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P.H value of water
Precautions
1. Preparation of Buffer solution.
• Take 100 ml of sample in a beaker
• Put the buffer tablet in the sample.
• Disperse the buffer tablet in the sample water by
continuously stirring Action.
• Prepare the buffer solution of pH value 4.0, 7.0 and 9.2
Calibration of the instrument.
The instrument should be calibrated before beginning the
measurement
• First clean the electrode with distilled water and dries its bulb
by using tissuePaper.
• Dip the electrode in a buffer solution of pH 7.
• Set the temperature © control to the room temperature. Set
the function selector to pH position and adjust the CALIBRATE
control Until the meter displays the precise pH of buffer
solution.
• Now the set the function selector switched to STAND
BY position.
• Remove the electrode from buffer solution. Wash it with
distilled water and wipe out with tissue paper.
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• Repeat the above procedure for calibration with buffer
solution of 4.0 and 92 pH value.
Operation of Instrument
• Calibrate the pH meter with two standard buffer solutions as
per the above Procedure.
• Clean and rinse the electrode thoroughly with distilled water
and carefully Wipe with tissue paper.
• Dip the electrode into the sample of solution. Stir the solution
by keeping on Magnetic stirrer or stir it manually.
•Wait up to 1 minute for steady reading +0.1 pH unit.
•Record reading in steady condition after one minute.
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Precautions :-
1. The standardization of pH meter is essential before use.
2. The reading must be noted when it is stable at least for 30
seconds.
3. The use of electrode should be done very carefully as it is
very sensitive and breakable.
4. Record the temperature of room.
5. Clean and wipe out electrode every time of immersion.
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Experimental setup
Digital pH meter
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Observations :-
• *Sample calculation
• For observation No :- 1
Observed average value of pH for River Sample
6.67+7.06
• Average pH = pH (1) + (2) /2 = 2
•Results
The pH value of untreated or raw water is observed as 8.12.
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• Turbidity of water Samples •
Turbidity in water
• is an optical property that broadly describes the clarity or
cloudiness of water. It is related to colour, but has more to
do with the loss of transparency due to the effect of
suspended particles and colloidal material.
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Procedure
1. Calibration and standardization
Turbidity Meter calibration: The manufacturer’s operating
instructions should beFollowed. Measure standards on the
turbidity meter covering the range of interest. If the instrument
is already calibrated in standard turbidity units, this procedure
will check the accuracy of the calibration scales. At least one
standard should run in each instrument range to be used. Some
instruments permit adjustments of sensitivity so that scale
values will correspond to turbidities Solid standards, such as
those made of Lucite blocks, should never be used due to
potential calibration changes caused by surface scratches. If a
pre-calibrated scale is not supplied, calibration curves should
be prepared for each range of the instrument.
2. Measurement
• Turbidities less than 40 units: If possible, allow samples to
come to room temperature before analysis. Mix the sample to
thoroughly disperse the solids present in it. Wait until air
bubbles disappear and then pour the sample into the turbid
meter tube. Read the turbidity directly from the instrument
scale or from the appropriate calibration curve.
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• Turbidities exceeding 40 units; Dilute the sample with one or
more volumes of turbidity-free water until the turbidity falls
below 40 units. The turbidity of the original sample is then
computed from the turbidity of the diluted sample and the
dilution factor. For example, if 5 volumes of turbidity-free
water were added to 1 volume of sample, and the diluted
sample showed a turbidity of 30 units, then theTurbidity of the
original sample was 180 units.
• Some Turbidity Meters are equipped with several separate
scales. The higher scales are to be used only as indicators of
required dilution volumes to reduce readings to less than 40
NTU.
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•Experimental sesetup
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Observations :-
*Sample calculation
• For observation No :- 1
132.3+ 133
•average Turbidity= Reading (1) + Reading (2)/2 = 2
•Results
The Turbidity of given water sample is observed as132.65 NTU.
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CONCLUSION :-
This report is a review of variety of options that may be
employed in the treatment, recovery and reuse of wastewater.
It is apparent that a variety of options are feasible for use in the
developing world and even more apparent that many low-
technology options can be mixed and matched for very high
efficiencies. Natural treatment technologies are attracting a
significant level of interest by environmental managers.
Natural treatment technologies are considered viable because
of their low capital costs, their ease of maintenance, their
potentially longer life-cycles and their ability to recover a
variety of resources including: treated effluent for irrigation,
organic humus for soil amendment and energy in the form of
biogas.
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