Professional Documents
Culture Documents
Foreword 4
Introduction 4
1 Scope 5
2 Normative and informative references 5
2.1 Normative references 5
2.2 Informative references 5
3 Terms, definitions and abbreviations 5
3.1 Terms and definitions 5
3.2 Abbreviations 7
4 Responsibilities 8
4.1 Purchasers responsibility 8
4.2 Manufacturers responsibility 8
4.3 Responsibilities of Qualifying Company 8
5 Qualification of manufacturers 8
5.1 Basis for qualification of manufacturers 8
5.2 Evaluation for acceptance 8
5.3 Acceptance of qualification 8
5.4 Proof of acceptance 8
6 Validity of qualification 9
6.1 Term of validity 9
6.2 Renewal of qualification 9
6.3 Transitional arrangements 9
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7 General requirements 9 2
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7.1 Knowledge and relevant experience 9 6
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7.2 Manufacturing facilities and equipment 10
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7.3 Sub-contractors 10 1
7.4 Quality requirements for test laboratories and manufacturers of welded products 10 0
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8 Manufacturing Summary 10 s
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8.1 Requirements for Manufacturing Summary 10 u
8.2 Content of the Manufacturing Summary 10 o
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9 Heat treatment 12 a
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9.1 Heat treatment facilities and equipment 12 S
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9.2 Heat treatment procedure 13 s
9.3 Verification of heat treatment procedure 14 o
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10 Qualification of the manufacturing process 15 a
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10.1 Objective of qualification testing 15 g
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10.2 Essential variables 15 r
10.3 Qualification testing 17 o
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10.4 Welding procedure qualifications 20 S
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11 Qualification test record (QTR) 20
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11.1 General 20 n
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11.2 Content of qualification test record (QTR) 20 l
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11.3 Required copies and distribution of qualification test record (QTR) 21 O
Annex A (Informative) Manufacturing Summary front page and example 22 d
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Annex B (Normative) Additional requirements to API Spec 6A:2010/ISO 10423:2009 , Annex M, and d
ASTM A 991 27 n
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Annex C (Informative Verification of heat treatment procedure –
procedure – Example 28 S
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Annex D (Normative) Form for Qualification Test Record (QTR) Front Page 29 b
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Foreword
The NORSOK standards are developed by the Norwegian petroleum industry to ensure adequate safety,
value adding and cost effectiveness for petroleum industry developments and operations. Furthermore,
NORSOK standards are, as far as possible, intended to replace oil company specifications and serve as
references in the authorities’ regulations.
The NORSOK standards are normally based on recognised international standards, adding the provisions
deemed necessary to fill the broad needs of the Norwegian petroleum industry. Where relevant, NORSOK
standards will be used to provide the Norwegian industry input to the international standardisation process.
Subject to development and publication of international standards, the relevant NORSOK standard will be
withdrawn.
The NORSOK standards are developed according to the consensus principle generally applicable for most
standards work and according to established procedures defined in NORSOK A-001.
The NORSOK standards are prepared and published with support by The Norwegian Oil Industry Association
(OLF), The Federation of Norwegian Industry, Norwegian Shipowners’ Association and The Petroleum Safety
Authority Norway.
Introduction
1 Scope
This NORSOK standard establishes a set of qualification requirements to verify that the manufacturer has
sufficient competence and experience of the relevant material grades, and necessary facilities and equipment
to manufacture these in the required shapes and sizes with acceptable properties.
This standard is applicable to the following material grades and product forms:
This NORSOK standard is also applicable to critical components or product forms in other materials and for
special manufacturing/fabrication processes, e.g. titanium and nickel alloys in other product forms than
casting, carbon steel and low alloy steel products and induction/cold bending.
NOTE For the purpose of this standard this is normally an oil company.
3.1.3
equalization time
the time used to ensure a uniform pre-set temperature throughout a heat treatment load and/or throughout all
section thicknesses of a component (see also figure in Annex C)
3.1.4
heat sink
separate block of material made from the same generic type of material as the parts being heat treated to
monitor temperature during heat treatment
3.1.5
high alloyed austenitic SS
austenitic SS with PREN ≥ 40 or Ni + 2 x Mo > 30 (Mo > 2)
EXAMPLES SS type 6Mo, UNS S31266, UNS S32654, UNS S34565, UNS J95370.
3.1.6
holding time
time from the controlling thermocouple (normally furnace thermocouple) has reached set temperature until
the specified soaking time is completed.
NOTE Holding time consist of equalization time + soaking time. (see also figure in Annex C).
3.1.7
main contractor 3
party, which carry out all or part of the design, engineering, procurement, construction, commissioning or 2
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management of a project, or operation or maintenance of a facility on a contract awarded by 6
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Company
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3.1.8 0
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manufacturer
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party, including sub-contractors, which carry out operations affecting the material properties of the finished l
product u
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NOTE These operations can include forming, heat treatment, etc. a
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3.1.9 +
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may o
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verbal form used to indicate a course of action permissible within the limits of this NORSOK standard a
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pitting resistance equivalent PREN r
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PREN = %Cr + 3.3 x %Mo + 16 x %N
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3.1.11 A
purchaser
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party that purchase a product from a manufacturer l
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3.1.12 d
Qualifying Company r
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party which monitor the qualification exercise and in the end accept the resulting qualification test record d
(QTR) by signing and stamping the QTR front page n
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The Qualifying Company can be the Company, the main contractor, the purchaser or a party authorised to act S
on their behalf. Qualifying Company shall be independent of the manufacturer. y
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shall d
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verbal form used to indicate requirements strictly to be followed in order to conform to this NORSOK standard o
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and from which no deviation is permitted, unless accepted by all involved parties P
3.1.14
should
verbal form used to indicate that among several possibilities one is recommended as particularly suitable,
without mentioning or excluding others, or that a certain course of action is preferred but not necessarily
required
3.1.15
soaking time
time that the entire part being heat treated (throughout its cross sections) remains at the specified set
temperature
3.1.16
type 22Cr duplex
ferritic/austenitic stainless steel alloys with 22 % Cr
3.1.17
type 25Cr duplex
ferritic/austenitic stainless steel alloys with 25 % Cr and PREN ≥ 40
EXAMPLES UNS S S32505, UNS S32550, UNS S32750, UNS S32760 and UNS S39274.
3.1.18
type 6Mo 3
austenitic stainless steel alloys with 6 % Mo and PREN ≥ 40 2
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EXAMPLES UNS S31254, UNS N08367 and UNS N08926. 0
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3.1.19 1
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test directions 2
test directions are defined relative to the geometry of the component to be tested s
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For the purpose of this NORSOK standard the definitions in AST M A370-11, sect. 4, apply with axial defined o
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as the longitudinal axis of test specimen located parallel to the main axis of the component. a
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3.2 Abbreviations +
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API American Petroleum Institute o
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ASTM American Society for Testing and Materials a
CD compact disc n
EN European Standard
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HIP hot isostatic pressed r
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IEC International Electrotechnical Commission
ISO International Organization for Standardization S
MDS material data sheet A
MOM minutes of meeting e
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NDE non-destructive examination l
PREN pitting resistance equivalent n
PWHT post weld heat treatment
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QTR qualification test record
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SS stainless steel a
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UNS unified numbering system n
WPQR welding procedure qualification record a
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WPS welding procedure specification S
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4 Responsibilities
A manufacturer acquiring a "NORSOK M-650 qualification" assumes an obligation to carry out manufacturing
in accordance with the qualified Manufacturing Summary including its referred procedures. If an order
requiring "NORSOK M-650 qualification" is outside the qualified range, as defined in 10.2, the purchaser shall
be informed.
The Qualifying Company shall monitor the qualification exercise, review and in the end accept the resulting
qualification test record (QTR) and as proof of the acceptance sign and stamp the QTR front page.
It is important for acceptance of the QTR by other customers that the verification exercise is carried out by a
recognized Qualifying Company. 3
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5 Qualification of manufacturers 0
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5.1 Basis for qualification of manufacturers 0
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Basis for qualification of manufacturers including their nominated sub-contractors shall be as follows: s
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a) knowledge and relevant manufacturing experience with the type of material to be qualified (see Clause 7); o
b) acceptable manufacturing facilities and equipment (see Clause 7 and Clause 9); b
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c) established Manufacturing Summary (procedure) covering all manufacturing steps from melting or semi
product to finished products (see Clause 8); S
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d) an established heat treatment procedure (see Clause 9); s
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e) manufacturers quality system, which shall fulfil the requirements of ISO 9001; t
f) results of testing in compliance with this NORSOK standard (see Clause 10). a
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5.2 Evaluation for acceptance r
The Qualifying Company shall carry out a review of the manufacturers facilities, equipment, implementation o
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of procedures and documentation as required by this NORSOK standard at the m anufacturers and sub- S
suppliers premises. The evaluation for acceptance shall concentrate on facilities and equipment for m elting, A
refining, forming, welding, heat treatment, etc. e
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The review shall be carried out by technical competent personnel, with knowledge of metallurgical aspects of n
the applicable alloys, including precipitation diagrams, effect of hot forming, welding, heat treatment, etc., and O
who has experience relevant for the manufacturing process to be evaluated. d
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The result of the evaluation shall be documented in an evaluation report or a MOM. d
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5.3 Acceptance of qualification S
A complete QTR with content in compliance with Clause 11 shall be established for possible acceptance. y
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5.4 Proof of acceptance e
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The original signed and filled in QTR front page is the only valid proof of being accepted according to this v
NORSOK standard. o
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NOTE There is no official listing in the name of NORSOK of accepted manufacturers according to this NORSOK standard.
6 Validity of qualification
a) a manufacturer with regular production of the originally qualified products and alloys is considered re-
qualified and additional testing is normally not required. It is a pre-requisite that all test requirements in the
current revision of this NORSOK standard are complied with;
b) evaluation and review at the manufacturers and sub-suppliers premises according to 5.2 shall be carried
out by the Qualifying Company;
c) the Manufacturing Summary and referred procedures shall be reviewed, updated and a decision made
whether retesting is required;
d) the heat treatment procedure and its corresponding verification, see 9.3, shall be reviewed, and a
decision made whether a new verification is required;
e) a minutes of meeting (MOM) listing actual parts of the QTR which shall be updated and with conclusions
for renewal of the qualification shall be included in the re-qualified QTR;
f) a new QTR front page shall be established and properly signed.
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6.3 Transitional arrangements 2
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Subject to purchasers acceptance, Revision 3 qualifications are considered to fulfil the Edition 4 requirements 6
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of this NORSOK standard until the validity of the Revision 3 qualification expires on the c onditions stated 4
below. There are no transitional arrangements for flanges or valves machined from forgings. For these 1
products it is presupposed that the qualification shall be in accordance with Edition 4 of this NORSOK 0
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standard. s
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Transitional conditions are as follows: u
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a) the Manufacturing Summary, see 8.2, is updated, and a heat treatment procedure, see 9.2, is b
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established/updated;
b) verification of the heat treatment procedure, as specified in 9.3, has been carried out; S
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c) the additional test requirements in 10.3.3, as specified for selected product forms in Table 2, are fulfilled. s
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In such case a statement shall be included in the box “Other information” on the original Revision 3 QTR front a
page and signed off by the Qualifying Company. The original Revision 3 validity date shall be maintained. n
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7 General requirements
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7.1 Knowledge and relevant experience e
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7.1.1 Knowledge n
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The manufacturer shall have in-house knowledge of relevant metallurgical aspects of the applicable alloys
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including precipitation diagrams, effects of hot forming, welding, and heat treatment parameters, etc. as
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applicable for his manufacturing process. d
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7.1.2 Relevant experience
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The manufacturer shall have relevant experience with manufacture of the type of material to be qualified. y
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Relevant experience should be supported by statistical data presented in the form of a histogram for key d
parameters, e.g. tensile strength, impact thoughness, corrosion resistance, etc. In addition a relevant e
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reference list from the last 2 years production for the products, materials and the range of sizes to be v
qualified shall be included. o
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New manufacturers with less than 2 years of documented production for actual product and material may be
qualified to this NORSOK standard, but with a validity period limited to 2 years, after which a new evaluation
shall be carried out. A note to this effect shall be included on the QTR front page.
Requirements for heat treatment facilities and equipment are further described in 9.1.
7.3 Sub-contractors
If parts of the production are carried out by a sub-contractor, the manufacturer is responsible for ensuring that
the sub-contractor meets the requirements of this NORSOK standard for the manufacturing steps that the
sub-contractor is performing.
7.4 Quality requirements for test laboratories and manufacturers of welded products
8.2.2 Content
8.2.2.1 General
The Manufacturing Summary shall include, but not be limited to, the requirements in 8.2.2.2 to 8.2.2.15.
8.2.2.2 The product type and the manufacturer ’s requirements (purchasing specification) regarding start
material. Apply especially when semi finished products such as ingot, bar, pipe, plate, strip, etc., are used as
a basis for the manufacture. In such cases the manufacturer of the start material shall also be given.
For duplex steels in particular more than one etchants m ay be required for detecting intermetallic phases,
carbides and nitrides.
9 Heat treatment
9.1.1 General
Heat treatment facilities and equipment shall fulfil the requirements in 9.1.2 to 9.1.8. In addition, API 6HT
should be used as a guideline.
9.1.2 Foundries
Foundries shall have heat treatment facilities within their own premises or they shall be located in their close
vicinity.
For large components it is recognised that a transfer time of 60 s may be difficult to achieve. In such cases a
longer transfer time may be specifically qualified. Qualification tests shall comprise both thin and heavy
sections of such components as agreed with the Qualifying Company. Details of the extended transfer time
including for, which products it is applicable for, shall be highlighted on the QTR front page.
The transfer time is measured from the time the furnace door is fully open or the furnace roof is fully removed
and until the component(s) is completely submerged into the quenching bath.
9.2.1 General
A specific heat treatment procedure shall be established. Content of the procedure shall as a minimum be as
given in 9.2.2 to 9.2.6.
1) how traceability of heat and heat treatment lot is ensured throughout the whole heat treatment process,
2) how components within each heat treatment load are identified,
3) how components used for production testing in each heat treatment load are identified.
9.3.1 General
Verification is required of procedures for heat treatment except for stress relieving heat treatment in
accordance with this NORSOK standard.
9.3.2 Objective
The objective of the verification is to ensure that the specified parameters in the established heat treatment
procedure are correct by comparing the readings of the furnace controlling thermocouple and the contact
thermocouples fixed onto the load/components.
9.3.5 Reporting
A report shall be established identifying the furnace verified, describing the heat treatment load used and
location of thermocouples within the load (photograph). The superimposed time temperature curves from the
contact thermocouples and the controlling thermocouple(s) of the furnace shall be included in the report.
9.3.6 Witnessing
The verification of the heat treatment procedure shall be witnessed by the Qualifying Company, who also
shall sign the final report onto completion of the verification exercise.
a) demonstrate that the proposed manufacturing route and production parameters result in products meeting
the specified requirements,
b) verify that the proposed production test sampling gives results, which are representative of the properties
of the actual components they represent.
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10.2 Essential variables 6
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10.2.1 General 4
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A change in one or more of the manufacturing parameters stated in 10.2.2 to 10.2.13 requires re-qualification 0
of the manufacturing process. 2
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10.2.2 Thickness limitations and weight u
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The maximum qualified weight and thickness shall be according to limits given in Table 1, but shall in no case b
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exceed the limits specified in the Manufacturing Summary.
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Table 1 - Qualified maximum thickness and weight for applicable products t
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Type of product Type of material Tested Qualified Weight of Qualified g
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thickness thickness tested weight r
(T) component o
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mm mm kg A
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Strip, plate, pipe, High alloyed T 40 T + 25 %, N/A N/A l
tube and wrought austenitic SS + SS maximum 40 n
fittings type 25Cr duplex O
T > 40 T d
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SS type 22Cr T 60 T + 25 %, N/A N/A a
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duplex maximum 60 n
T > 60 T a
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Castings, forgings, High alloyed T 60 T + 10 %, G 250 G + 100 % S
bars and HIP austenitic SS, Ni- maximum 60 y
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alloys + SS type
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25Cr duplex e
T > 60 T G > 250 All d
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SS type 22Cr T 120 T + 10 %, G 250 G + 100 % v
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duplex maximum 120
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Components for testing shall be from regular production or from test production m anufactured according to
the normal manufacturing route and with regular production equipment.
10.3.2 Testing
a) production testing with test sampling as specified in NORSOK M-630: MDSs, other applicable standard
and/or the Manufacturing Summary,
b) additional testing for qualification according to Table 2,
c) for forged flanges, contour forged valves and similar products with integral prolongations testing shall be
carried out on both the prolongation and the product itself.
d) non-destructive testing as specified in NORSOK M-630 and relevant MDSs and/or other relevant material
specifications.
The type of tests to be performed and minimum requirements shall be as specified in NORSOK M-630 and
relevant MDS (or material standard/specification if materials are not covered by a MDS).
HIP components Integral test blocks. Testing shall be made from thin and thick sections of a sacrificial
except flanges product. Except for the additional testing test results shall fulfil the
requirements in the respective MDSs . Additional testing 3
according to 10.3.3 shall be carried out if section thickness 2
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exceeds 50 mm for all materials requiring impact- or corrosion 6
testing according to MDS/applicable specifications . 0
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Plates Cut from plate. Both ends on one plate shall be tested with three sets of tests at 4
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each end located in the middle and at each edge. Test specimens 0
shall be located in the mid-thickness. 2
Ring rolled products Tests from prolongation Additional testing according to 10.3.3 shall be carried out if s
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on actual forging or section thickness exceeds 50 mm for all materials requiring u
separate forged test impact- or corrosion testing according to MDS/applicable o
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ring. specifications. a
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Rolled and forged Cut from over-length of Tests shall be carried out at one end and in the mid-length S
bars bar. position of one bar. Additional testing according to 10.3.3 shall be +
carried out if section thickness exceeds 50 mm for all materials s
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requiring impact- or corrosion testing according to t
MDS/applicable specifications . a
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Seamless pipe and Cut from over-length of One pipe/tube shall be tested at one end and in the mid-length g
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tube pipe position. r
Strip Cut from strip. One end on one coil shall be tested with three set of tests at each o
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end located in the middle and at each edge. S
Valves machined Tests from prolongation Testing according to the applicable MDSs. Additional testing may A
from forgings on actual forging be required depending on shape and functionality of the forging e
as agreed with purchaser and Qualifying Company. n
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Welded pipe and Cut from over-length of Weld and base material shall be tested at one end and in the mid- n
tube pipe or from test plate length position on one pipe. O
welded as prolongation d
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of the pipe/tube weld. a
Wrought fittings - Cut from sacrificial One fitting of each type shall be tested at one end as a minimum. d
seamless and fitting, over-length of In addition different locations with different deformation ratio n
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welded fitting or for welded should be tested, e.g. inner- and outer radii and neutral zone for
fittings test plates elbows. Tees should be tested both on one end and in the crotch S
welded as a area. For welded fittings testing shall comprise base material and y
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prolongation of the weld(s). d
fitting weld. e
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For all materials having section thickness/diameter exceeding 50 mm and requiring impact- or corrosion
testing according to MDS/applicable specifications, additional testing shall be carried out as follows using
specimens located in the mid thickness position (T/2) and at a distance from any second surface of T or at
least 100 mm:
a) impact testing in axial and tangential direction. The minimum absorbed energy shall be minimum
27 J/20 J (average/single values) tested at -46 ºC;
b) corrosion and micro-examination in accordance with the requirements specified by the applicable MDS.
NOTE It is recognized that for certain applications corrosion properties and microstructure in mid-thickness are not important for the
functionality of the component as agreed with purchaser and Qualifying Company. In such cases it may be agreed that the
tests shall be carried out for information only and a note about this shall be included on the QTR front page.
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Annex A
(Informative)
Manufacturing Summary front page and example
Plant(s) and location(s): Actual plants, locations and equipment facilities where
this procedure is relevant.
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SEAMLESS PIPE
CUTTING
MARKING
EXPANDING
OVALIZATION OVALIZATION
(ELBOWS ONLY)
CALIBRATION RE-HEATING
RE-HEATING
FORMING
ELBOWS ONLY QUENCH
Annex B
(Normative)
Additional requirements to
API Spec 6A:2010/ISO 10423:2009 , Annex M, and ASTM A 991
B.1 General
Temperature uniformity survey of quality heat treatment furnaces shall be performed according to API Spec
6A:2010/ISO 10423:2009, Annex M, or ASTM A 991 with the following additional requirements:
a) the alternatives of attaching thermocouples to the extremities of each load, see ASTM A 991, Para 1.4, or
the alternative surveying techniques described in ASTM A 991, Para 7.7, are not acceptable as an
alternative to the specified temperature uniform ity survey;
b) the temperature uniformity survey shall be carried out at the maximum set point temperature for the actual
materials to be processed in the furnace. The m aximum limit of 1 100 ºC stated in ASTM A 991, Para
6.1.1.2, shall not apply;
c) the calibration shall be carried out with maximum load in the furnace. This is to demonstrate that the
required temperature uniformity and the maximum temperature specified can be reached. Subsequent
calibrations, which shall be carried out annually, may be carried out with empty furnace;
d) the documentation of the temperature uniformity survey shall include sketch of the furnace with working
zone of furnace and number and location of thermocouples used for the survey, see API Spec
6A:2010/ISO 10423:2009, Annex M, subclause M 3.3, or ASTM A 991, Paras 8.2.7 and 8.2.8;
e) uniformity survey shall to be performed annually for actual furnaces included in Manufacturing Summary 3
for solution heat treatment;
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f) the manufacturer shall establish a procedure for how to carry out the temperature uniformity survey. 6
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B.2 Batch type furnaces 4
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The following additional requirements to ASTM A991 apply: 2
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a) for furnaces with set point temperature in the working zone above 800 ºC the temperature at any point l
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shall not vary by more than ± 14 ºC from the furnace set point temperature after the furnace working zone o
has been brought up to temperature; b
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b) for furnaces with set point temperature in the working zone below 800 ºC shall not vary by more than
± 8 ºC from the furnace set point temperature after the furnace working zone has been brought up to
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temperature; s
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c) once the furnace temperature has reached the set point temperature, the temperature of all test locations t
shall be recorded at maximum 2 min intervals for at least 10 min. Then readings shall be taken at a
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maximum 5 min intervals for sufficient time to determine the recurrent temperature pattern of the furnace g
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working zone for at least 30 min. r
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B.3 Continuous conveyance and semi continuous conveyance furnaces
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The temperature uniformity check may be carried out as verification of the heat treatment procedure, see 9.3. A
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In any case the following requirements apply: n
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a) the survey shall verify that O
1) the specified heat treatment temperature for a material can be kept uniform within specified tolerances d
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through the working zone of the furnace as defined in the heat treatment procedure, a
2) the defined component travel speeds in the heat treatment procedure results in the minimum specified d
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soaking time being achieved, measured from when the set temperature is reached. a
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b) the temperature survey shall be carried out on actual products. A minimum of two surveys shall be carried S
out with products representing respectively the smallest (thinnest) and largest (thickness) sizes to be heat y
treated. b
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Annex C
(Informative
Verification of heat treatment procedure – Example
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Comparison of time temperature curves of the contact thermocouples (3 of f) fixed to the load itself with the d
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furnace thermocouple. Note the time difference to reach set temperature between the furnace thermocouple v
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and the contact thermocouples fixed onto the load.
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Annex D
(Normative)
Form for Qualification Test Record (QTR) Front Page
This form is available as a word file at the NORSOK home page http://www.standard.no/.
At the attached form examples of how to fill in the form is given.
NORSOK M-650
Rev. No.:
Manufacturer
name/address/
Web page:
Reference standard NORSOK M-650, Edition 4