CHEM 1070 EXPERIMENT 1 A CHEM 1070 EXPERINENT 1 PART A REPORT SHEET ACCURACY AND PRECISION CALIBRATION OF A PIPETTE Name:_Toswua _WseRiceecad Date:__%/ 421 Lab Day: Demonstrator; Dowwa — HITEAL PRE-LAB EXERCISE 1. Ina class of 8 students the titre value of an acid base titration was found to be 12.10, 12.00, 12.15, 12.20, 11.95, 12.10, 12.05 and 11.98 mL. Answer the following questions. (i) Give the mean, median and modal titre values? 6 marks Mean (210 t (2-oof 12-15 $ [2.20 $U.96 FIZ fo $ DoS tWAG ge \20F Median 12-20 ¢ 1.4572 = (2.0% mL Mode. 2 «ko ml (ii) Calculate the standard deviation s, and the Gossett’s t-function 4. Standard deviation s : 2 marks as Ji 5" -%)? = 0.0497 Virieey Gossett’s t-function 2 2 marks Az Set(on-) = O.O8TX 2-365 = O.O7 be ve DATA ANALYSIS ‘Nominal volume of pipette. Vaom = {Om 2 marks Temperature of water at start of measurement. Ti 29 °C, Temperature of water at end of measurement. Tr=__ 249 °c. ‘Mean temperature. T-_2j °C 2 marks 3. Density of water (from graph at temperature T) p20 = 0.998 __g mL" 6 marksCHEM 1070 EXPERIMENT | A Table of mass of water in 4 pipette trials ‘Wass of waterlg \O. O185 4. INA 410.0942 sone 4.448% H Mean Mass: 15 -o1gv¢ 40 aap 44. ord ‘2 marks ‘Mean volume of water: ml Corrected Mean Mass: g Comrected Mean Volume: ml 1. (b) Calculation of mean volume of water. 2 marks ett « Leo L Nobo Ces 40 O42 FOAM AO TST STO. TOS | Volume = maze/ density —> 10.021 -49Eal_= 10 OF (FHL ‘2. Calculation of corrected mean mass. marks rechion Lob mw rant made = Corre > 9.4b484 + O.co106, = Q4xb4g 4. Calculation of corrected mean volume 2 marks Volume= mons} density. ‘5. Comment on the accuracy ofthe pipette based on the four measurements made, 2 marks The A oa ‘i d Vig oCounacs, due to VOL oe a loeing cleCHEM 1070 EXPERIMENT 1 A 6. Table of mass & volume of water in 8 pipete trials Trial? | Massof | Volume ofwater, | __(-)/mL a Im? waterfg | afb. I 10.0195 | 10.0346 0.0041 | ©. c0n043 | 2 4.9414 | 94919 =O. 0346 0.00 3 | 10.0942) 10.1144 ©.0¢44| 0.00712 4 | 4.9498 | 10.0198 -0.0104/ 0. 5_| 4.9652) 94.976. —0-9543| 0.002945 6 | (0.013) | lo. 033) 0.0036 | ©.000013 | T_| 10-0064 [0.0265 | —0.00%,| 0.000009 [3 lo-o146|_ 10.0347 O.0052| 0.900021 Tee =| O.08 334 .08Q5 6 marks Mean volume= 3@=6%= ~ mL. 6.(a) Calculation of mean volume of wate. 2 marks Mean = (10-038 + 9.94144 10 ITH + WD. 018% £ 9.9452 + 10-0331 + 19.0265 + Ip.o344) +% = jo@2qoml 6.(b) Calculate the standard deviation, s, of the volume discharged by the pipette. 2 marks Oa = [ye -onse) 2 Seeks vg 0.041446 6. (0) Calculate the Gossett’st-function, 2, ofthe volume discharged by the pipette, 2 marks A= setlon) = Q0242b5 = O.041F He X25 a = 0.035099CHEM 1070 EXPERIMENT | A 7.(a) Volume of pipette Kets 10.0165 0.041996 mL out 7.(b) Vota 2 marks 10 olf + 0.035094 mL 7.(c) Comment on the precision of the pipette. 2 matks ——Thhe_exgerioment Irae Qroven Mneasals Caladahions sat Hu Glerdond deviahon un» mince flonetore AI i s SoD Accuracy fpipete Wien Geemnarey 1 matk Precision ofpipette == Hel PEGSICg mark OVERALL CONCLUSIONS/ANY OTHER COMMENTS