, i.e., the formation in an unstable way. The tendency of the integrities for the whole
and stable propagation of macrocracks (BC). As the successive samples and RIOs are nearly the same. The integrity decreases
increase of axial stress and microcracks coalesce, macrocracks gradually and fluctuates sharply with increasing axial stress.
form and propagate in a stable way. The integrities for the whole It might be caused by unstable propagation of macrocracks.
samples of C2–C4 almost remain constant, which implies the 5. The fifth stage (V) is the failure of rocks (DE). At the final stage
stable propagation of macrocracks. However, the integrities for of the evolution process of cracks, the integrities for the whole
RIOs fluctuate slightly, which might be caused by the incom- samples and RIOs fluctuates sharply due to unstable propaga-
plete cutting of the cropped RIO. The tendency of integrities tion of macrocracks, leading to the complete failure of rocks.
from RIOs is still approximately similar to that from the whole In total, the RIOs can be applied to replace the whole samples to
samples. discuss the characteristics and evolution process of cracks.
Fig. 12. Microstructures with pores and cracks of samples C2–C4 at the typical I-V stages: (a) 3D reconstructed micromodel for pore-
fracture (2562 × 40) C2-I; (b) 3D reconstructed micromodel for pore-fracture (2562 × 40) C3-I; (c) 3D reconstructed micromodel for pore-fracture
(2562 × 40) C4-I; (d) 3D reconstructed micromodel for pore-fracture (2562 × 40) C2-II; (e) 3D reconstructed micromodel for pore-
fracture (2562 × 40) C3-II; (f) 3D reconstructed micromodel for pore-fracture (2562 × 40) C4-II; (g) 3D reconstructed micromodel for pore-
fracture (2562 × 40) C2-III; (h) 3D reconstructed micromodel for pore-fracture (2562 × 40) C3-III; (i) 3D reconstructed micromodel for pore-fracture
(2562 × 40) C4-III; (j) 3D reconstructed micromodel for pore-fracture (2562 × 40) C2-IV; (k) 3D reconstructed micromodel for pore-
fracture (2562 × 40) C3-IV; (l) 3D reconstructed micromodel for pore-fracture (2562 × 40) C4-IV; (m) 3D reconstructed micromodel for pore-fracture
(2562 × 40) C2-V; (n) 3D reconstructed micromodel for pore-fracture (2562 × 40) C3-V; and (o) 3D reconstructed micromodel for pore-fracture
(2562 × 40) C4-V.
Characterizations of 3D Cracks at Microscale Initially, the initial fissures in sandstone samples C2–C4 are
To investigate the characteristics of 3D cracks in microscale, the compressed and closed. No apparent damage characteristics are ob-
RIOs with a size of 141 × 141 pixels for sandstone samples C2–C4 served, as shown in Figs. 12(a–c).
are cropped. The corresponding microstructures with cracks and Then, primary microcracks, such as symmetrical double shell
pores are reconstructed using the proposed digital analysis ap- cracks in sample C2, oblique cracks with the small dip angle in
proach. Fig. 12 shows the microstructures with cracks and pores sample C3, and oblique cracks with the large dip angle in sample
from each stage of the failure process of sandstone samples C2–C4 C4, initiate and propagate, as shown in Figs. 12(d–f). With the in-
under the confining pressure of 10, 20, and 30 MPa. crease of the axial stress, primary microcracks coalesce to form
Fig. 13. Cloud maps of samples C2–C4 at the typical I-V stage: (a) cloud map for sample C2 in stage I; (b) cloud map for sample C3 in stage I;
(c) cloud map for sample C4 in stage I; (d) cloud map for sample C2 in stage II; (e) cloud map for sample C3 in stage II; (f) cloud map for sample C4 in
stage II; (g) cloud map for sample C2 in stage III; (h) cloud map for sample C3 in stage III; (i) cloud map for sample C4 in stage III; (j) cloud map for
sample C2 in stage IV; (k) cloud map for sample C3 in stage IV; (l) cloud map for sample C4 in stage IV; (m) cloud map for sample C2 in stage V;
(n) cloud map for sample C3 in stage V; and (o) cloud map for sample C4 in stage V.
Fig. 15. Comparison analysis of the numerical and experimental stress–strain relationships (a, c, and e) stress–strain curve for C2–C4; and
(b, d, and f) cloud map of stress for C2–C4.
to understand the microstructural characteristics and evolution Sci. Eng. 146 (Oct): 111–120. https://doi.org/10.1016/j.petrol.2016.04
process of 3D cracks as well as the mechanical properties of sand- .023.
Huang, X. C., and X. P. Zhou. 2020. “Probabilistic assessment for slope
stone samples. In addition, the numerical stress–strain curves are
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in good agreement with the experimental stress–strain curves for
06020003. https://doi.org/10.1061/(ASCE)GM.1943-5622.0001638.
the sandstone samples, which implies the accuracy of the proposed Jiang, Z., M. I. J. Van Dijke, S. Geiger, J. Ma, G. D. Couples, and X. Li.
method. 2017. “Pore network extraction for fractured porous media.” Adv. Water
In future work, the generated pore-crack microstructure mesh Resour. 107 (Sep): 280–289. https://doi.org/10.1016/j.advwatres.2017
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erties and transport properties of rock reservoirs, which are helpful Lai, J., G. Wang, Z. Wang, J. Chen, X. Pang, S. Wang, Z. Zhou, Z. He,
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contacting the corresponding author Xiao-Ping Zhou upon reason- Li, J., H. Jiang, C. Wang, Y. Zhao, Y. Gao, Y. Pei, C. Wang, and H. Dong.
able request. 2017b. “Pore-scale 518 investigation of microscopic remaining oil
variation characteristics in water-wet sandstone using ct scanning.”
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Li, Y., A. Kalantari-Dahaghi, A. Zolfaghari, P. Dong, S. Negahban, and D.
This work was supported by National Natural Science Foundation Zhou. 2018. “Fractal-based real gas flow model in shales: An interplay
of China (Grant Nos. 51839009 and 51679017). of nano-pore and nano-fracture networks.” Int. J. Heat Mass Transfer
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