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3D Digital Analysis of Cracking Behaviors of

Rocks through 3D Reconstruction Model


under Triaxial Compression
Zhi Zhao 1 and Xiao-Ping Zhou 2

Abstract: The cracking behaviors of rocks significantly affect their mechanical properties. In this paper, a digital analysis approach with
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X-ray Computed Tomography (CT) imagery is developed to investigate the cracking and mechanical behaviors of rocks. The damage ratio,
integrity, and porosity of rocks subjected to triaxial compression are firstly defined based on X-ray CT image and the pixel coordinate system.
Then, the evolution process of two-dimensional (2D) and three-dimensional (3D) cracks are studied via 2D CT images and reconstructed 3D
fracture models, respectively. Finally, the stress–strain relationship of rocks is simulated by converting the reconstructed models to the finite-
element (FE) models. The results show that the rock damage ratio, integrity, and porosity are good factors to describe the cracking behaviors,
in which the evolution process of cracks is divided into five stages including: (1) the compaction of initial fissures; (2) the initiation and
propagation of microcracks; (3) microcracks coalescence, i.e., the formation and stable propagation of macrocracks; (4) the unstable propa-
gation of macrocracks; and (5) the complete failure of rock samples. The numerical stress–strain curves are in good agreement with the
experiment data. DOI: 10.1061/(ASCE)EM.1943-7889.0001822. © 2020 American Society of Civil Engineers.
Author keywords: Digital rock X-ray computed tomography (CT) image; Damage ratio; 3D reconstruction; 2D and 3D crack evolution
process; Stress–strain relations.

Introduction sizes of pores and throats to create a topologically equivalent repre-


sentation of void space in sandstone and carbonate using X-ray
The nonnegligible fissures, cracks, and pore structures play signifi- CT images. Ebrahimi et al. (2013) proposed a genetic-based pore
cant roles in the failure mechanism of rocks (Fu 2016; Su et al. network extraction method based on microcomputed tomography
2017; Li et al. 2017a; Zhou et al. 2018b; Huang and Zhou images, and several pore scale variables are used to optimize the ex-
2020). Sandstone is the common building material, storage carriers tracted pore network. Sharqawy (2016) developed a nonlinear pro-
of coal seams, and transportation pathways of some oil-gas energy graming and optimization technique to construct the pore networks
sources. Thus, the study of cracking behaviors of sandstone is im- based on CT images of Berea and Fontainebleau sandstones, which
portant and crucial. With the improvement of image technologies, are applied to conduct fluid transport simulations including single-
various studies on the characteristics, evolution process, and damage and two-phase flow. Li et al. (2017b) analyzed six natural water-wet
mechanism of cracks emerge based on nuclear the magnetic reso- sandstone cores of different permeability and porosity visually and
nance (NMR) technique (Shao et al. 2017; Zhao et al. 2016), scan- quantitatively with the aid of CT scanning and image processing. Tao
ning electron microscope (SEM) technique (Nie et al. 2015; He et al. and Zheng (2018) investigated the real-time damage characteristics
2016), fan tomography technique (Liu et al. 2017), unmanned aerial of hydrous sandstone by combing the acoustic emission (AE) and
vehicle (UAV) and objet-base imaging technique (Rau et al. 2017), CT imaging techniques. The previous studies indicate that X-ray
laser scanning survey (Valença et al. 2017), sonar image analysis CT technique becomes a promising tool to investigate the inner mi-
(Shi et al. 2017), and X-ray Computed Tomography (CT) technique crostructures of rocks.
(Masaki et al. 2017; Mathews et al. 2017). The X-ray CT scanning In addition, the cracking behaviors significantly affect the me-
technique is widely used due to its advantages of nondestructive, chanical properties of rocks. Thus, it is necessary and crucial to
dynamic, and stable testing, and the ability to reconstruct the mi- investigate the cracking behaviors of rocks. Wang et al. (2003) de-
crostructure of sandstone. Øren and Bakke (2003) presented an fined the crack interval and damage surface area based on the X-ray
integrated method to evaluate the permeability, conductivity, and CT slices and its 3D reconstructed model. Dyskin et al. (2003)
capillary pressure of Berea sandstone based on the three-dimensional discussed the effect of shape and location of 3D cracks on their
(3D) reconstruction model obtained from two-dimensional (2D) growth. Elaqra et al. (2007) studied the damage mechanism and
X-ray CT images. Al-Kharusi and Blunt (2007) proposed a novel crack failure process through the X-ray tomography. Nasseri et al.
methodology to extract networks, which computes the location and (2011) measured the morphology of cracks and analyzed the frac-
ture damage zone in anisotropic granitic rocks using 3D X-ray CT
1
Ph.D. Candidate, School of Civil Engineering, Chongqing Univ., scanning techniques. Shiozawa et al. (2014) quantitatively evaluated
Chongqing 400045, China. Email: zzhao@cqu.edu.cn the shape of torsion fatigue cracks and investigated the transition of
2
Professor, School of Civil Engineering, Chongqing Univ., Chongqing
crack propagation from the shear mode to the tensile mode from
400045, China (corresponding author). Email: cqxpzhou@hotmail.com
Note. This manuscript was submitted on October 11, 2019; approved on
the 3D perspective using X-ray imaging. Yang et al. (2015) explored
March 26, 2020; published online on June 11, 2020. Discussion period the mechanical behavior and internal damage mechanism of sand-
open until November 11, 2020; separate discussions must be submitted stone using X-ray CT technique and triaxial compression test. Zhou
for individual papers. This paper is part of the Journal of Engineering et al. (2018a) investigated the evolution of fracture networks in coal
Mechanics, © ASCE, ISSN 0733-9399. during loading using X-ray CT with a uniaxial compression facility.

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J. Eng. Mech., 2020, 146(8): 04020084


However, these previous works almost focused on the failure pro- Material and Methodology
cess of planar cracks, or only referring to the 3D surface cracks. A
few studies have reported the microstructural characteristics of rock Sample Collection and Description
materials with crack and pore microstructures at microscale. Mean-
while, the spatial characteristics of 3D spatial cracks are not well The experiment materials used in this work are all taken from fine
understood. In other words, the previous works mainly involved in sandstone stratum in Xujiahe group located in Mazongxiang mine
the single pore network or single fracture network, and few studies region of Chongqing, China, as shown in Fig. 1. It is an upper
have previously investigated the connected pore-fracture networks Triassic sandstone stratum composed of Xishan, Luoguanshan,
at microscale in rock reservoirs (Jiang et al. 2017; Lai et al. 2018; Li and Xindianzi anticlines with a dip angle of 17°. In this work, three
et al. 2018). In addition, the structural characterization of fracture samples with the dimension of Φ50 × 100 mm are polished and
networks and their evolutionary behaviors are changed under differ- prepared, as suggested by International Society of Rock Mechanics
(Hatheway 2009). According to the result of X-ray diffraction
ent states (Li et al. 2017c; Zhou et al. 2018a; Brewick et al. 2019).
(XRD), the main minerals are quartz (65.58%), feldspar (17.65%),
In this paper, a digital analysis approach is developed based on
calcite (10.84%), and a small quantity of chlorite (4.32%) and
X-ray CT imaging and 3D reconstruction technology. On the basis
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kaolinite (2.7%), respectively. The physical parameters (e.g., poros-


of this approach, the characteristics and the evolution process of 2D
ity and air average permeability) are measured by an AP608 auto-
and 3D cracks with microstructures are discussed. The 3D micro-
mated Permeameter-Porosimeter (CORETEST, Dallas, Texas), and
structure model of region of interest (ROI) is converted to the FE
the average results are shown in Table 1.
model to simulate the stress–strain relationship under confining
pressure of 10, 20, and 30 MPa.
Experiment Devices and Testing
In this work, a multifunction triaxial rock testing system (Rock
600-50 HT PLUS, GCTS Company, Tempe, Arizona) with a
SIEMENS-SOMATOM scope X-ray CT scanner (Shanghai Sie-
mens Medical Equipment, Shanghai, China) are employed to con-
duct the triaxial compression and X-ray CT scanning test. Figs. 2(a
and b) show the mechanical loading system and mechanical control
system of the Rock 600-50 HT PLUS. The axial loading velocity
is 0.01–10 kN=s, with a confining pressure loading velocity of
0.001–20 MPa=s. Figs. 2(c–d) show the composition architecture
of the X-ray CT scanner with a scanning time of 1,500 ms for a
single slice. The X-ray CT tests are divided into two levels.
One is the X-ray CT test at millimeter scale with a spatial resolution
of 0.35 × 0.35 mm and slice interval thickness of 0.75 mm. The
other is the X-ray CT test at micrometer scale with a spatial reso-
lution of 2 μm. The quality of image is influenced by the scanning
voltage and electricity, which are set as 130 kV and 81 μA in this
Fig. 1. Rock stratum distribution of Xujiahe group (xj) in the work, respectively.
Mazongxiang mine region of Chongqing. The triaxial compression tests on sandstone samples C2–C4
under the confining stress of 10, 20, and 30 MPa are conducted to
obtain the complete stress-stain curves, respectively. Fig. 3 shows
sandstone samples C2–C4 before and after the triaxial compres-
sion test. In the X-ray CT test, sandstone samples C2–C4 are firstly
Table 1. Average physical parameters of sandstone scanned before the triaxial compression test. Finally, the damaged
Scale (mm) γ (kN=m3 ) ϕ (%) KðmDÞ SSA (m2 =g) sandstone samples subjected to triaxial compression are scanned.
In this work, 158, 158, 158 slices, and 158, 158, 156 slices for intact
Φ50 × 100 26.27 27.256 0.05 0.421
and damaged samples C2–C4 are obtained, respectively. The size of
Note: γ = unit weight; ϕ = porosity; K = average permeability; and each X-ray CT image is 512 × 512 pixels, and the ROI with a size of
SSA = specific surface area. 141 × 141 pixels is cropped from the original image to save

Fig. 2. Experiment devices: (a) mechanical loading system; (b) mechanical control system; (c) X-ray CT scanning system; and (d) Dicom image
process system. (Images by Zhi Zhao.)

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Fig. 3. Intact and damaged sandstone samples C2–C4.

Fig. 4. Sketch maps of obtaining and cropping process of X-ray CT images: (a) sandstone sample; (b) CT slice; (c) 3D region of interest; and
(d) simplified 2D model.

computing time and memory space, which are then applied to study where I f represents the digital image; N = dimension of the re-
the evolution process of 3D cracks and simulate the stress-stain re- sampling scale of image; ∯ represents the resampling function;
lationship, as shown in Fig. 4. fbr ðx; yÞ = gray level before reconstruction; and Π denotes the
quantifying and reconstructing function.
Once all the location and amplitude values of pixels in an image
Digital Analysis Approach are discrete and constrained within a certain range, the original im-
age can be converted to digital image.
Digital X-Ray CT Image Fig. 5 shows the digitalization procedure of image. The most
advantage of digital image is that different objects have different
Usually, the obtained DICOM images from the X-ray CT scanner gray intensities, and can be distinguished from each other. Mean-
cannot be directly used for the image analysis by computers. Thus, while, the objects can be separated by threshold segmentation al-
an image digitalization preprocessing step is first applied to convert gorithm and reproduced by imagesec in image toolboxes.
the DICOM image to the common digital image (bmp) for image
analysis. A digital image is composed of a pixel matrix consisted of
a series of gray intensity values with coordinates. X-ray CT images Digital Image Processing
can be converted to digital images represented by a 2D function Considering an X-ray CT image of rocks while it is digitalized, the
of gray intensity values fðx; yÞ in the pixel coordinate system using expression of the image can be written as
image digitalization procedure. Image digitalization is the pro-
 
cess of resampling, quantifying, and reconstructing the coordinates  fð1; 1Þ fð1; 2Þ · · · fð1; NÞ 
 
and amplitude values of pixels in a DICOM image, which is ex-  
X
N −1 X
N −1  fð2; 1Þ fð2; 2Þ · · · fð2; 1Þ 
pressed as  
  If ¼ fðx; yÞ ¼ .. .. .. ..  ð2Þ
X
N −1 X
N −1  . . . . 
i¼1 j¼1  
If ¼ fðx; yÞ ¼ Π ∯ ½fbr ðx; yÞN×N ð1Þ  
 fðN; 1Þ fðN; 2Þ · · · fðN; NÞ 
i¼1 j¼1

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!
XC Þ
L−χðP
σ2T ðT 2 Þ ¼ arg wi ðui − uÞ ð4Þ
i¼0

where χðPC Þ denotes gray scale subsets of gray intensity values of


crack space.
As the pore space segmentation threshold T 2 is determined, the
gray intensity values of the digital pixels representing pores and
solid objects are, respectively, marked as 0 and 1, and the pore space
PP can be represented by the set of these digital pixels. Finally, the
crack, pores and solids objects can be segmented by the crack seg-
mentation threshold and pore segmentation threshold, which can be
expressed by
8
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> f ðx; yÞ ¼ NaN; fε½0; T 1  for cracks


Fig. 5. Digitalization procedure of image. < b
fb ðx; yÞ ¼ fb ðx; yÞ ¼ 0; fε½T 1 ; T 2  for pores ð5Þ
>
:
fb ðx; yÞ ¼ 1; fε½T 2 ; 255 for solids

where ½x; y = coordinate sets; and fðx; yÞ = gray intensity at loca-


where f b ðx; yÞ = binary value of digital pixel in X-ray CT image.
tion ðx; yÞ. Thus, each pixel has different discrete gray intensities,
Actually, to present the digital image intuitively and conven-
and represents different components of objects.
iently, the value of digital pixel in crack space is also considered
Sandstone is a kind of multiphase porous geo-material. In this
to be 0. Thus, the digital image can be expressed as
paper, the intact sandstone consists of solid objects phase and void
space phase containing crack and pore space. Because the original 8
> f ðx; yÞ ¼ NaN ¼ 0; fεPC
X-ray CT images (in DICOM format) of sandstone samples are X
N−1 X
N−1 < b
converted to the digital images, the digital image is considered If ¼ fðx; yÞ ¼ fb ðx; yÞ ¼ 0; fεPP
>
:
to be the dataset of gray intensity of each pixel in the digital image. i¼1 j¼1
fb ðx; yÞ ¼ 1; fεΩ − PC − PP
As a result, the solid objects and void space of the sandstone sample
are represented by different subsets of gray intensity values. Thus, ð6Þ
the solid objects and void space can be segmented by a given
threshold value. However, the segmentation of crack and pore space where Ω denotes the digital pixels of X-ray CT image.
is challengeable for Ostu’s image segmentation method (Otsu Thus, with the aid of other image-processing functions such
1979), because both cracks and pores are the structural components as the image denoising and image enhancement function, the final
of void space with adjacent but different ranges of gray intensities. image can be reproduced by imagesec in image toolboxes. Fig. 6
Therefore, to obtain the microstructure of pore-fracture networks, shows the whole flowchart of the digital image-processing pro-
a modified Ostu’s image segmentation method is proposed to seg- cedure. Figs. 7(a and d) show the original digital macroimages ob-
ment the crack, pore, and solid objects by calculating segmentation tained from the intact and damaged samples. Figs. 7(b and e) show
threshold value for cracks and pores. The modified segmentation the original digital microimages obtained from the intact and dam-
procedure is firstly conducted to separate the crack from pores and aged samples. Figs. 7(c and f) show the corresponding segmented
solid objects by pore space and crack-pore space image obtained by Eqs. (3)–(6).

!
X
L Definition of Pore Network Variables
σ2T ðT 1 Þ ¼ arg wi ðui − uÞ ð3Þ
i¼0
Once the digital images of rock X-ray CT images are segmented by
Eqs. (3)–(6), the digital pixel sets of crack and pore space for each
image can be obtained. On the basis of the pixel coordinate system,
where σ2T = maximum of the square deviations; L = gray scale sub- the digital pixel set for crack space and pore space can be written as
sets of gray intensity values of digital image; wi and ui = probability
and average grayscale of each grayscale subset divided by the op- PC ¼ fλðx; yÞjλðx; yÞεΩg
timal crack segmentation threshold T 1 , respectively; u = total aver-
PP ¼ fλ̄ðx; yÞjλ̄ðx; yÞεΩg ð7Þ
age grayscale; and arg represents the searching function of the
maximum.
For the determination of the crack segmentation threshold, the where PC , PP , and Ω = digital pixel sets for crack space, pores
P space, and the image, respectively.
probability wi ¼ ðGS < T i Þ=M (GS is the grayscale and M is the
Thus, the whole void space set can be represented by P ¼
level of grayscale) and average grayscale ui ¼ meanðGS < T i Þ for
PP þ PC , as shown in Fig. 7(d). According to the digital image-
the divided section are first computed. Then, the crack the crack
processing principles (phase segmentation) and the definition of
segmentation threshold T 1 is determined by solving Eq. (3). Once
porosity (pore phase ratio), the damage ratio, integrity, and porosity
the crack segmentation threshold T 1 is determined, the gray inten-
based on the digital image-processing technology can be respec-
sity values of the digital pixels representing crack are marked as
tively written as (Fang et al. 2015; Zhao et al. 2020)
NaN, and the crack space PC can be represented by the set of these
digital pixels. Then, after the crack space set PC is excluded, the P P
PC ½ΓðλÞ Γ½λðx; yÞjλðx; yÞεΩ
segmentation procedure is also implemented to segment the pores DS ¼ P ð1 − ηÞ ¼ P ð1 − ηÞ ð8Þ
ΩðΓÞ Γ½ðx; yÞjx; yεΩ
and solid objects by

© ASCE 04020084-4 J. Eng. Mech.

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P P
P1 − P 2 j P1 ½nðλ̄ þ λÞ − P2 ½nðλ̄ þ λÞj
η¼ ¼ P ð11Þ
P1 P1 ½nðλ̄ þ λÞ

where P1 and P2 = digital pixel sets before and after the sandstone
specimen is damaged.
Based on the definition of the void space, the void ratio can be
expressed by
P P
½Γðλ̄ þ λÞ Γ½ðλ̄ðx; yÞ þ λðx; yÞjðλ̄ðx; yÞ þ λðx; yÞεΩ
η¼ P ¼ P
ΩðΓÞ Γ½ðx; yÞjx; yεΩ
ð12Þ
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where DV = void ratio of sandstone. Based on these pore network


variances, the characteristics of 2D crack can be described in detail.

Digital 3D Reconstruction Approach


3D reconstruction technology is a fine tool to represent the micro-
structure of material intuitively. Usually, 3D reconstruction meth-
ods can be simply classified into surface reconstruction methods
and volume reconstruction methods. Surface reconstruction meth-
ods have a small amount of computation and high reconstruction
speed, although they lose some spatial information for microstruc-
tures. A reliable reconstruction model can be obtained by volume
reconstruction methods with complete detail information. However,
it is limited to higher hardware demands and slower reconstruction
speed. The splatting reconstruction method (Westover 1990), be-
longing to volume reconstruction methods, has the advantages of
Fig. 6. Flowchart of digital image processing. high reconstruction speed, fast searching for pixel information,
lower memory requirements, and progressive display of a 3D recon-
struction model, which is modified to reconstruct the 3D models
based on the digital X-ray CT images of sandstone.
P Considering a sandstone specimen, its volumetric data consists
P ½ΓðλÞ
DI ¼ 1 −PC ð1 − ηÞ ~ and D
of a discrete 3D dataset of digital voxels: FðDÞ, ~ i, D
~ j , and D
~k
ΩðΓÞ
P ~
are the coordinate components of digital voxel D in the x, y, z di-
Γ½λðx; yÞjλðx; yÞεΩ
¼1− P ð1 − ηÞ ð9Þ rection, respectively. As the reconstruction procedure is imple-
Γ½ðx; yÞjx; yεΩ
mented, the discrete data set of digital voxels are converted to the
vector dataset, which can be expressed by
P P X
PP ½Γðλ̄Þ Γ½λ̄ðx; yÞjλ̄ðx; yÞεΩ SD~ ðx; y; zÞ ¼ ~ i; y − D
HP ðx − D ~ j; z − D
~ k ÞFðDÞ
~ ð13Þ
DP ¼ P ¼ P ð10Þ
ΩðΓÞ Γ½ðx; yÞjx; yεΩ ~
Dϵpok

where DS , DI , and DP = damage ratio, integrity, and the porosity, where SD~ ðx; y; zÞ = vector data set of digital voxels; and pok =
respectively; Γ = counter of digital pixel; and η = correction factor, set of digital voxels within the nonzero kernel Hp , which is modi-
which is expressed as fied as

Fig. 7. Digital image-processing results: (a) original macroimage for intact image; (b) original microimage for intact sample; (c) segmented image for
intact sample; (d) original macroimage for damaged image; (e) original micromage for damaged sample; and (f) segmented image for damaged
sample.

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qffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi Z
X ~ −1 =2 × Fϑ ðDÞ ~ −1 =2 X
N2 ∞
F1 ðDÞ PRD ¼ ~ nÞ
FðD ~ nx ; y − D
HP ðx − D ~ nz ; z − D
~ nz ÞdR ð17Þ
~ Fϑ ðDÞ
HP ½F1 ðDÞ; ~ ¼ ð14Þ
~ 1=4 ~ 1=4 −∞
ϑ F1 ðDÞ × Fϑ ðDÞ n¼1

where Fϑ ðDÞ ~ denotes the neighbor voxel toward the direction of where PRD denotes the collected discrete data set of 3D digital
ϑ ¼ 0, 45, 90, and 135 in each XOY, XOZ, and YOZ plane. voxel.
While a digital voxel is crossed through by a ray beam (R), and Thus, based on this modified method, the reconstructed 3D mod-
projected to the vector data field, the contribution of the single sam- els with good qualities [compared with the failed sandstone samples
pling voxel D ~ to the ray at point x, y, z can be written as in Figs. 3(b, d, and f), respectively] are obtained, from which the
Z ∞ reliable and accurate 3D data can be extracted by Eq. (17).
~ x; y − D
~ y; z − D
~ z ÞFðDÞdR
~ Figs. 8(a–c) show the 3D real models of samples C2–C4.
Ssingle ðx; y; zÞ ¼ HP ðx − D ð15Þ
−∞ Figs. 8(d–f) show the 3D microstructure models with cracks and
pores. Obviously, the 3D microstructure models with crack and
~ is a constant. Thus, along
Apparently, the integral term FðDÞ pores are almost the same as the real models and the original sam-
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with the z axis direction of the ray, Eq. (13) is modified as ples shown in Fig. 3, and display the intuitive microstructures of
Z ∞ cracks and pores in sandstone. It is easy to find that the failure mode
~
Ssingle ðx; yÞ ¼ FðDÞ ~ x; y − D
HP ðx − D ~ y ; zÞdz ¼ FðDÞ
~  Ssplat of all specimens is shear failure. The failure surfaces have slight
−∞ differences with each other, the sample C2 is failed by the approxi-
ð16Þ mate half cross-shaped cracks, and samples C3–C4 are failed by the
oblique shear crack with different angles. Therefore, the evolution
where Ssplat ðx; yÞ ¼ ∫ ∞
−∞ H P ðx; y; zÞdz = weight value of a single process of 3D cracks in microscale can be investigated by analyz-
pixel contributed to the projection ray; and x, y = given location of ing the microstructures using the ReMESH method (Attene and
sampling pixel from the center of the pixel’s image plane projection Falcidieno 2006). Moreover, this microstructure models are con-
in shadow area. verted to the FE models to simulate the stress–strain relations in
Considering a digital image of X-ray CT image with a size of microscale. Fig. 9 shows the mesh model of first digital image from
N × N, once all the digital voxels are crossed through by the ray, the sample C3. The mesh segmentation threshold is set as 0.7 for
and projected on the digital image plane (Fig. 5), the projection of pore space matrix [Fig. 9(a)], and 0.1 for solid matrix [Fig. 9(b)].
this digital image can be written as The size of each triangular patch and its maximal volume are 5 μm

Fig. 8. Reconstructed failed sandstone samples C2–C4: (a) 3D reconstructed macro-models for C2; (b) 3D reconstructed macro-models for C3;
(c) 3D reconstructed macro-models for C4; (d) 3D reconstructed micro-models for C2; (e) 3D reconstructed micro-models for C3; and
(f) 3D reconstructed micro-models for C4.

Fig. 9. 3D mesh model reconstructed from X-ray CT images of intact sandstone sample C3 with a scale of 2562 × 40 pixels: (a) 3D reconstructed
micromodel for solid objects (2562 × 40); and (b) 3D reconstructed micromodel for pore space (2562 × 40).

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Fig. 10. Porosity distribution curves of sandstone samples C2–C4 and the histogram of damage ratio-void ratio-porosity of typical X-ray CT slices:
(a) porosity for sample C2; (b) porosity for sample C3; (c) porosity for sample C4; and (d) damage ratio, void ratio, and porosity from typical stage for
sample C2–C4.

and 50 μm3 for pore space and 2 μm and 10 μm3 for solid objects, process of rock are in the range of 0.41‰–8.98‰, which is a rea-
respectively. sonable error range. Meanwhile, the estimated porosity distributions
of sandstone samples C2–C4 are almost the same, which agrees well
with the experimental value of 27.256 (Table 1). Therefore, it can be
Results and Discussions concluded that the proposed digital analysis method is feasible and
reliable to investigate the damage ratio, integrity, and porosity of
porous geo-materials.
Evolution Process of 2D Cracks
Except for the porosity, the distribution of integrity or damage
Digital X-ray CT image of rocks is not only applicable to show ratio is also discussed. The statistics of the integrity from samples
the different components, but also to show the microstructures. C2–C4 subjected to the confining pressure of 10, 20, and 30 MPa
Pore network variables have significant effect on the physical and indicate that the failure process of sandstone samples shares ap-
mechanical characteristics. In this subsection, pore network varia- proximately the same characteristics, and the integrity distribution
bles of damaged sandstone samples C2–C4 are calculated by curves are corresponding with the complete failure process of sand-
Eqs. (8)–(12). In addition, the evolution process of 2D cracks is stone. Meanwhile, the evolution processes of cracks in the whole
discussed based on the integrity of intact X-ray CT images and their samples and corresponding cropped ROIs are similar to each other.
corresponding ROIs. The complete failure processes of sandstone samples C2–C4 are
Fig. 10 shows the distribution curves of porosity obtained from classified into five stages based on the integrity (Fig. 11), and are
sandstone samples C2–C4 and the histogram of damage ratio-void concluded as follows:
ratio-porosity of typical X-ray CT slices in different damage stages. 1. The first stage (I) is the compaction of initial fissures (OA). The
Figs. 10(a–c) show the porosity distribution of X-ray CT slices initial fissures in sandstone samples are compressed and closed
in the range of 22.018%–31.917% with the average value of under axial stress. No apparent damage characteristics are ob-
26.548% for the sample C2, 22.018%–31.917% with the average served. The integrity of sandstone samples almost is 1.
value of 27.348% for the sample C3, and 21.957%–32.858% with 2. The second stage (II) is the initiation and propagation of mi-
the average value of 27.032% for the sample C4, respectively. crocracks (AB). With the increase of axial stress, microcracks
Fig. 10(d) shows the histogram of damage ratio-void ratio-porosity initiate and propagate. The integrity decreases gradually. The
of the typical X-ray CT slices during the failure process of sand- tendency and descent rate of integrity from RIOs of samples
stone samples C2–C4, and the corresponding data is listed in C2–C4 are nearly the same as those from the whole samples.
Table 2. The errors of the porosity before and after the failure However, compared to the whole samples, the tendency and

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Table 2. Quantitative parameters for typical X-ray CT images of sandstone samples C2–C4
Categories Phase Sequence number Damage ratio (%) Void ratio (%) Porosity (%) Error (‰) Triangle patch Joint number
C2 I 23 0 23.696 23.648 2.03 80,986 55,057
II 84 6.78 32.040 25.342 3.25 80,806 54,466
III 106 8.21 35.847 27.681 1.59 80,840 88,456
IV 121 4.86 31.432 26.650 2.93 80,972 55,019
V 132 3.13 35.020 31.903 0.41 80,926 56,821
C3 I 23 0 29.694 29.635 1.99 80,234 55,312
II 74 4.80 34.052 29.289 1.25 80,232 54,670
III 90 5.59 36.438 30.903 1.78 80,142 54,506
IV 106 5.73 29.114 23.443 2.52 80,296 54,466
V 122 7.70 34.671 27.050 2.91 80,246 54,977
C4 I 25 0 29.014 28.963 1.76 80,164 55,330
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II 76 8.58 27.679 21.957 5.83 80,376 55,005


III 86 6.71 28.931 22.322 4.54 80,240 53,839
IV 105 6.39 35.127 28.821 8.98 80,130 53,902
V 120 3.04 33.469 30.498 2.26 80,222 54,926

Fig. 11. Integrity distribution and failure process of samples C2–C4: (a) integrity and failure process of intact sample C2; (b) integrity and failure
process of intact sample C3; (c) integrity and failure process of intact sample C4; (d) integrity and failure process of ROI for sample C2; (e) integrity
and failure process of ROI for sample C3; and (f) integrity and failure process of ROI for sample C4.

descent rate of integrity from RIOs show better agreement with 4. The fourth stage (IV) is unstable propagation of macrocracks
each other. (CD). At this stage, the macroscopic cracks gradually propagate
3. The third stage (II) is microcracks coalescence, i.e., the formation in an unstable way. The tendency of the integrities for the whole
and stable propagation of macrocracks (BC). As the successive samples and RIOs are nearly the same. The integrity decreases
increase of axial stress and microcracks coalesce, macrocracks gradually and fluctuates sharply with increasing axial stress.
form and propagate in a stable way. The integrities for the whole It might be caused by unstable propagation of macrocracks.
samples of C2–C4 almost remain constant, which implies the 5. The fifth stage (V) is the failure of rocks (DE). At the final stage
stable propagation of macrocracks. However, the integrities for of the evolution process of cracks, the integrities for the whole
RIOs fluctuate slightly, which might be caused by the incom- samples and RIOs fluctuates sharply due to unstable propaga-
plete cutting of the cropped RIO. The tendency of integrities tion of macrocracks, leading to the complete failure of rocks.
from RIOs is still approximately similar to that from the whole In total, the RIOs can be applied to replace the whole samples to
samples. discuss the characteristics and evolution process of cracks.

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Fig. 12. Microstructures with pores and cracks of samples C2–C4 at the typical I-V stages: (a) 3D reconstructed micromodel for pore-
fracture (2562 × 40) C2-I; (b) 3D reconstructed micromodel for pore-fracture (2562 × 40) C3-I; (c) 3D reconstructed micromodel for pore-fracture
(2562 × 40) C4-I; (d) 3D reconstructed micromodel for pore-fracture (2562 × 40) C2-II; (e) 3D reconstructed micromodel for pore-
fracture (2562 × 40) C3-II; (f) 3D reconstructed micromodel for pore-fracture (2562 × 40) C4-II; (g) 3D reconstructed micromodel for pore-
fracture (2562 × 40) C2-III; (h) 3D reconstructed micromodel for pore-fracture (2562 × 40) C3-III; (i) 3D reconstructed micromodel for pore-fracture
(2562 × 40) C4-III; (j) 3D reconstructed micromodel for pore-fracture (2562 × 40) C2-IV; (k) 3D reconstructed micromodel for pore-
fracture (2562 × 40) C3-IV; (l) 3D reconstructed micromodel for pore-fracture (2562 × 40) C4-IV; (m) 3D reconstructed micromodel for pore-fracture
(2562 × 40) C2-V; (n) 3D reconstructed micromodel for pore-fracture (2562 × 40) C3-V; and (o) 3D reconstructed micromodel for pore-fracture
(2562 × 40) C4-V.

Characterizations of 3D Cracks at Microscale Initially, the initial fissures in sandstone samples C2–C4 are
To investigate the characteristics of 3D cracks in microscale, the compressed and closed. No apparent damage characteristics are ob-
RIOs with a size of 141 × 141 pixels for sandstone samples C2–C4 served, as shown in Figs. 12(a–c).
are cropped. The corresponding microstructures with cracks and Then, primary microcracks, such as symmetrical double shell
pores are reconstructed using the proposed digital analysis ap- cracks in sample C2, oblique cracks with the small dip angle in
proach. Fig. 12 shows the microstructures with cracks and pores sample C3, and oblique cracks with the large dip angle in sample
from each stage of the failure process of sandstone samples C2–C4 C4, initiate and propagate, as shown in Figs. 12(d–f). With the in-
under the confining pressure of 10, 20, and 30 MPa. crease of the axial stress, primary microcracks coalesce to form

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Fig. 13. Cloud maps of samples C2–C4 at the typical I-V stage: (a) cloud map for sample C2 in stage I; (b) cloud map for sample C3 in stage I;
(c) cloud map for sample C4 in stage I; (d) cloud map for sample C2 in stage II; (e) cloud map for sample C3 in stage II; (f) cloud map for sample C4 in
stage II; (g) cloud map for sample C2 in stage III; (h) cloud map for sample C3 in stage III; (i) cloud map for sample C4 in stage III; (j) cloud map for
sample C2 in stage IV; (k) cloud map for sample C3 in stage IV; (l) cloud map for sample C4 in stage IV; (m) cloud map for sample C2 in stage V;
(n) cloud map for sample C3 in stage V; and (o) cloud map for sample C4 in stage V.

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macrocracks, and macrocracks propagate in a stable way as in sand- Table 3. Mechanical parameters for the stress-stain simulation
stone samples C2–C4, as shown in Figs. 12(g–i). Density Young’s modulus
As the axial stress continues to increase, macrocracks propa- Categories (g=cm3 ) (GPa) Poisson ratio
gate gradually in an unstable way. Meanwhile, secondary cracks are
C2 2.376 17.663 0.174
initiated from tips of macrocracks in sandstone samples C2–C4, C3 2.375 19.543 0.183
as shown in Figs. 12(j–l). Finally, macrocracks propagate to boun- C4 2.451 20.719 0.179
dary of samples, leading to the failure of the samples, as shown in
Figs. 12(m–o).

Point Cloud Characterization of 3D Cracks


To show the propagation process of secondary cracks intuitively,
the failure process of sandstone samples C2–C4 is reproduced
by the extracted 3D data obtained from Eq. (17). To discuss the
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characteristics and evolution process of 3D cracks, the typical point


cloud maps are extracted at each stage.
Fig. 13 shows point cloud maps of sandstone samples C2–C4
subjected to confining pressures of 10, 20, and 30 MPa at each
stage. Based on these point cloud maps, the characteristics and evo-
lution process of 3D cracks are illustrated, and the propagation pro-
cess of secondary cracks in each sample is shown intuitively and Fig. 14. Representation of (a) 3D real microstructure model; and
well interpreted. (b) 3D mechanical reference mesh model.
At first, the initial fissures and pores are gradually compressed
and closed, and point cloud maps are uniform, which implies no
damage in samples, as shown in Figs. 13(a–c). Then, primary mi-
crocracks, such as the symmetrical double shell cracks in sample
C2, the oblique cracks with the small dip angle in sample C3, and follows: (1) the displacement and confining pressure are loaded on
the oblique cracks with the large dip angle in the C4, are initiated the rigid plate; (2) the bottom rigid plate is fixed, and remains stable
from the edge of samples and propagate along the direction of axial without displacement and rotations along all directions; and (3) the
stress. Point cloud maps in primary microcrack zone are nonuni- top rigid plate is fixed in the X-Y plane with free Z-axis, and it is
form, as shown in Figs. 13(d–f). loaded in displacement control way along the Z-axis direction.
With the increase of axial stress, primary microcracks coalesce Fig. 14 shows the 3D real microstructure model and its corre-
to form macrocracks, and macrocracks propagate in a stable way in sponding reference FE model to sumulate the stess-stain curves.
sandstone samples C2–C4. Point cloud maps in macrocrack zones Fig. 15 shows the numerical results of the stress–strain curves
are nonuniform, as shown in Figs. 13(g–i). under confining pressures of 10, 20, and 30 MPa. The numer-
With the successive increase of the axial stress, macrocracks ical stress–strain curves are compared with the experimental
propagate toward the boundary of samples in an unstable way. stress–strain curves. Obviously, the correlation coefficients be-
Meanwhile, secondary cracks initiate and propagate. At this stage, tween the experimental and numerical results in sandstone samples
there are obvious different characteristics of the 3D cracks in these C2–C4 are respectively 0.98864, 0.94238, and 0.97570, as shown
samples. In sandstone sample C2, the secondary cracks propagate in Table 4. This implies that the numerical stress-stain curves
and coalesce with the symmetrical double shell cracks. In sandstone of sandstone samples C2–C4 are in good agreement with the
sample C3, the secondary cracks with a small inclination angle experimental stress-stain curves of sandstone samples C2–C4.
initiate from the upper edge of macrocracks, and propagate along However, the experimental peak strength (144.295, 170.548, and
the direction of macrocracks. In sandstone sample C4, two secon- 198.315 MPa) is slightly smaller than the numerical peak strength
dary cracks initiates from the upper and lower edge of macrocracks, in sandstone samples C2–C4 (144.89, 170.568, and 199.409 MPa).
and propagate toward the boundary of the sample, as shown in Therefore, this is remarkable evidence for the reliability and accu-
Figs. 13(j–l). racy of the proposed digital 461 analysis approach.
Finally, macrocracks propagate to boundary of samples, leading
to the complete failure of the samples, and point cloud maps in the
failure zones are incomplete, as shown in Figs. 13(m–o). Summaries and Conclusions
In this work, X-ray CT scanning tests and digital analysis tech-
Stress–Strain Curves niques combined with the 3D reconstruction method are applied
At the ROI measurement scale, the 3D microstructures of sandstone to study the cracking behaviors and mechanical properties during
are employed to simulate stress–strain curves using ABAQUS with the failure process of sandstone sample subjected to triaxial com-
the Mohr-Coulomb strength criterion (Hackston and Rutter 2016), pression tests with the confining pressures of 10, 20, and 30 MPa.
in which the 3D microstructures are exported as the STL files to be The main conclusions are drawn as follows.
imported into ABAQUS. The damage ratio, integrity, and porosity are defined to describe
In this paper, the 3D microstructures models (141 × 141 × the characteristics of cracks based on the X-ray CT images. Based
40 pixels) are converted to the FE models to obtain the stress–strain on these variables and the microstructure variation of sandstone
curves, and the details can be seen in our previous works (Zhou and samples, their cracking process is well studied and is divided into
Xiao 2019; Zhao and Zhou 2019). The mechanical parameters used five stages including: (1) the compaction of initial fissure; (2) the
to simulate stress-stain curves are listed in Table 3. The loading initiation and propagation of microcracks; (3) microcracks coales-
conditions to simulate the triaxial compression are determined as cence, i.e., the formation and stable propagation of macrocracks;

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Fig. 15. Comparison analysis of the numerical and experimental stress–strain relationships (a, c, and e) stress–strain curve for C2–C4; and
(b, d, and f) cloud map of stress for C2–C4.

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Table 4. Comparison of the numerical and experimental maximum triaxial compression.” Chin. J. Rock Mech. Eng. 34 (10): 1976–1984. https://
compression stress doi.org/10.13722/j.cnki.jrme.2015.0974.
Fu, C. 2016. “Dynamic behavior of a simply supported bridge with a
ETCS MTCS Correlation
switching crack subjected to seismic excitations and moving trains.”
Categories (MPa) (MPa) coefficient
Eng. Struct. 110 (Mar): 59–69. https://doi.org/10.1016/j.engstruct.2015
C2 144.295 145.89 0.98864 .11.055.
C3 170.548 170.568 0.94238 Hackston, A., and E. Rutter. 2016. “The mohr–coulomb criterion for intact
C4 199.315 199.409 0.9757 rock strength and friction—A re-evaluation and consideration of failure
under polyaxial stresses.” Solid Earth 7 (2): 493–508. https://doi.org/10
.5194/se-7-493-2016.
Hatheway, A. W. 2009. “The complete ISRM suggested methods for rock
(4) the unstable propagation of macrocracks; and (5) the failure of characterization, testing and monitoring; 1974–2006” Environ. Eng.
rock samples. Geosci. 15 (1): 47–48. https://doi.org/10.2113/gseegeosci.15.1.47.
Based on the digital analysis and 3D reconstruction algorithm, He, Z., G. Li, S. Tian, H. Wang, Z. Shen, and J. Li. 2016. “Sem analysis on
3D real microstructural models can be obtained and can be applied rock failure mechanism by supercritical Co2, jet impingement.” J. Pet.
Downloaded from ascelibrary.org by University of Exeter on 06/16/20. Copyright ASCE. For personal use only; all rights reserved.

to understand the microstructural characteristics and evolution Sci. Eng. 146 (Oct): 111–120. https://doi.org/10.1016/j.petrol.2016.04
process of 3D cracks as well as the mechanical properties of sand- .023.
Huang, X. C., and X. P. Zhou. 2020. “Probabilistic assessment for slope
stone samples. In addition, the numerical stress–strain curves are
using the generalized Chebyshev inequalities.” Int. J. Geomech. 20 (4):
in good agreement with the experimental stress–strain curves for
06020003. https://doi.org/10.1061/(ASCE)GM.1943-5622.0001638.
the sandstone samples, which implies the accuracy of the proposed Jiang, Z., M. I. J. Van Dijke, S. Geiger, J. Ma, G. D. Couples, and X. Li.
method. 2017. “Pore network extraction for fractured porous media.” Adv. Water
In future work, the generated pore-crack microstructure mesh Resour. 107 (Sep): 280–289. https://doi.org/10.1016/j.advwatres.2017
models would be applied to numerically study the hydraulic prop- .06.025.
erties and transport properties of rock reservoirs, which are helpful Lai, J., G. Wang, Z. Wang, J. Chen, X. Pang, S. Wang, Z. Zhou, Z. He,
to oil resource and shale-gas exploration in energy engineering. Z. Qin, and X. Fan. 2018. “A review on pore structure characterization
in tight sandstones.” Earth Sci. Rev. 177 (Feb): 436–457. https://doi.org
/10.1016/j.earscirev.2017.12.003.
Li, G., X. Zhao, K. Du, F. Ru, and Y. Zhang. 2017a. “Recognition and
Data Availability Statement evaluation of bridge cracks with modified active contour model and
greedy search-based support vector machine.” Autom. Constr. 78 (Jun):
Some or all datasets and codes for this paper can be obtained by 51–61. https://doi.org/10.1016/j.autcon.2017.01.019.
contacting the corresponding author Xiao-Ping Zhou upon reason- Li, J., H. Jiang, C. Wang, Y. Zhao, Y. Gao, Y. Pei, C. Wang, and H. Dong.
able request. 2017b. “Pore-scale 518 investigation of microscopic remaining oil
variation characteristics in water-wet sandstone using ct scanning.”
J. Nat. Gas Sci. Eng. 48 (Dec): 36–45. https://doi.org/10.1016/j.jngse
Acknowledgments .2017.04.003.
Li, Y., A. Kalantari-Dahaghi, A. Zolfaghari, P. Dong, S. Negahban, and D.
This work was supported by National Natural Science Foundation Zhou. 2018. “Fractal-based real gas flow model in shales: An interplay
of China (Grant Nos. 51839009 and 51679017). of nano-pore and nano-fracture networks.” Int. J. Heat Mass Transfer
127 (Dec): 1188–1202. https://doi.org/10.1016/j.ijheatmasstransfer.2018
.08.077.
References Li, Z., D. Liu, Y. Cai, P. G. Ranjith, and Y. Yao. 2017c. “Multi-scale quan-
titative characterization of 3-D pore-fracture networks in bituminous
Al-Kharusi, A. S., and M. J. Blunt. 2007. “Network extraction from and anthracite coals using FIB-SEM tomography and X-ray μ-CT.”
sandstone and carbonate pore space images.” J. Pet. Sci. Eng. 56 (4): Fuel 209 (Dec): 43–53. https://doi.org/10.1016/j.fuel.2017.07.088.
219–231. https://doi.org/10.1016/j.petrol.2006.09.003. Liu, S., S. Sang, G. Wang, J. Ma, X. Wang, W. Wang, Y. Du, and T. Wang.
Attene, M., and B. Falcidieno. 2006. “ReMESH: An interactive environ- 2017. “Fib-sem and X-ray CT characterization of interconnected pores
ment to edit and repair triangle meshes.” In Proc., IEEE Int. Conf. on in high-rank coal formed from regional metamorphism.” J. Pet. Sci.
Shape Modeling and Applications, 41. New York: IEEE. https://doi.org Eng. 148 (Jan): 21–31. https://doi.org/10.1016/j.petrol.2016.10.006.
/10.1109/SMI.2006.29. Masaki, K., Y. Sano, and K. Kajiwara. 2017. “Os05f096 investigation of
Brewick, P. T., V. G. DeGiorgi, A. B. Geltmacher, and S. M. Qidwai. 2019. fatigue crack propagation behavior by CT with synchrotron radiation.”
“Modeling the influence of microstructure on the stress distributions of Biophys. Chem. 104 (1): 14.
corrosion pits.” Corros. Sci. 158 (Sep): 108111. https://doi.org/10.1016 Mathews, J. P., Q. P. Campbell, H. Xu, and P. Halleck. 2017. “A review of
/j.corsci.2019.108111. the application of X-ray computed tomography to the study of coal.”
Dyskin, A. V., E. Sahouryeh, R. J. Jewell, H. Joer, and K. B. Ustinov. 2003. Fuel 209 (Dec): 10–24. https://doi.org/10.1016/j.fuel.2017.07.079.
“Influence of shape and locations of initial 3-D cracks on their growth in Nasseri, M. H. B., F. Rezanezhad, and R. P. Young. 2011. “Analysis of
uniaxial compression.” Eng. Fract. Mech. 70 (15): 2115–2136. https:// fracture damage zone in anisotropic granitic rock using 3D X-ray CT
doi.org/10.1016/S0013-7944(02)00240-0. scanning techniques.” Int. J. Fract. 168 (1): 1. https://doi.org/10.1007
Ebrahimi, A. N., S. Jamshidi, S. Iglauer, and R. B. Boozarjomehry. /s10704-010-9551-0.
2013. “Genetic algorithm-based pore network extraction from micro- Nie, B., X. Liu, L. Yang, J. Meng, and X. Li. 2015. “Pore structure char-
computed tomography images.” Chem. Eng. Sci. 92 (14): 157–166. acterization of different rank coals using gas adsorption and scanning
https://doi.org/10.1016/j.ces.2013.01.045. electron microscopy.” Fuel 158 (Oct): 908–917. https://doi.org/10.1016
Elaqra, H., N. Godin, G. Peix, M. R’ Milli, and G. Fantozzi. 2007. /j.fuel.2015.06.050.
“Damage evolution analysis in mortar, during compressive loading Øren, P. E., and S. Bakke. 2003. “Reconstruction of berea sandstone
using acoustic emission and X-ray tomography: Effects of the sand/ and pore-scale modelling of wettability effects.” J. Pet. Sci. Eng.
cement ratio.” Cem. Concr. Res. 37 (5): 703–713. https://doi.org/10 39 (3–4): 177–199. https://doi.org/10.1016/S0920-4105(03)00062-7.
.1016/j.cemconres.2007.02.008. Otsu, N. 1979. “A threshold selection method from gray-level histogram.”
Fang, J. Y., F. N. Dang, Y. T. Xiao, W. H. Ding, and J. X. Fang. 2015. IEEE Trans. Syst. Man Cybern. 9 (1): 62–66. https://doi.org/10.1109
“Quantitative study on the CT test process of siltstone under triaxial /TSMC.1979.4310076.

© ASCE 04020084-13 J. Eng. Mech.

J. Eng. Mech., 2020, 146(8): 04020084


Rau, J. Y., K. W. Hsiao, J. P. Jhan, S. H. Wang, W. C. Fang, and J. L. Wang. Mech. Mater. 35 (8): 777–790. https://doi.org/10.1016/S0167-6636(02)
2017. “Bridge crack detection using multi-rotary uav and object-base 00206-5.
image analysis.” Int. Arch. Photogramm. Remote Sens. Spatial Inf. Westover, L. 1990. “Footprint evaluation for volume rendering.” In
Sci. 42: 311–318. https://doi.org/10.5194/isprs-archives-XLII-2-W6 Vol. 24 of Proc., 17th Annual Conf. on Computer Graphics and
-311-2017. Interactive Techniques, 367–376.
Shao, X., X. Pang, F. Jiang, L. Li, Y. Huayan, and D. Zheng. 2017. Yang, S. Q., P. G. Ranjith, and Y. L. Gui. 2015. “Experimental study
“Reservoir characterization of tight sandstones using NMR and IPMI of mechanical behavior and X-ray micro CT observations of sandstone
experiments: Implication for tight sand gas reservoir quality.” Energy under conventional triaxial compression.” Geotech. Test. J. 38 (2):
Fuel 31 (10): 10420–10431. https://doi.org/10.1021/acs.energyfuels
20140209. https://doi.org/10.1520/GTJ20140209.
.7b01184.
Zhao, Y., Y. Sun, S. Liu, K. Wang, and Y. Jiang. 2016. “Pore structure
Sharqawy, M. H. 2016. “Construction of pore network models for berea
characterization of coal by NMR cryoporometry.” Fuel 190 (Feb):
and Fontainebleau sandstones using non-linear programing and optimi-
zation techniques.” Adv. Water Resour. 98 (Dec): 198–210. https://doi 359–369. https://doi.org/10.1016/j.fuel.2016.10.121.
.org/10.1016/j.advwatres.2016.10.023. Zhao, Z., and X. P. Zhou. 2019. “Digital energy grade-based approach for
Shi, P., X. Fan, J. Ni, Z. Khan, and L. Min. 2017. “A novel underwater crack path prediction based on 2D X-ray CT images of geomaterials.”
Fatigue Fract. Eng. Mater. Struct. 42 (6): 1292–1307. https://doi.org
Downloaded from ascelibrary.org by University of Exeter on 06/16/20. Copyright ASCE. For personal use only; all rights reserved.

dam crack detection and classification approach based on sonar images.”


PLoS One 12 (6): e0179627. https://doi.org/10.1371/journal.pone /10.1111/ffe.12979.
.0179627. Zhao, Z., X. P. Zhou, and Q. H. Qian. 2020. “Fracture characterization and
Shiozawa, D., Y. Nakai, T. Murakami, and H. Nosho. 2014. “Observation permeability prediction by pore scale variables extracted from X-ray
of 3d shape and propagation mode transition of fatigue cracks in CT images of porous geomaterials.” In Science China technological
TI–6AL–4V under cyclic torsion using ct imaging with ultra-bright syn- sciences, 1–13. Beijing: Science China Press.
chrotron radiation.” Int. J. Fatigue 58 (Jan): 158–165. https://doi.org/10 Zhou, H. W., J. C. Zhong, W. G. Ren, X. Y. Wang, and H. Y. Yi. 2018a.
.1016/j.ijfatigue.2013.02.018. “Characterization of pore-fracture networks and their evolution at vari-
Su, K., X. Zhou, X. Tang, X. Xu, and Q. Liu. 2017. “Mechanism of cracking ous measurement scales in coal samples using X-ray μCT and a fractal
in dams using a hybrid fe-meshfree method.” Int. J. Geomech. 17 (9): method.” Int. J. Coal Geol. 189 (Mar): 35–49. https://doi.org/10.1016/j
04017071. https://doi.org/10.1061/(ASCE)GM.1943-5622.0000950.
.coal.2018.02.007.
Tao, K., and W. Zheng. 2018. “Real-time damage assessment of hydrous
Zhou, X. P., X. C. Huang, P. F. Liu, and T. F. Li. 2018b. “A probabilistic
sandstone based on synergism of AE-CT techniques.” Eng. Fail. Anal.
method to analyze collapse failure of shallow rectangular tunnels.”
91 (Sep): 465–480. https://doi.org/10.1016/j.engfailanal.2018.04.046.
Valença, J., I. Puente, E. Júlio, H. González-Jorge, and P. Arias-Sánchez. Tunnelling Underground Space Technol. 82 (Dec): 9–19. https://doi
2017. “Assessment of cracks on concrete bridges using image processing .org/10.1016/j.tust.2018.07.029.
supported by laser scanning survey.” Constr. Build. Mater. 146 (Aug): Zhou, X. P., and N. Xiao. 2019. “Analysis of fracture properties of
668–678. https://doi.org/10.1016/j.conbuildmat.2017.04.096. three-dimensional reconstructed rock model using hierarchical-fractal
Wang, L. B., J. D. Frost, G. Z. Voyiadjis, and T. P. Harman. 2003. “Quan- annealing algorithm.” Eng. Geol. 256 (Jun): 39–56. https://doi.org/10
tification of damage parameters using X-ray tomography images.” .1016/j.enggeo.2019.04.017.

© ASCE 04020084-14 J. Eng. Mech.

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