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A BS TRA CT
INTRODUCTION
TYPES OF GEOMEMBRANE
G O A L S OF S E A M I N G G E O M E M B R A N E S
M E T H O D S OF S E A M I N G G E O M E M B R A N E S OF
D I F F E R E N T TYPES
LAP SEAM
p--R.-,~
p . . . . . . . . . . . . . . . . . . . . . ] Made with an adhesive,
I . . . . . . . . . . . . . . . . . . . . . . 1 heat seaming, dielectric
R= Required ovedap of fabric seaming, solvent welding,
(fabric - reinfopced FMLs only) and h u t gun
/
Extruded area
Similar to above, except
Buffed area ~ ~ Buffed area
a heat gun is used to tack
edge of FML
I ~ ' ~ Hot t J - - i
BUTTERFLY SEAM
Made by a special
1 / heat sealing device
Fig. 1. Configurations of seams used in joining geomembrane sheets and panels and
method of seaming. The 'tacks' used sometimes in preparing the fillet weld seams are not
part of the seam.
374 Henry E. Haxo, Jr, Lawrence C. Kamp
Other types of seam have been used: (1) a butterfly type, in which two
sheets of unreinforced g e o m e m b r a n e are plied together under heat, and
(2) sewn seams which have been used with geomembranes having a
nonwoven geotextile backing and extruding a small bead at the apex on the
coating side of the seam.
The various types of seaming method that are used in the factory and in
the field to join the geomembranes based on different polymers are
summarized in Table 1. Of particular interest is the Environmental
Protection Agency's Technical Guidance Document on fabrication of PE
field seams. 7
D E S T R U C T I V E TESTS OF SEAMS
Thermal methods
Base p o l y m e r Type of Place Neat Bodied Heat Heat Di- Lap Fillet Hot Ultra-
compound a used seal b gun electric c wedge sonic
seaming
e~
1 ? -i
(a) (b) (c)
Fig. 2. Modes of testing the seam strength. (a) Shear; (b) 'T' peel; (c) 180 ° peel. The 180 °
peel is used only with flexible geomembranes. Depending on the convention, 'T' peel is
sometimes considered 90 ° peel and sometimes 180 ° peel.
(100 mm) in width and has a total length of 9 in (230 mm) plus the width of
the seam (Fig. 3). The faces of the clamps used to secure the specimen in
the testing device measure 1 × 1 in (25 x 25 mm). The required distance
between the clamps at the start of the test is 6 in (152 mm) plus the width of
the seam, with the seam centered between the clamps. The rate of grip
separation is 12 in/min (305 mm/min). Five specimens are tested, and the
maximum stress applied to each specimen at yield or breakage as well as
the location of the break are recorded.
The peel strength of fabric-reinforced geomembrane seams is deter-
mined in accordance with the NSF Standard 54,9 which is a modification of
ASTM D413. 8 In this test, a 1 in (25 mm) wide strip specimen is peeled at
180 ° (by convention, usually 'T' peel) at a rate of 2 in/min (50 mm/min).
Five specimens are tested. The peel strength is calculated by drawing a line
on the stress-strain chart that best represents the average of the highest
and lowest force values necessary to separate the specimen. If an initial
high peak value occurs which is not typical of the remainder of the
stress-strain curve, then this value is ignored during calculations. The
locations of the breaks, e.g. the plane in which the specimens peel, are
recorded. Any voids or unbonded areas noted during testing are also
recorded. In the case of a film-tear bond, fabric-reinforced specimens
frequently separate at the plane of the scrim with the result that the ply
adhesion of the parent sheeting is actually being measured. Testing is
discontinued after 2 in (50 mm) of peeling in this manner.
Most specifications for field seams of reinforced (as well as unrein-
forced) thermoplastic geomembranes call for a minimum overlap area. A
bonded width of 4 in (100 mm) is frequently required for adhesive-welded
Destructive testing of geomembrane seams 377
4"
Seam
Z Clamp
i
i
Fig. 3. Specimen for testing seam strength of fabric-reinforcedgeomembranes in accord-
ance with NSF Standard 54. 9 (Note: one inch -- 2.54 cm.)
seams. This area begins at the part of the seam that will be in contact with
the waste. If excessive adhesive has squeezed out during the seaming
process causing a larger than 4 in (100 mm) wide bonded area, specimens
being prepared for peel testing are usually separated by hand up to the 4 in
(100 ram) width.
Seam samples cut from a liner should have a minimum length of 30 in
(760 mm) in the direction of the seam to accommodate 5 specimens in peel
and 5 specimens in shear. The width of the sample cut from the
g e o m e m b r a n e depends on the width of the seam to meet the dimensions
required for the shear test specimen (Fig. 3). At the time the test
specimens are cut from the sample, the peel and shear specimens, if
possible, are alternated across the length of the seam sample.
For specification testing, dielectric or heat-sealed seam samples should
be conditioned for 24 h at 23°C prior to testing. Adhesive-welded seam
378 Henry E. Haxo, Jr, Lawrence C. Kamp
samples should not have a solvent odor at the time of testing. The NSF
Standard 54 [9] requires conditioning of adhesive-welded seam samples
for a minimum of 12 days at 23°C, during which time the solvent can diffuse
and evaporate from the bonded area of the sample. If, after conditioning,
the sample still has an odor of solvent, the sample can be oven-aged at 70°C
for 3 h and allowed to rest at 23°C for 48 h before testing. Exposing the
samples to direct sunlight can hasten the solvent evaporation or curing
cycle.
dumbbell specimen, then the specimen may not break when tested in the
shear mode before the maximum extension of the tensile testing machine
is reached. The dumbbell-shaped specimen also prevents slippage in the
grips.
Determination of seam strength in the shear mode is performed in
accordance with a test method based on ASTM D638/3083. 8 The seam is
centered between the grips. Initial grip separation is approximately
4.5-5.0 in (115-127 mm). Rate of grip separation is 2.0 in/min (50 mm/
min). The maximum stress applied to the specimen at yield or break and
the location of break are recorded. In the case of fillet-weld-type seams, it
should be noted that the hot-tack portion of the specimen is not part of the
seam and should be opened prior to testing; thus, only the fillet-weld part
of the seam is tested. It is sometimes necessary to cut through the hot-tack
in order to open up the seam.
Determination of seam strength in the peel mode is performed in
accordance with a modified version of ASTM D4138 that allows for the use
of the ASTM D6388 Type I dumbbell test specimen. The rate of grip
separation is 2.0 in/min (50 mm/min) and the maximum stresses applied
are recorded. When dual-thermal-weld samples are tested, that part of the
weld that would be in contact with the waste is tested first and the sample
specimen is then reversed and the second weld is tested. The maximum
stress applied and the location of the break are recorded. If during the peel
test a specimen partially separates but then breaks, it would be classified as
a film-tear bond. However, the percentage of the area that is separated is
compared with the total seam area.
A few brittle fracture failures across and adjacent to weld areas of PE
geomembranes have been reported 1° and, as a result, a need has arisen for
the development of new test criteria. In response, several options to
develop new criteria are being investigated. One option involves recording
the elongation of the specimens at yield and at break when tested in the
shear mode. The method of calculating this elongation value needs to be
investigated further. A seam usually results in a mass of much greater
thickness than the parent sheeting and, consequently, will elongate less at
a particular stress than the parent sheeting. This causes stress concentra-
tion above and below the seam between the upper and lower grips of the
tensile testing equipment (see Fig. 4). The following parameters need to
be standardized before the industry can begin to specify criteria based on
the amount of elongation:
- - T h e length to be used in calculating elongation.
--Total grip separation distance at start of test.
--Distance where elongation is occurring from the grip to the edge of
the seam.
380 Henry E. Haxo, Jr, Lawrence C. Kamp
Griparea "I[
I Areaofelongation I---1
,.~
Areaof Areaof
elongation
ii';e
r iiilt,on
elongation
• !
Griparea "1 .]
Fig. 4. The areas of elongation of the fillet-weld and dual-thermal-wedge seam specimens
under shear test.
R E Q U I R E M E N T S IN SPECIFICATIONS
Sampling requirement
No standard frequency for sampling the in-place factory and field seams
for seam strength testing has been established. Sampling has been
specified both on randomized and judgemental bases of the number and
size of samples to be cut out per unit length of seam. Both factory and field
seams should be tested; however, the frequency needed for sampling
Destructive testing of geomembrane seams 381
Variations in sampling
Options are usually included in the project specification to provide for
additional sampling when certain conditions or changes in conditions
occur, such as:
1. Different or changing contour (slope, bottom).
2. Weather changes during installation (cloud cover, moisture, exces-
sive heat or cold).
3. Windblown dust or dirt.
4. Changes in seaming crew personnel.
5. Equipment changes or repairs.
6. Work stoppage, e.g. continuation after lunch hour or breaks.
Usually, if new equipment is being used or if there is a change in crew
382 Henry E. Haxo, Jr, Lawrence C. Kamp
personnel, a trial weld will be made and tested. For the other conditions,
additional samples will be taken from the seams and tested. The frequency
of sampling would be at the discretion of the quality control engineer/
inspector.
parent sheeting) when the seam is tested in the shear mode. Being able to
obtain numerical values of the peel test is important, as a seaming process
could yield a seam that would have a film-tear bond in peel, but severely
weaken and distort the parent sheeting. This possibility justifies the need
to test the seam strength both in the peel and shear modes. It is desirable,
regardless of the membrane, to have the specimen break as a film-tear
bond in the peel mode.
Locus-of-break code
A C C E P T A N C E C R I T E R I A FOR D E S T R U C T I V E
TESTING OF SEAMS
The generally used acceptance criteria for bonded seam strength (that is,
the strength of seams tested in shear) specify that the average of the
maximum strength of the five tested specimens be at least 80% of the value
for breaking strength of the parent sheeting called for in the specification.
The values appearing in NSF Standard 549 for the breaking strength of the
parent sheeting are often used in specifications. Some specifications may
call for 80% of the actual breaking strength of the geomembrane. In
addition to meeting a strength requirement, the specimens are usually
required to break so as to indicate a film-tear bond (FTB); that is, all of the
tested specimens must break at the seam edge (SE) or in the sheeting
outside the seam area (BRK). These criteria for strength and locus of
break are the same for both factory and field seams. Representative test
results are presented in Table 2 for samples cut from field seams of 30 mil
(0.74 mm) and 40 mil (1.0 mm) PVC geomembranes. They show that all
the specimens tested in the shear mode broke in the parent sheeting, and
that all the 30 mil (0.74 mm) specimens and most of the 40 mil (1-0 mm)
specimens met the value requirements.
384 Henry E. Haxo, Jr, Lawrence C. Kamp
Schematic of
Untested Specimen
Direction
of Peel X-X We~ Top Sheet
I
--0
Bottom Sheet
Locus-el-Break Break
Types of Breaks Code Oeecrlptlon Classification a
Clamp
% CL Break in sheeting
i - i
at clamp edge.
Ji i
i
BRK Break in sheeting. FTB
- i
%ru ,, I
}sE Break at seam edge. FTB
/
%
~:~ Break in s h e e t i n g
t ~ AD-BRK after some adhesion FTB
' failure between t h e
sheets.
Di;ection
~ Fabric
~ . ~ Plies of
" ' Polymer
Seam
Locus-of-Break Break Claesl-
Types of Breaks Code Description flciUon a
S c h w t t s t l c of
Untested Specimen
Bead Outer Area
, ~ ~ L f r.. Buffed Area
Off-Center Bead
3 1
2 Break in the sheet. Use 1 to
indicate bottom sheet and 2
I '---' BRK to indicate top sheet. If break FTB
/
is in buffed area, indicate
1
with "(1B)'.
Break in the bottom ihlNiting
• , AD-BRK alter ~ IKIhllion l=llure FTB
the filet m~l the bottom
sheet. (~aplicllble to peel only).
Break ill the edge of the
, HT hot tack tot specimens which NO Test
could not be delamlnated in
the hot tack.
Specified acceptance criteria for peel strength usually require that the
samples meet a specified minimum strength value or break with an FTB.
For factory-made seams, NSF Standard 549 requires an FFB or a peel
strength greater than 10 ppi (1.75 kN/m). In almost all tests of factory
seams, the seams are FTB. Consequently, an acceptance criterion of
greater than 10 ppi (1.75 kN/m) which is frequently specified, does not
reflect the peel values that are commonly obtained. For most field seams of
Destructive testing of geomembrane seams 387
Schematic of
U n t e s t e d Specimen
W ~ o p Sheet
Locus-of-Break Break
Types of Break Code Description Classification a
Fig. 8. Locus-of-break codes and descriptions of test breaks for dual-wedge-thermal weld
seams. (aFFB = film-tear bond. Diagram not to scale.)
PVC geomembranes, the peel strength values are generally much higher,
as is shown in Table 2, thus indicating that higher values are possible and
should be specified for PVC seams. Low values may reflect partial
retention of the solvent by the PVC at the bond. A minimum peel strength
of 15 ppi (2-63 kN/m) is suggested for field seams of PVC geomembranes
up to and including 40 mil (1.0 mm) thicknesses. The recommended
criterion for factory-fabricated seams is an FTB or a peel strength greater
than 20 ppi (3.5 kN/m).
TABLE 2
Analysis of Representative Test Results for Samples of Field Seams of Unreinforced
Polyvinyl Chloride Thermoplastic Geomembranes
Seam specification ~
Minimum value
(ppi b) (kN/m) 10(1.75) 55-2(9.66) 10(1.75) 73.6(12.88)
Class of break FTB c FrB C FTB c FFB ~
Number of samples
in test 22 22 24 24
Test values
Range of values
(ppi) (kN/m):
Low 13-0(2.28) 59.0(10-33) 6.2(1.09) 65-3(11.43)
High 30.6(5.36) 76.0(13.30) 30.0(5.25) 86.0(15.05)
Median value
(ppi) (kN/m) 21.1(3.69) 67.0(11.73) 17.6(3.08) 74-6(13.06)
Mean value
(ppi) (kN/m) 21.0(3.68) 66.9(11-71) 16.0(2.80) 75.6(13.23)
Standard deviation
(ppi) (kN/m) 5-0(0.88) 4.8(0.84) 5.7(1.00) 5.6(0.98)
Locus of break
Class of break
(%)~:
FFB c 68.2 100 13-4 100
NonFFB" 31-8 0 86.6 0
Type of break e
(%) AD (31-8) SE (97.3) AD (86.6) SE (94.2)
AD-BRK (57.3) BRK (2-7) AD-BRK (9.2) BRK (4-2)
SE (10.9) SE (4-2) AD-BRK (1.6)
of the parent sheeting, which is usually 200 ppi (35 kN/m) for 36 mil
(0.91 mm) CSPE-R and 250 ppi (43.8 kN/m) for 45 mil (1.14 mm) CSPE-
R. The reinforcing fabric in both geomembranes is a 10 x 10-1000 denier
polyester scrim and is the strength component of this type of geomem-
brane. The locus-of-break code should be a film-tear bond (SE or BRK).
However, if pullout or slippage of the fabric occurs during testing, the
Destructive testing o f geomembrane seams 389
TABLE 3
Analysis of Representative Test Results for Samples of Field
Seams of Fabric-Reinforced Chiorosulfonated Polyethylene Geomembranes
Seam specification a
Minimum value
(ppi b) (kN/m) 10(1-75) 200(35-0) 10(1.75) 250(43.8)
Class of break FFB c FFB c FrB C FrB c
Number of samples 11 11 21 21
in test
Test values
Range of values
(ppi) (kN/m):
Low 11-2(1-96) 265(46-4) 14-6(2.56) 245(42.9)
High 15.2(2.66) 343(60-0) 23-7(4.15) 328(57.4)
Median value
(ppi) (kN/m) 13.2(2.31) 320(56.0) 19.1(3.34) 302(52.9)
Mean value
(ppi) (kN/m) 13-1(2.29) 314(56.0) 19-4(3-40) 305(53-4)
Standard deviation
(ppi) (kN/m) 1-2(0.21) 23(4.02) 2.8(0.49) 16(2.80)
Locus of break
Class of break (%)d:
FTB ~ 100 100 100 100
NonFTB ~ 0 0 0 0
Type of break e DEL(100) BRK (100) D E L (100) BRK (100)
results are generally discarded and new specimens are tested. Representa-
tive test results for these geomembranes are presented in Table 3.
Specifications for peel adhesion of the seams of fabric-reinforced
thermoplastic geomembranes generally require a film-tear bond and a
minimum peel value. An FTB break of fabric-reinforced geomembranes
results in the ply separation at the plane of the scrim of one of the plies of
parent sheeting. The ply adhesion of this type of geomembrane is
specified. Factory-fabricated seams should always achieve an FFB.
NonFTB breaks have been observed in field-fabricated samples because
390 Henry E. Haxo, Jr, Lawrence C. Kamp
In general, the current acceptance criterion for the bonded seam strength
of seams of semicrystalline thermoplastic geomembranes, e.g. H D P E , is a
minimum value equal to 90% of the yield strength of the parent sheeting.
As with the other types of geomembranes, NSF Standard 549 is commonly
used as the source for the strength requirement. Because most require-
ments for yield strength are conservative, as is the case with those in NSF
Standard 54, 9 it has been suggested that the acceptance criterion for
bonded seam strength should be equal to or greater than 110% of the
specified yield strength. Also, all specimens tested in shear for bonded
seam strength should break in the parent sheeting, that is they should be
FTB breaks. Low values in shear are usually the result of damage to the
sheeting, e.g. severe buffing or gouging, during the seaming operation.
In many specifications, the acceptance criterion for peel strength of PE
seams is also related to the specified yield strength of the parent sheeting.
The minimum values for peel strength are often 60% of specified yield
strength. Other minimum values that have been specified include 65% of
specified yield value for extrusion fillet-type welds and 70% of yield value
for dual-thermal-wedge welds. The locus-of-break specified also must be
FFB; however, some specifications allow one nonFTB break in a set of five
specimens that meet the strength criterion of acceptance. In such cases,
the specification must be explicit as to strength values and to the number of
nonFTB breaks for a given number of specimens.
Examples of the seam strength values and the respective loci of breaks
(see Figs 7 and 8) obtained in the testing of samples of field seams made by
fillet- and dual-wedge-thermal welding are presented in Tables 4 and 5
respectively. Table 4 presents the results of testing samples of fillet welds
of H D P E geomembranes of 40, 60 and 100 mil (1-0, 1-5 and 2.5 mm)
thicknesses. The results show the significantly higher strength values both
in shear and peel than were specified, thus indicating that higher values
could be used in specifications. It is to be noted that there were a significant
TABLE 4
T e s t R e s u l t s f o r S a m p l e s o f F i e l d S e a m s o f Fillet W e l d s o f H D P E Geomembranes
40 rail (I .00 ram) 60 rail (1.50 ram) 100 rail (2.54 ram)
Seam specification ~
Minimum value (ppi b) (kN/m) 63 (11.0) -- 108 (18.9) -- 135 (23.6) --
Class of break' FrB d FTB PFB FTB FTB FTB
Number of samples in test 13 13 21 21 18 18
Thickness (mil) (mm)
e~
Median 40-5 (1-03) 64.8 (1.65) 106.4 (2-70)
Mean 39.9 (l.01) --~ 65-6 (1-67) --~ 106.0 (2-69) --~
Standard deviation 1.8 (0.046) 3.7 (0-094) 4.6 (0.117)
Test values
Range of values (ppi) 92-128 50-110 170-199 78-133 255-311 130-234
(kN/m) (16-1-22.4) (8-76-19-3) (29.8-31.8) (13-6-23.3) (44-6-54-4) (22-8-41-0)
Median value (ppi) (kN/m) 120 (21-0) 80 (14-0) 182 (31.9) 101 (17.7) 280 (49-0) 162 (28.4)
e~
Mean value (ppi) (kN/m) 116 (20-3) 77 (13.5) 181 (31-7) 105 (18.4) 280 (49.0) 167 (29-2)
Standard deviation (ppi) (kN/m) 9-6 (1-68) 16-5 (2-89) 10.5 (1.84) 16.0 (2.80) 14-4 (2.52) 24.2 (4.24)
Class and locus of break"
(% of specimens)~
Film-tear bond: SE 80 83 87 76 72 76
BRK 15 5 8 0 11 0
AD-BRK 0 0 0 10 0 0
Nonfilm-tear bond: A D 0 12 0 10 0 0
AD-WLD 0 0 0 1 16 24
No test: HT 5 0 5 3 1 0
Total 100 100 100 100 100 100
TABLE 5
Tests of Field Seams of Dual-Wedge-Thermal Welds
of 40 mil (1.00 mm) HDPE Geomembranes
Adhesive strength
(peel)
Bond strength
Parameter (shear) Weld A Weld B
Seam specification a
Minimum value (ppi b) (kN/m) 63 (11.0)
Class of break c FTB a FFB FTB
Number of samples in test 30 30 30
Thickness
Range of values (rail)
(mm) 34--43 1
(0.86-1.09)
Median (rail) (mm) 37.2 (0.94)
Mean (mil) (mm) 37.4 (0-95)
Standard deviation 2.0 (0.051)
Test values
Range of values (ppi) 98-117 61-94 65-98
(kN/m) (17.2-20-5) (10.7-16.5) (11.4-17.2)
Median value (ppi) (kN/m) 105 (18.4) 85 (14.9) 85 (14.9)
Mean value (ppi) (kN/m) 105 (18.4) 83 (14.5) 84 (14-7)
Standard deviation (ppi) (kN/m) 4.5 (0.79) 7.1 (1.24) 7-4 (1.30)
Class and locus of break"
(% of specimens) e
Film-tear bond:
SE 100 91 88
BRK 0 0 0
AD-BRK 0 3 3
Nonfilm-tear bond:
AD 0 6 9
Total 100 100 100
DISCUSSION
REFERENCES